#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:20:43 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181007 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/87/2208780.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208780_Fobs loop_ _publ_author_name 'Xie, Yong-Rong' 'Lui, Gui-Rong' 'Yuan, Xiao-Yong' _publ_section_title ; Potassium 2-methyl-5-nitrobenzenesulfonate ; _journal_coeditor_code AC2015 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1016 _journal_page_last m1017 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.652 _cell_angle_gamma 90.000 _cell_length_a 14.1394 _cell_length_b 9.3670 _cell_length_c 7.1241 _exptl_crystal_F_000 520.00 _reflns_d_resolution_high 0.7606 _cod_data_source_file ac2015Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' lgr in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 223.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4519.12 4661.13 79.92 o 2 0 0 1014.73 1007.08 12.65 o 3 0 0 2387.44 2393.24 46.58 o 4 0 0 10900.83 11218.72 136.49 o 5 0 0 7200.86 7531.19 90.59 o 6 0 0 7116.20 7647.45 92.19 o 7 0 0 238.39 255.46 4.62 o 8 0 0 140.84 143.03 4.70 o 9 0 0 3.26 6.33 1.65 o 10 0 0 319.87 286.25 5.95 o 11 0 0 2888.44 2838.76 36.36 o 12 0 0 804.88 821.70 12.70 o 13 0 0 245.82 253.31 8.96 o 14 0 0 0.56 3.98 3.98 o 15 0 0 1669.18 1664.85 33.44 o 16 0 0 448.98 462.92 14.03 o 17 0 0 105.78 120.28 8.31 o 18 0 0 7.39 4.33 6.47 o 1 1 0 737.50 732.74 6.50 o 2 1 0 2740.41 2842.39 24.32 o 3 1 0 962.75 977.60 10.11 o 4 1 0 2754.78 2641.97 26.33 o 5 1 0 9.35 3.87 0.66 o 6 1 0 3.84 1.07 0.71 o 7 1 0 313.39 323.00 3.85 o 8 1 0 0.33 1.04 0.92 o 9 1 0 176.10 173.63 4.91 o 10 1 0 1203.80 1190.21 11.69 o 11 1 0 113.18 120.18 2.90 o 12 1 0 0.92 2.14 1.94 o 13 1 0 243.47 249.21 5.18 o 14 1 0 19.79 19.21 3.20 o 15 1 0 40.06 38.30 3.85 o 16 1 0 87.05 83.72 6.54 o 17 1 0 9.04 7.07 5.87 o 18 1 0 28.80 11.20 6.67 o 0 2 0 7528.56 7617.45 92.17 o 1 2 0 40.58 45.26 0.93 o 2 2 0 1636.48 1595.30 12.44 o 3 2 0 643.10 684.61 6.51 o 4 2 0 4975.03 4975.60 46.65 o 5 2 0 1936.67 1974.92 25.12 o 6 2 0 761.06 811.22 9.15 o 7 2 0 2812.56 2854.38 29.05 o 8 2 0 2160.25 1990.76 18.06 o 9 2 0 1047.61 1085.11 10.65 o 10 2 0 64.97 68.48 2.11 o 11 2 0 159.46 168.76 4.29 o 12 2 0 246.92 239.22 4.93 o 13 2 0 248.90 248.51 7.41 o 14 2 0 85.64 90.90 4.54 o 15 2 0 67.68 67.58 6.02 o 16 2 0 9.83 9.06 5.47 o 17 2 0 73.57 81.02 7.86 o 1 3 0 1057.84 1156.80 15.35 o 2 3 0 413.48 365.40 3.42 o 3 3 0 97.25 77.44 1.42 o 4 3 0 322.20 307.97 3.86 o 5 3 0 124.14 113.44 3.23 o 6 3 0 20.18 18.15 1.10 o 7 3 0 187.94 203.82 11.28 o 8 3 0 300.56 338.00 5.06 o 9 3 0 11.90 10.09 1.56 o 10 3 0 200.18 211.07 4.23 o 11 3 0 130.30 124.97 3.53 o 12 3 0 2.25 -2.40 2.55 o 13 3 0 235.04 224.67 8.88 o 14 3 0 89.88 102.18 5.13 o 15 3 0 97.78 95.55 5.92 o 16 3 0 3.89 -0.50 4.88 o 17 3 0 32.54 39.22 6.57 o 0 4 0 174.06 154.79 2.60 o 1 4 0 187.77 206.07 2.80 o 2 4 0 344.14 334.31 5.12 o 3 4 0 461.66 469.52 5.43 o 4 4 0 522.10 524.01 4.91 o 5 4 0 54.75 59.12 1.67 o 6 4 0 43.67 41.73 1.52 o 7 4 0 1108.78 1139.83 11.07 o 8 4 0 1163.75 1160.91 13.16 o 9 4 0 718.23 718.71 11.66 o 10 4 0 64.73 58.38 9.23 o 11 4 0 46.93 45.61 3.50 o 12 4 0 79.21 83.84 7.64 o 13 4 0 301.65 300.10 16.52 o 14 4 0 57.57 51.98 5.08 o 15 4 0 0.14 0.77 3.81 o 16 4 0 0.20 0.50 5.28 o 1 5 0 79.30 90.97 2.10 o 2 5 0 396.79 328.78 3.21 o 3 5 0 445.29 421.51 4.28 o 4 5 0 492.86 482.24 4.11 o 5 5 0 143.46 140.78 2.30 o 6 5 0 157.51 158.31 7.51 o 7 5 0 66.76 64.43 2.55 o 8 5 0 175.30 170.66 4.10 o 9 5 0 2.11 1.01 2.43 o 10 5 0 345.34 338.20 7.70 o 11 5 0 3.95 4.87 2.91 o 12 5 0 115.74 110.24 5.06 o 13 5 0 187.94 192.82 7.19 o 14 5 0 157.85 168.14 6.58 o 15 5 0 90.06 84.89 5.64 o 16 5 0 0.21 -1.64 6.82 o 0 6 0 1513.44 1568.70 20.35 o 1 6 0 1848.63 1816.43 13.49 o 2 6 0 752.34 745.40 6.24 o 3 6 0 742.44 768.92 7.18 o 4 6 0 207.84 219.14 3.59 o 5 6 0 2070.46 2109.93 19.55 o 6 6 0 10.24 10.95 2.16 o 7 6 0 1350.26 1299.33 15.16 o 8 6 0 1608.88 1549.19 20.45 o 9 6 0 1.21 0.17 2.74 o 10 6 0 54.37 51.99 3.94 o 11 6 0 0.01 1.34 2.94 o 12 6 0 7.54 2.19 3.59 o 13 6 0 42.99 42.48 4.58 o 14 6 0 162.55 148.90 6.62 o 15 6 0 250.31 247.28 12.84 o 1 7 0 46.43 52.89 2.94 o 2 7 0 1.69 2.80 1.31 o 3 7 0 177.99 185.95 3.11 o 4 7 0 3.09 1.72 1.30 o 5 7 0 3962.20 3999.82 35.64 o 6 7 0 1477.59 1531.86 21.52 o 7 7 0 749.44 767.83 13.63 o 8 7 0 61.89 61.13 3.43 o 9 7 0 427.50 412.00 9.07 o 10 7 0 1108.01 1155.15 25.06 o 11 7 0 408.56 436.18 9.97 o 12 7 0 72.51 72.45 4.97 o 13 7 0 114.27 108.98 6.04 o 14 7 0 93.54 105.48 6.43 o 0 8 0 115.45 141.07 5.95 o 1 8 0 375.00 377.03 6.99 o 2 8 0 121.33 122.28 3.18 o 3 8 0 33.53 30.43 2.11 o 4 8 0 75.01 70.78 2.66 o 5 8 0 130.67 131.35 4.00 o 6 8 0 15.01 19.17 2.62 o 7 8 0 1.08 3.30 2.95 o 8 8 0 0.65 1.13 2.64 o 9 8 0 150.73 175.74 5.28 o 10 8 0 14.73 20.68 4.09 o 11 8 0 56.03 70.37 9.88 o 12 8 0 66.53 64.76 9.78 o 1 9 0 439.00 394.86 8.46 o 2 9 0 292.08 346.29 6.43 o 3 9 0 151.59 167.05 5.88 o 4 9 0 4.22 4.29 3.17 o 5 9 0 109.29 107.89 10.50 o 6 9 0 91.32 102.63 4.19 o 7 9 0 16.04 18.17 3.26 o 8 9 0 13.64 10.83 3.24 o 9 9 0 146.82 147.42 6.88 o 10 9 0 205.78 214.39 8.16 o 11 9 0 2.47 1.85 4.73 o 0 10 0 860.48 795.85 19.66 o 1 10 0 122.31 122.60 5.47 o 2 10 0 3.38 6.72 4.98 o 3 10 0 2.96 1.00 5.13 o 4 10 0 82.44 77.49 5.02 o 5 10 0 110.75 104.11 9.75 o 6 10 0 192.24 176.87 6.78 o 7 10 0 5.10 5.48 4.22 o 8 10 0 11.80 16.40 4.71 o 9 10 0 0.77 1.64 6.52 o 10 10 0 0.13 -0.40 6.82 o 1 11 0 163.37 173.83 9.65 o 2 11 0 165.34 170.89 9.70 o 3 11 0 80.46 72.01 7.81 o 4 11 0 3.69 -0.70 6.47 o 5 11 0 13.20 18.81 7.02 o 6 11 0 17.59 17.92 7.51 o 8 11 0 8.62 4.78 7.42 o 2 12 0 71.52 75.79 8.96 o -18 1 1 37.86 39.02 7.17 o -17 1 1 10.86 10.73 4.19 o -16 1 1 202.11 220.05 7.09 o -15 1 1 112.80 101.97 4.89 o -14 1 1 11.91 9.13 2.94 o -13 1 1 7.16 9.19 2.67 o -12 1 1 853.33 847.93 13.62 o -11 1 1 2094.08 2048.19 24.67 o -10 1 1 653.99 642.25 8.23 o -9 1 1 333.17 323.66 4.13 o -8 1 1 2119.22 2186.41 19.60 o -7 1 1 2942.56 2977.44 26.11 o -6 1 1 3786.21 3826.46 29.46 o -5 1 1 32.86 32.62 1.30 o -4 1 1 3888.46 4187.06 31.97 o -3 1 1 5914.59 6043.89 51.48 o -2 1 1 1489.02 1604.31 13.88 o -1 1 1 712.43 746.35 7.48 o 0 1 1 1413.15 1479.07 12.85 o 1 1 1 4142.55 4285.62 34.96 o 2 1 1 1247.17 1232.66 23.24 o 3 1 1 1850.72 1829.20 20.12 o 4 1 1 2002.78 1838.70 23.35 o 5 1 1 915.20 863.48 14.89 o 6 1 1 3.15 1.50 0.90 o 7 1 1 234.31 221.76 3.13 o 8 1 1 134.58 128.45 2.49 o 9 1 1 477.59 452.82 5.42 o 10 1 1 177.43 186.15 5.12 o 11 1 1 100.08 80.31 2.43 o 12 1 1 313.33 321.70 5.37 o 13 1 1 0.34 2.91 2.17 o 14 1 1 8.04 6.49 2.52 o 15 1 1 1.76 1.34 4.73 o 16 1 1 42.86 42.95 6.42 o 17 1 1 75.84 80.67 7.81 o -17 2 1 401.08 419.87 14.48 o -16 2 1 71.60 76.84 7.17 o -15 2 1 64.70 73.15 9.70 o -14 2 1 2.14 1.22 2.90 o -13 2 1 7.90 6.63 2.27 o -12 2 1 205.08 195.42 4.52 o -11 2 1 548.78 522.81 7.40 o -10 2 1 832.42 821.54 10.09 o -9 2 1 1411.26 1455.35 16.00 o -8 2 1 5.19 2.38 0.96 o -7 2 1 1884.61 2053.47 16.43 o -6 2 1 407.31 417.62 4.66 o -5 2 1 6831.36 7525.52 57.13 o -4 2 1 588.01 624.76 6.11 o -3 2 1 1911.45 1931.57 16.94 o -2 2 1 5613.92 5658.12 43.06 o -1 2 1 5004.25 5084.36 35.15 o 0 2 1 4167.77 4320.38 29.15 o 1 2 1 3.34 5.10 0.68 o 2 2 1 320.84 323.39 5.03 o 3 2 1 4509.17 4611.23 45.38 o 4 2 1 2003.20 1986.53 20.19 o 5 2 1 3703.95 3677.65 36.67 o 6 2 1 4411.32 4735.21 47.06 o 7 2 1 644.08 689.88 9.38 o 8 2 1 2.13 4.68 1.80 o 9 2 1 162.98 173.01 3.12 o 10 2 1 77.96 87.25 2.39 o 11 2 1 0.61 1.23 1.55 o 12 2 1 183.83 186.81 14.83 o 13 2 1 327.80 304.92 7.24 o 14 2 1 401.69 389.37 8.76 o 15 2 1 218.84 215.95 7.05 o 16 2 1 43.42 50.61 6.17 o 17 2 1 0.11 1.89 6.72 o -17 3 1 25.79 28.57 6.22 o -16 3 1 62.87 60.42 7.07 o -15 3 1 193.92 210.51 10.05 o -14 3 1 167.38 175.00 6.23 o -13 3 1 142.65 146.39 4.45 o -12 3 1 81.80 94.51 3.32 o -11 3 1 27.95 32.77 2.33 o -10 3 1 5.25 5.03 1.76 o -9 3 1 250.99 268.81 4.66 o -8 3 1 615.22 602.87 6.67 o -7 3 1 6.19 3.66 1.08 o -6 3 1 304.67 445.76 5.05 o -5 3 1 1485.96 1507.71 15.52 o -4 3 1 5960.46 6221.32 47.65 o -3 3 1 6458.96 6425.32 62.48 o -2 3 1 2290.99 2367.58 18.69 o -1 3 1 1194.20 1105.30 7.32 o 0 3 1 453.73 395.83 3.61 o 1 3 1 4498.85 4211.90 50.23 o 2 3 1 8169.17 7839.14 75.37 o 3 3 1 395.54 406.01 6.42 o 4 3 1 63.46 81.36 3.36 o 5 3 1 387.32 435.56 5.42 o 6 3 1 14.07 8.54 1.15 o 7 3 1 1.34 12.62 3.50 o 8 3 1 313.04 334.99 5.05 o 9 3 1 13.69 13.19 2.29 o 10 3 1 155.84 148.09 3.68 o 11 3 1 223.57 231.02 6.12 o 12 3 1 396.07 404.70 10.25 o 13 3 1 84.43 98.48 4.70 o 14 3 1 42.22 38.88 4.25 o 15 3 1 95.91 110.76 5.73 o 16 3 1 322.07 331.20 9.40 o -16 4 1 1.33 6.52 5.28 o -15 4 1 95.07 99.03 7.27 o -14 4 1 529.43 548.52 11.10 o -13 4 1 23.30 16.20 3.55 o -12 4 1 20.47 29.34 4.28 o -11 4 1 37.07 59.90 4.53 o -10 4 1 1213.09 1134.26 13.44 o -9 4 1 886.06 865.71 9.20 o -8 4 1 1423.82 1441.96 13.82 o -7 4 1 132.44 138.81 4.07 o -6 4 1 98.37 80.10 2.07 o -5 4 1 0.20 0.74 0.79 o -4 4 1 1339.28 1301.33 10.77 o -3 4 1 1685.71 1712.55 12.47 o -2 4 1 6377.95 6993.76 43.61 o -1 4 1 233.11 228.99 2.56 o 0 4 1 499.90 615.56 4.95 o 1 4 1 5893.43 6365.22 48.41 o 2 4 1 20.58 25.86 1.14 o 3 4 1 495.24 548.91 8.05 o 4 4 1 192.69 180.64 3.38 o 5 4 1 1345.46 1298.64 26.65 o 6 4 1 2484.86 2434.55 31.47 o 7 4 1 4460.83 4360.92 54.55 o 8 4 1 618.76 597.91 10.13 o 9 4 1 20.73 24.86 3.88 o 10 4 1 710.42 661.01 13.81 o 11 4 1 1697.03 1618.18 23.08 o 12 4 1 375.66 381.57 8.57 o 13 4 1 396.43 394.44 18.31 o 14 4 1 10.13 5.23 3.71 o 15 4 1 223.76 203.51 7.51 o 16 4 1 5.89 1.75 4.47 o -15 5 1 10.89 5.23 4.18 o -14 5 1 3.09 5.41 3.84 o -13 5 1 12.49 15.87 3.68 o -12 5 1 965.55 942.39 24.81 o -11 5 1 62.05 79.31 13.46 o -10 5 1 47.64 40.07 2.74 o -9 5 1 12.73 8.02 2.17 o -8 5 1 249.11 265.47 5.00 o -7 5 1 656.02 687.55 7.56 o -6 5 1 766.04 742.69 7.88 o -5 5 1 261.90 257.42 3.23 o -4 5 1 48.77 44.88 1.21 o -3 5 1 248.17 268.57 3.15 o -2 5 1 344.04 362.72 5.48 o -1 5 1 301.10 360.81 3.42 o 0 5 1 1917.37 2065.72 14.98 o 1 5 1 264.85 292.72 3.54 o 2 5 1 679.06 780.86 8.02 o 3 5 1 308.42 326.73 4.48 o 4 5 1 188.99 186.09 3.14 o 5 5 1 280.69 269.55 4.66 o 6 5 1 64.29 67.71 3.22 o 7 5 1 110.82 104.09 5.42 o 8 5 1 422.24 441.12 8.57 o 9 5 1 210.27 198.94 5.58 o 10 5 1 50.14 49.21 5.00 o 11 5 1 294.36 271.13 7.24 o 12 5 1 66.16 74.10 4.63 o 13 5 1 292.16 264.91 11.00 o 14 5 1 19.66 7.50 4.11 o 15 5 1 0.30 1.03 4.12 o 16 5 1 5.96 6.42 7.37 o -16 6 1 204.36 248.33 13.34 o -15 6 1 0.18 -2.33 4.66 o -14 6 1 150.81 159.22 6.72 o -13 6 1 123.13 120.33 5.81 o -12 6 1 56.27 61.71 5.60 o -11 6 1 0.00 1.11 2.96 o -10 6 1 109.74 111.90 3.95 o -9 6 1 83.54 80.83 3.35 o -8 6 1 81.92 84.63 3.16 o -7 6 1 70.53 71.78 3.51 o -6 6 1 170.66 162.39 3.96 o -5 6 1 588.09 572.09 6.53 o -4 6 1 22.70 24.21 1.19 o -3 6 1 100.06 91.46 1.65 o -2 6 1 6.41 5.53 0.98 o -1 6 1 387.37 369.21 4.15 o 0 6 1 205.78 202.73 2.59 o 1 6 1 500.50 474.23 4.98 o 2 6 1 184.76 176.29 3.47 o 3 6 1 84.37 87.79 2.84 o 4 6 1 435.46 446.93 5.60 o 5 6 1 41.26 44.95 2.39 o 6 6 1 1579.74 1555.16 25.58 o 7 6 1 627.01 608.65 10.71 o 8 6 1 0.09 -1.67 2.40 o 9 6 1 21.16 23.23 3.27 o 10 6 1 245.90 241.01 6.97 o 11 6 1 501.17 474.01 17.44 o 12 6 1 203.73 194.30 6.81 o 13 6 1 0.68 2.38 3.96 o 14 6 1 162.31 152.99 6.87 o -14 7 1 16.06 17.90 4.89 o -13 7 1 6.64 4.67 4.27 o -12 7 1 8.55 8.29 3.96 o -11 7 1 8.36 12.66 3.02 o -10 7 1 0.73 0.52 2.62 o -9 7 1 91.07 94.65 3.80 o -8 7 1 1.42 0.16 2.12 o -7 7 1 76.89 87.85 3.36 o -6 7 1 224.96 217.23 9.58 o -5 7 1 42.53 40.58 2.55 o -4 7 1 448.37 401.38 6.30 o -3 7 1 30.77 30.96 1.86 o -2 7 1 6.77 5.63 1.50 o -1 7 1 195.91 191.61 3.09 o 0 7 1 20.24 20.69 1.48 o 1 7 1 9.86 9.86 1.84 o 2 7 1 34.57 31.03 1.65 o 3 7 1 1.52 1.63 1.32 o 4 7 1 2.40 4.39 1.42 o 5 7 1 61.30 55.34 2.42 o 6 7 1 192.45 205.87 7.19 o 7 7 1 94.53 91.98 10.60 o 8 7 1 187.06 196.88 9.03 o 9 7 1 0.96 0.32 3.20 o 10 7 1 3.11 2.52 3.28 o 11 7 1 0.19 -1.31 3.64 o 12 7 1 13.90 14.66 4.07 o 13 7 1 0.98 0.74 4.39 o -13 8 1 128.80 137.41 11.20 o -12 8 1 239.33 260.54 8.67 o -11 8 1 184.07 188.42 5.72 o -10 8 1 21.85 20.90 3.30 o -9 8 1 0.28 -1.87 2.76 o -8 8 1 10.95 12.75 2.81 o -7 8 1 124.50 123.35 6.42 o -6 8 1 346.61 334.66 6.36 o -5 8 1 0.04 -0.19 2.10 o -4 8 1 34.37 30.25 3.15 o -3 8 1 518.94 520.53 9.72 o -2 8 1 1596.64 1536.23 17.57 o -1 8 1 1515.99 1488.74 17.13 o 0 8 1 387.02 391.91 6.50 o 1 8 1 158.48 158.45 4.14 o 2 8 1 772.85 756.35 7.66 o 3 8 1 925.20 893.82 8.74 o 4 8 1 305.89 318.02 6.44 o 5 8 1 143.10 141.91 3.29 o 6 8 1 0.47 2.92 2.46 o 7 8 1 192.91 195.74 6.52 o 8 8 1 3.43 -2.04 3.34 o 9 8 1 65.25 63.47 4.63 o 10 8 1 38.95 43.18 6.42 o 11 8 1 21.38 24.74 4.59 o 12 8 1 19.93 19.23 6.12 o -12 9 1 335.65 341.04 14.13 o -11 9 1 132.67 123.66 6.95 o -10 9 1 34.92 39.21 4.13 o -9 9 1 13.79 18.01 3.61 o -8 9 1 125.31 126.32 9.83 o -7 9 1 99.90 94.76 6.72 o -6 9 1 556.39 551.86 11.03 o -5 9 1 78.56 72.75 4.54 o -4 9 1 0.29 0.25 3.08 o -3 9 1 1.80 1.13 3.00 o -2 9 1 4.88 4.08 3.02 o -1 9 1 100.35 79.11 3.41 o 0 9 1 165.40 163.16 4.69 o 1 9 1 84.80 89.52 3.63 o 2 9 1 0.82 1.63 2.51 o 3 9 1 374.87 364.45 6.82 o 4 9 1 209.56 198.88 5.20 o 5 9 1 133.65 122.78 8.19 o 6 9 1 13.64 11.50 2.97 o 7 9 1 96.04 103.78 5.55 o 8 9 1 44.07 42.80 4.78 o 9 9 1 259.67 256.98 8.38 o 10 9 1 83.36 79.50 8.76 o 11 9 1 46.16 44.29 7.76 o -9 10 1 372.74 401.16 14.83 o -8 10 1 248.54 262.45 8.68 o -7 10 1 51.22 49.21 5.06 o -6 10 1 66.81 65.02 5.18 o -5 10 1 151.06 174.14 6.59 o -4 10 1 197.60 190.80 17.59 o -3 10 1 54.27 58.12 4.62 o -2 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