#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:19:58 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181004 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/84/2208499.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208499_Fobs loop_ _publ_author_name 'da Silva, Luiz Everson' 'Joussef, Antonio Carlos' 'Andrighetti-Fr\"ohner, Carla Regina' 'Sim\~oes, Cl\'audia Maria Olivra' 'Bortoluzzi, Adailton Jos\'e' _publ_section_title ; 5-(5-Ethyl-1,3,4-thiadiazol-2-ylaminomethylene)-2,2-dimethyl-1,3-dioxane- 4,6-dione ; _journal_coeditor_code BH6071 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1520 _journal_page_last o1521 _journal_volume 62 _journal_year 2006 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.7330 _cell_length_b 9.8420 _cell_length_c 24.6500 _exptl_crystal_F_000 1184.00 _reflns_d_resolution_high 0.8115 _cod_data_source_file bh6071Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 49cp in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 355.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 145.17 129.58 6.89 o 4 0 0 15542.30 15333.15 192.96 o 6 0 0 1263.42 1513.94 44.40 o 8 0 0 1119.77 1076.17 34.23 o 10 0 0 110.52 112.41 19.77 o 12 0 0 4.27 -25.76 49.03 o 2 1 0 644.90 575.59 17.96 o 4 1 0 5211.79 5505.70 116.81 o 6 1 0 3045.45 2981.79 77.61 o 8 1 0 560.79 507.81 24.97 o 10 1 0 5.19 8.92 16.95 o 12 1 0 991.30 1122.60 47.45 o 0 2 0 55697.44 45841.95 234.19 o 2 2 0 3142.43 3036.24 71.85 o 4 2 0 149.61 161.32 10.62 o 6 2 0 697.68 880.62 26.66 o 8 2 0 1313.00 1191.63 38.86 o 10 2 0 965.40 1005.11 39.31 o 12 2 0 582.48 562.83 37.28 o 2 3 0 871.22 806.06 22.03 o 4 3 0 1053.07 943.09 28.58 o 6 3 0 972.91 910.44 27.00 o 8 3 0 55.64 73.54 17.28 o 10 3 0 98.56 123.25 20.11 o 12 3 0 235.96 317.79 29.60 o 0 4 0 348.46 374.84 12.99 o 2 4 0 1032.55 972.80 27.57 o 4 4 0 4503.51 4988.74 133.08 o 6 4 0 1574.46 1649.05 45.87 o 8 4 0 932.25 914.96 33.55 o 10 4 0 42.64 58.41 18.87 o 12 4 0 302.00 249.22 29.94 o 2 5 0 1550.74 1485.58 43.04 o 4 5 0 2047.02 2247.02 69.36 o 6 5 0 0.07 -14.69 30.16 o 8 5 0 2559.69 2460.19 76.03 o 10 5 0 0.53 18.87 13.90 o 12 5 0 38.32 83.83 21.35 o 0 6 0 2253.67 2273.45 68.12 o 2 6 0 15.82 8.13 30.05 o 4 6 0 361.80 386.03 20.33 o 6 6 0 5.82 10.62 33.44 o 8 6 0 192.67 215.21 22.14 o 10 6 0 8.44 0.00 34.34 o 2 7 0 67.95 70.61 13.78 o 4 7 0 436.88 474.14 24.40 o 6 7 0 4024.72 4240.30 121.11 o 8 7 0 2.79 28.58 45.75 o 10 7 0 161.50 131.39 26.10 o 0 8 0 1994.01 1997.69 64.06 o 2 8 0 1480.49 1428.53 39.88 o 4 8 0 83.92 84.39 16.27 o 6 8 0 158.67 136.36 21.13 o 8 8 0 83.74 100.21 18.75 o 2 9 0 841.00 696.36 32.54 o 4 9 0 507.98 573.67 30.84 o 6 9 0 1042.99 1039.12 43.04 o 8 9 0 50.98 82.13 20.33 o 0 10 0 871.29 888.07 36.49 o 2 10 0 502.06 436.19 29.15 o 4 10 0 255.13 283.79 26.77 o 6 10 0 440.62 436.98 31.63 o 2 11 0 163.74 160.42 27.57 o 4 11 0 110.77 139.41 21.13 o 0 12 0 120.10 147.43 24.29 o 1 1 1 10.91 9.04 4.07 o 2 1 1 17.89 63.26 6.67 o 3 1 1 141.93 141.78 8.47 o 4 1 1 8332.46 8293.51 144.38 o 5 1 1 484.36 493.01 17.28 o 6 1 1 509.98 460.70 20.90 o 7 1 1 2.49 -4.41 30.84 o 8 1 1 0.20 39.31 11.64 o 9 1 1 18.66 16.04 15.14 o 10 1 1 2.37 -34.91 39.31 o 11 1 1 59.33 54.45 20.56 o 12 1 1 75.16 102.69 22.37 o 13 1 1 0.21 -50.16 66.20 o 0 2 1 5537.09 5524.79 83.15 o 1 2 1 1035.11 1032.68 27.79 o 2 2 1 11150.64 10985.07 136.13 o 3 2 1 2073.95 1904.37 46.66 o 4 2 1 2080.20 2467.99 58.52 o 5 2 1 5625.14 5774.46 138.73 o 6 2 1 123.49 138.05 12.54 o 7 2 1 74.96 26.21 13.56 o 8 2 1 179.19 149.12 18.75 o 9 2 1 641.66 564.41 29.03 o 10 2 1 1.20 -27.45 45.41 o 11 2 1 41.54 38.07 19.09 o 12 2 1 88.98 78.18 22.59 o 13 2 1 16.40 9.60 55.13 o 1 3 1 250.47 258.37 10.62 o 2 3 1 434.51 427.37 13.90 o 3 3 1 222.27 226.17 10.62 o 4 3 1 3192.43 3059.51 69.48 o 5 3 1 23.93 31.86 9.83 o 6 3 1 1125.36 1037.08 31.18 o 7 3 1 129.09 116.47 16.49 o 8 3 1 1061.44 1034.37 33.21 o 9 3 1 1.66 -24.29 43.49 o 10 3 1 634.94 578.53 32.87 o 11 3 1 53.63 64.17 19.43 o 12 3 1 1419.07 1454.29 53.66 o 0 4 1 3451.30 3255.29 90.15 o 1 4 1 1749.96 1788.35 48.92 o 2 4 1 4424.43 4279.16 109.36 o 3 4 1 23.69 25.31 8.13 o 4 4 1 2.92 10.62 22.82 o 5 4 1 8.77 -21.24 21.24 o 6 4 1 1213.90 1172.54 40.11 o 7 4 1 74.04 94.90 14.69 o 8 4 1 1636.52 1558.00 46.77 o 9 4 1 870.64 846.84 34.57 o 10 4 1 901.27 940.61 39.65 o 11 4 1 1.07 -32.42 45.64 o 12 4 1 150.05 96.82 25.87 o 1 5 1 44.90 45.41 8.13 o 2 5 1 3453.85 3415.71 79.08 o 3 5 1 36.26 0.00 25.31 o 4 5 1 169.22 219.17 15.48 o 5 5 1 7.86 0.00 26.21 o 6 5 1 2285.62 2255.15 65.52 o 7 5 1 215.11 230.01 19.54 o 8 5 1 1910.38 1729.04 52.42 o 9 5 1 0.83 0.00 37.62 o 10 5 1 468.11 469.51 29.60 o 11 5 1 43.54 59.99 18.87 o 12 5 1 566.79 592.99 38.75 o 0 6 1 3706.28 3652.39 86.08 o 1 6 1 247.00 284.12 16.27 o 2 6 1 6015.97 6354.34 164.26 o 3 6 1 20.01 15.36 10.51 o 4 6 1 64.28 69.14 12.20 o 5 6 1 712.03 751.04 28.47 o 6 6 1 2703.28 2752.11 90.60 o 7 6 1 179.72 187.08 21.24 o 8 6 1 148.67 166.30 21.24 o 9 6 1 85.24 84.84 20.45 o 10 6 1 0.15 48.24 15.59 o 11 6 1 0.51 -43.38 43.38 o 1 7 1 12.80 17.85 24.40 o 2 7 1 40.11 17.85 12.99 o 3 7 1 7.98 27.57 10.51 o 4 7 1 41.73 24.29 13.78 o 5 7 1 10.72 11.41 34.91 o 6 7 1 4144.14 4042.03 120.65 o 7 7 1 35.50 40.90 16.38 o 8 7 1 417.12 340.27 27.68 o 9 7 1 116.14 119.98 19.54 o 10 7 1 87.56 84.96 21.24 o 0 8 1 83.52 75.47 14.57 o 1 8 1 81.11 73.88 15.48 o 2 8 1 11.79 26.77 12.20 o 3 8 1 53.84 71.40 15.36 o 4 8 1 0.15 12.20 34.12 o 5 8 1 161.04 164.71 18.64 o 6 8 1 78.32 51.97 19.54 o 7 8 1 179.50 147.54 23.61 o 8 8 1 34.25 50.50 18.75 o 9 8 1 2.47 -17.06 49.59 o 1 9 1 46.16 24.29 42.14 o 2 9 1 0.84 -37.28 37.28 o 3 9 1 203.96 191.94 21.01 o 4 9 1 62.34 31.63 16.27 o 5 9 1 2.14 -41.46 41.46 o 6 9 1 52.64 38.18 48.80 o 7 9 1 54.19 63.49 17.85 o 8 9 1 261.72 236.90 27.57 o 0 10 1 89.37 77.84 19.43 o 1 10 1 1.67 21.13 44.62 o 2 10 1 490.57 564.18 29.15 o 3 10 1 57.86 59.20 17.85 o 4 10 1 383.65 410.43 30.84 o 5 10 1 5.23 8.13 17.06 o 6 10 1 88.90 0.00 65.86 o 7 10 1 5.43 8.92 38.98 o 1 11 1 36.95 25.08 18.64 o 2 11 1 1029.46 1085.44 45.41 o 3 11 1 10.17 17.85 16.27 o 4 11 1 109.00 34.91 50.39 o 5 11 1 0.05 0.00 49.59 o 0 12 1 7.61 15.36 17.85 o 1 12 1 87.68 62.36 24.29 o 0 0 2 38561.35 31444.67 495.83 o 1 0 2 1437.44 1415.20 35.93 o 2 0 2 23623.42 19315.98 160.42 o 3 0 2 19896.46 17928.68 186.07 o 4 0 2 5032.33 5044.09 114.21 o 5 0 2 177.84 199.85 13.22 o 6 0 2 654.13 689.81 22.82 o 7 0 2 0.71 0.00 24.63 o 8 0 2 977.78 1006.58 33.33 o 9 0 2 1147.42 1174.12 38.75 o 10 0 2 1147.00 1168.58 43.04 o 11 0 2 605.64 572.88 33.33 o 12 0 2 15.48 0.00 42.82 o 13 0 2 9.82 9.60 48.80 o 1 1 2 22284.75 19302.99 136.81 o 2 1 2 6410.97 6182.63 94.44 o 3 1 2 5035.97 4811.71 97.61 o 4 1 2 9950.45 9247.79 153.19 o 5 1 2 776.07 832.49 25.31 o 6 1 2 5393.81 5339.97 147.54 o 7 1 2 108.10 99.75 14.12 o 8 1 2 706.58 665.29 28.36 o 9 1 2 8.75 -6.21 32.99 o 10 1 2 30.70 49.14 15.14 o 11 1 2 13.69 -16.04 41.91 o 12 1 2 749.54 725.73 40.22 o 13 1 2 44.81 76.71 23.16 o 0 2 2 4340.40 4712.97 79.19 o 1 2 2 3644.40 3326.13 69.48 o 2 2 2 3382.34 3072.50 74.67 o 3 2 2 3292.17 3024.60 82.47 o 4 2 2 409.83 452.34 14.23 o 5 2 2 517.55 609.37 20.90 o 6 2 2 1208.72 1151.86 32.08 o 7 2 2 481.80 474.26 22.93 o 8 2 2 2055.68 1860.09 53.77 o 9 2 2 193.72 178.61 19.66 o 10 2 2 2044.53 1859.97 57.73 o 11 2 2 8.81 -18.19 19.09 o 12 2 2 129.07 122.80 24.40 o 13 2 2 118.44 131.27 24.51 o 1 3 2 3525.53 3443.28 84.05 o 2 3 2 1023.91 941.06 27.90 o 3 3 2 93.02 84.96 9.04 o 4 3 2 5629.37 5328.11 129.58 o 5 3 2 167.91 199.17 13.22 o 6 3 2 39.03 18.19 10.73 o 7 3 2 101.79 83.03 14.12 o 8 3 2 49.97 34.34 16.72 o 9 3 2 616.56 637.61 31.97 o 10 3 2 356.36 346.94 27.79 o 11 3 2 48.03 46.77 19.54 o 12 3 2 180.49 224.93 27.23 o 0 4 2 1642.43 1656.17 47.34 o 1 4 2 1081.09 1062.16 31.75 o 2 4 2 1238.36 1243.15 35.93 o 3 4 2 3.78 23.72 6.55 o 4 4 2 0.19 6.55 9.04 o 5 4 2 683.42 693.87 23.72 o 6 4 2 2146.60 2067.62 59.76 o 7 4 2 0.22 14.80 33.67 o 8 4 2 55.96 62.47 18.08 o 9 4 2 15.40 -25.64 43.04 o 10 4 2 329.66 347.95 26.55 o 11 4 2 4.01 -48.35 48.35 o 12 4 2 103.62 84.96 25.19 o 1 5 2 163.42 170.25 12.99 o 2 5 2 358.27 381.17 17.06 o 3 5 2 1802.46 1913.18 63.60 o 4 5 2 669.41 691.16 23.72 o 5 5 2 1242.92 1286.41 36.72 o 6 5 2 2.24 -31.07 31.07 o 7 5 2 774.07 779.62 31.07 o 8 5 2 822.47 891.58 35.13 o 9 5 2 257.25 221.65 21.35 o 10 5 2 36.22 58.41 18.08 o 11 5 2 119.37 125.29 21.46 o 12 5 2 24.89 -28.13 53.77 o 0 6 2 282.46 270.68 16.27 o 1 6 2 1515.75 1427.18 45.41 o 2 6 2 157.59 173.07 14.57 o 3 6 2 832.96 869.09 26.89 o 4 6 2 689.57 659.53 26.10 o 5 6 2 0.01 -24.51 24.51 o 6 6 2 668.60 671.39 30.16 o 7 6 2 784.70 825.94 32.65 o 8 6 2 113.11 99.64 19.54 o 9 6 2 26.24 36.83 50.72 o 10 6 2 201.04 196.12 24.63 o 11 6 2 32.34 0.00 58.18 o 1 7 2 85.64 76.26 12.99 o 2 7 2 144.40 162.23 14.57 o 3 7 2 23.27 49.48 12.20 o 4 7 2 1036.31 1018.33 34.12 o 5 7 2 1.17 -28.58 37.62 o 6 7 2 1030.66 996.87 36.72 o 7 7 2 63.01 58.63 17.06 o 8 7 2 226.98 217.92 26.10 o 9 7 2 11.14 -50.61 50.61 o 10 7 2 74.68 138.62 22.03 o 0 8 2 1325.60 1285.96 36.49 o 1 8 2 28.59 54.34 12.99 o 2 8 2 1081.68 1101.03 35.70 o 3 8 2 40.47 50.27 13.78 o 4 8 2 177.53 166.52 19.54 o 5 8 2 35.39 -12.99 48.80 o 6 8 2 77.61 113.88 17.06 o 7 8 2 221.09 222.67 23.61 o 8 8 2 143.07 148.11 21.92 o 9 8 2 53.93 0.00 51.29 o 1 9 2 2.95 -14.57 14.57 o 2 9 2 632.18 620.44 31.63 o 3 9 2 38.34 0.00 35.70 o 4 9 2 974.54 848.19 36.60 o 5 9 2 13.14 48.01 16.27 o 6 9 2 191.33 191.60 21.92 o 7 9 2 46.21 99.08 18.64 o 8 9 2 118.20 81.23 25.19 o 0 10 2 615.85 598.30 32.42 o 1 10 2 7.99 12.20 16.27 o 2 10 2 251.87 237.58 24.29 o 3 10 2 135.25 152.51 21.13 o 4 10 2 1.42 7.34 50.39 o 5 10 2 44.53 32.42 58.41 o 6 10 2 205.91 232.61 26.77 o 7 10 2 7.74 0.00 38.07 o 1 11 2 0.80 5.65 15.36 o 2 11 2 36.87 0.00 44.74 o 3 11 2 121.64 131.73 22.71 o 4 11 2 153.57 144.60 22.71 o 5 11 2 23.02 0.00 49.37 o 0 12 2 152.51 198.49 25.08 o 1 12 2 0.02 18.64 46.32 o 1 1 3 8009.21 7957.19 95.01 o 2 1 3 33.52 52.53 6.78 o 3 1 3 2662.52 2869.04 78.63 o 4 1 3 177.78 186.74 11.18 o 5 1 3 543.04 565.43 20.11 o 6 1 3 2100.97 2409.81 70.72 o 7 1 3 13.50 14.12 21.13 o 8 1 3 95.97 116.02 15.93 o 9 1 3 77.12 31.07 49.71 o 10 1 3 553.49 533.91 29.49 o 11 1 3 0.91 -32.08 57.05 o 12 1 3 42.68 37.39 22.26 o 13 1 3 71.66 157.71 24.06 o 0 2 3 4691.14 4692.52 83.37 o 1 2 3 1276.99 1344.48 33.78 o 2 2 3 387.14 370.21 11.52 o 3 2 3 2185.79 2064.34 49.37 o 4 2 3 1027.52 1060.47 32.65 o 5 2 3 372.57 358.12 16.04 o 6 2 3 81.07 64.28 11.86 o 7 2 3 1104.18 1056.06 32.42 o 8 2 3 1112.19 1065.67 35.81 o 9 2 3 60.77 47.34 16.38 o 10 2 3 766.80 807.64 35.47 o 11 2 3 5.79 -7.80 19.09 o 12 2 3 3.41 -27.00 46.21 o 1 3 3 173.41 146.30 9.04 o 2 3 3 2652.83 2481.89 53.89 o 3 3 3 366.62 367.39 13.10 o 4 3 3 4268.71 4320.96 117.04 o 5 3 3 27.52 23.95 10.73 o 6 3 3 2511.32 2718.34 78.06 o 7 3 3 5.37 4.97 29.26 o 8 3 3 6.06 37.05 13.44 o 9 3 3 285.28 247.63 23.61 o 10 3 3 270.16 254.87 23.84 o 11 3 3 6.37 -16.16 32.42 o 12 3 3 421.79 377.10 33.33 o 0 4 3 572.30 576.72 17.06 o 1 4 3 2074.38 2126.36 54.79 o 2 4 3 69.83 90.04 9.04 o 3 4 3 70.56 87.44 10.62 o 4 4 3 373.97 414.27 18.87 o 5 4 3 18.96 35.25 9.83 o 6 4 3 2471.35 2408.34 78.06 o 7 4 3 29.81 37.05 12.31 o 8 4 3 2501.54 2425.06 74.56 o 9 4 3 107.41 106.31 18.30 o 10 4 3 1628.67 1501.63 53.44 o 11 4 3 0.08 0.00 45.41 o 12 4 3 377.83 433.02 32.08 o 1 5 3 578.90 643.49 20.33 o 2 5 3 3261.88 3227.73 76.60 o 3 5 3 249.74 255.99 15.59 o 4 5 3 3672.27 3590.82 88.12 o 5 5 3 203.18 210.02 17.17 o 6 5 3 243.07 204.93 19.66 o 7 5 3 347.84 333.61 22.93 o 8 5 3 293.94 322.65 23.84 o 9 5 3 1.87 -27.90 35.36 o 10 5 3 30.71 52.87 16.49 o 11 5 3 246.32 225.04 28.13 o 0 6 3 5433.50 4887.06 144.27 o 1 6 3 102.45 111.50 12.99 o 2 6 3 2042.24 2104.78 56.26 o 3 6 3 170.09 188.66 15.48 o 4 6 3 46.40 52.08 12.99 o 5 6 3 28.17 39.20 11.41 o 6 6 3 1046.67 994.83 34.23 o 7 6 3 65.69 35.13 17.96 o 8 6 3 135.20 131.05 20.45 o 9 6 3 11.29 0.00 44.29 o 10 6 3 123.54 123.82 22.14 o 11 6 3 38.84 70.72 18.87 o 1 7 3 15.39 4.86 28.36 o 2 7 3 90.74 87.55 14.57 o 3 7 3 24.06 26.10 11.41 o 4 7 3 965.76 1031.89 34.23 o 5 7 3 196.66 181.43 18.75 o 6 7 3 7.11 6.55 37.39 o 7 7 3 33.73 20.45 38.41 o 8 7 3 757.90 714.66 35.93 o 9 7 3 150.04 116.02 21.24 o 10 7 3 9.10 16.38 18.87 o 0 8 3 511.90 536.17 25.98 o 1 8 3 34.49 50.27 12.99 o 2 8 3 412.73 424.32 24.29 o 3 8 3 138.99 174.09 18.75 o 4 8 3 24.80 -12.20 43.95 o 5 8 3 61.99 77.16 15.48 o 6 8 3 0.47 27.68 46.43 o 7 8 3 84.19 50.50 18.75 o 8 8 3 2.66 8.13 44.85 o 9 8 3 20.26 -26.10 44.85 o 1 9 3 16.96 0.00 34.00 o 2 9 3 0.01 -25.19 38.98 o 3 9 3 598.62 645.86 30.95 o 4 9 3 37.50 13.78 48.69 o 5 9 3 3.78 0.00 35.59 o 6 9 3 235.73 238.71 25.19 o 7 9 3 282.96 314.29 25.19 o 8 9 3 18.87 25.98 18.75 o 0 10 3 8.07 12.99 16.27 o 1 10 3 48.73 -43.04 46.21 o 2 10 3 5.36 -43.04 43.04 o 3 10 3 7.56 -7.34 40.67 o 4 10 3 177.75 176.69 21.92 o 5 10 3 3.75 28.36 15.36 o 6 10 3 4.68 -34.00 52.65 o 7 10 3 32.19 17.85 21.13 o 1 11 3 16.11 24.40 37.39 o 2 11 3 88.46 104.84 23.61 o 3 11 3 12.90 17.06 37.28 o 4 11 3 188.48 228.32 25.08 o 5 11 3 13.13 0.00 49.37 o 0 12 3 11.64 8.92 39.77 o 1 12 3 151.64 144.94 25.87 o 0 0 4 1391.07 1349.00 39.20 o 1 0 4 309.39 243.68 8.92 o 2 0 4 11314.87 10503.47 130.82 o 3 0 4 405.24 413.14 12.54 o 4 0 4 352.96 376.42 14.35 o 5 0 4 6995.86 7415.38 159.52 o 6 0 4 3921.50 4070.16 92.07 o 7 0 4 49.58 56.60 12.43 o 8 0 4 2532.69 2433.31 69.93 o 9 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2124.29 2324.06 62.93 o 5 3 4 3827.63 3865.68 87.21 o 6 3 4 1544.83 1509.42 43.49 o 7 3 4 296.77 299.83 19.32 o 8 3 4 347.85 357.10 22.71 o 9 3 4 7.27 -45.87 45.87 o 10 3 4 425.72 435.62 28.92 o 11 3 4 9.82 -32.42 35.81 o 12 3 4 106.97 145.62 23.95 o 0 4 4 62.83 73.54 8.13 o 1 4 4 1687.97 1812.53 52.19 o 2 4 4 1626.41 1607.71 50.72 o 3 4 4 3032.56 3224.23 74.45 o 4 4 4 744.29 757.03 23.72 o 5 4 4 315.47 308.08 18.08 o 6 4 4 693.44 715.11 26.44 o 7 4 4 90.81 62.13 14.91 o 8 4 4 89.56 137.71 18.30 o 9 4 4 205.03 158.50 22.48 o 10 4 4 49.87 65.41 18.41 o 11 4 4 0.86 34.57 16.04 o 12 4 4 1.42 28.02 48.35 o 1 5 4 1216.98 1155.03 33.44 o 2 5 4 1063.33 1197.50 34.23 o 3 5 4 47.59 64.39 10.62 o 4 5 4 1130.48 1274.10 34.34 o 5 5 4 187.19 162.23 16.38 o 6 5 4 987.52 913.49 31.97 o 7 5 4 6.02 6.55 14.80 o 8 5 4 16.13 0.00 40.33 o 9 5 4 5.53 -2.49 14.91 o 10 5 4 14.67 34.80 17.40 o 11 5 4 0.10 -35.02 38.30 o 0 6 4 342.94 268.53 17.06 o 1 6 4 805.18 797.13 25.31 o 2 6 4 1.79 8.13 29.37 o 3 6 4 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11 199.64 249.22 18.87 o 2 7 11 729.46 751.26 32.08 o 3 7 11 35.11 18.08 40.33 o 4 7 11 134.89 123.70 18.98 o 5 7 11 130.27 128.45 17.28 o 6 7 11 112.80 100.77 19.77 o 7 7 11 600.12 568.59 34.80 o 8 7 11 49.98 33.21 48.13 o 9 7 11 4.18 -26.55 46.43 o 0 8 11 58.31 39.99 14.69 o 1 8 11 717.90 677.27 31.86 o 2 8 11 188.46 227.41 19.66 o 3 8 11 433.12 358.35 25.53 o 4 8 11 47.49 53.44 17.28 o 5 8 11 407.87 420.82 29.60 o 6 8 11 7.23 -7.46 42.03 o 7 8 11 177.20 207.08 23.16 o 8 8 11 0.54 18.19 39.77 o 1 9 11 204.46 179.51 22.82 o 2 9 11 36.03 31.86 16.38 o 3 9 11 25.05 30.28 16.38 o 4 9 11 40.96 38.64 18.08 o 5 9 11 62.26 51.74 18.87 o 6 9 11 3.96 -34.57 43.61 o 7 9 11 162.38 176.69 25.53 o 0 10 11 27.84 69.82 20.33 o 1 10 11 58.08 83.94 21.24 o 2 10 11 34.87 -24.51 57.95 o 3 10 11 8.47 -8.13 44.96 o 4 10 11 0.68 9.04 48.35 o 5 10 11 2.72 -45.08 54.90 o 1 11 11 3.73 -44.74 54.45 o 2 11 11 12.34 -43.04 43.04 o 0 0 12 1483.76 1414.41 40.44 o 1 0 12 1349.93 1250.04 39.43 o 2 0 12 1406.81 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