#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:22:55 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181013 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/93/2209334.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209334_Fobs loop_ _publ_author_name 'Khawar Rauf, M.' 'Badshah, Amin' 'Bolte, Michael' _publ_section_title ; 1-(3-Chlorobenzoyl)-3-(2,4,6-trichlorophenyl)thiourea ; _journal_coeditor_code TK2039 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2444 _journal_page_last o2445 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.379 _cell_angle_gamma 90.000 _cell_length_a 12.4021 _cell_length_b 9.2723 _cell_length_c 14.5212 _exptl_crystal_F_000 792.00 _reflns_d_resolution_high 0.8214 _cod_data_source_file tk2039Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' rauf6 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 253.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 2541.81 2419.68 36.38 o 6 0 0 85.49 85.42 5.46 o 8 0 0 340.31 354.22 34.88 o 10 0 0 46.56 73.51 17.64 o 12 0 0 14.24 4.06 18.53 o 14 0 0 325.42 321.37 26.04 o 2 1 0 1397.93 1275.26 41.59 o 3 1 0 4176.08 3933.74 33.87 o 4 1 0 2073.21 1966.47 34.11 o 5 1 0 117.67 109.79 4.29 o 6 1 0 1171.32 1101.57 24.40 o 7 1 0 2105.85 2256.65 51.29 o 8 1 0 2311.99 2389.83 43.41 o 9 1 0 92.08 93.55 6.88 o 10 1 0 1943.73 1945.45 84.43 o 11 1 0 943.38 977.88 19.96 o 12 1 0 650.62 684.30 18.65 o 13 1 0 49.79 55.72 14.39 o 14 1 0 0.64 5.29 12.45 o 0 2 0 8821.37 8038.29 117.92 o 1 2 0 3822.95 3346.55 71.49 o 2 2 0 2708.05 2510.69 53.89 o 3 2 0 3955.85 3750.26 74.73 o 4 2 0 395.94 427.16 8.96 o 5 2 0 86.65 50.25 3.30 o 6 2 0 632.38 642.39 10.03 o 7 2 0 165.90 136.56 5.82 o 8 2 0 3.07 8.39 4.80 o 9 2 0 613.97 606.71 19.79 o 10 2 0 1422.47 1470.11 26.40 o 11 2 0 1027.77 1054.66 20.52 o 12 2 0 0.69 16.26 13.72 o 13 2 0 142.26 118.13 12.90 o 14 2 0 547.26 547.82 20.81 o 1 3 0 1203.49 1129.93 57.96 o 2 3 0 698.58 622.47 15.28 o 3 3 0 478.78 368.19 12.07 o 4 3 0 1537.34 1637.01 45.05 o 5 3 0 387.41 398.00 12.02 o 6 3 0 5344.67 5372.10 177.75 o 7 3 0 2025.13 2155.61 70.45 o 8 3 0 1253.39 1327.32 16.14 o 9 3 0 505.87 478.33 29.35 o 10 3 0 1676.47 1723.08 25.70 o 11 3 0 6.62 14.62 11.66 o 12 3 0 181.40 181.77 12.49 o 13 3 0 398.39 376.09 17.75 o 0 4 0 430.70 449.62 16.92 o 1 4 0 1203.12 1177.65 38.55 o 2 4 0 4283.52 4263.66 88.96 o 3 4 0 738.23 760.12 25.89 o 4 4 0 7394.51 7728.82 232.99 o 5 4 0 44.83 64.38 6.14 o 6 4 0 2010.87 2089.62 125.73 o 7 4 0 0.33 8.69 7.01 o 8 4 0 6.47 14.42 11.76 o 9 4 0 501.94 500.30 14.30 o 10 4 0 0.12 3.05 11.90 o 11 4 0 0.05 4.62 10.25 o 12 4 0 300.30 338.97 24.84 o 13 4 0 46.21 59.53 13.96 o 1 5 0 719.31 741.89 15.37 o 2 5 0 1615.74 1719.37 59.39 o 3 5 0 43.09 58.59 5.46 o 4 5 0 889.26 812.86 30.27 o 5 5 0 289.82 277.89 11.15 o 6 5 0 296.00 293.22 12.35 o 7 5 0 484.42 449.53 14.26 o 8 5 0 148.02 143.85 14.35 o 9 5 0 8.15 5.26 14.14 o 10 5 0 734.87 665.75 18.42 o 11 5 0 64.04 82.64 17.31 o 12 5 0 213.86 261.38 20.57 o 0 6 0 902.51 910.45 23.64 o 1 6 0 154.18 173.47 9.04 o 2 6 0 399.62 440.85 12.70 o 3 6 0 221.28 215.83 11.45 o 4 6 0 2315.48 2328.35 45.68 o 5 6 0 202.86 174.69 10.42 o 6 6 0 195.23 208.03 11.21 o 7 6 0 881.26 894.41 21.40 o 8 6 0 140.11 153.25 11.70 o 9 6 0 491.98 473.66 16.20 o 10 6 0 0.65 -0.44 10.31 o 11 6 0 349.49 355.00 21.44 o 12 6 0 26.89 10.85 19.26 o 1 7 0 1673.88 1724.30 24.50 o 2 7 0 1242.56 1310.94 35.22 o 3 7 0 526.07 621.70 12.73 o 4 7 0 1283.21 1307.32 25.60 o 5 7 0 231.56 261.41 17.05 o 6 7 0 1379.08 1389.52 24.68 o 7 7 0 836.95 847.87 19.88 o 8 7 0 11.65 37.15 15.91 o 9 7 0 265.12 282.10 19.27 o 10 7 0 103.45 117.94 18.71 o 11 7 0 19.01 20.83 19.14 o 0 8 0 1772.30 1711.22 35.82 o 1 8 0 45.88 47.14 8.65 o 2 8 0 198.29 214.72 11.96 o 3 8 0 22.82 26.05 7.59 o 4 8 0 183.04 187.30 9.51 o 5 8 0 146.90 161.99 12.29 o 6 8 0 31.61 33.11 16.09 o 7 8 0 371.32 389.49 20.41 o 8 8 0 393.39 399.45 17.07 o 9 8 0 21.96 16.80 19.36 o 10 8 0 85.52 85.71 19.72 o 1 9 0 183.89 184.13 13.06 o 2 9 0 1.45 6.99 10.87 o 3 9 0 47.43 52.11 9.43 o 4 9 0 30.05 27.72 9.52 o 5 9 0 331.36 347.77 14.77 o 6 9 0 380.77 402.16 21.15 o 7 9 0 50.94 43.54 14.42 o 8 9 0 198.49 172.88 20.85 o 0 10 0 2043.89 1966.77 42.46 o 1 10 0 240.56 231.96 14.18 o 2 10 0 4.80 10.58 10.10 o 3 10 0 7.36 14.58 10.46 o 4 10 0 2.67 5.95 11.26 o 5 10 0 48.07 51.25 10.80 o 6 10 0 372.68 385.64 17.83 o 1 11 0 238.90 216.08 19.49 o 2 11 0 20.93 17.08 11.29 o -13 0 1 0.94 14.51 18.50 o -11 0 1 5044.39 5491.95 191.10 o -9 0 1 10721.17 10918.70 351.17 o -7 0 1 3861.96 3744.83 162.85 o -5 0 1 2753.02 2686.14 30.99 o -3 0 1 51.08 60.17 34.54 o 3 0 1 62.53 36.54 6.41 o 5 0 1 293.23 310.55 14.45 o 7 0 1 11778.98 12037.44 120.80 o 9 0 1 8640.04 9372.23 101.05 o 11 0 1 2804.57 2772.38 48.69 o 13 0 1 71.48 99.92 21.81 o -14 1 1 186.93 192.34 14.88 o -13 1 1 972.84 982.52 79.60 o -12 1 1 0.66 4.85 8.63 o -11 1 1 210.11 222.54 7.96 o -10 1 1 3964.15 4246.22 69.57 o -9 1 1 324.00 334.12 9.58 o -8 1 1 53.53 53.98 5.20 o -7 1 1 22.86 28.35 3.62 o -6 1 1 397.63 394.13 8.16 o -5 1 1 2282.26 2266.71 29.25 o -4 1 1 778.89 672.60 11.11 o -3 1 1 11913.31 11805.00 285.41 o -2 1 1 185.36 149.38 10.75 o 2 1 1 1788.56 1607.89 33.27 o 3 1 1 6894.06 6440.50 189.72 o 4 1 1 7588.63 7068.53 65.32 o 5 1 1 4657.85 4561.89 157.28 o 6 1 1 383.30 438.51 12.22 o 7 1 1 298.33 295.63 10.68 o 8 1 1 925.52 988.39 30.60 o 9 1 1 788.18 768.40 21.56 o 10 1 1 33.41 26.66 11.05 o 11 1 1 8.38 18.83 11.46 o 12 1 1 23.13 35.28 13.41 o 13 1 1 568.53 543.95 17.63 o 14 1 1 260.94 226.57 27.15 o -14 2 1 20.43 33.03 16.57 o -13 2 1 398.91 377.83 20.23 o -12 2 1 127.96 135.64 13.67 o -11 2 1 564.22 593.22 19.68 o -10 2 1 1169.10 1220.45 41.61 o -9 2 1 1522.30 1643.92 47.77 o -8 2 1 92.92 101.84 5.50 o -7 2 1 1710.61 1701.04 20.32 o -6 2 1 819.87 877.41 11.30 o -5 2 1 1695.67 1706.94 26.33 o -4 2 1 5542.40 5345.33 40.57 o -3 2 1 11465.51 10857.92 258.78 o -2 2 1 6048.63 5811.25 41.81 o -1 2 1 0.18 0.00 1.84 o 0 2 1 329.23 271.32 12.73 o 1 2 1 213.27 191.01 14.35 o 2 2 1 4212.14 3896.59 59.29 o 3 2 1 60.25 36.51 5.18 o 4 2 1 1522.75 1435.92 33.69 o 5 2 1 1316.66 1263.38 21.48 o 6 2 1 461.46 445.55 12.83 o 7 2 1 3486.97 3392.09 84.04 o 8 2 1 1105.12 1095.79 19.53 o 9 2 1 1673.37 1713.67 25.01 o 10 2 1 124.04 118.58 11.39 o 11 2 1 86.91 74.25 11.81 o 12 2 1 1022.26 978.69 20.57 o 13 2 1 101.77 93.29 12.30 o -14 3 1 104.28 80.55 13.86 o -13 3 1 43.99 57.18 14.28 o -12 3 1 2.26 2.96 12.37 o -11 3 1 514.44 470.88 28.28 o -10 3 1 12.09 12.27 6.65 o -9 3 1 45.11 47.56 6.76 o -8 3 1 690.13 697.45 10.89 o -7 3 1 223.75 236.98 6.52 o -6 3 1 1680.78 1560.37 34.28 o -5 3 1 199.31 186.12 5.54 o -4 3 1 127.27 125.08 5.60 o -3 3 1 5726.15 5483.66 109.25 o -2 3 1 1183.22 1135.23 29.44 o -1 3 1 2866.26 2811.59 33.24 o 0 3 1 3466.48 3382.48 42.01 o 1 3 1 24799.55 24847.00 988.29 o 2 3 1 229.01 165.47 8.27 o 3 3 1 388.01 418.95 13.53 o 4 3 1 3964.28 4537.80 51.25 o 5 3 1 286.26 266.15 11.36 o 6 3 1 1317.60 1393.95 50.60 o 7 3 1 71.10 92.52 7.73 o 8 3 1 1363.47 1411.75 40.83 o 9 3 1 466.00 457.99 17.34 o 10 3 1 586.04 571.16 25.30 o 11 3 1 595.05 588.25 32.55 o 12 3 1 124.25 106.65 11.55 o 13 3 1 203.61 186.12 16.33 o -13 4 1 102.70 77.65 12.40 o -12 4 1 18.64 23.76 14.29 o -11 4 1 460.64 464.84 17.10 o -10 4 1 25.26 26.63 7.78 o -9 4 1 18.76 30.64 5.92 o -8 4 1 365.68 366.85 17.97 o -7 4 1 5001.27 4970.68 131.22 o -6 4 1 3020.27 2854.69 32.57 o -5 4 1 883.44 777.69 11.80 o -4 4 1 3343.35 3595.88 98.82 o -3 4 1 810.74 816.22 27.06 o -2 4 1 110.99 91.07 9.27 o -1 4 1 476.09 439.29 24.55 o 0 4 1 481.68 464.59 17.79 o 1 4 1 256.29 251.14 13.70 o 2 4 1 4803.93 4854.35 100.34 o 3 4 1 7440.53 7933.08 213.89 o 4 4 1 2.86 -1.84 4.52 o 5 4 1 2631.04 2596.52 33.20 o 6 4 1 39.46 33.11 9.96 o 7 4 1 104.75 92.30 10.92 o 8 4 1 616.20 611.29 18.02 o 9 4 1 11.11 5.51 13.41 o 10 4 1 191.74 193.28 12.59 o 11 4 1 56.85 55.90 11.96 o 12 4 1 68.64 68.61 17.66 o 13 4 1 942.80 1023.79 28.80 o -13 5 1 390.08 388.49 17.90 o -12 5 1 96.86 118.83 20.01 o -11 5 1 55.05 62.50 16.36 o -10 5 1 91.18 97.33 15.76 o -9 5 1 102.09 105.97 14.28 o -8 5 1 661.01 608.97 12.26 o -7 5 1 278.08 270.40 9.66 o -6 5 1 1.00 4.36 5.84 o -5 5 1 34.90 43.46 4.87 o -4 5 1 121.85 128.69 8.63 o -3 5 1 613.81 617.76 11.76 o -2 5 1 249.49 227.29 7.03 o -1 5 1 709.62 718.75 37.85 o 0 5 1 297.90 304.34 9.90 o 1 5 1 4395.76 4483.62 191.36 o 2 5 1 957.69 1088.95 40.46 o 3 5 1 53.19 47.00 5.73 o 4 5 1 321.86 379.07 13.72 o 5 5 1 840.94 840.66 18.18 o 6 5 1 313.40 320.62 15.49 o 7 5 1 332.73 319.08 12.52 o 8 5 1 75.59 61.40 13.99 o 9 5 1 121.26 119.17 12.76 o 10 5 1 944.46 928.54 20.26 o 11 5 1 1288.82 1340.68 28.83 o 12 5 1 547.07 473.36 18.07 o -12 6 1 458.60 377.75 17.65 o -11 6 1 444.73 392.47 21.86 o -10 6 1 6.75 20.91 11.09 o -9 6 1 332.15 301.26 17.73 o -8 6 1 276.90 294.29 16.36 o -7 6 1 230.35 222.17 12.17 o -6 6 1 6.05 15.60 9.60 o -5 6 1 1224.77 1182.63 39.60 o -4 6 1 57.71 69.11 6.99 o -3 6 1 1.69 12.06 6.51 o -2 6 1 0.26 2.47 8.17 o -1 6 1 322.65 325.17 11.02 o 0 6 1 241.61 270.28 10.10 o 1 6 1 0.46 7.22 6.99 o 2 6 1 5243.90 5665.66 100.30 o 3 6 1 26.47 13.43 6.61 o 4 6 1 1040.79 1119.32 26.17 o 5 6 1 527.12 509.01 17.73 o 6 6 1 236.65 263.85 14.72 o 7 6 1 954.93 964.55 20.39 o 8 6 1 46.29 40.86 14.81 o 9 6 1 259.76 297.49 18.13 o 10 6 1 1.19 -5.39 11.44 o 11 6 1 1532.59 1499.97 31.52 o -11 7 1 23.97 46.15 19.51 o -10 7 1 382.40 440.37 21.83 o -9 7 1 21.15 43.93 15.84 o -8 7 1 112.72 119.13 11.92 o -7 7 1 499.12 507.83 19.71 o -6 7 1 94.90 94.25 12.00 o -5 7 1 1750.66 1737.49 46.46 o -4 7 1 547.04 555.70 12.07 o -3 7 1 70.12 74.04 7.65 o -2 7 1 1038.03 1099.24 23.92 o -1 7 1 69.71 63.66 11.47 o 0 7 1 614.69 609.90 14.58 o 1 7 1 1188.48 1253.48 29.53 o 2 7 1 13.73 14.34 8.28 o 3 7 1 1257.88 1286.48 17.91 o 4 7 1 1.24 -2.69 8.76 o 5 7 1 175.87 189.72 15.27 o 6 7 1 553.61 531.54 19.70 o 7 7 1 427.17 426.15 19.67 o 8 7 1 113.79 126.60 16.23 o 9 7 1 477.70 500.91 21.83 o 10 7 1 99.75 106.40 19.48 o -10 8 1 169.33 111.30 19.35 o -9 8 1 2014.81 1911.77 33.26 o -8 8 1 0.29 1.94 12.13 o -7 8 1 85.97 75.44 11.80 o -6 8 1 30.56 29.95 11.77 o -5 8 1 21.31 19.89 9.05 o -4 8 1 293.60 284.78 14.47 o -3 8 1 31.56 33.19 8.06 o -2 8 1 2214.33 2293.27 84.16 o -1 8 1 48.44 48.33 11.07 o 0 8 1 47.55 52.19 8.58 o 1 8 1 3.46 13.95 9.64 o 2 8 1 1.10 -0.11 12.25 o 3 8 1 4.35 14.17 8.43 o 4 8 1 313.52 306.37 11.44 o 5 8 1 79.49 85.11 15.84 o 6 8 1 107.03 111.91 12.44 o 7 8 1 422.91 406.57 16.01 o 8 8 1 8.52 20.93 12.89 o 9 8 1 9.48 14.27 13.29 o -8 9 1 12.57 34.26 19.21 o -7 9 1 91.08 79.48 18.56 o -6 9 1 203.43 222.72 15.02 o -5 9 1 0.55 1.45 10.60 o -4 9 1 172.68 192.21 9.62 o -3 9 1 1224.69 1225.05 18.76 o -2 9 1 773.09 807.15 20.32 o -1 9 1 413.18 422.58 13.49 o 0 9 1 85.03 99.99 11.83 o 1 9 1 376.69 353.88 14.60 o 2 9 1 93.37 102.97 11.55 o 3 9 1 501.17 536.32 18.01 o 4 9 1 16.04 24.29 11.30 o 5 9 1 263.99 294.38 15.53 o 6 9 1 34.94 17.52 17.36 o 7 9 1 134.73 127.07 14.97 o 8 9 1 445.88 428.66 23.18 o -6 10 1 155.84 168.65 20.50 o -5 10 1 41.85 51.12 12.47 o -4 10 1 0.02 1.94 8.55 o -3 10 1 645.34 579.50 37.10 o -2 10 1 11.69 18.43 9.61 o -1 10 1 521.67 491.81 31.45 o 0 10 1 1248.04 1174.62 26.15 o 1 10 1 5.63 17.11 12.10 o 2 10 1 327.62 318.68 13.29 o 3 10 1 42.82 53.11 10.76 o 4 10 1 0.14 6.35 11.06 o 5 10 1 76.78 100.41 19.87 o 6 10 1 11.78 11.95 19.95 o -3 11 1 289.41 282.09 14.37 o -2 11 1 367.19 307.54 13.21 o -1 11 1 766.24 700.56 27.25 o 0 11 1 30.72 31.72 13.83 o 1 11 1 274.46 260.64 16.79 o 2 11 1 116.37 99.25 12.20 o -14 0 2 144.10 149.85 22.87 o -12 0 2 376.62 424.42 19.25 o -10 0 2 1782.94 1834.69 59.61 o -8 0 2 252.06 265.46 16.96 o -6 0 2 4519.61 4536.31 336.94 o -4 0 2 73.12 50.98 4.52 o -2 0 2 1984.59 1792.82 31.04 o 4 0 2 57.73 59.55 6.98 o 6 0 2 550.48 590.03 19.92 o 8 0 2 2585.27 2508.76 43.11 o 10 0 2 144.44 157.48 17.87 o 12 0 2 366.78 364.48 22.94 o -14 1 2 111.67 131.31 21.16 o -13 1 2 11.57 16.52 8.05 o -12 1 2 515.80 540.23 10.84 o -11 1 2 2287.92 2373.62 58.53 o -10 1 2 0.48 3.72 5.82 o -9 1 2 20.86 32.67 4.10 o -8 1 2 1101.82 1138.60 29.53 o -7 1 2 172.79 177.20 5.42 o -6 1 2 15232.93 14627.39 284.03 o -5 1 2 1.09 1.86 1.59 o -4 1 2 5111.74 4808.08 87.88 o -3 1 2 5740.71 5456.23 37.48 o -2 1 2 896.08 706.90 12.59 o -1 1 2 8143.39 7421.35 141.93 o 0 1 2 465.79 348.62 26.84 o 1 1 2 72.87 40.06 5.87 o 2 1 2 668.63 632.64 29.98 o 3 1 2 110.07 124.11 8.85 o 4 1 2 7365.25 6752.96 64.57 o 5 1 2 2226.27 2460.85 31.32 o 6 1 2 777.35 685.77 18.41 o 7 1 2 206.13 195.43 9.41 o 8 1 2 245.17 250.46 11.00 o 9 1 2 19.29 34.65 11.53 o 10 1 2 798.51 814.34 21.50 o 11 1 2 456.18 444.62 14.14 o 12 1 2 100.40 104.30 14.48 o 13 1 2 283.05 243.70 15.13 o -14 2 2 403.88 386.04 18.01 o -13 2 2 24.39 30.06 8.75 o -12 2 2 532.37 548.15 13.83 o -11 2 2 661.37 697.45 28.80 o -10 2 2 413.59 437.70 10.02 o -9 2 2 2398.45 2517.92 42.33 o -8 2 2 173.93 178.34 5.90 o -7 2 2 1727.51 1670.31 27.80 o -6 2 2 1919.39 1928.43 48.75 o -5 2 2 949.74 935.70 25.47 o -4 2 2 2085.15 2041.07 47.71 o -3 2 2 193.97 199.80 6.59 o -2 2 2 64187.72 70339.10 1303.53 o -1 2 2 4169.10 3813.98 66.28 o 0 2 2 5677.80 5327.17 61.20 o 1 2 2 82.61 63.96 7.39 o 2 2 2 3150.65 2984.55 99.95 o 3 2 2 355.29 307.30 10.52 o 4 2 2 10872.19 11085.44 355.85 o 5 2 2 13752.62 13869.29 103.63 o 6 2 2 502.07 530.40 13.37 o 7 2 2 2001.57 2124.33 66.97 o 8 2 2 784.99 801.00 17.86 o 9 2 2 2508.58 2453.36 31.11 o 10 2 2 3.91 12.50 8.51 o 11 2 2 19.66 31.08 11.65 o 12 2 2 46.34 51.48 13.25 o 13 2 2 77.72 74.28 13.11 o -14 3 2 27.27 20.76 12.01 o -13 3 2 148.58 157.47 12.21 o -12 3 2 671.41 684.55 11.66 o -11 3 2 38.65 38.46 7.37 o -10 3 2 10.90 14.50 6.41 o -9 3 2 0.89 9.44 4.89 o -8 3 2 1483.47 1466.09 28.48 o -7 3 2 3050.77 3043.52 92.08 o -6 3 2 15.45 16.98 3.43 o -5 3 2 701.99 725.17 16.04 o -4 3 2 542.16 527.27 8.77 o -3 3 2 5090.75 5253.01 123.54 o -2 3 2 37.22 26.66 2.80 o -1 3 2 910.81 951.00 26.76 o 0 3 2 547.10 430.12 13.48 o 1 3 2 0.28 121.10 103.80 o 2 3 2 626.80 537.22 13.45 o 3 3 2 1790.41 1763.52 30.40 o 4 3 2 202.75 175.18 9.18 o 5 3 2 692.82 766.92 19.12 o 6 3 2 177.43 194.14 10.44 o 7 3 2 7.67 16.41 7.59 o 8 3 2 7657.03 7820.88 94.16 o 9 3 2 7.38 3.85 8.25 o 10 3 2 195.33 190.29 14.05 o 11 3 2 0.10 12.50 12.83 o 12 3 2 558.82 507.95 19.33 o 13 3 2 72.97 70.47 13.42 o -13 4 2 459.20 452.69 16.67 o -12 4 2 573.87 549.82 14.26 o -11 4 2 192.10 200.81 9.51 o -10 4 2 1.03 2.56 6.78 o -9 4 2 4.98 10.52 5.39 o -8 4 2 20.91 21.53 5.48 o -7 4 2 2.17 14.78 5.36 o -6 4 2 1328.50 1202.52 36.91 o -5 4 2 220.66 199.94 6.71 o -4 4 2 9277.18 9593.02 249.18 o -3 4 2 569.14 542.41 11.14 o -2 4 2 284.72 347.93 14.79 o -1 4 2 0.30 4.33 2.73 o 0 4 2 3.78 2.17 2.58 o 1 4 2 2955.11 2719.74 85.06 o 2 4 2 82.47 72.54 5.76 o 3 4 2 130.64 112.29 7.96 o 4 4 2 1907.48 1834.66 28.63 o 5 4 2 1052.84 1140.19 21.52 o 6 4 2 310.57 307.69 13.88 o 7 4 2 3.82 -4.85 11.56 o 8 4 2 129.46 142.79 13.82 o 9 4 2 374.39 370.20 14.63 o 10 4 2 227.00 215.40 13.49 o 11 4 2 80.98 95.07 12.47 o 12 4 2 144.10 143.05 13.45 o -13 5 2 25.91 38.35 19.23 o -12 5 2 429.14 465.69 19.89 o -11 5 2 19.62 29.04 8.33 o -10 5 2 196.92 236.11 15.46 o -9 5 2 74.30 73.39 9.44 o -8 5 2 5694.30 5962.08 179.66 o -7 5 2 354.20 345.45 9.27 o -6 5 2 261.31 259.15 7.41 o -5 5 2 210.08 177.86 8.09 o -4 5 2 60.96 63.18 5.77 o -3 5 2 2595.02 2537.83 38.49 o -2 5 2 4511.16 4502.06 90.13 o -1 5 2 58.61 55.32 5.60 o 0 5 2 1421.43 1540.35 76.47 o 1 5 2 4341.16 4604.46 182.75 o 2 5 2 3480.13 3764.56 131.51 o 3 5 2 298.24 307.66 11.91 o 4 5 2 47.61 63.26 9.72 o 5 5 2 42.06 58.26 10.72 o 6 5 2 1430.93 1469.53 26.16 o 7 5 2 2.12 -12.54 12.54 o 8 5 2 934.61 904.72 19.25 o 9 5 2 203.55 212.47 13.30 o 10 5 2 140.54 146.82 13.75 o 11 5 2 8.80 9.97 17.44 o 12 5 2 32.08 30.38 18.89 o -12 6 2 41.20 53.52 13.55 o -11 6 2 65.83 73.59 18.23 o 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