#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:21:17 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181009 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/89/2208964.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2208964_Fobs loop_ _publ_author_name 'Ohuchi, Yuko' 'Noda, Kyoko' 'Suzuki, Takayoshi' 'Kashiwabara, Kazuo' 'Takagi, Hideo D.' _publ_section_title ; trans-Bis(O-ethylxanthato)bis(triphenylphosphine)ruthenium(III) hexafluorophosphate monohydrate ; _journal_coeditor_code OB2010 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1077 _journal_page_last m1078 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.904 _cell_angle_gamma 90.000 _cell_length_a 13.9877 _cell_length_b 16.2122 _cell_length_c 20.5103 _exptl_crystal_F_000 2100.00 _reflns_d_resolution_high 0.7701 _cod_data_source_file ob2010Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Ru(S2COEt)2(PPh3)2]PF6_brown' _shelx_refln_list_code 4 _shelx_f_calc_maximum 761.10 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 363.32 345.48 51.89 o 6 0 0 3441.62 3751.92 139.89 o 8 0 0 2563.46 2029.35 124.04 o 10 0 0 18190.61 19410.92 433.89 o 12 0 0 15590.17 16927.26 502.38 o 14 0 0 706.83 506.97 134.01 o 16 0 0 12.13 198.36 77.69 o 18 0 0 1355.75 1188.42 214.41 o 2 1 0 16404.70 19444.27 190.80 o 3 1 0 160.26 107.73 1382.78 o 4 1 0 4094.11 3342.72 76.70 o 5 1 0 154.22 133.13 33.76 o 6 1 0 3475.15 3846.57 109.21 o 7 1 0 27.14 36.81 22.26 o 8 1 0 23288.31 25213.61 353.35 o 9 1 0 1310.18 1214.14 89.01 o 10 1 0 25415.03 26247.21 371.57 o 11 1 0 709.90 724.27 77.82 o 12 1 0 55.88 96.72 39.88 o 13 1 0 167.51 149.91 41.92 o 14 1 0 4219.66 4130.45 189.22 o 15 1 0 77.60 152.13 56.34 o 16 1 0 27.51 131.32 44.78 o 17 1 0 128.13 147.34 52.48 o 18 1 0 48.61 155.34 68.99 o 2 2 0 5815.69 3754.54 60.06 o 3 2 0 155.01 19.68 854.46 o 4 2 0 1629.58 1830.40 70.90 o 5 2 0 556.93 765.06 58.32 o 6 2 0 2130.26 2891.70 93.23 o 7 2 0 72.34 50.26 23.97 o 8 2 0 1025.28 1113.08 73.81 o 9 2 0 1050.11 1324.49 81.35 o 10 2 0 15059.00 14804.22 261.42 o 11 2 0 2157.10 2076.17 121.71 o 12 2 0 2039.35 2558.83 126.37 o 13 2 0 19.28 95.27 37.90 o 14 2 0 252.05 166.71 46.67 o 15 2 0 375.65 325.64 63.04 o 16 2 0 13.74 55.69 51.03 o 17 2 0 160.09 74.99 53.20 o 1 3 0 4296.16 4639.73 67.58 o 2 3 0 10366.24 14014.04 359.85 o 3 3 0 5251.27 5990.98 105.69 o 4 3 0 13630.28 15499.42 249.15 o 5 3 0 6512.30 6244.78 128.92 o 6 3 0 272.71 338.19 45.05 o 7 3 0 6.60 45.90 29.42 o 8 3 0 9916.42 9190.01 202.46 o 9 3 0 188.97 186.81 37.73 o 10 3 0 3279.28 3616.09 142.24 o 11 3 0 147.46 146.39 49.84 o 12 3 0 216.57 153.98 44.16 o 13 3 0 36.84 64.37 37.16 o 14 3 0 1138.99 1238.69 124.84 o 15 3 0 11.29 82.89 47.42 o 16 3 0 674.52 695.19 110.37 o 17 3 0 746.31 495.60 119.18 o 0 4 0 49550.23 51675.48 806.16 o 1 4 0 138.85 56.57 10.21 o 2 4 0 1.18 84.23 18.80 o 3 4 0 3412.68 4236.98 89.28 o 4 4 0 1120.72 711.21 49.80 o 5 4 0 5005.41 5042.00 121.85 o 6 4 0 12222.04 11296.06 214.12 o 7 4 0 2535.21 2342.94 101.27 o 8 4 0 4491.09 4226.05 125.39 o 9 4 0 874.76 927.36 78.65 o 10 4 0 3492.43 3554.73 137.70 o 11 4 0 892.00 964.49 85.24 o 12 4 0 921.14 803.86 96.41 o 13 4 0 0.96 88.77 42.63 o 14 4 0 415.57 330.46 74.63 o 15 4 0 64.53 47.50 47.01 o 16 4 0 494.91 293.77 66.04 o 17 4 0 190.58 119.51 57.62 o 1 5 0 3191.30 3637.62 50.18 o 2 5 0 83.27 71.73 17.68 o 3 5 0 3780.17 3153.10 76.31 o 4 5 0 28584.70 27187.36 334.71 o 5 5 0 2226.65 2260.98 85.49 o 6 5 0 5.13 56.13 24.95 o 7 5 0 11996.70 12151.80 238.42 o 8 5 0 11202.64 11953.04 255.49 o 9 5 0 2094.72 2027.24 108.14 o 10 5 0 429.44 466.42 60.68 o 11 5 0 331.00 467.91 70.88 o 12 5 0 194.09 173.30 54.28 o 13 5 0 4.65 70.16 37.73 o 14 5 0 1153.43 1075.04 111.15 o 15 5 0 196.32 224.77 62.55 o 16 5 0 2823.69 2908.34 169.09 o 17 5 0 0.73 39.20 52.44 o 0 6 0 9954.48 11270.66 342.45 o 1 6 0 2652.13 2480.28 40.60 o 2 6 0 3470.51 3044.97 61.24 o 3 6 0 6110.30 6333.15 119.63 o 4 6 0 171.28 290.78 36.90 o 5 6 0 8690.90 8897.58 178.43 o 6 6 0 5732.53 6753.21 164.40 o 7 6 0 693.12 684.68 57.07 o 8 6 0 7462.93 7174.53 174.68 o 9 6 0 112.03 95.56 32.22 o 10 6 0 7154.87 7827.64 216.32 o 11 6 0 201.58 170.56 48.18 o 12 6 0 508.24 434.84 74.82 o 13 6 0 664.62 416.09 84.41 o 14 6 0 70.44 97.76 45.53 o 15 6 0 69.54 74.23 53.88 o 16 6 0 107.71 145.87 45.66 o 17 6 0 1649.02 1606.77 162.60 o 1 7 0 3595.04 3723.00 74.42 o 2 7 0 7171.00 7579.43 127.59 o 3 7 0 548.82 515.48 37.75 o 4 7 0 4668.43 4928.59 129.19 o 5 7 0 225.17 182.59 34.01 o 6 7 0 190.33 226.04 42.99 o 7 7 0 2834.71 3143.32 117.07 o 8 7 0 572.62 569.50 54.37 o 9 7 0 8038.42 8118.49 182.68 o 10 7 0 3244.67 3296.08 134.64 o 11 7 0 3658.87 3627.75 157.18 o 12 7 0 833.66 837.99 102.94 o 13 7 0 102.90 98.48 37.00 o 14 7 0 1206.96 1221.94 118.05 o 15 7 0 94.85 158.14 49.42 o 16 7 0 667.97 388.45 82.70 o 17 7 0 422.95 432.36 145.06 o 0 8 0 36569.08 36952.20 752.31 o 1 8 0 48523.72 48184.83 826.39 o 2 8 0 5557.80 5148.23 97.02 o 3 8 0 59.25 66.47 20.84 o 4 8 0 533.04 427.98 37.95 o 5 8 0 511.09 467.66 41.67 o 6 8 0 2078.23 2327.06 95.64 o 7 8 0 2.89 69.50 29.73 o 8 8 0 3601.71 4151.42 142.00 o 9 8 0 322.86 466.97 65.32 o 10 8 0 5160.91 5811.94 186.76 o 11 8 0 5095.35 4915.99 184.24 o 12 8 0 2937.92 2888.97 154.06 o 13 8 0 3097.21 3155.94 163.83 o 14 8 0 19.02 108.39 34.23 o 15 8 0 130.78 191.95 50.27 o 16 8 0 236.31 221.74 56.67 o 1 9 0 2265.98 1994.91 103.47 o 2 9 0 2844.70 2734.36 69.66 o 3 9 0 392.59 385.15 39.46 o 4 9 0 259.65 340.09 38.26 o 5 9 0 615.54 572.21 51.11 o 6 9 0 10.38 55.66 24.18 o 7 9 0 11.31 36.34 24.44 o 8 9 0 3.56 58.84 29.27 o 9 9 0 10978.69 11809.14 264.48 o 10 9 0 4859.97 5493.63 199.59 o 11 9 0 1232.35 1233.09 101.78 o 12 9 0 69.65 115.12 36.10 o 13 9 0 433.85 231.56 46.60 o 14 9 0 488.88 375.99 79.20 o 15 9 0 122.51 72.04 46.73 o 16 9 0 0.16 73.95 68.88 o 0 10 0 14371.12 13250.06 633.27 o 1 10 0 21296.44 20523.88 370.70 o 2 10 0 1927.14 1681.20 65.02 o 3 10 0 14.01 26.14 13.92 o 4 10 0 2799.86 2914.38 102.65 o 5 10 0 250.18 226.41 37.71 o 6 10 0 202.58 145.24 37.52 o 7 10 0 91.01 111.45 23.02 o 8 10 0 3252.15 3132.56 126.07 o 9 10 0 720.46 546.91 69.10 o 10 10 0 1123.18 1097.12 84.18 o 11 10 0 3948.40 4439.81 192.09 o 12 10 0 431.57 419.76 85.92 o 13 10 0 1771.93 1821.24 127.13 o 14 10 0 107.24 137.30 57.47 o 15 10 0 264.48 186.02 52.84 o 1 11 0 2178.05 2073.75 118.39 o 2 11 0 518.76 543.52 33.22 o 3 11 0 3679.00 3484.38 106.38 o 4 11 0 1203.75 1286.88 64.15 o 5 11 0 3576.03 3510.83 118.82 o 6 11 0 1191.91 1338.86 77.08 o 7 11 0 854.04 822.61 71.42 o 8 11 0 2190.06 2405.97 129.52 o 9 11 0 7004.06 7375.85 236.06 o 10 11 0 2444.68 2330.50 122.44 o 11 11 0 444.46 451.96 95.04 o 12 11 0 5.00 79.14 40.82 o 13 11 0 115.82 157.95 66.91 o 14 11 0 336.80 205.19 65.69 o 15 11 0 446.47 407.64 121.57 o 0 12 0 2612.89 2571.52 185.43 o 1 12 0 3099.33 3073.42 161.41 o 2 12 0 1600.34 1738.99 110.26 o 3 12 0 1431.22 1488.58 117.24 o 4 12 0 687.00 591.53 83.73 o 5 12 0 9886.86 10358.01 312.67 o 6 12 0 864.75 808.92 81.52 o 7 12 0 7041.64 6854.19 211.39 o 8 12 0 1990.10 2064.50 143.37 o 9 12 0 1130.61 1169.11 103.28 o 10 12 0 37.80 66.82 36.77 o 11 12 0 378.47 293.22 61.23 o 12 12 0 136.95 138.04 54.90 o 13 12 0 488.06 246.36 114.99 o 14 12 0 110.36 174.05 70.21 o 1 13 0 2359.39 2432.67 155.39 o 2 13 0 229.14 409.74 77.30 o 3 13 0 3577.62 3632.70 159.60 o 4 13 0 159.51 107.41 39.46 o 5 13 0 1474.31 1396.18 114.10 o 6 13 0 258.58 226.06 76.67 o 7 13 0 2580.42 2322.33 156.58 o 8 13 0 52.16 88.30 36.02 o 9 13 0 1695.10 1630.51 137.67 o 10 13 0 10.72 166.79 70.88 o 11 13 0 98.48 227.20 91.69 o 12 13 0 102.29 42.47 90.29 o 13 13 0 173.63 69.05 96.80 o 14 13 0 45.07 73.41 68.17 o 0 14 0 1430.18 1486.06 228.68 o 1 14 0 35.87 73.09 37.19 o 2 14 0 1509.44 1640.95 116.14 o 3 14 0 178.08 206.36 59.53 o 4 14 0 134.44 147.17 59.71 o 5 14 0 5264.23 5481.68 273.08 o 6 14 0 129.14 73.67 40.89 o 7 14 0 4164.40 4536.08 214.24 o 8 14 0 80.93 168.37 47.13 o 9 14 0 36.10 48.19 50.01 o 10 14 0 767.59 662.58 173.47 o 11 14 0 279.09 275.66 115.15 o 12 14 0 112.97 56.73 52.76 o 13 14 0 594.35 318.83 115.76 o 1 15 0 3417.37 3889.84 193.99 o 2 15 0 0.15 33.05 39.30 o 3 15 0 4419.09 4606.29 215.31 o 4 15 0 437.18 341.53 93.92 o 5 15 0 4.65 90.43 50.94 o 6 15 0 172.72 158.54 46.71 o 7 15 0 39.97 10.16 48.59 o 8 15 0 78.71 138.16 66.26 o 9 15 0 2374.93 2439.65 213.32 o 10 15 0 26.99 56.50 50.45 o 11 15 0 31.72 89.49 95.06 o 12 15 0 1268.27 1298.50 205.47 o 0 16 0 584.26 620.28 147.17 o 1 16 0 8086.38 8461.75 300.44 o 2 16 0 545.15 576.05 103.25 o 3 16 0 18.58 69.19 48.69 o 4 16 0 1.51 7.34 54.24 o 5 16 0 475.19 453.03 122.27 o 6 16 0 24.18 70.21 48.11 o 7 16 0 508.35 372.78 118.61 o 8 16 0 1073.17 986.11 181.07 o 9 16 0 195.81 224.93 88.17 o 10 16 0 229.98 190.04 89.23 o 11 16 0 3040.95 3331.53 266.96 o 1 17 0 3645.84 3736.79 201.21 o 2 17 0 9.78 95.48 53.22 o 3 17 0 1178.49 1379.04 148.98 o 4 17 0 16.25 91.40 59.12 o 5 17 0 64.27 158.38 60.45 o 6 17 0 105.45 171.86 73.53 o 7 17 0 59.92 139.21 59.47 o 8 17 0 467.97 479.23 131.81 o 9 17 0 2865.23 2826.17 227.42 o 10 17 0 651.23 453.76 110.58 o 0 18 0 64.91 166.16 82.20 o 1 18 0 2225.17 1969.75 162.48 o 2 18 0 1947.28 2059.70 201.38 o 3 18 0 21.12 125.54 59.86 o 4 18 0 2.63 35.33 49.84 o 5 18 0 62.01 182.18 93.26 o 6 18 0 10.42 98.04 54.19 o 7 18 0 122.93 140.13 63.51 o 8 18 0 203.92 220.64 78.70 o 9 18 0 2.07 100.37 82.75 o 1 19 0 1104.10 1080.25 197.73 o 2 19 0 272.45 151.80 67.93 o 3 19 0 896.59 775.36 218.19 o 4 19 0 125.15 78.52 64.79 o 5 19 0 133.07 208.30 73.76 o 6 19 0 18.66 34.34 89.32 o 7 19 0 71.44 53.74 67.13 o 0 20 0 17.71 91.76 94.78 o 1 20 0 141.25 100.98 149.43 o 2 20 0 501.67 286.85 181.52 o 3 20 0 44.51 73.75 49.00 o 4 20 0 5.81 65.01 71.84 o 5 20 0 1704.76 1763.12 224.62 o 1 21 0 0.47 131.57 89.97 o -17 0 1 92.44 84.18 76.27 o -15 0 1 289.52 163.28 60.53 o -13 0 1 1044.90 1000.57 136.45 o -11 0 1 37074.07 40595.52 633.53 o -9 0 1 21345.82 21058.55 547.83 o -7 0 1 12.50 67.79 40.32 o -5 0 1 372.61 234.26 61.11 o -3 0 1 322996.38 329171.25 57277.43 o 3 0 1 831.57 399.77 78.16 o 7 0 1 3823.67 3285.21 148.57 o 9 0 1 19814.29 20058.32 536.76 o 11 0 1 10.73 134.87 79.90 o 13 0 1 2709.03 2853.75 260.48 o 15 0 1 322.07 329.86 127.00 o 17 0 1 354.41 230.46 97.23 o -18 1 1 0.59 175.19 71.58 o -17 1 1 12.20 157.83 49.39 o -16 1 1 133.21 153.05 49.39 o -15 1 1 44.86 109.53 52.40 o -14 1 1 107.29 111.68 44.60 o -13 1 1 10582.46 11756.25 341.38 o -12 1 1 2152.13 2632.25 172.79 o -11 1 1 8296.36 8578.40 196.17 o -10 1 1 5080.49 4655.32 157.06 o -9 1 1 3863.68 4281.40 131.55 o -8 1 1 574.68 604.59 51.02 o -7 1 1 51.05 207.31 41.12 o -6 1 1 1250.52 1253.68 68.07 o -5 1 1 73.64 59.24 23.76 o -4 1 1 62.66 95.66 24.83 o -3 1 1 38451.79 41883.03 419.59 o -2 1 1 1779.57 3126.84 45.32 o 2 1 1 1.95 352.10 24.92 o 3 1 1 1095.36 428.29 273.47 o 5 1 1 464.75 530.67 67.08 o 6 1 1 1141.12 1111.95 79.92 o 8 1 1 112.40 114.59 35.95 o 9 1 1 10206.33 10124.58 233.14 o 10 1 1 157.20 124.97 40.82 o 11 1 1 29200.49 30399.86 421.48 o 12 1 1 9.68 76.72 32.15 o 13 1 1 212.94 185.95 51.10 o 14 1 1 130.33 184.57 64.45 o 15 1 1 49.32 100.60 39.04 o 16 1 1 13.35 128.06 55.13 o 17 1 1 445.00 199.44 56.35 o -18 2 1 33.42 8.43 59.68 o -17 2 1 343.89 198.15 56.07 o -16 2 1 113.48 164.28 49.84 o -15 2 1 4.14 47.70 41.06 o -14 2 1 104.87 152.28 56.28 o -13 2 1 1820.09 1809.91 128.22 o -12 2 1 183.00 148.55 45.39 o -11 2 1 11377.21 11430.36 227.05 o -10 2 1 1146.93 1213.85 78.92 o -9 2 1 3587.96 3287.71 122.26 o -8 2 1 899.62 874.75 71.29 o -7 2 1 3.19 67.50 26.33 o -6 2 1 2057.79 2185.74 94.12 o -5 2 1 1381.11 1796.38 72.78 o -4 2 1 5313.77 5968.37 110.23 o -3 2 1 18547.10 16475.41 248.29 o -2 2 1 1243.38 2154.58 49.79 o -1 2 1 556.64 22.31 5.68 o 4 2 1 160.10 390.43 40.08 o 5 2 1 173.92 116.29 29.34 o 6 2 1 2104.87 1560.16 403.39 o 8 2 1 266.72 225.57 50.57 o 9 2 1 11159.41 11503.55 278.38 o 10 2 1 792.08 722.60 73.04 o 11 2 1 67.16 160.64 45.68 o 12 2 1 759.71 806.74 85.96 o 13 2 1 225.31 133.40 40.98 o 14 2 1 35.24 166.34 55.11 o 15 2 1 1053.45 908.38 122.11 o 16 2 1 266.29 211.53 64.45 o 17 2 1 288.92 244.97 71.63 o -17 3 1 935.44 723.27 123.74 o -16 3 1 526.46 460.97 82.30 o -15 3 1 119.96 173.78 58.46 o -14 3 1 1180.22 1141.46 98.88 o -13 3 1 1992.52 1982.65 123.26 o -12 3 1 0.72 128.76 44.62 o -11 3 1 1333.79 1412.48 89.56 o -10 3 1 1955.17 1951.79 121.38 o -9 3 1 215.58 327.60 52.82 o -8 3 1 721.58 733.70 59.56 o -7 3 1 3166.39 2420.39 91.62 o -6 3 1 102.09 72.67 24.02 o -5 3 1 18902.95 20010.09 251.69 o -4 3 1 761.58 1071.25 55.04 o -3 3 1 3229.36 2106.01 65.29 o -2 3 1 2086.10 2256.30 62.74 o -1 3 1 2973.47 1894.52 47.47 o 0 3 1 7155.51 8332.02 175.20 o 1 3 1 10908.05 12678.54 151.41 o 3 3 1 28252.40 33146.60 378.64 o 4 3 1 653.05 502.30 42.00 o 5 3 1 4652.08 3905.17 1199.26 o 6 3 1 15.42 22.38 22.86 o 7 3 1 8389.08 7914.07 175.37 o 8 3 1 179.05 231.72 48.15 o 9 3 1 4819.27 5107.66 149.70 o 10 3 1 0.61 33.46 33.14 o 11 3 1 2871.82 3038.55 184.41 o 12 3 1 76.68 58.39 30.29 o 13 3 1 30.05 46.67 39.42 o 14 3 1 58.37 104.74 32.87 o 15 3 1 14.25 73.69 51.16 o 16 3 1 28.44 165.49 58.36 o 17 3 1 2839.83 2828.02 186.49 o -17 4 1 1742.53 1669.02 179.54 o -16 4 1 77.15 109.20 43.37 o -15 4 1 141.58 165.29 49.89 o -14 4 1 468.95 269.21 62.33 o -13 4 1 162.49 163.07 43.93 o -12 4 1 1563.59 1426.39 99.69 o -11 4 1 868.61 868.46 78.21 o -10 4 1 127.61 108.27 31.96 o -9 4 1 4480.48 4415.75 137.37 o -8 4 1 829.34 895.60 71.73 o -7 4 1 1609.00 1523.17 95.93 o -6 4 1 12106.99 12820.14 232.68 o -5 4 1 36556.26 36437.73 385.10 o -4 4 1 9700.09 8509.41 160.58 o -3 4 1 58791.97 63984.04 575.70 o -2 4 1 160.61 394.24 27.35 o -1 4 1 779.68 572.46 34.52 o 0 4 1 219.89 150.33 19.11 o 1 4 1 6529.70 6930.76 87.37 o 3 4 1 260.59 418.98 46.89 o 4 4 1 175.78 288.98 37.40 o 5 4 1 1341.60 1153.21 73.36 o 6 4 1 120.70 141.26 36.45 o 7 4 1 39689.25 42026.50 561.59 o 8 4 1 3806.70 3772.94 134.89 o 9 4 1 8062.85 7899.63 196.93 o 10 4 1 161.50 158.02 40.97 o 11 4 1 0.16 52.18 34.96 o 12 4 1 354.93 400.68 66.65 o 13 4 1 315.25 193.13 57.12 o 14 4 1 57.39 129.56 46.67 o 15 4 1 2884.22 2784.85 197.27 o 16 4 1 183.08 147.17 51.26 o 17 4 1 174.19 125.49 49.57 o -17 5 1 231.61 166.84 68.28 o -16 5 1 43.15 107.48 49.33 o -15 5 1 681.61 623.05 83.04 o -14 5 1 583.98 562.51 117.93 o -13 5 1 592.16 636.54 89.91 o -12 5 1 5.63 41.03 32.29 o -11 5 1 222.81 150.10 41.46 o -10 5 1 49.40 92.13 35.47 o -9 5 1 1040.85 916.49 87.32 o -8 5 1 2734.58 2411.51 107.02 o -7 5 1 19537.55 19682.99 321.52 o -6 5 1 3515.75 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