#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/83/2208334.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208334_Fobs loop_ _publ_author_name 'Lipstman, Sophia' 'George, Sumod' 'Goldberg, Israel' _publ_section_title ; (4-Acetylpyridine)(tetraphenylporphyrinato)zinc(II) ; _journal_coeditor_code HB6319 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m417 _journal_page_last m419 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.631 _cell_angle_gamma 90.000 _cell_length_a 16.2055 _cell_length_b 11.0902 _cell_length_c 21.4881 _exptl_crystal_F_000 1656.00 _reflns_d_resolution_high 0.7513 _[local]_cod_data_source_file hb6319Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound so4-sg225' _shelx_refln_list_code 4 _shelx_f_calc_maximum 375.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 11153.48 10500.21 214.14 o 4 0 0 2291.92 2314.90 69.44 o 5 0 0 5092.24 4385.58 121.92 o 6 0 0 9.38 -5.57 7.43 o 7 0 0 672.96 982.55 35.90 o 8 0 0 1297.41 1458.23 43.69 o 9 0 0 2248.03 1945.48 54.83 o 10 0 0 89.04 149.21 13.37 o 11 0 0 2163.56 2134.18 52.85 o 12 0 0 3717.75 3394.61 208.69 o 13 0 0 11.44 20.49 57.68 o 14 0 0 1519.91 1763.40 275.78 o 15 0 0 1172.68 1458.23 167.22 o 16 0 0 1273.77 1319.23 178.92 o 17 0 0 50.60 106.57 97.10 o 18 0 0 1920.51 2677.57 239.45 o 19 0 0 2155.85 2120.44 233.69 o 20 0 0 1375.56 1989.61 279.61 o 21 0 0 617.32 430.50 188.89 o 2 1 0 3884.95 3630.47 59.97 o 3 1 0 1014.22 1062.08 22.71 o 4 1 0 334.91 307.59 9.59 o 5 1 0 3316.69 2834.27 76.80 o 6 1 0 1654.08 1576.44 51.37 o 7 1 0 740.30 684.93 28.65 o 8 1 0 256.71 318.17 21.29 o 9 1 0 1116.93 1256.72 44.06 o 10 1 0 474.54 489.11 27.54 o 11 1 0 38.42 45.80 17.14 o 12 1 0 5137.38 5978.29 130.77 o 13 1 0 485.10 551.49 31.56 o 14 1 0 38.26 -16.65 17.27 o 15 1 0 1028.37 1058.86 30.76 o 16 1 0 58.18 -83.18 55.45 o 17 1 0 72.06 148.60 67.34 o 18 1 0 49.73 -112.82 99.39 o 19 1 0 2.46 -4.39 119.26 o 21 1 0 0.02 112.82 128.98 o 0 2 0 10582.25 11047.56 423.57 o 1 2 0 396.77 521.54 22.71 o 2 2 0 9100.22 8927.37 202.13 o 3 2 0 219.15 155.34 13.00 o 4 2 0 743.03 640.12 25.19 o 5 2 0 793.24 581.14 19.19 o 6 2 0 12.56 44.44 7.98 o 7 2 0 2394.08 2148.04 41.53 o 8 2 0 1707.16 1858.71 55.76 o 9 2 0 6894.29 6609.62 141.60 o 10 2 0 1291.46 1274.42 49.76 o 11 2 0 2430.08 2443.50 73.77 o 12 2 0 4614.06 5037.52 134.18 o 13 2 0 206.18 231.77 28.78 o 14 2 0 7674.79 8791.58 205.29 o 15 2 0 601.88 589.55 41.09 o 16 2 0 74.47 107.63 26.86 o 17 2 0 39.87 42.83 24.07 o 18 2 0 1177.82 1543.02 156.33 o 19 2 0 207.81 176.51 118.33 o 20 2 0 11.43 27.29 108.37 o 21 2 0 17.32 99.02 101.99 o 1 3 0 8563.46 7883.30 194.39 o 2 3 0 3910.05 3986.52 116.23 o 3 3 0 383.05 356.54 25.37 o 4 3 0 316.49 306.72 20.92 o 5 3 0 3113.49 2914.29 64.49 o 6 3 0 2.89 -0.62 10.64 o 7 3 0 2724.15 3052.86 65.97 o 8 3 0 144.39 123.10 13.24 o 9 3 0 355.11 380.43 14.54 o 10 3 0 1190.87 1088.19 47.59 o 11 3 0 48.15 23.52 26.06 o 12 3 0 1665.35 1792.80 67.40 o 13 3 0 757.79 747.50 42.15 o 14 3 0 846.09 774.97 48.46 o 15 3 0 243.22 248.79 37.69 o 16 3 0 33.96 -19.19 30.94 o 17 3 0 13.42 1.86 36.70 o 18 3 0 228.23 184.49 102.05 o 19 3 0 2.79 240.19 131.08 o 20 3 0 38.83 -284.44 189.63 o 0 4 0 6819.52 5920.67 187.59 o 1 4 0 2087.72 1947.71 57.06 o 2 4 0 2857.31 2623.79 73.90 o 3 4 0 1935.60 1865.15 57.99 o 4 4 0 5779.44 5719.54 131.70 o 5 4 0 13182.76 13485.74 260.00 o 6 4 0 2869.10 2693.04 64.55 o 7 4 0 7356.73 7430.52 137.27 o 8 4 0 1385.12 1454.45 43.63 o 9 4 0 5967.51 5806.43 113.75 o 10 4 0 667.27 638.88 25.13 o 11 4 0 1342.78 1465.84 72.41 o 12 4 0 835.48 805.73 55.08 o 13 4 0 480.04 487.99 52.73 o 14 4 0 611.84 776.34 61.02 o 15 4 0 362.78 384.27 53.66 o 16 4 0 978.43 1042.71 75.50 o 17 4 0 204.51 179.79 52.73 o 18 4 0 605.76 272.87 171.80 o 19 4 0 201.57 72.41 138.45 o 20 4 0 5.23 -205.16 136.77 o 1 5 0 7469.31 7409.11 158.44 o 2 5 0 191.90 291.25 28.84 o 3 5 0 5240.75 5659.50 134.73 o 4 5 0 2374.06 2248.30 70.80 o 5 5 0 448.80 481.43 31.69 o 6 5 0 3838.56 3986.52 91.10 o 7 5 0 931.49 993.50 39.24 o 8 5 0 455.85 426.35 28.78 o 9 5 0 1208.41 1240.94 45.55 o 10 5 0 158.30 123.65 21.04 o 11 5 0 119.46 129.22 18.69 o 12 5 0 952.34 1023.52 30.26 o 13 5 0 178.49 123.10 45.24 o 14 5 0 3.13 -9.84 38.19 o 15 5 0 539.66 421.22 57.19 o 16 5 0 75.55 52.05 42.70 o 17 5 0 582.28 466.27 67.71 o 18 5 0 343.23 373.62 188.51 o 19 5 0 784.48 575.13 153.92 o 20 5 0 541.24 679.73 180.28 o 0 6 0 15133.35 16116.27 435.82 o 1 6 0 1273.26 1450.68 60.65 o 2 6 0 2885.78 2813.10 84.42 o 3 6 0 1552.02 1531.32 58.42 o 4 6 0 34.02 38.37 24.63 o 5 6 0 1658.02 1782.28 60.90 o 6 6 0 180.53 177.13 29.15 o 7 6 0 366.58 301.52 29.40 o 8 6 0 188.27 167.97 27.11 o 9 6 0 1311.82 1361.13 49.57 o 10 6 0 603.09 616.41 34.60 o 11 6 0 746.41 761.17 38.43 o 12 6 0 1152.68 1037.88 43.26 o 13 6 0 1038.98 1063.69 35.71 o 14 6 0 2008.18 2171.13 115.92 o 15 6 0 19.15 59.48 55.64 o 16 6 0 365.35 366.94 71.48 o 17 6 0 11.53 54.59 57.74 o 18 6 0 192.75 -77.98 173.10 o 19 6 0 801.12 1159.92 233.82 o 1 7 0 1329.63 1161.60 55.95 o 2 7 0 6271.67 6838.12 160.48 o 3 7 0 304.72 276.15 36.39 o 4 7 0 229.45 151.01 35.46 o 5 7 0 7639.91 8445.13 192.04 o 6 7 0 1128.98 1190.62 56.63 o 7 7 0 0.15 -13.00 21.72 o 8 7 0 1227.17 1225.16 52.23 o 9 7 0 3.28 6.19 22.28 o 10 7 0 4709.81 4852.10 131.70 o 11 7 0 729.43 648.97 43.07 o 12 7 0 1520.84 1588.32 61.46 o 13 7 0 1310.40 1263.77 53.04 o 14 7 0 38.20 21.66 15.97 o 15 7 0 85.63 24.76 62.63 o 16 7 0 20.36 -59.85 77.36 o 17 7 0 418.76 367.87 109.73 o 18 7 0 294.44 448.20 163.26 o 0 8 0 938.29 968.56 78.97 o 1 8 0 1257.58 1292.24 64.36 o 2 8 0 435.38 411.07 45.36 o 3 8 0 570.95 615.18 48.15 o 4 8 0 1093.93 1075.07 58.73 o 5 8 0 572.25 491.34 49.63 o 6 8 0 1257.65 1311.99 64.86 o 7 8 0 698.75 687.53 50.87 o 8 8 0 845.15 740.69 50.13 o 9 8 0 80.74 65.79 37.94 o 10 8 0 731.65 652.74 47.04 o 11 8 0 23.72 19.19 27.91 o 12 8 0 2766.63 2852.84 95.68 o 13 8 0 90.60 37.75 28.41 o 14 8 0 690.03 716.55 43.94 o 15 8 0 0.43 89.86 75.44 o 16 8 0 479.72 448.20 111.65 o 17 8 0 323.83 293.79 145.81 o 1 9 0 2709.25 2794.66 115.73 o 2 9 0 29.07 31.07 34.10 o 3 9 0 2625.97 2935.83 115.92 o 4 9 0 2474.55 2343.68 101.19 o 5 9 0 513.80 545.68 55.76 o 6 9 0 263.83 277.02 43.07 o 7 9 0 330.09 296.39 47.96 o 8 9 0 372.46 436.69 47.84 o 9 9 0 296.71 269.59 42.46 o 10 9 0 462.09 515.91 47.47 o 11 9 0 347.75 252.69 39.55 o 12 9 0 154.39 109.67 35.46 o 13 9 0 760.56 704.61 52.85 o 14 9 0 3.93 19.80 42.77 o 15 9 0 836.48 518.13 116.66 o 16 9 0 8.22 4.89 145.93 o 0 10 0 860.30 711.23 90.23 o 1 10 0 0.85 52.79 44.06 o 2 10 0 1117.86 1146.37 75.81 o 3 10 0 869.09 717.85 69.32 o 4 10 0 195.14 160.35 48.52 o 5 10 0 783.72 888.23 72.66 o 6 10 0 439.54 357.47 51.74 o 7 10 0 2067.92 2264.89 111.28 o 8 10 0 9.30 3.09 40.41 o 9 10 0 183.55 164.13 47.16 o 10 10 0 393.96 388.23 51.99 o 11 10 0 13.30 28.35 42.64 o 12 10 0 25.80 5.57 44.56 o 13 10 0 225.55 215.44 62.82 o 14 10 0 169.96 114.99 159.49 o 15 10 0 75.41 298.06 127.99 o 1 11 0 1398.15 1620.19 106.14 o 2 11 0 2.61 -32.74 40.17 o 3 11 0 1653.38 1799.11 103.42 o 4 11 0 765.75 754.30 76.49 o 5 11 0 2230.51 2104.41 114.12 o 6 11 0 516.42 440.84 62.69 o 7 11 0 418.84 425.30 59.54 o 8 11 0 1092.56 1084.91 85.22 o 9 11 0 624.34 628.85 73.59 o 10 11 0 194.20 249.54 64.43 o 11 11 0 171.98 267.11 66.65 o 12 11 0 347.53 375.54 86.77 o 13 11 0 715.51 906.12 193.22 o 0 12 0 41.12 109.67 80.27 o 1 12 0 74.65 129.84 61.77 o 2 12 0 77.61 52.05 46.29 o 3 12 0 128.36 42.15 64.92 o 4 12 0 438.46 330.73 67.89 o 5 12 0 4.78 22.34 63.75 o 6 12 0 216.35 198.29 73.59 o 7 12 0 10.41 -12.32 51.12 o 8 12 0 49.03 86.09 73.90 o 9 12 0 9.14 -53.10 64.18 o 10 12 0 89.88 -16.65 64.12 o 11 12 0 0.43 8.05 61.95 o 12 12 0 16.36 146.18 190.12 o 1 13 0 971.38 1153.12 155.47 o 2 13 0 254.25 162.89 76.19 o 3 13 0 891.43 919.67 141.85 o 4 13 0 351.40 319.04 90.67 o 5 13 0 9.74 -129.22 94.44 o 6 13 0 1030.79 956.19 135.41 o 7 13 0 3.14 -29.71 60.71 o 8 13 0 114.54 105.03 95.37 o 9 13 0 20.23 44.44 98.84 o 0 14 0 2.54 43.45 163.02 o 1 14 0 56.41 -92.71 87.20 o 2 14 0 14.88 -6.81 78.10 o 3 14 0 0.10 59.48 125.88 o 4 14 0 10.85 -47.16 94.63 o 5 14 0 4.83 82.93 113.26 o 6 14 0 16.35 66.16 110.91 o -21 1 1 171.77 -126.44 120.87 o -20 1 1 9.37 115.48 111.21 o -19 1 1 162.41 171.87 92.65 o -18 1 1 937.84 1206.09 133.06 o -17 1 1 117.39 208.19 96.18 o -16 1 1 4150.87 4883.35 239.88 o -15 1 1 584.05 776.34 98.40 o -14 1 1 4440.51 5749.68 150.89 o -13 1 1 164.47 142.59 20.18 o -12 1 1 11136.44 11883.87 238.64 o -11 1 1 36.15 39.61 17.21 o -10 1 1 192.07 188.58 19.80 o -9 1 1 2793.28 2545.37 67.77 o -8 1 1 425.13 590.73 30.26 o -7 1 1 7429.58 6694.84 158.75 o -6 1 1 210.36 175.83 17.14 o -5 1 1 14813.07 13770.37 291.93 o -4 1 1 15908.52 15017.68 237.78 o -3 1 1 189.65 220.57 9.59 o -2 1 1 9628.37 8693.86 143.83 o -1 1 1 8120.42 7464.87 197.74 o 1 1 1 240.19 179.79 12.69 o 2 1 1 33987.85 32217.08 482.24 o 3 1 1 9163.23 9524.66 174.84 o 4 1 1 1555.05 1558.74 33.42 o 5 1 1 419.48 407.04 15.04 o 6 1 1 3300.91 3291.01 62.82 o 7 1 1 4994.24 4981.20 91.29 o 8 1 1 1401.33 1394.36 31.56 o 9 1 1 1887.70 1713.65 51.49 o 10 1 1 281.37 250.34 23.64 o 11 1 1 2060.22 2090.74 63.68 o 12 1 1 4845.87 5090.62 117.16 o 13 1 1 53.26 12.32 20.92 o 14 1 1 3865.07 4280.80 107.44 o 15 1 1 498.95 433.59 25.87 o 16 1 1 667.96 800.10 129.47 o 17 1 1 106.83 64.18 77.73 o 18 1 1 1365.65 1852.28 160.60 o 19 1 1 76.67 -8.05 113.88 o 20 1 1 875.57 1180.35 141.85 o 21 1 1 79.30 56.81 135.41 o -21 2 1 39.22 -41.53 126.32 o -20 2 1 5.66 145.56 144.08 o -19 2 1 34.41 -174.34 116.23 o -18 2 1 0.32 133.80 111.09 o -17 2 1 166.50 151.01 23.83 o -16 2 1 100.09 25.25 25.25 o -15 2 1 4067.08 4602.38 124.89 o -14 2 1 392.57 422.27 33.73 o -13 2 1 500.74 529.52 40.04 o -12 2 1 759.47 950.06 49.08 o -11 2 1 341.05 246.44 25.00 o -10 2 1 999.87 1042.71 44.99 o -9 2 1 406.89 387.24 27.42 o -8 2 1 276.60 325.29 25.13 o -7 2 1 2546.08 2797.32 81.57 o -6 2 1 1954.05 1761.36 39.67 o -5 2 1 1599.70 1525.50 36.95 o -4 2 1 479.42 450.30 20.05 o -3 2 1 1620.85 1709.50 49.39 o -2 2 1 24353.22 24059.48 447.64 o -1 2 1 391.75 254.30 15.10 o 0 2 1 367.35 604.10 23.21 o 1 2 1 7005.45 7520.88 176.94 o 2 2 1 3723.76 3803.33 89.00 o 3 2 1 394.20 355.61 15.97 o 4 2 1 4415.04 4261.31 81.20 o 5 2 1 1329.42 1211.29 31.19 o 6 2 1 1182.97 1021.91 28.65 o 7 2 1 173.91 213.95 13.12 o 8 2 1 1.47 6.19 9.28 o 9 2 1 486.76 587.14 34.97 o 10 2 1 39.97 3.65 19.06 o 11 2 1 1.45 -11.76 20.98 o 12 2 1 940.79 838.53 44.68 o 13 2 1 24.44 41.53 25.31 o 14 2 1 296.93 215.44 32.86 o 15 2 1 451.09 397.08 45.61 o 16 2 1 70.47 66.16 27.91 o 17 2 1 31.00 13.00 25.31 o 18 2 1 463.34 489.11 103.42 o 19 2 1 110.90 117.09 99.58 o 20 2 1 8.89 -38.37 111.90 o -20 3 1 43.21 -79.77 119.51 o -19 3 1 1824.69 2011.89 196.37 o -18 3 1 1787.82 2377.53 186.78 o -17 3 1 69.27 92.21 38.25 o -16 3 1 19.44 -6.19 33.42 o -15 3 1 765.88 912.12 57.12 o -14 3 1 1396.59 1529.40 71.98 o -13 3 1 371.33 425.30 37.94 o -12 3 1 1824.85 1753.01 64.55 o -11 3 1 604.68 450.30 38.00 o -10 3 1 5491.50 5674.48 142.41 o -9 3 1 3898.69 4018.02 110.41 o -8 3 1 6295.62 6557.14 120.87 o -7 3 1 3628.96 3391.70 72.41 o -6 3 1 922.24 885.26 29.58 o -5 3 1 8738.50 8408.61 155.09 o -4 3 1 15.34 15.47 11.76 o -3 3 1 15652.37 15158.23 294.03 o -2 3 1 13309.33 12388.14 243.66 o -1 3 1 138.28 139.06 18.20 o 0 3 1 22122.02 21492.45 459.53 o 1 3 1 5337.26 5544.02 155.59 o 2 3 1 1792.77 1426.11 58.24 o 3 3 1 2565.26 2850.18 82.37 o 4 3 1 31.94 68.20 13.12 o 5 3 1 7658.99 7259.95 148.41 o 6 3 1 5291.59 5219.23 104.22 o 7 3 1 5438.99 5126.21 99.77 o 8 3 1 150.93 137.89 13.43 o 9 3 1 6456.02 6460.84 111.96 o 10 3 1 2199.64 2118.15 70.99 o 11 3 1 4487.04 4558.62 117.59 o 12 3 1 9.27 16.03 24.69 o 13 3 1 1240.25 1219.96 60.84 o 14 3 1 1656.42 1809.70 71.98 o 15 3 1 49.43 14.30 34.78 o 16 3 1 1613.77 1684.93 77.61 o 17 3 1 155.98 109.17 42.08 o 18 3 1 1300.42 1119.57 128.17 o 19 3 1 1487.42 1368.49 165.68 o 20 3 1 201.91 59.48 191.48 o -20 4 1 1.62 -54.59 188.95 o -19 4 1 61.81 -58.30 164.13 o -18 4 1 1.30 3.09 52.79 o -17 4 1 626.65 510.27 61.83 o -16 4 1 16.75 19.19 41.40 o -15 4 1 65.45 43.45 33.48 o -14 4 1 9.10 35.34 34.04 o -13 4 1 1560.08 1726.02 82.68 o -12 4 1 101.39 71.11 36.08 o -11 4 1 441.14 411.07 43.38 o -10 4 1 289.86 267.98 17.08 o -9 4 1 15.43 8.60 11.70 o -8 4 1 1107.75 1111.28 36.51 o -7 4 1 303.13 332.53 21.78 o -6 4 1 2028.88 1919.24 52.30 o -5 4 1 2488.63 2527.80 70.06 o -4 4 1 332.72 328.88 24.38 o -3 4 1 4696.05 4615.93 118.33 o -2 4 1 55.23 66.16 17.39 o -1 4 1 2126.01 1978.53 59.78 o 0 4 1 596.96 631.33 33.73 o 1 4 1 1567.62 1576.44 51.37 o 2 4 1 1177.32 1226.95 45.30 o 3 4 1 3223.19 3133.13 80.77 o 4 4 1 238.65 208.94 22.28 o 5 4 1 1948.05 1974.14 53.04 o 6 4 1 1440.94 1310.19 39.61 o 7 4 1 1542.53 1550.88 52.92 o 8 4 1 379.94 330.73 22.59 o 9 4 1 83.03 80.64 16.09 o 10 4 1 165.55 132.07 16.03 o 11 4 1 604.94 556.20 19.93 o 12 4 1 292.03 283.64 40.23 o 13 4 1 115.25 99.02 42.58 o 14 4 1 1015.37 943.93 67.27 o 15 4 1 133.88 34.78 40.17 o 16 4 1 0.10 46.48 44.06 o 17 4 1 788.82 752.94 68.26 o 18 4 1 89.05 128.67 160.29 o 19 4 1 84.72 121.98 174.77 o 20 4 1 84.91 78.41 150.70 o -20 5 1 147.06 234.87 212.71 o -19 5 1 77.39 -128.11 177.44 o -18 5 1 583.01 469.49 140.18 o -17 5 1 791.44 665.55 73.15 o -16 5 1 248.96 258.26 51.18 o -15 5 1 844.12 835.63 71.92 o -14 5 1 990.09 1081.63 76.93 o -13 5 1 457.47 429.45 51.55 o -12 5 1 105.29 15.47 35.21 o -11 5 1 1334.48 1232.15 40.17 o -10 5 1 699.82 699.35 31.56 o -9 5 1 4061.57 4100.46 95.56 o -8 5 1 820.55 790.26 33.54 o -7 5 1 5629.86 5939.86 122.73 o -6 5 1 65.97 17.89 16.65 o -5 5 1 10456.88 10715.40 216.30 o -4 5 1 3808.63 3827.96 98.53 o -3 5 1 11408.86 12299.70 248.30 o -2 5 1 381.34 267.98 25.25 o -1 5 1 113.39 55.70 24.14 o 0 5 1 9194.10 9259.46 225.03 o 1 5 1 871.30 825.60 41.47 o 2 5 1 2212.17 2074.89 65.73 o 3 5 1 2784.60 2839.59 79.53 o 4 5 1 9597.24 9573.30 223.91 o 5 5 1 20.91 -9.22 22.22 o 6 5 1 61.94 31.63 14.85 o 7 5 1 1435.86 1330.12 45.36 o 8 5 1 1118.44 1137.95 41.96 o 9 5 1 2317.60 2307.72 62.14 o 10 5 1 1.83 5.57 18.01 o 11 5 1 153.53 112.82 19.00 o 12 5 1 1818.47 1891.02 49.76 o 13 5 1 270.38 231.77 48.46 o 14 5 1 3233.96 3505.64 132.57 o 15 5 1 0.24 62.57 50.01 o 16 5 1 1491.11 1560.66 96.30 o 17 5 1 238.30 238.64 65.35 o 18 5 1 50.17 -74.08 113.07 o 19 5 1 17.09 220.57 183.25 o -19 6 1 228.44 56.44 198.85 o -18 6 1 1073.18 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