#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2207780.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207780_Fobs loop_ _publ_author_name 'Curtis, Neil F.' 'Pawley, Rebekah' 'Robinson, Ward T.' _publ_section_title ; C-meso-(3,5,7,7,10,12,12,14-Octamethyl-1,4,8,11-tetraazacyclotetradeca-4,11-diene)nickel(II) bis(thiocyanate) ; _journal_coeditor_code HG6270 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m80 _journal_page_last m82 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 69.917 _cell_angle_beta 86.852 _cell_angle_gamma 88.965 _cell_length_a 7.3383 _cell_length_b 8.0955 _cell_length_c 10.2042 _exptl_crystal_F_000 258.00 _reflns_d_resolution_high 0.7466 _[local]_cod_data_source_file hg6270Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Ni16b_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 92.09 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1065.52 1044.41 7.40 o 2 0 0 516.76 503.03 3.19 o 3 0 0 656.19 694.26 5.38 o 4 0 0 1410.45 1445.69 10.40 o 5 0 0 438.08 450.27 4.43 o 6 0 0 138.18 134.90 3.38 o 7 0 0 389.67 378.55 6.62 o 8 0 0 13.44 11.58 1.36 o 9 0 0 272.69 295.14 6.54 o -9 1 0 115.44 114.09 4.04 o -8 1 0 338.57 346.29 6.86 o -7 1 0 123.82 122.64 3.57 o -6 1 0 91.44 88.19 2.74 o -5 1 0 666.16 663.74 8.57 o -4 1 0 43.13 45.14 1.48 o -3 1 0 1950.30 2022.11 19.57 o -2 1 0 1141.54 1322.99 13.01 o -1 1 0 839.09 937.10 9.26 o 0 1 0 2584.75 2622.05 18.97 o 1 1 0 6423.93 6283.82 72.34 o 2 1 0 1418.47 1494.89 12.85 o 3 1 0 146.41 152.31 1.58 o 4 1 0 1607.74 1613.84 9.35 o 5 1 0 16.14 17.78 1.19 o 6 1 0 545.91 533.53 7.58 o 7 1 0 13.18 14.86 1.32 o 8 1 0 74.21 78.72 3.00 o 9 1 0 18.77 20.49 1.73 o -9 2 0 91.78 94.35 3.70 o -8 2 0 287.53 281.10 6.12 o -7 2 0 174.93 159.88 4.14 o -6 2 0 909.48 914.48 8.23 o -5 2 0 271.98 271.07 3.45 o -4 2 0 369.59 392.76 5.83 o -3 2 0 5.18 5.54 0.65 o -2 2 0 1997.13 2068.45 14.34 o -1 2 0 312.87 307.47 4.79 o 0 2 0 1276.33 1347.90 9.13 o 1 2 0 8480.99 8722.24 80.32 o 2 2 0 163.27 189.31 2.68 o 3 2 0 772.67 759.75 8.28 o 4 2 0 237.13 237.63 2.82 o 5 2 0 2036.10 2011.08 14.77 o 6 2 0 231.63 230.98 3.27 o 7 2 0 89.30 92.41 2.93 o 8 2 0 89.51 87.74 3.12 o 9 2 0 2.65 1.35 0.95 o -8 3 0 18.20 16.83 1.62 o -7 3 0 546.17 539.88 8.61 o -6 3 0 547.89 543.18 5.90 o -5 3 0 1220.50 1221.47 14.44 o -4 3 0 707.87 724.19 9.40 o -3 3 0 282.96 289.95 2.99 o -2 3 0 3478.38 3733.64 25.79 o -1 3 0 7.92 10.33 0.47 o 0 3 0 1771.99 1790.96 12.14 o 1 3 0 748.68 796.98 7.44 o 2 3 0 2438.14 2487.35 41.70 o 3 3 0 4.23 5.40 0.48 o 4 3 0 160.80 159.17 2.29 o 5 3 0 1638.58 1591.49 17.49 o 6 3 0 613.14 588.95 6.02 o 7 3 0 581.58 570.11 6.22 o 8 3 0 7.31 7.15 1.18 o 9 3 0 187.45 206.97 5.28 o -8 4 0 41.43 38.02 2.41 o -7 4 0 45.76 45.79 2.32 o -6 4 0 112.89 105.45 3.56 o -5 4 0 361.35 369.01 6.71 o -4 4 0 392.06 403.19 6.82 o -3 4 0 1496.55 1525.05 11.33 o -2 4 0 6.82 5.65 0.44 o -1 4 0 1728.30 1806.13 12.90 o 0 4 0 313.37 329.50 3.02 o 1 4 0 6.81 8.49 0.48 o 2 4 0 968.61 978.69 11.60 o 3 4 0 61.81 61.86 1.32 o 4 4 0 89.48 83.00 1.69 o 5 4 0 42.42 43.40 1.34 o 6 4 0 870.34 845.90 7.92 o 7 4 0 64.44 61.08 1.85 o 8 4 0 214.94 208.88 4.97 o -8 5 0 21.95 15.14 1.65 o -7 5 0 41.11 37.57 2.16 o -6 5 0 192.08 189.41 5.19 o -5 5 0 16.85 15.72 1.64 o -4 5 0 529.45 536.97 8.70 o -3 5 0 53.81 57.99 2.49 o -2 5 0 284.76 286.41 3.27 o -1 5 0 2563.60 2651.48 20.07 o 0 5 0 512.26 528.77 4.58 o 1 5 0 424.14 421.86 3.95 o 2 5 0 6.25 6.40 0.56 o 3 5 0 1683.60 1708.25 12.69 o 4 5 0 3.83 3.14 0.79 o 5 5 0 69.00 70.28 1.76 o 6 5 0 75.91 75.23 1.97 o 7 5 0 169.54 164.65 3.17 o 8 5 0 146.12 150.53 4.97 o -7 6 0 130.31 114.40 3.78 o -6 6 0 128.58 128.58 4.59 o -5 6 0 499.17 487.29 9.05 o -4 6 0 44.07 41.74 2.50 o -3 6 0 10.43 14.07 1.50 o -2 6 0 584.92 588.82 9.20 o -1 6 0 101.65 98.54 1.95 o 0 6 0 1790.25 1811.54 10.92 o 1 6 0 468.18 463.02 7.07 o 2 6 0 342.36 328.09 3.67 o 3 6 0 253.35 249.11 3.29 o 4 6 0 336.54 319.71 6.25 o 5 6 0 155.31 149.93 4.28 o 6 6 0 5.44 4.91 1.17 o 7 6 0 373.77 382.88 8.13 o -7 7 0 8.40 6.23 1.65 o -6 7 0 174.65 178.83 5.82 o -5 7 0 192.12 186.54 5.73 o -4 7 0 0.99 1.28 0.97 o -3 7 0 209.87 213.11 5.66 o -2 7 0 0.80 1.57 0.96 o -1 7 0 1.52 -0.77 0.77 o 0 7 0 115.00 114.16 2.41 o 1 7 0 387.74 387.78 4.99 o 2 7 0 183.17 181.60 5.20 o 3 7 0 0.76 1.90 0.83 o 4 7 0 687.15 672.47 10.31 o 5 7 0 17.90 16.40 1.70 o 6 7 0 115.77 116.28 4.21 o -5 8 0 71.39 76.69 4.03 o -4 8 0 381.96 386.25 8.85 o -3 8 0 38.47 37.39 2.75 o -2 8 0 40.14 51.25 2.92 o -1 8 0 156.88 156.93 4.91 o 0 8 0 10.36 9.71 1.54 o 1 8 0 316.94 326.88 4.62 o 2 8 0 5.61 3.53 0.70 o 3 8 0 100.00 97.41 3.42 o 4 8 0 68.00 68.73 3.11 o 5 8 0 572.33 605.60 10.47 o -2 9 0 100.10 111.98 4.57 o -1 9 0 113.85 108.20 4.48 o 0 9 0 175.19 189.56 5.69 o 1 9 0 25.57 24.00 2.19 o 2 9 0 157.24 190.86 6.25 o 3 9 0 1.72 0.46 1.73 o 4 9 0 1.08 1.32 0.97 o -1 -9 1 120.94 133.60 4.72 o 0 -9 1 95.79 95.95 4.11 o 2 -9 1 31.51 21.88 2.31 o -5 -8 1 55.02 56.70 3.03 o -4 -8 1 122.57 142.58 4.45 o -3 -8 1 3.44 2.16 0.95 o -1 -8 1 40.08 41.31 2.47 o 0 -8 1 217.29 212.56 5.69 o 1 -8 1 301.40 327.10 7.44 o 2 -8 1 40.02 37.57 2.71 o 4 -8 1 9.05 10.38 1.93 o -6 -7 1 0.42 0.00 0.86 o -5 -7 1 239.80 237.71 5.83 o -4 -7 1 48.25 48.70 2.45 o -3 -7 1 2.07 3.45 0.94 o -2 -7 1 32.38 31.91 1.75 o -1 -7 1 13.77 12.38 0.86 o 0 -7 1 160.74 173.72 5.33 o 1 -7 1 9.53 9.80 1.41 o 2 -7 1 561.26 587.46 10.12 o 3 -7 1 37.56 29.02 2.30 o 4 -7 1 334.38 336.43 7.80 o 5 -7 1 266.56 273.14 7.22 o 6 -7 1 9.43 8.05 1.72 o -6 -6 1 74.17 73.27 2.41 o -5 -6 1 73.91 68.19 1.96 o -4 -6 1 235.04 242.78 3.48 o -3 -6 1 196.89 187.92 4.22 o -2 -6 1 75.54 72.52 1.36 o -1 -6 1 52.54 55.35 1.40 o 0 -6 1 3.41 4.69 0.47 o 1 -6 1 581.77 588.87 9.20 o 2 -6 1 33.01 38.55 2.27 o 3 -6 1 40.84 36.72 2.29 o 5 -6 1 140.12 141.48 4.81 o 6 -6 1 464.64 471.82 9.54 o 7 -6 1 1.12 1.56 1.43 o -8 -5 1 8.51 8.37 1.19 o -7 -5 1 100.04 100.85 2.52 o -6 -5 1 123.77 115.08 2.53 o -5 -5 1 8.76 8.21 0.76 o -4 -5 1 956.46 915.28 13.74 o -3 -5 1 530.51 530.57 4.73 o -2 -5 1 297.97 272.28 2.64 o -1 -5 1 1.53 2.63 0.67 o 0 -5 1 431.31 442.48 3.52 o 1 -5 1 555.27 506.10 12.61 o 2 -5 1 5.83 4.61 0.92 o 3 -5 1 837.64 864.61 11.90 o 4 -5 1 136.87 131.54 4.06 o 5 -5 1 273.76 280.05 6.40 o 6 -5 1 194.60 184.89 5.35 o 7 -5 1 361.57 343.32 7.87 o -8 -4 1 5.45 4.79 1.09 o -7 -4 1 164.58 158.69 4.07 o -6 -4 1 13.37 13.28 1.36 o -5 -4 1 220.59 210.39 3.12 o -4 -4 1 4.15 2.05 0.45 o -3 -4 1 561.59 562.54 6.74 o -2 -4 1 611.48 560.82 4.99 o -1 -4 1 301.11 321.07 2.68 o 0 -4 1 1041.93 1076.19 7.24 o 1 -4 1 23.85 26.10 0.78 o 2 -4 1 981.06 949.21 7.47 o 3 -4 1 33.32 31.57 1.79 o 4 -4 1 5.13 3.70 0.95 o 5 -4 1 18.62 16.69 1.56 o 6 -4 1 119.82 110.07 3.86 o 7 -4 1 264.94 263.27 7.01 o 8 -4 1 19.32 23.51 1.90 o -8 -3 1 119.75 125.20 3.86 o -7 -3 1 49.65 47.06 2.23 o -6 -3 1 364.22 361.86 4.98 o -5 -3 1 205.06 181.49 2.77 o -4 -3 1 4.04 4.37 0.61 o -3 -3 1 44.77 31.41 2.32 o -2 -3 1 285.17 304.66 3.08 o -1 -3 1 1220.11 1144.04 9.01 o 0 -3 1 13.47 15.81 0.80 o 1 -3 1 2558.97 2719.58 18.60 o 2 -3 1 1717.15 1846.63 12.95 o 3 -3 1 40.33 42.33 0.88 o 4 -3 1 342.43 342.94 6.00 o 5 -3 1 91.96 93.20 3.16 o 6 -3 1 397.36 401.89 7.38 o 7 -3 1 22.20 21.97 1.67 o 8 -3 1 149.21 136.88 4.27 o -9 -2 1 365.95 402.71 7.80 o -8 -2 1 138.14 135.14 3.96 o -7 -2 1 110.19 107.45 3.20 o -6 -2 1 418.03 378.23 6.11 o -5 -2 1 324.33 328.10 3.83 o -4 -2 1 712.75 670.00 5.91 o -3 -2 1 3.89 1.64 0.32 o -2 -2 1 2061.20 2092.01 39.27 o -1 -2 1 39.70 32.17 1.46 o 0 -2 1 163.97 180.00 1.94 o 1 -2 1 4461.85 4558.84 32.81 o 2 -2 1 1007.41 1072.53 7.84 o 3 -2 1 2143.64 2214.73 22.16 o 4 -2 1 234.40 259.19 4.78 o 5 -2 1 735.03 731.27 9.93 o 6 -2 1 16.05 13.38 0.90 o 7 -2 1 404.97 419.18 7.28 o 8 -2 1 197.62 196.31 5.02 o -9 -1 1 157.68 161.52 4.70 o -8 -1 1 24.92 34.54 2.07 o -7 -1 1 590.74 571.41 8.59 o -6 -1 1 4.54 4.29 0.81 o -5 -1 1 1357.77 1352.41 14.64 o -4 -1 1 455.61 453.85 6.01 o -3 -1 1 370.73 368.73 3.49 o -2 -1 1 310.41 352.60 3.12 o -1 -1 1 455.18 467.59 5.24 o 0 -1 1 1927.56 2082.73 12.91 o 1 -1 1 962.52 1004.66 10.21 o 2 -1 1 318.94 301.18 4.27 o 3 -1 1 275.64 299.47 4.60 o 4 -1 1 828.65 803.76 9.75 o 5 -1 1 605.17 604.76 5.79 o 6 -1 1 12.14 12.82 0.98 o 7 -1 1 242.03 245.62 5.21 o 8 -1 1 22.62 25.54 1.87 o 9 -1 1 220.27 230.71 5.78 o -9 0 1 0.61 1.14 0.84 o -8 0 1 243.59 263.36 5.80 o -7 0 1 2.20 1.96 0.77 o -6 0 1 286.32 285.28 5.16 o -5 0 1 515.10 512.44 7.00 o -4 0 1 3420.76 3610.96 24.55 o -3 0 1 1057.05 1097.06 7.78 o -2 0 1 1173.65 1240.07 12.04 o -1 0 1 2425.88 2693.65 27.28 o 0 0 1 1319.73 1255.32 14.03 o 1 0 1 52.18 54.97 0.84 o 2 0 1 346.52 355.25 3.03 o 3 0 1 38.47 42.33 0.91 o 4 0 1 298.92 285.60 3.16 o 5 0 1 71.48 74.04 2.15 o 6 0 1 1424.60 1355.77 15.27 o 7 0 1 4.79 4.35 0.88 o 8 0 1 590.33 609.21 9.58 o 9 0 1 38.51 34.68 2.31 o -9 1 1 272.87 295.68 6.69 o -8 1 1 89.35 83.42 3.21 o -7 1 1 42.62 46.32 2.25 o -6 1 1 305.17 305.48 5.46 o -5 1 1 72.95 68.47 1.62 o -4 1 1 2501.90 2599.10 17.56 o -3 1 1 1635.63 1817.07 22.33 o -2 1 1 5543.93 5721.80 54.96 o -1 1 1 16.22 20.34 0.57 o 1 1 1 5044.46 5096.85 29.66 o 2 1 1 432.75 437.46 2.86 o 3 1 1 996.54 1002.15 6.04 o 4 1 1 28.95 31.88 0.74 o 5 1 1 542.74 511.05 3.93 o 6 1 1 195.20 193.60 4.05 o 7 1 1 347.60 348.29 6.20 o 8 1 1 154.49 139.76 3.98 o 9 1 1 122.31 124.25 4.07 o -9 2 1 246.22 241.53 6.00 o -8 2 1 1.84 0.73 0.88 o -7 2 1 359.00 360.91 6.60 o -6 2 1 3.27 4.66 0.84 o -5 2 1 537.94 512.49 5.17 o -4 2 1 127.85 136.24 2.01 o -3 2 1 2812.54 3014.61 20.38 o -2 2 1 1278.59 1363.63 13.51 o -1 2 1 94.44 119.07 1.87 o 0 2 1 2430.32 2544.82 18.44 o 1 2 1 3531.60 3689.51 35.60 o 2 2 1 595.71 614.74 3.86 o 3 2 1 80.51 76.67 1.02 o 4 2 1 317.11 321.74 2.66 o 5 2 1 124.55 115.97 1.60 o 6 2 1 22.86 21.39 1.00 o 7 2 1 265.94 264.71 5.20 o 8 2 1 81.11 82.51 3.03 o 9 2 1 280.16 285.54 6.28 o -8 3 1 395.87 427.35 7.91 o -7 3 1 23.69 20.09 1.60 o -6 3 1 382.83 398.02 6.63 o -5 3 1 140.07 132.72 2.31 o -4 3 1 410.90 383.33 5.83 o -3 3 1 1084.10 1083.87 15.72 o -2 3 1 1.74 0.70 0.24 o -1 3 1 853.65 844.35 8.93 o 0 3 1 123.23 139.69 1.45 o 1 3 1 5154.48 5397.13 37.23 o 2 3 1 2650.87 2889.80 19.37 o 3 3 1 419.31 411.29 3.80 o 4 3 1 505.08 516.65 10.81 o 5 3 1 39.43 38.11 1.18 o 6 3 1 617.52 587.45 5.91 o 7 3 1 30.86 31.97 1.31 o 8 3 1 247.59 239.14 5.27 o 9 3 1 7.75 10.74 1.36 o -8 4 1 396.21 366.87 7.30 o -7 4 1 215.78 214.93 5.02 o -6 4 1 367.58 348.86 4.59 o -5 4 1 179.85 202.85 4.57 o -4 4 1 2154.24 2121.73 17.29 o -3 4 1 8.94 8.73 0.54 o -2 4 1 1469.47 1465.11 10.81 o -1 4 1 531.43 566.38 6.62 o 0 4 1 27.80 13.75 0.49 o 1 4 1 55.92 52.25 0.94 o 2 4 1 1742.79 1828.01 12.77 o 3 4 1 2222.07 2232.79 15.62 o 4 4 1 36.80 40.63 1.14 o 5 4 1 546.81 532.32 5.33 o 6 4 1 92.22 91.17 2.01 o 7 4 1 345.23 335.92 4.67 o 8 4 1 322.45 322.50 5.99 o 9 4 1 19.00 19.82 1.94 o -8 5 1 15.72 11.92 1.47 o -7 5 1 339.31 340.76 6.63 o -6 5 1 23.90 20.78 1.18 o -5 5 1 1120.47 1160.29 14.84 o -4 5 1 68.30 68.87 2.70 o -3 5 1 314.18 314.69 6.90 o -2 5 1 386.84 416.84 4.26 o -1 5 1 281.12 300.06 4.42 o 0 5 1 376.63 352.01 3.30 o 1 5 1 211.62 223.15 2.48 o 2 5 1 544.58 517.93 4.60 o 3 5 1 163.36 185.99 3.31 o 4 5 1 182.65 179.08 2.60 o 5 5 1 91.88 97.34 2.68 o 6 5 1 147.21 154.10 14.80 o 7 5 1 385.70 392.53 5.18 o 8 5 1 2.19 2.46 1.03 o -7 6 1 6.05 5.35 1.01 o -6 6 1 313.01 310.34 7.04 o -5 6 1 269.07 252.59 6.07 o -4 6 1 235.88 238.25 5.61 o -3 6 1 1490.06 1446.62 17.40 o -2 6 1 13.26 15.63 0.88 o -1 6 1 682.93 681.27 6.36 o 0 6 1 337.05 359.90 5.46 o 1 6 1 895.87 845.30 6.85 o 2 6 1 30.69 32.21 1.66 o 3 6 1 318.71 317.08 5.75 o 4 6 1 216.82 219.56 4.89 o 5 6 1 0.68 1.89 0.84 o 6 6 1 480.88 474.65 8.59 o 7 6 1 73.45 73.27 3.28 o -6 7 1 167.57 159.21 5.34 o -5 7 1 3.75 1.58 1.13 o -4 7 1 788.61 787.82 12.30 o -3 7 1 200.01 201.30 5.39 o -2 7 1 659.23 665.25 10.48 o -1 7 1 73.97 73.39 2.01 o 0 7 1 705.96 723.82 9.41 o 1 7 1 632.73 630.22 8.73 o 2 7 1 49.23 42.36 2.00 o 3 7 1 375.71 342.82 6.34 o 4 7 1 91.05 89.02 3.18 o 5 7 1 130.77 127.61 4.11 o 6 7 1 2.08 2.77 1.14 o -5 8 1 241.56 272.97 7.37 o -4 8 1 14.25 12.59 1.89 o -3 8 1 11.96 16.99 1.98 o -2 8 1 184.69 175.91 5.22 o -1 8 1 46.52 48.46 2.70 o 0 8 1 303.64 307.02 4.38 o 1 8 1 142.57 155.20 2.94 o 2 8 1 409.90 402.57 7.05 o 3 8 1 0.58 0.61 0.77 o 4 8 1 261.26 263.37 6.07 o 5 8 1 94.57 96.39 3.78 o -3 9 1 177.98 190.98 6.13 o -2 9 1 7.24 5.52 1.40 o -1 9 1 224.07 227.25 6.34 o 0 9 1 0.55 2.40 1.00 o 1 9 1 497.61 544.03 9.86 o 2 9 1 343.78 350.67 5.05 o 3 9 1 120.39 136.50 4.29 o 4 9 1 85.50 85.77 3.54 o 0 10 1 20.57 24.17 2.25 o 1 10 1 29.64 25.12 2.20 o 2 10 1 116.63 117.91 5.91 o 0 -9 2 150.28 155.89 5.39 o 1 -9 2 33.56 26.05 2.46 o -4 -8 2 1.14 2.45 1.47 o 0 -8 2 16.99 20.62 2.03 o 1 -8 2 4.97 4.10 1.28 o 2 -8 2 23.22 27.85 2.40 o 3 -8 2 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121.66 3.86 o 4 -5 2 43.94 45.72 2.60 o 5 -5 2 40.80 42.70 2.62 o 6 -5 2 178.85 175.00 5.48 o 7 -5 2 3.52 3.62 1.46 o -8 -4 2 155.90 157.04 4.49 o -7 -4 2 7.25 7.40 1.12 o -6 -4 2 406.81 405.63 6.83 o -5 -4 2 65.66 64.68 1.75 o -4 -4 2 141.47 137.49 5.82 o -3 -4 2 198.61 192.27 2.68 o -2 -4 2 334.32 302.93 3.45 o -1 -4 2 957.36 892.07 5.87 o 0 -4 2 315.05 316.15 2.70 o 1 -4 2 380.85 340.18 2.78 o 2 -4 2 96.41 97.84 3.02 o 3 -4 2 794.88 801.21 11.03 o 4 -4 2 2.27 2.70 0.95 o 5 -4 2 71.03 73.12 3.13 o 6 -4 2 647.87 623.60 10.57 o 7 -4 2 61.19 61.91 3.27 o 8 -4 2 53.64 49.42 2.67 o -8 -3 2 2.25 2.90 0.99 o -7 -3 2 12.65 12.53 1.36 o -6 -3 2 63.95 67.11 2.46 o -5 -3 2 23.14 22.15 1.05 o -4 -3 2 302.25 279.30 3.45 o -3 -3 2 28.81 28.97 0.80 o -2 -3 2 1605.09 1566.83 9.17 o -1 -3 2 517.68 563.29 3.91 o 0 -3 2 450.22 449.26 3.24 o 1 -3 2 6.92 13.90 0.43 o 2 -3 2 5.00 1.28 0.59 o 3 -3 2 324.98 308.34 5.61 o 4 -3 2 1.02 0.99 0.77 o 5 -3 2 9.38 10.43 1.33 o 6 -3 2 1.56 4.60 1.13 o 7 -3 2 641.39 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