#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:24:03 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181016 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/96/2209623.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2209623_Fobs loop_ _publ_author_name 'Chopra, Deepak' 'Mohan, T. P.' 'Vishalakshi, B.' _publ_section_title ; 4-Fluoro-N'-(4-fluoro-3-phenoxybenzoyl)-3-phenoxybenzohydrazide ; _journal_coeditor_code OB2033 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3085 _journal_page_last o3086 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.680 _cell_angle_gamma 90.000 _cell_length_a 18.3752 _cell_length_b 18.2358 _cell_length_c 6.5954 _exptl_crystal_F_000 952.00 _reflns_d_resolution_high 0.8410 _cod_data_source_file ob2033Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' dc in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 239.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1898.56 2109.66 32.81 o 3 0 0 551.73 570.32 23.54 o 4 0 0 9033.86 9699.90 70.07 o 5 0 0 286.33 261.46 19.04 o 6 0 0 2937.81 3011.45 42.22 o 7 0 0 21002.26 22770.05 136.62 o 8 0 0 3163.23 3336.61 55.83 o 9 0 0 388.49 445.84 25.13 o 10 0 0 68.36 76.02 18.69 o 11 0 0 51.87 82.45 17.22 o 12 0 0 36.57 66.77 25.84 o 13 0 0 192.87 204.29 44.84 o 14 0 0 137.49 109.78 38.57 o 15 0 0 149.12 171.68 35.61 o 16 0 0 209.81 225.98 38.88 o 17 0 0 452.94 413.25 68.91 o 18 0 0 330.36 327.29 46.26 o 19 0 0 0.57 1.02 34.95 o 20 0 0 99.96 62.91 112.76 o 21 0 0 8.84 52.32 46.82 o 1 1 0 101.10 26.46 7.91 o 2 1 0 30.23 27.20 6.38 o 3 1 0 3589.25 3770.55 31.64 o 4 1 0 414.33 368.40 12.24 o 5 1 0 1876.58 2028.18 26.16 o 6 1 0 110.84 107.65 10.21 o 7 1 0 715.03 740.93 19.27 o 8 1 0 0.00 1.82 9.03 o 9 1 0 1015.32 1096.24 25.15 o 10 1 0 188.18 144.47 13.88 o 11 1 0 609.85 638.46 21.76 o 12 1 0 202.02 200.35 23.15 o 13 1 0 1.79 9.97 17.07 o 14 1 0 54.94 62.98 18.33 o 15 1 0 24.41 53.59 19.53 o 16 1 0 181.98 227.76 28.45 o 17 1 0 650.06 576.44 44.07 o 18 1 0 4.39 58.50 21.16 o 19 1 0 4.31 57.89 22.44 o 20 1 0 95.32 157.33 30.52 o 21 1 0 5.15 69.10 27.58 o 0 2 0 980.53 1044.49 36.93 o 1 2 0 98.10 110.34 7.63 o 2 2 0 263.77 264.04 9.43 o 3 2 0 53.11 64.09 7.98 o 4 2 0 3566.86 3797.10 33.45 o 5 2 0 250.12 275.06 12.95 o 6 2 0 16.65 17.72 10.52 o 7 2 0 55.03 73.70 10.11 o 8 2 0 85.51 105.46 11.94 o 9 2 0 1.90 14.52 9.64 o 10 2 0 198.33 201.05 14.14 o 11 2 0 352.10 373.86 20.59 o 12 2 0 131.36 164.37 22.49 o 13 2 0 7.32 26.59 16.19 o 14 2 0 2.78 16.66 24.65 o 15 2 0 56.66 85.59 21.43 o 16 2 0 24.79 17.19 17.80 o 17 2 0 28.44 35.61 20.46 o 18 2 0 0.32 57.77 21.36 o 19 2 0 0.20 50.84 23.16 o 20 2 0 20.19 43.38 56.92 o 21 2 0 18.90 49.21 87.37 o 1 3 0 10.95 -0.44 6.66 o 2 3 0 4570.94 4779.38 39.28 o 3 3 0 1849.13 2165.51 29.40 o 4 3 0 7185.25 7800.27 49.03 o 5 3 0 46.06 38.04 8.79 o 6 3 0 471.41 470.70 16.23 o 7 3 0 234.87 250.99 13.93 o 8 3 0 1159.36 1159.01 26.71 o 9 3 0 459.93 507.12 19.90 o 10 3 0 1815.59 1949.75 36.07 o 11 3 0 922.94 802.12 26.44 o 12 3 0 550.64 528.51 42.93 o 13 3 0 32.75 12.61 16.88 o 14 3 0 3.39 7.65 17.53 o 15 3 0 9.85 22.10 19.99 o 16 3 0 59.50 76.89 21.25 o 17 3 0 73.09 59.34 32.95 o 18 3 0 0.26 59.03 22.93 o 19 3 0 0.32 34.76 23.59 o 20 3 0 2.41 30.93 34.76 o 21 3 0 3.04 137.23 41.19 o 0 4 0 57564.22 65623.97 294.20 o 1 4 0 342.18 303.84 11.93 o 2 4 0 196.61 171.48 12.56 o 3 4 0 517.48 452.54 16.59 o 4 4 0 54.98 61.71 9.09 o 5 4 0 73.86 78.76 9.80 o 6 4 0 1113.43 1157.84 24.16 o 7 4 0 35.36 45.37 10.04 o 8 4 0 1514.02 1661.78 31.44 o 9 4 0 125.58 144.22 14.00 o 10 4 0 210.75 232.03 15.70 o 11 4 0 448.89 465.49 20.81 o 12 4 0 0.14 45.15 15.19 o 13 4 0 112.83 129.76 21.01 o 14 4 0 32.09 30.42 18.05 o 15 4 0 8.82 3.19 17.51 o 16 4 0 0.69 93.59 23.87 o 17 4 0 36.85 58.54 23.39 o 18 4 0 82.24 57.13 60.01 o 19 4 0 34.51 84.33 37.07 o 20 4 0 13.27 18.99 34.05 o 21 4 0 0.21 75.67 36.23 o 1 5 0 1511.10 1552.15 23.33 o 2 5 0 7031.13 7791.66 60.24 o 3 5 0 3270.55 3442.39 42.05 o 4 5 0 36.58 38.86 12.59 o 5 5 0 102.94 107.42 10.38 o 6 5 0 1.08 -0.20 8.83 o 7 5 0 307.52 274.24 15.06 o 8 5 0 49.34 70.60 11.55 o 9 5 0 1078.45 1045.89 27.65 o 10 5 0 26.34 42.29 11.34 o 11 5 0 611.61 630.69 25.66 o 12 5 0 15.36 30.15 17.16 o 13 5 0 176.80 218.74 21.64 o 14 5 0 29.89 41.53 20.65 o 15 5 0 2.91 65.52 23.08 o 16 5 0 315.06 295.16 36.33 o 17 5 0 352.78 275.44 46.53 o 18 5 0 10.44 30.45 31.45 o 19 5 0 7.78 17.44 31.99 o 20 5 0 59.31 82.04 37.86 o 21 5 0 0.38 5.93 33.23 o 0 6 0 26103.01 28892.72 149.17 o 1 6 0 251.04 282.66 13.45 o 2 6 0 3832.19 3991.82 37.49 o 3 6 0 21.72 22.70 10.23 o 4 6 0 0.95 -1.25 9.90 o 5 6 0 110.20 102.42 12.40 o 6 6 0 207.13 215.90 13.43 o 7 6 0 7.44 9.78 9.67 o 8 6 0 829.61 846.86 24.58 o 9 6 0 554.59 542.54 21.48 o 10 6 0 3.25 20.99 10.73 o 11 6 0 372.58 315.75 19.06 o 12 6 0 26.17 32.39 16.63 o 13 6 0 139.28 131.32 34.17 o 14 6 0 14.54 70.95 22.63 o 15 6 0 49.39 63.90 33.96 o 16 6 0 33.80 62.11 30.37 o 17 6 0 2.86 -5.44 31.10 o 18 6 0 6.65 86.13 69.57 o 19 6 0 29.15 48.91 34.81 o 20 6 0 49.17 70.51 40.55 o 1 7 0 233.28 233.31 13.52 o 2 7 0 6.81 25.23 8.94 o 3 7 0 2505.31 2531.91 41.40 o 4 7 0 891.36 967.78 27.38 o 5 7 0 188.53 185.13 15.22 o 6 7 0 495.90 488.31 22.03 o 7 7 0 14.45 24.12 10.09 o 8 7 0 171.52 173.29 14.08 o 9 7 0 162.59 169.78 14.40 o 10 7 0 17.05 16.33 11.96 o 11 7 0 10.88 22.67 12.97 o 12 7 0 1.13 23.17 15.86 o 13 7 0 622.17 634.61 58.74 o 14 7 0 306.30 329.02 51.43 o 15 7 0 55.54 138.47 44.84 o 16 7 0 8.42 -10.80 24.25 o 17 7 0 92.78 92.92 53.08 o 18 7 0 338.12 346.43 59.68 o 19 7 0 45.09 55.84 35.68 o 20 7 0 38.75 19.69 32.27 o 0 8 0 42.15 20.87 15.16 o 1 8 0 0.35 10.00 10.24 o 2 8 0 1809.90 1846.59 30.59 o 3 8 0 586.55 593.80 17.44 o 4 8 0 154.18 153.40 15.54 o 5 8 0 102.32 117.18 14.51 o 6 8 0 1282.72 1192.33 33.30 o 7 8 0 400.22 365.25 20.62 o 8 8 0 47.68 46.03 14.65 o 9 8 0 26.11 46.58 13.25 o 10 8 0 46.77 48.42 13.85 o 11 8 0 53.78 61.77 16.90 o 12 8 0 317.44 308.68 32.32 o 13 8 0 1.55 40.73 29.28 o 14 8 0 109.85 120.65 35.96 o 15 8 0 8.31 19.22 29.89 o 16 8 0 13.69 -11.29 71.54 o 17 8 0 13.35 63.97 52.09 o 18 8 0 27.78 101.58 39.23 o 19 8 0 62.29 85.58 38.41 o 20 8 0 1.31 57.09 38.02 o 1 9 0 56.12 78.66 12.93 o 2 9 0 2540.83 2568.96 38.09 o 3 9 0 13.86 30.38 14.06 o 4 9 0 385.92 420.37 22.32 o 5 9 0 212.01 222.01 19.10 o 6 9 0 57.68 48.97 12.72 o 7 9 0 0.43 11.00 18.75 o 8 9 0 288.88 289.36 20.22 o 9 9 0 223.35 197.80 22.45 o 10 9 0 845.71 778.67 38.54 o 11 9 0 118.01 127.92 19.45 o 12 9 0 72.50 96.98 26.29 o 13 9 0 18.62 23.35 26.74 o 14 9 0 25.03 40.77 35.61 o 15 9 0 21.15 18.55 32.94 o 16 9 0 9.67 66.54 36.10 o 17 9 0 57.23 64.89 32.68 o 18 9 0 39.99 59.51 38.16 o 19 9 0 17.37 62.78 36.52 o 0 10 0 3766.90 3859.58 70.71 o 1 10 0 324.66 322.97 18.07 o 2 10 0 16.37 26.79 11.13 o 3 10 0 1.84 16.49 9.76 o 4 10 0 13.69 22.06 12.87 o 5 10 0 100.33 106.78 22.36 o 6 10 0 18.14 36.46 12.43 o 7 10 0 292.94 272.88 25.75 o 8 10 0 200.67 181.67 22.82 o 9 10 0 151.74 130.87 21.85 o 10 10 0 570.58 543.21 34.71 o 11 10 0 291.43 304.26 34.40 o 12 10 0 126.15 160.91 28.75 o 13 10 0 134.43 160.52 60.84 o 14 10 0 153.68 168.17 40.83 o 15 10 0 42.26 71.40 33.80 o 16 10 0 159.44 123.17 39.90 o 17 10 0 0.37 -6.18 44.84 o 18 10 0 3.70 34.14 47.81 o 19 10 0 44.70 -26.47 75.17 o 1 11 0 83.02 86.43 14.01 o 2 11 0 9.88 32.87 11.47 o 3 11 0 304.97 328.95 22.11 o 4 11 0 165.87 172.88 18.28 o 5 11 0 158.27 182.52 18.20 o 6 11 0 1.03 -9.47 17.92 o 7 11 0 77.44 67.06 19.67 o 8 11 0 46.92 60.13 19.19 o 9 11 0 17.74 64.55 20.54 o 10 11 0 2.91 30.74 18.59 o 11 11 0 0.09 3.01 23.15 o 12 11 0 71.78 96.45 26.82 o 13 11 0 948.61 1006.32 58.96 o 14 11 0 172.69 220.11 44.98 o 15 11 0 88.67 59.59 35.87 o 16 11 0 3.57 55.26 36.60 o 17 11 0 43.85 36.25 60.66 o 18 11 0 55.14 109.68 37.07 o 0 12 0 1558.31 1415.85 49.21 o 1 12 0 385.88 410.48 20.70 o 2 12 0 24.17 40.43 15.35 o 3 12 0 4.75 6.36 18.04 o 4 12 0 50.30 34.70 18.92 o 5 12 0 14.47 8.65 18.96 o 6 12 0 61.92 96.12 21.69 o 7 12 0 130.41 111.77 23.33 o 8 12 0 76.01 60.03 21.55 o 9 12 0 246.30 238.73 27.96 o 10 12 0 19.70 31.60 19.30 o 11 12 0 68.48 103.79 46.07 o 12 12 0 69.22 76.07 27.41 o 13 12 0 1.84 36.45 25.78 o 14 12 0 18.77 52.25 49.78 o 15 12 0 7.91 49.51 32.94 o 16 12 0 7.34 42.41 31.99 o 17 12 0 23.26 53.95 60.01 o 18 12 0 44.57 91.36 43.19 o 1 13 0 44.72 66.44 16.57 o 2 13 0 102.66 105.83 18.76 o 3 13 0 105.35 109.53 22.37 o 4 13 0 4.59 19.36 18.24 o 5 13 0 1.09 38.88 21.99 o 6 13 0 217.52 254.72 27.70 o 7 13 0 70.81 67.76 22.48 o 8 13 0 9.05 12.73 20.38 o 9 13 0 10.61 16.89 19.81 o 10 13 0 21.17 28.12 20.58 o 11 13 0 425.88 355.11 42.36 o 12 13 0 159.08 141.32 30.80 o 13 13 0 40.91 88.05 27.43 o 14 13 0 194.65 187.21 51.10 o 15 13 0 47.55 89.64 37.01 o 16 13 0 11.16 99.68 37.53 o 17 13 0 31.02 51.83 37.38 o 0 14 0 287.64 246.32 38.10 o 1 14 0 1.60 23.95 22.47 o 2 14 0 37.92 48.03 25.03 o 3 14 0 3.39 10.28 18.67 o 4 14 0 75.35 89.01 23.25 o 5 14 0 11.66 22.31 20.80 o 6 14 0 24.39 15.03 21.05 o 7 14 0 1.49 34.23 22.23 o 8 14 0 1.07 33.63 20.65 o 9 14 0 35.95 41.86 22.23 o 10 14 0 499.94 518.48 38.59 o 11 14 0 57.57 73.50 29.51 o 12 14 0 7.82 63.78 30.20 o 13 14 0 68.45 142.67 34.56 o 14 14 0 90.54 59.68 79.13 o 15 14 0 4.37 107.84 49.10 o 16 14 0 103.15 269.82 74.84 o 1 15 0 6.25 -16.49 21.77 o 2 15 0 267.33 311.67 37.57 o 3 15 0 118.69 145.90 23.75 o 4 15 0 34.17 31.99 20.83 o 5 15 0 28.52 23.35 30.46 o 6 15 0 17.61 64.53 22.68 o 7 15 0 307.87 312.74 31.79 o 8 15 0 0.93 65.36 22.65 o 9 15 0 87.33 94.03 23.18 o 10 15 0 47.92 39.51 20.74 o 11 15 0 86.81 119.94 30.16 o 12 15 0 30.09 44.99 29.06 o 13 15 0 51.75 122.01 32.64 o 14 15 0 1.18 96.51 40.93 o 15 15 0 5.51 91.50 42.62 o 0 16 0 141.61 159.57 51.43 o 1 16 0 2.43 -18.58 25.87 o 2 16 0 34.44 42.90 55.72 o 3 16 0 148.01 218.39 33.68 o 4 16 0 73.87 102.92 30.21 o 5 16 0 4.98 47.85 29.14 o 6 16 0 0.00 5.03 29.24 o 7 16 0 54.61 121.25 45.47 o 8 16 0 200.39 191.14 27.54 o 9 16 0 77.97 128.23 24.89 o 10 16 0 123.98 97.98 24.53 o 11 16 0 147.32 232.21 36.10 o 12 16 0 2.75 51.43 28.60 o 13 16 0 154.62 262.81 53.69 o 14 16 0 199.96 194.89 46.51 o 1 17 0 45.30 -3.94 27.25 o 2 17 0 113.83 85.37 81.11 o 3 17 0 9.80 71.65 47.48 o 4 17 0 0.45 35.75 32.28 o 5 17 0 0.77 34.09 25.80 o 6 17 0 63.84 60.22 31.50 o 7 17 0 86.12 103.48 25.70 o 8 17 0 46.36 58.50 22.24 o 9 17 0 125.50 177.65 27.18 o 10 17 0 26.99 31.41 21.41 o 11 17 0 28.73 109.28 30.81 o 12 17 0 5.95 77.05 29.72 o 13 17 0 154.90 261.81 45.06 o 0 18 0 293.18 186.61 60.66 o 1 18 0 199.11 122.51 34.16 o 2 18 0 150.92 120.88 37.01 o 3 18 0 55.95 52.16 43.52 o 4 18 0 78.03 94.53 36.36 o 5 18 0 174.48 202.69 42.62 o 6 18 0 74.58 115.84 36.13 o 7 18 0 247.40 271.43 37.59 o 8 18 0 705.49 643.59 106.00 o 9 18 0 337.55 376.42 36.05 o 10 18 0 151.03 153.53 33.13 o 11 18 0 0.04 90.30 31.48 o 12 18 0 95.18 127.97 44.91 o 1 19 0 78.37 135.85 36.13 o 2 19 0 47.72 50.08 31.16 o 3 19 0 41.03 84.89 33.80 o 4 19 0 70.89 112.34 37.95 o 5 19 0 40.93 2.82 32.34 o 6 19 0 0.04 -11.42 29.62 o 7 19 0 4.81 46.32 33.69 o 8 19 0 6.77 58.03 36.93 o 9 19 0 0.36 67.93 29.06 o 10 19 0 0.15 12.54 54.73 o 0 20 0 107.17 96.27 44.84 o 1 20 0 18.07 71.65 31.26 o 2 20 0 13.45 80.68 52.75 o 3 20 0 106.12 150.82 40.82 o 4 20 0 70.67 114.06 37.69 o 5 20 0 2.78 91.82 37.46 o 6 20 0 35.25 89.05 37.95 o 7 20 0 31.66 70.71 37.90 o 8 20 0 0.51 110.66 38.87 o 1 21 0 0.00 40.34 74.51 o 2 21 0 22.12 122.70 47.81 o 3 21 0 8.25 91.76 41.87 o 4 21 0 10.87 75.19 39.89 o 5 21 0 108.29 200.32 45.22 o -21 1 1 0.70 45.32 36.58 o -20 1 1 3.85 82.95 29.54 o -19 1 1 48.40 32.69 22.37 o -18 1 1 27.61 55.83 21.89 o -17 1 1 98.61 112.67 24.01 o -16 1 1 170.18 199.92 31.22 o -15 1 1 250.33 286.52 38.45 o -14 1 1 61.51 93.82 21.48 o -13 1 1 512.70 474.76 27.17 o -12 1 1 31.53 47.60 12.68 o -11 1 1 17.12 31.85 12.40 o -10 1 1 4.87 16.53 10.72 o -9 1 1 31.31 19.29 11.10 o -8 1 1 80.14 71.89 11.99 o -7 1 1 5974.00 6344.84 58.94 o -6 1 1 19.05 10.62 8.94 o -5 1 1 4414.82 4582.29 44.19 o -4 1 1 10731.44 11472.64 64.80 o -3 1 1 3895.15 4065.32 36.51 o -2 1 1 916.72 958.17 17.56 o -1 1 1 188.72 217.73 9.35 o 0 1 1 0.99 -1.00 5.37 o 1 1 1 763.60 773.67 15.22 o 2 1 1 9888.20 11308.70 56.37 o 3 1 1 25705.53 28529.27 95.35 o 4 1 1 13734.59 13966.82 76.82 o 5 1 1 103.84 83.03 9.77 o 6 1 1 3566.38 3632.90 39.74 o 7 1 1 810.10 728.15 29.93 o 8 1 1 167.98 195.81 20.46 o 9 1 1 3101.20 3206.79 65.34 o 10 1 1 1163.55 1102.61 42.65 o 11 1 1 915.69 908.87 41.44 o 12 1 1 302.13 316.08 31.03 o 13 1 1 466.29 354.61 29.23 o 14 1 1 8.03 11.44 18.87 o 15 1 1 177.18 158.08 23.89 o 16 1 1 31.48 55.68 26.65 o 17 1 1 104.54 100.80 38.83 o 18 1 1 16.27 -5.18 34.62 o 19 1 1 16.37 106.35 24.17 o 20 1 1 1.74 20.22 29.50 o 21 1 1 2.06 50.90 26.29 o -21 2 1 66.49 96.05 38.02 o -20 2 1 3.32 48.01 32.46 o -19 2 1 28.51 54.78 32.06 o -18 2 1 113.75 133.59 29.45 o -17 2 1 174.70 171.98 27.05 o -16 2 1 123.70 161.44 26.87 o -15 2 1 128.77 142.98 24.25 o -14 2 1 549.24 498.88 34.32 o -13 2 1 30.85 25.22 15.33 o -12 2 1 281.09 244.11 18.07 o -11 2 1 15.85 14.81 11.81 o -10 2 1 56.90 62.45 12.28 o -9 2 1 1365.40 1290.00 31.22 o -8 2 1 2069.23 2082.78 36.74 o -7 2 1 1.64 14.55 9.30 o -6 2 1 4163.55 4536.71 47.10 o -5 2 1 5307.41 5650.63 49.10 o -4 2 1 907.72 989.77 20.80 o -3 2 1 4859.01 5257.18 40.51 o -2 2 1 14750.60 16472.00 68.60 o -1 2 1 21.82 37.32 7.34 o 0 2 1 19901.35 22605.07 80.78 o 1 2 1 6064.36 6818.60 44.70 o 2 2 1 4.16 12.03 8.03 o 3 2 1 266.03 332.96 13.37 o 4 2 1 9104.15 9493.04 56.52 o 5 2 1 5606.57 5468.78 42.62 o 6 2 1 4501.81 4516.60 50.13 o 7 2 1 21.53 50.69 9.87 o 8 2 1 185.29 216.22 18.39 o 9 2 1 53.60 48.37 13.61 o 10 2 1 45.51 53.53 12.34 o 11 2 1 587.78 684.88 37.75 o 12 2 1 36.88 28.57 18.18 o 13 2 1 238.02 228.54 28.58 o 14 2 1 153.81 172.03 31.31 o 15 2 1 96.86 107.44 27.10 o 16 2 1 21.88 36.83 21.09 o 17 2 1 13.07 1.08 18.93 o 18 2 1 78.21 153.50 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