#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:22:55 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181013 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/93/2209341.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209341_Fobs loop_ _publ_author_name 'Reiss, Guido J.' 'Kurteva, Vanya' _publ_section_title ; trans,trans-2,3,4-Triphenylazetidinium bromide ; _journal_coeditor_code WN2026 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2141 _journal_page_last o2143 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 107.500 _cell_angle_beta 90.460 _cell_angle_gamma 92.119 _cell_length_a 6.0658 _cell_length_b 10.9797 _cell_length_c 13.8090 _exptl_crystal_F_000 376.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file wn2026Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title triphenylazetidine _shelx_refln_list_code 4 _shelx_f_calc_maximum 110.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 0.93 6.21 1.43 o 2 0 0 5569.25 5363.24 104.68 o 3 0 0 1922.31 2066.28 51.26 o 4 0 0 609.56 617.62 29.00 o 5 0 0 138.50 131.36 4.37 o 6 0 0 10.56 2.44 2.51 o 7 0 0 129.52 107.61 9.43 o -7 1 0 132.11 100.61 11.44 o -6 1 0 413.60 418.66 17.93 o -5 1 0 416.03 370.35 24.52 o -4 1 0 55.20 49.51 2.20 o -3 1 0 87.88 71.98 2.71 o -2 1 0 201.83 210.72 5.85 o -1 1 0 897.17 868.60 4.57 o 2 1 0 3290.53 3122.72 239.67 o 3 1 0 208.04 174.45 7.13 o 4 1 0 1083.81 1103.36 37.29 o 5 1 0 22.06 14.38 2.33 o 6 1 0 201.43 182.83 24.20 o 7 1 0 10.06 8.76 5.21 o -7 2 0 2.90 1.72 4.43 o -6 2 0 396.58 360.81 31.37 o -5 2 0 45.16 38.24 3.72 o -4 2 0 903.72 944.89 44.68 o -3 2 0 646.48 663.59 27.00 o -2 2 0 6303.05 6415.41 54.17 o 1 2 0 5407.13 5566.94 348.48 o 2 2 0 52.15 69.91 4.38 o 3 2 0 1133.56 1113.28 54.63 o 4 2 0 310.61 353.96 18.31 o 5 2 0 1166.71 1261.58 52.98 o 6 2 0 51.75 54.67 8.98 o 7 2 0 35.41 27.11 12.09 o -7 3 0 19.21 24.39 8.03 o -6 3 0 133.24 112.02 5.68 o -5 3 0 222.89 212.35 6.92 o -4 3 0 1039.02 1080.85 20.44 o -3 3 0 84.60 75.08 2.18 o -2 3 0 3819.00 3912.84 151.34 o -1 3 0 1582.85 1662.25 45.01 o 0 3 0 3334.73 3166.76 13.88 o 1 3 0 46.83 41.96 1.08 o 2 3 0 1385.83 1396.16 28.77 o 3 3 0 619.04 673.39 17.34 o 4 3 0 4.40 6.35 1.44 o 5 3 0 490.84 510.21 26.17 o 6 3 0 10.80 4.89 3.56 o -6 4 0 114.70 113.69 13.02 o -5 4 0 315.74 318.17 8.41 o -4 4 0 0.23 1.71 1.67 o -3 4 0 666.86 659.43 17.10 o -2 4 0 1887.63 1935.45 24.94 o -1 4 0 2333.48 2381.60 101.63 o 0 4 0 2682.97 2600.49 10.54 o 1 4 0 652.49 623.94 5.43 o 2 4 0 1781.90 2046.84 119.94 o 3 4 0 597.94 763.31 106.66 o 4 4 0 200.78 248.05 7.05 o 5 4 0 22.53 27.76 4.72 o 6 4 0 356.55 400.54 28.91 o -6 5 0 168.97 185.52 9.14 o -5 5 0 117.07 114.01 8.01 o -4 5 0 642.42 644.56 11.62 o -3 5 0 145.07 161.54 4.49 o -2 5 0 4.50 2.88 1.33 o -1 5 0 1647.15 1795.56 65.99 o 0 5 0 527.12 554.87 6.26 o 1 5 0 1272.46 1262.26 15.65 o 2 5 0 483.32 476.84 9.36 o 3 5 0 361.09 429.60 72.14 o 4 5 0 30.47 35.50 5.16 o 5 5 0 27.18 26.35 11.60 o 6 5 0 13.52 18.98 4.70 o -6 6 0 139.04 137.60 7.94 o -5 6 0 88.44 80.53 4.59 o -4 6 0 426.02 438.27 10.99 o -3 6 0 6.69 7.00 1.64 o -2 6 0 599.87 611.03 15.06 o -1 6 0 39.51 46.99 2.84 o 0 6 0 190.65 158.70 4.27 o 1 6 0 321.72 309.13 14.29 o 2 6 0 198.79 195.61 9.00 o 3 6 0 1284.04 1322.94 17.80 o 4 6 0 150.46 144.40 9.27 o 5 6 0 255.72 307.13 70.26 o 6 6 0 0.29 2.79 4.56 o -6 7 0 23.08 20.80 5.22 o -5 7 0 341.58 348.73 9.77 o -4 7 0 83.06 89.43 11.94 o -3 7 0 2052.85 2127.74 49.12 o -2 7 0 78.39 77.39 4.47 o -1 7 0 734.03 761.48 17.50 o 0 7 0 1348.33 1418.05 51.73 o 1 7 0 559.11 619.41 27.70 o 2 7 0 545.72 519.00 7.79 o 3 7 0 171.86 170.64 6.12 o 4 7 0 105.02 105.31 10.05 o 5 7 0 55.20 64.16 9.27 o -5 8 0 149.83 155.14 8.85 o -4 8 0 63.05 73.22 6.32 o -3 8 0 473.32 503.42 10.55 o -2 8 0 133.52 140.70 4.84 o -1 8 0 697.32 743.65 16.42 o 0 8 0 197.34 211.26 5.47 o 1 8 0 439.59 452.94 15.37 o 2 8 0 39.07 32.01 2.96 o 3 8 0 221.13 243.51 7.59 o 4 8 0 130.30 129.55 10.52 o 5 8 0 34.39 31.80 9.89 o -5 9 0 75.95 59.58 6.95 o -4 9 0 99.43 112.62 7.63 o -3 9 0 18.59 18.81 3.46 o -2 9 0 528.93 608.32 8.36 o -1 9 0 3.10 2.55 1.59 o 0 9 0 145.33 162.13 5.04 o 1 9 0 141.58 142.84 4.47 o 2 9 0 134.30 131.71 4.58 o 3 9 0 86.94 90.81 7.12 o 4 9 0 0.20 3.94 6.97 o -4 10 0 42.44 50.68 6.81 o -3 10 0 333.30 357.38 10.14 o -2 10 0 432.25 481.50 16.12 o -1 10 0 103.77 103.04 4.93 o 0 10 0 657.94 696.04 16.90 o 1 10 0 16.57 13.28 2.99 o 2 10 0 350.01 352.22 10.11 o 3 10 0 129.46 127.82 7.87 o 4 10 0 39.11 25.57 8.89 o -3 11 0 78.92 83.13 6.03 o -2 11 0 0.86 2.69 2.39 o -1 11 0 158.42 172.19 5.70 o 0 11 0 12.09 11.72 3.75 o 1 11 0 105.15 109.88 5.64 o 2 11 0 45.87 41.16 4.45 o 3 11 0 115.24 115.84 8.16 o -2 12 0 101.95 107.66 6.98 o -1 12 0 61.54 62.20 4.96 o 0 12 0 27.59 24.60 4.53 o 1 12 0 94.50 87.82 6.37 o -2 -12 1 4.62 0.65 4.76 o -1 -12 1 84.63 78.83 6.22 o 0 -12 1 30.64 26.20 5.32 o 1 -12 1 52.28 57.17 4.95 o 2 -12 1 51.44 42.29 4.41 o -3 -11 1 6.35 6.69 3.57 o -2 -11 1 17.43 17.16 3.49 o -1 -11 1 81.28 90.38 6.22 o 0 -11 1 144.94 143.11 5.43 o 1 -11 1 64.61 70.36 4.65 o 2 -11 1 14.14 13.84 3.59 o 3 -11 1 279.17 300.72 9.67 o -4 -10 1 60.83 63.95 8.33 o -3 -10 1 42.67 54.21 6.41 o -2 -10 1 564.51 599.83 23.00 o -1 -10 1 0.90 1.61 1.60 o 0 -10 1 410.16 432.24 9.70 o 1 -10 1 78.26 79.55 4.09 o 2 -10 1 105.82 115.19 4.84 o 3 -10 1 109.15 109.40 5.66 o 4 -10 1 67.89 73.21 12.46 o -4 -9 1 0.22 0.25 3.53 o -3 -9 1 217.05 220.06 7.73 o -2 -9 1 2.15 2.92 1.73 o -1 -9 1 218.35 223.36 5.89 o 0 -9 1 305.19 322.45 9.32 o 1 -9 1 415.37 418.62 10.69 o 2 -9 1 333.67 346.25 13.16 o 3 -9 1 49.95 54.26 3.46 o 4 -9 1 299.44 331.91 9.58 o 5 -9 1 3.94 0.77 4.29 o -5 -8 1 12.06 6.07 4.78 o -4 -8 1 106.28 101.80 9.35 o -3 -8 1 77.71 85.12 8.10 o -2 -8 1 100.16 98.82 3.77 o -1 -8 1 757.82 821.69 27.30 o 0 -8 1 33.07 33.35 2.56 o 1 -8 1 903.98 933.81 22.16 o 2 -8 1 7.16 5.88 2.30 o 3 -8 1 301.36 326.49 5.52 o 4 -8 1 18.99 15.35 4.45 o 5 -8 1 203.04 205.25 8.41 o -5 -7 1 65.53 72.43 6.98 o -4 -7 1 217.54 207.91 10.36 o -3 -7 1 3.95 3.16 3.99 o -2 -7 1 525.00 492.63 9.82 o -1 -7 1 63.91 65.17 3.15 o 0 -7 1 636.53 642.44 29.98 o 1 -7 1 445.97 497.86 7.83 o 2 -7 1 330.94 326.61 7.07 o 3 -7 1 486.23 494.44 6.78 o 4 -7 1 6.54 6.60 2.74 o 5 -7 1 388.93 427.53 24.72 o 6 -7 1 0.55 0.00 4.49 o -6 -6 1 5.32 3.48 4.52 o -5 -6 1 191.17 184.19 8.38 o -4 -6 1 3.86 1.63 2.53 o -3 -6 1 631.14 656.28 13.90 o -2 -6 1 292.63 298.85 10.24 o -1 -6 1 2026.39 2170.10 135.77 o 0 -6 1 808.20 861.95 33.30 o 1 -6 1 464.66 459.08 8.02 o 2 -6 1 2128.41 2127.78 46.09 o 3 -6 1 13.65 12.49 1.66 o 4 -6 1 795.86 875.55 37.83 o 5 -6 1 59.42 56.50 4.40 o 6 -6 1 183.66 182.17 8.88 o -6 -5 1 325.41 385.63 40.00 o -5 -5 1 167.31 164.72 7.45 o -4 -5 1 474.96 600.59 91.14 o -3 -5 1 1277.68 1299.33 15.61 o -2 -5 1 156.40 145.18 7.91 o -1 -5 1 2504.68 2400.09 44.40 o 0 -5 1 26.05 32.23 1.94 o 1 -5 1 768.65 697.18 20.15 o 2 -5 1 763.45 758.98 15.22 o 3 -5 1 291.61 272.80 4.91 o 4 -5 1 193.99 202.70 6.65 o 5 -5 1 56.10 47.88 5.07 o 6 -5 1 310.66 288.20 9.25 o -6 -4 1 15.00 7.50 3.11 o -5 -4 1 1.15 1.56 1.47 o -4 -4 1 237.28 296.55 14.68 o -3 -4 1 9.61 12.43 2.95 o -2 -4 1 236.58 192.56 6.83 o -1 -4 1 716.25 684.15 13.02 o 0 -4 1 3066.53 2757.05 77.05 o 1 -4 1 303.64 269.31 5.18 o 2 -4 1 1189.16 1168.33 8.76 o 3 -4 1 866.04 874.39 7.82 o 4 -4 1 257.69 283.91 5.44 o 5 -4 1 238.15 250.33 10.85 o 6 -4 1 19.93 12.24 4.10 o -6 -3 1 68.09 82.09 7.08 o -5 -3 1 909.80 1000.30 47.30 o -4 -3 1 23.00 19.51 2.46 o -3 -3 1 1525.31 1842.14 71.92 o -2 -3 1 404.90 526.74 16.68 o -1 -3 1 3119.14 2823.50 76.85 o 0 -3 1 12178.10 9554.79 277.69 o 1 -3 1 550.77 554.81 26.06 o 2 -3 1 4895.41 4514.16 45.42 o 3 -3 1 1007.62 1060.43 18.43 o 4 -3 1 1261.49 1311.55 43.28 o 5 -3 1 224.41 216.76 7.07 o 6 -3 1 308.64 257.81 22.30 o 7 -3 1 164.53 143.85 26.05 o -7 -2 1 38.92 35.19 14.87 o -6 -2 1 103.12 103.03 11.58 o -5 -2 1 265.99 267.27 9.23 o -4 -2 1 183.41 197.73 11.84 o -3 -2 1 1260.88 1275.28 73.14 o -2 -2 1 646.69 737.40 53.59 o -1 -2 1 253.21 275.79 3.15 o 2 -2 1 1078.72 1087.25 11.21 o 3 -2 1 299.86 269.62 12.21 o 4 -2 1 1084.42 1198.14 51.24 o 5 -2 1 31.45 23.27 3.20 o 6 -2 1 162.85 139.85 11.81 o 7 -2 1 6.49 1.19 4.10 o -7 -1 1 19.52 16.53 5.38 o -6 -1 1 140.01 127.97 24.70 o -5 -1 1 42.09 38.05 4.60 o -4 -1 1 1363.14 1365.31 61.86 o -3 -1 1 510.24 551.91 24.23 o -2 -1 1 2662.81 2664.09 169.79 o -1 -1 1 134.97 106.40 7.78 o 2 -1 1 3835.95 3694.76 181.45 o 3 -1 1 908.32 943.91 27.83 o 4 -1 1 38.49 35.50 2.32 o 5 -1 1 420.01 395.63 28.63 o 6 -1 1 4.38 3.16 2.57 o 7 -1 1 68.99 57.16 10.19 o -7 0 1 104.37 86.08 10.30 o -6 0 1 30.64 22.56 3.81 o -5 0 1 288.66 294.55 7.30 o -4 0 1 336.87 349.83 4.17 o -3 0 1 51.22 31.85 1.38 o -2 0 1 1600.80 1686.18 13.88 o -1 0 1 2109.63 1774.85 362.07 o 2 0 1 3795.09 3534.75 184.17 o 3 0 1 592.21 561.33 22.45 o 4 0 1 883.06 909.27 47.10 o 5 0 1 437.86 450.70 8.07 o 6 0 1 220.89 186.45 19.95 o 7 0 1 89.18 66.31 7.20 o -7 1 1 144.46 129.65 8.59 o -6 1 1 239.23 249.15 9.03 o -5 1 1 354.17 349.99 8.06 o -4 1 1 841.10 953.21 15.44 o -3 1 1 1665.16 1787.68 75.21 o -2 1 1 83.93 98.78 1.68 o 2 1 1 1627.45 1522.65 40.09 o 3 1 1 279.55 278.00 10.91 o 4 1 1 627.51 643.48 18.80 o 5 1 1 87.07 83.56 5.04 o 6 1 1 344.65 326.03 20.10 o 7 1 1 5.66 5.77 4.75 o -7 2 1 4.00 3.25 4.27 o -6 2 1 349.67 349.22 18.07 o -5 2 1 8.09 5.68 2.24 o -4 2 1 1060.06 1140.80 33.36 o -3 2 1 1731.72 2022.12 33.48 o -2 2 1 513.57 501.09 4.93 o -1 2 1 2512.69 2825.74 78.65 o 1 2 1 1088.54 1263.85 101.58 o 2 2 1 2.92 5.80 1.25 o 3 2 1 571.56 605.96 20.72 o 4 2 1 22.99 15.50 1.94 o 5 2 1 164.80 158.06 4.57 o 6 2 1 3.60 3.40 1.95 o 7 2 1 60.27 48.98 6.60 o -7 3 1 41.82 38.58 5.33 o -6 3 1 114.24 89.96 6.28 o -5 3 1 104.77 113.94 6.05 o -4 3 1 442.41 424.70 15.47 o -3 3 1 430.44 446.40 8.18 o -2 3 1 1749.63 1862.58 14.58 o -1 3 1 302.83 304.20 6.08 o 0 3 1 1804.83 1766.65 38.20 o 1 3 1 63.96 62.98 3.26 o 2 3 1 1991.16 1991.83 59.27 o 3 3 1 904.11 1014.04 33.80 o 4 3 1 685.08 790.43 48.82 o 5 3 1 115.13 125.64 4.57 o 6 3 1 7.40 4.83 2.21 o -6 4 1 150.70 138.63 6.10 o -5 4 1 384.80 421.40 19.16 o -4 4 1 179.68 189.81 5.85 o -3 4 1 1476.64 1542.37 39.74 o -2 4 1 90.52 82.72 2.66 o -1 4 1 3052.45 3100.04 98.89 o 0 4 1 1278.69 1281.43 25.29 o 1 4 1 1382.90 1359.16 22.47 o 2 4 1 3417.76 3451.57 124.21 o 3 4 1 37.56 46.11 7.09 o 4 4 1 1092.94 1277.97 80.11 o 5 4 1 120.88 135.96 9.62 o 6 4 1 169.80 187.86 8.68 o -6 5 1 239.75 250.32 11.08 o -5 5 1 81.30 76.97 4.66 o -4 5 1 869.58 949.35 54.34 o -3 5 1 692.68 744.89 21.12 o -2 5 1 108.60 125.59 4.45 o -1 5 1 3840.82 4078.61 29.18 o 0 5 1 21.25 23.13 2.97 o 1 5 1 573.23 557.26 27.88 o 2 5 1 0.37 2.05 0.96 o 3 5 1 335.76 406.10 58.63 o 4 5 1 301.27 343.02 38.07 o 5 5 1 164.66 173.17 29.27 o 6 5 1 96.03 115.72 19.62 o -6 6 1 70.10 74.06 5.95 o -5 6 1 92.20 87.00 4.97 o -4 6 1 155.19 178.92 16.53 o -3 6 1 116.98 113.22 3.93 o -2 6 1 559.54 570.52 19.32 o -1 6 1 72.73 84.09 3.99 o 0 6 1 863.21 860.77 21.23 o 1 6 1 3.31 2.87 1.35 o 2 6 1 368.63 356.75 9.43 o 3 6 1 180.05 201.35 8.73 o 4 6 1 87.50 111.65 17.74 o 5 6 1 130.79 167.87 39.07 o 6 6 1 11.21 13.84 5.01 o -6 7 1 17.99 16.06 5.85 o -5 7 1 204.51 233.77 22.02 o -4 7 1 106.97 113.79 13.99 o -3 7 1 1594.20 1598.08 15.82 o -2 7 1 350.58 374.61 7.50 o -1 7 1 546.74 561.37 10.14 o 0 7 1 2644.84 2916.24 105.08 o 1 7 1 252.64 248.21 9.76 o 2 7 1 1032.92 1041.41 18.85 o 3 7 1 84.92 82.79 5.56 o 4 7 1 516.93 509.35 15.09 o 5 7 1 0.47 0.00 6.45 o -5 8 1 6.20 6.36 2.81 o -4 8 1 193.47 238.31 27.72 o -3 8 1 6.72 4.20 1.93 o -2 8 1 269.63 280.80 7.13 o -1 8 1 277.68 301.47 9.45 o 0 8 1 2.03 1.93 1.17 o 1 8 1 476.61 504.10 17.37 o 2 8 1 294.44 306.35 5.56 o 3 8 1 158.51 162.09 7.31 o 4 8 1 181.14 174.70 10.92 o 5 8 1 33.05 31.09 8.85 o -5 9 1 37.25 41.65 5.42 o -4 9 1 293.06 369.12 57.04 o -3 9 1 58.41 42.00 5.54 o -2 9 1 781.14 836.30 30.61 o -1 9 1 15.98 16.70 2.96 o 0 9 1 225.45 235.46 6.28 o 1 9 1 118.89 123.79 5.61 o 2 9 1 202.20 218.51 4.86 o 3 9 1 34.42 36.07 6.22 o 4 9 1 0.39 4.30 4.50 o -4 10 1 17.43 20.52 6.82 o -3 10 1 71.15 79.30 5.73 o -2 10 1 118.49 126.96 6.11 o -1 10 1 125.12 124.44 6.25 o 0 10 1 254.79 270.63 6.95 o 1 10 1 31.14 24.10 3.37 o 2 10 1 88.60 72.07 3.94 o 3 10 1 0.13 1.56 3.42 o -3 11 1 85.63 101.25 6.41 o -2 11 1 7.96 6.48 2.67 o -1 11 1 367.78 399.21 11.73 o 0 11 1 0.53 1.30 5.29 o 1 11 1 183.41 185.42 7.95 o 2 11 1 203.85 205.80 5.62 o -1 12 1 58.33 56.89 4.48 o 0 12 1 10.57 11.22 3.65 o -2 -12 2 0.31 1.95 3.06 o -1 -12 2 170.81 178.50 6.12 o 0 -12 2 39.18 31.07 4.04 o 1 -12 2 251.92 282.35 8.32 o 2 -12 2 71.31 60.51 5.20 o -3 -11 2 18.38 6.67 3.32 o -2 -11 2 46.59 41.46 4.32 o -1 -11 2 102.31 111.70 6.70 o 0 -11 2 86.53 82.94 4.90 o 1 -11 2 176.14 208.22 6.84 o 2 -11 2 0.46 2.83 2.35 o 3 -11 2 176.63 192.87 6.65 o -4 -10 2 117.49 120.22 8.65 o -3 -10 2 1.31 1.60 2.15 o -2 -10 2 321.49 342.98 12.92 o -1 -10 2 69.03 68.63 4.17 o 0 -10 2 246.35 263.54 8.60 o 1 -10 2 8.75 4.40 2.00 o 2 -10 2 343.89 362.75 13.48 o 3 -10 2 128.66 129.01 5.69 o 4 -10 2 163.55 181.46 9.42 o -4 -9 2 20.29 13.63 5.50 o -3 -9 2 364.13 365.55 8.97 o -2 -9 2 46.86 43.94 3.11 o -1 -9 2 535.53 566.18 21.79 o 0 -9 2 148.61 154.85 4.24 o 1 -9 2 557.16 594.85 10.20 o 2 -9 2 283.97 311.82 10.28 o 3 -9 2 2.04 1.55 1.74 o 4 -9 2 404.71 436.47 27.75 o 5 -9 2 0.01 2.40 4.29 o -5 -8 2 10.49 8.10 5.24 o -4 -8 2 292.66 285.31 8.68 o -3 -8 2 162.27 161.66 7.40 o -2 -8 2 34.75 22.69 2.16 o -1 -8 2 511.92 542.72 25.17 o 0 -8 2 222.56 239.14 9.44 o 1 -8 2 778.85 755.58 10.55 o 2 -8 2 17.33 16.07 2.57 o 3 -8 2 829.93 884.08 43.62 o 4 -8 2 10.24 10.43 3.92 o 5 -8 2 110.22 108.79 12.38 o -5 -7 2 108.43 110.55 7.88 o -4 -7 2 56.42 63.17 5.85 o -3 -7 2 114.68 118.88 6.37 o -2 -7 2 640.38 644.48 26.01 o -1 -7 2 2.80 4.03 1.65 o 0 -7 2 295.25 241.38 9.11 o 1 -7 2 351.48 355.19 13.20 o 2 -7 2 880.31 906.69 32.75 o 3 -7 2 41.83 33.80 3.23 o 4 -7 2 23.57 26.25 3.35 o 5 -7 2 140.38 153.95 5.73 o 6 -7 2 30.67 26.19 5.20 o -6 -6 2 22.91 10.66 4.66 o -5 -6 2 218.72 209.79 8.02 o -4 -6 2 11.82 10.12 3.93 o -3 -6 2 629.74 624.89 9.81 o -2 -6 2 36.78 33.76 2.39 o -1 -6 2 1527.69 1576.19 86.30 o 0 -6 2 700.75 750.33 37.33 o 1 -6 2 981.63 1024.38 38.04 o 2 -6 2 1696.66 1745.97 47.94 o 3 -6 2 22.26 15.19 2.01 o 4 -6 2 1631.89 1739.28 16.91 o 5 -6 2 3.94 3.23 2.92 o 6 -6 2 297.31 276.22 9.64 o -6 -5 2 44.59 38.74 5.73 o -5 -5 2 44.17 47.24 12.47 o -4 -5 2 234.54 219.09 7.08 o -3 -5 2 684.53 761.63 9.19 o -2 -5 2 325.40 281.41 4.73 o -1 -5 2 1346.38 1182.02 25.31 o 0 -5 2 959.35 1011.82 30.13 o 1 -5 2 276.42 223.26 9.70 o 2 -5 2 2.17 1.33 0.79 o 3 -5 2 1120.76 1134.52 24.93 o 4 -5 2 90.50 85.40 4.01 o 5 -5 2 17.75 25.64 3.90 o 6 -5 2 168.61 188.77 19.52 o -6 -4 2 5.61 7.76 3.25 o -5 -4 2 35.17 42.87 4.35 o -4 -4 2 514.81 529.92 9.00 o -3 -4 2 110.98 118.47 6.68 o -2 -4 2 232.71 167.61 4.67 o -1 -4 2 1202.88 1126.46 27.28 o 0 -4 2 1735.01 1523.70 132.63 o 1 -4 2 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