#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/00/2210003.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210003_Fobs loop_ _publ_author_name 'Wang, Shu-Ping' 'Gao, Zhi-Hua' 'Xu, Li-Juan' 'Wang, Rui-Feng' _publ_section_title ; Tetra-\m-benzoato-bis[benzoato(2,2-bipyridyl)terbium(III)] ; _journal_coeditor_code SG2045 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1853 _journal_page_last m1855 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.435 _cell_angle_gamma 90.000 _cell_length_a 14.1379 _cell_length_b 15.3995 _cell_length_c 25.9625 _exptl_crystal_F_000 2688.00 _reflns_d_resolution_high 0.8399 _[local]_cod_data_source_file sg2045Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 50707A in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 578.27 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 334394.03 331375.53 10772.65 o 4 0 0 183158.95 183930.81 5991.15 o 6 0 0 206614.20 202224.53 6588.50 o 8 0 0 87605.73 84960.58 2795.59 o 10 0 0 45033.84 44796.82 1504.58 o 12 0 0 35124.48 35129.89 1205.25 o 14 0 0 14941.39 12475.73 731.28 o 16 0 0 4547.09 4486.61 450.30 o 1 1 0 20.93 -17.88 11.92 o 2 1 0 7564.22 7512.85 212.52 o 3 1 0 4250.50 4431.41 120.07 o 4 1 0 5606.31 5875.31 153.34 o 5 1 0 1.91 -35.50 35.44 o 6 1 0 33139.21 33646.61 791.92 o 7 1 0 117.54 108.63 52.46 o 8 1 0 22620.82 22702.32 550.53 o 9 1 0 439.78 639.23 76.27 o 10 1 0 13095.29 12736.49 350.89 o 11 1 0 41.16 90.26 88.03 o 12 1 0 19714.89 19294.19 571.37 o 13 1 0 92.64 -92.71 155.21 o 14 1 0 13304.76 14517.61 590.10 o 15 1 0 70.81 -90.80 244.77 o 16 1 0 6622.62 7342.20 391.79 o 0 2 0 318209.63 299073.66 13835.03 o 1 2 0 27868.20 29012.35 776.56 o 2 2 0 79118.73 79739.09 1828.40 o 3 2 0 13310.01 14283.93 339.60 o 4 2 0 102856.76 100160.67 2309.94 o 5 2 0 16856.21 16550.27 398.38 o 6 2 0 172043.94 172411.14 3977.10 o 7 2 0 16391.02 15547.54 384.32 o 8 2 0 54155.61 54024.82 1267.85 o 9 2 0 8941.71 9046.20 249.91 o 10 2 0 19717.59 19784.72 495.43 o 11 2 0 4336.39 4524.02 196.21 o 12 2 0 13553.09 13416.04 425.06 o 13 2 0 1635.71 1472.11 155.87 o 14 2 0 9725.77 9510.24 427.16 o 15 2 0 1052.71 1374.51 243.95 o 16 2 0 3044.93 3430.83 313.08 o 1 3 0 6579.25 7099.86 174.13 o 2 3 0 11493.95 12435.23 343.45 o 3 3 0 647.82 649.53 39.62 o 4 3 0 287.96 350.49 51.54 o 5 3 0 8229.32 8552.43 214.72 o 6 3 0 4867.44 4624.07 134.31 o 7 3 0 1157.44 1162.42 66.34 o 8 3 0 4824.71 4768.04 148.94 o 9 3 0 30.03 91.66 65.76 o 10 3 0 3411.88 3486.49 488.11 o 11 3 0 1005.45 1129.08 325.65 o 12 3 0 5858.64 5974.40 312.15 o 13 3 0 2418.39 2048.09 166.43 o 14 3 0 6168.10 6531.97 325.85 o 15 3 0 1826.07 1346.55 350.72 o 16 3 0 2561.25 3833.79 460.03 o 0 4 0 192500.33 196346.77 5190.68 o 1 4 0 19640.55 19771.29 377.00 o 2 4 0 94703.87 93421.02 2154.05 o 3 4 0 32833.16 31599.88 853.05 o 4 4 0 18212.42 17457.91 415.78 o 5 4 0 41252.10 40382.50 940.45 o 6 4 0 42894.84 43161.07 1014.46 o 7 4 0 35177.73 34921.18 827.37 o 8 4 0 25070.04 25190.78 704.77 o 9 4 0 19816.04 19237.82 1122.74 o 10 4 0 7592.92 7535.14 405.35 o 11 4 0 7127.18 7245.17 280.46 o 12 4 0 6995.25 7147.92 427.70 o 13 4 0 3620.04 3552.11 384.79 o 14 4 0 5802.98 6245.88 334.63 o 15 4 0 2864.11 3098.80 278.09 o 1 5 0 496.02 475.27 27.87 o 2 5 0 1255.82 1326.69 42.10 o 3 5 0 24.71 108.27 42.30 o 4 5 0 4059.21 4316.39 125.63 o 5 5 0 925.67 850.09 74.17 o 6 5 0 196.15 163.57 55.82 o 7 5 0 13099.41 13249.98 391.67 o 8 5 0 3734.43 3603.44 342.36 o 9 5 0 3561.83 3665.42 180.10 o 10 5 0 1894.80 1701.72 155.08 o 11 5 0 2678.06 2855.66 310.89 o 12 5 0 3238.43 3225.06 849.31 o 13 5 0 3783.62 3246.24 240.77 o 14 5 0 2668.80 2536.20 306.63 o 15 5 0 2799.09 2782.18 555.08 o 0 6 0 85371.98 86587.98 2300.78 o 1 6 0 102775.84 101370.97 1902.60 o 2 6 0 35166.60 34943.79 729.17 o 3 6 0 103295.59 103980.76 2400.72 o 4 6 0 11215.93 11083.70 275.70 o 5 6 0 77585.74 78289.94 1812.32 o 6 6 0 51913.20 52111.79 1220.61 o 7 6 0 84277.25 81780.20 1899.07 o 8 6 0 5009.52 5382.50 391.21 o 9 6 0 21774.57 22367.30 643.23 o 10 6 0 3253.18 3131.29 412.08 o 11 6 0 11450.29 11754.39 483.42 o 12 6 0 2198.12 2017.67 203.15 o 13 6 0 7897.56 8027.48 562.29 o 14 6 0 832.53 674.75 199.77 o 15 6 0 3119.37 3939.66 537.98 o 1 7 0 219.68 284.49 33.66 o 2 7 0 6302.93 6758.80 145.36 o 3 7 0 6519.07 6452.90 184.26 o 4 7 0 922.86 900.24 57.59 o 5 7 0 2197.65 2361.35 219.38 o 6 7 0 3295.59 3516.09 136.67 o 7 7 0 13251.68 12824.07 389.73 o 8 7 0 392.79 224.10 285.67 o 9 7 0 12062.04 12471.83 493.39 o 10 7 0 2140.38 2075.58 189.55 o 11 7 0 4059.99 4185.15 253.92 o 12 7 0 2032.01 1557.70 297.41 o 13 7 0 4792.12 4545.59 502.28 o 14 7 0 357.15 343.47 244.43 o 15 7 0 3592.51 3442.63 323.06 o 0 8 0 541.87 391.62 87.01 o 1 8 0 89538.37 87810.96 1652.76 o 2 8 0 13.62 16.59 34.70 o 3 8 0 56585.79 56209.40 1169.50 o 4 8 0 988.30 1003.29 58.68 o 5 8 0 52096.42 49996.71 1354.48 o 6 8 0 2689.21 2949.58 212.92 o 7 8 0 60381.20 58332.80 1583.07 o 8 8 0 12.52 -68.65 95.80 o 9 8 0 27860.78 25617.70 1023.49 o 10 8 0 341.75 50.32 147.45 o 11 8 0 13311.57 13475.36 543.99 o 12 8 0 1392.82 1281.53 198.35 o 13 8 0 8232.74 8234.77 612.76 o 14 8 0 3.14 -115.27 200.93 o 1 9 0 197.58 159.30 41.25 o 2 9 0 2126.04 2082.04 98.34 o 3 9 0 2571.50 2580.23 89.63 o 4 9 0 137.13 196.80 63.97 o 5 9 0 1706.63 1609.35 150.44 o 6 9 0 333.60 246.07 91.55 o 7 9 0 6624.28 6635.87 374.76 o 8 9 0 3693.25 3541.27 330.77 o 9 9 0 1894.17 1741.31 146.38 o 10 9 0 54.61 -25.85 156.30 o 11 9 0 4075.04 4179.42 326.08 o 12 9 0 23.36 143.40 182.74 o 13 9 0 3181.89 3714.52 945.20 o 14 9 0 5.14 -68.58 233.53 o 0 10 0 1935.39 1861.45 98.11 o 1 10 0 44188.03 43135.75 824.53 o 2 10 0 3968.71 3796.50 136.67 o 3 10 0 29421.83 29622.63 815.13 o 4 10 0 3560.70 3437.19 176.86 o 5 10 0 24056.58 24095.47 588.70 o 6 10 0 1728.17 1746.00 193.10 o 7 10 0 19035.82 19023.50 773.21 o 8 10 0 1765.34 1650.94 232.73 o 9 10 0 10600.64 10259.16 479.49 o 10 10 0 547.68 396.78 176.74 o 11 10 0 5287.13 5531.07 703.45 o 12 10 0 681.51 850.27 212.75 o 13 10 0 3351.08 3694.67 292.57 o 1 11 0 1991.99 2000.22 152.98 o 2 11 0 1182.74 1169.72 76.33 o 3 11 0 372.66 92.22 74.70 o 4 11 0 254.60 157.28 79.39 o 5 11 0 1506.22 1452.22 105.89 o 6 11 0 2.77 -94.48 88.40 o 7 11 0 2712.29 2796.87 248.85 o 8 11 0 176.83 198.18 101.62 o 9 11 0 1491.96 1294.00 150.93 o 10 11 0 263.70 368.49 273.94 o 11 11 0 2177.27 1627.43 238.63 o 12 11 0 246.66 358.26 211.48 o 13 11 0 918.65 1024.13 261.85 o 0 12 0 4235.05 4473.67 219.66 o 1 12 0 20404.43 20127.51 499.85 o 2 12 0 6099.19 5993.90 187.16 o 3 12 0 7961.54 7763.45 230.24 o 4 12 0 2588.57 2703.35 187.39 o 5 12 0 8967.26 9454.99 276.49 o 6 12 0 3386.46 3368.01 151.02 o 7 12 0 9057.44 8999.26 271.77 o 8 12 0 972.84 1217.59 195.22 o 9 12 0 3668.59 3842.14 277.74 o 10 12 0 2548.60 2401.74 164.77 o 11 12 0 1739.01 1888.25 252.09 o 12 12 0 1391.55 1031.49 241.35 o 1 13 0 1127.10 1047.46 120.05 o 2 13 0 1379.09 1188.00 127.39 o 3 13 0 47.04 50.94 111.03 o 4 13 0 30.06 -90.47 88.41 o 5 13 0 907.10 613.53 107.94 o 6 13 0 382.56 310.66 105.39 o 7 13 0 1992.64 1801.61 183.54 o 8 13 0 173.13 184.91 114.62 o 9 13 0 964.14 962.63 135.52 o 10 13 0 533.87 314.49 141.92 o 11 13 0 1071.00 765.09 190.55 o 0 14 0 2248.82 2061.07 243.76 o 1 14 0 6333.64 6189.47 554.29 o 2 14 0 1257.99 1196.13 127.83 o 3 14 0 4805.53 4558.35 204.88 o 4 14 0 5198.48 5740.34 471.19 o 5 14 0 974.66 1111.54 222.82 o 6 14 0 3515.53 3478.94 167.43 o 7 14 0 1347.98 1373.99 137.70 o 8 14 0 1313.84 1576.08 152.57 o 9 14 0 723.73 592.80 148.85 o 10 14 0 1163.22 1221.45 165.53 o 1 15 0 332.46 219.32 185.81 o 2 15 0 308.92 292.54 124.81 o 3 15 0 1.59 -97.94 124.10 o 4 15 0 2.60 -38.06 128.16 o 5 15 0 95.10 14.08 138.16 o 6 15 0 155.87 59.61 142.42 o 7 15 0 132.13 -91.87 127.73 o 8 15 0 288.18 167.18 146.03 o 9 15 0 90.76 120.48 149.87 o 0 16 0 2360.95 2554.96 290.03 o 1 16 0 4.85 -94.12 160.75 o 2 16 0 5399.97 5237.77 242.14 o 3 16 0 12.81 -47.02 133.22 o 4 16 0 2654.39 2622.64 196.75 o 5 16 0 189.71 53.58 149.52 o 6 16 0 1061.37 968.73 178.71 o 7 16 0 394.96 368.28 176.34 o 1 17 0 32.83 18.81 172.88 o 2 17 0 338.07 357.19 177.90 o 3 17 0 41.16 14.76 165.21 o 4 17 0 39.23 -92.56 159.92 o 5 17 0 180.21 122.30 171.99 o 6 17 0 257.57 170.78 180.01 o 0 18 0 811.67 457.35 311.49 o 1 18 0 8.56 -78.55 212.98 o 2 18 0 375.66 355.64 205.66 o 3 18 0 4.67 -170.01 204.19 o -15 0 1 1816.68 1819.66 356.42 o -13 0 1 2010.00 2525.12 299.76 o -11 0 1 1640.99 1738.36 155.14 o -9 0 1 315.78 125.81 99.65 o -7 0 1 11025.00 11421.20 410.14 o -5 0 1 15960.56 16350.53 555.62 o -3 0 1 6381.09 6078.88 215.75 o 1 0 1 95024.62 99489.03 4554.01 o 3 0 1 77026.62 79215.47 2585.61 o 5 0 1 38680.63 39572.05 1310.03 o 7 0 1 84180.34 84286.36 2769.04 o 9 0 1 35132.64 33666.25 1138.87 o 11 0 1 31387.94 31115.69 1063.92 o 13 0 1 15693.92 14917.04 817.79 o 15 0 1 10531.26 10697.99 685.35 o -16 1 1 415.01 517.12 276.12 o -15 1 1 10379.13 10611.68 544.02 o -14 1 1 1150.96 1033.70 257.68 o -13 1 1 23193.47 24135.05 705.91 o -12 1 1 962.70 952.47 129.13 o -11 1 1 45007.54 45228.79 1078.22 o -10 1 1 2456.72 2819.68 195.81 o -9 1 1 62765.80 62617.89 1464.48 o -8 1 1 917.75 982.16 75.91 o -7 1 1 179638.41 178494.86 4114.16 o -6 1 1 10673.59 10816.40 272.12 o -5 1 1 125236.13 124707.84 2877.03 o -4 1 1 35785.59 38094.41 886.75 o -3 1 1 165800.30 169320.14 3892.12 o -2 1 1 10756.35 11203.73 263.92 o -1 1 1 259457.80 248559.81 6563.89 o 1 1 1 182402.08 183578.25 5947.83 o 2 1 1 4214.62 4635.94 135.23 o 3 1 1 50524.61 49866.54 1155.39 o 4 1 1 33224.77 34345.60 802.85 o 5 1 1 39768.21 40217.68 940.11 o 6 1 1 506.18 545.14 52.01 o 7 1 1 11046.91 9435.71 245.94 o 8 1 1 3109.47 3152.18 117.13 o 9 1 1 15533.26 15392.31 402.80 o 10 1 1 2957.43 3081.74 127.30 o 11 1 1 11778.14 11111.36 362.46 o 12 1 1 260.15 229.99 115.71 o 13 1 1 4042.65 4074.32 253.31 o 14 1 1 8.69 66.23 184.16 o 15 1 1 645.46 681.41 219.81 o 16 1 1 286.93 -204.10 240.52 o -16 2 1 151.15 274.11 249.64 o -15 2 1 1004.99 878.44 218.93 o -14 2 1 36.83 66.62 143.51 o -13 2 1 1684.15 1776.45 191.10 o -12 2 1 133.84 275.45 198.64 o -11 2 1 1326.08 1299.23 126.68 o -10 2 1 6.90 -7.58 76.63 o -9 2 1 227.31 98.20 67.74 o -8 2 1 408.06 304.70 61.34 o -7 2 1 1176.58 1677.26 75.23 o -6 2 1 358.42 359.77 48.26 o -5 2 1 9946.79 10064.98 250.99 o -4 2 1 13508.31 14290.74 340.71 o -3 2 1 4236.25 4270.84 99.21 o -2 2 1 12871.79 13712.27 387.08 o -1 2 1 50429.33 52206.79 1196.01 o 0 2 1 998.74 1071.16 46.96 o 1 2 1 63918.57 65999.95 1514.71 o 2 2 1 16178.73 16987.28 460.85 o 3 2 1 5951.81 5711.81 170.93 o 4 2 1 49.83 131.85 57.93 o 5 2 1 17750.17 16772.38 402.98 o 6 2 1 3918.22 4223.32 126.07 o 7 2 1 52034.14 51214.45 1200.25 o 8 2 1 4734.71 4657.25 146.66 o 9 2 1 27414.50 26205.09 635.58 o 10 2 1 504.59 610.87 98.20 o 11 2 1 16154.23 16559.74 500.10 o 12 2 1 1795.33 1735.44 147.76 o 13 2 1 9906.66 10018.27 511.15 o 14 2 1 572.18 217.94 188.06 o 15 2 1 6173.41 6521.62 464.72 o 16 2 1 692.45 677.39 280.31 o -16 3 1 1764.93 1859.89 370.50 o -15 3 1 5383.12 5845.24 480.82 o -14 3 1 5039.44 4944.90 240.34 o -13 3 1 15505.72 16373.19 512.21 o -12 3 1 4598.72 4858.57 215.60 o -11 3 1 14750.28 15800.73 480.77 o -10 3 1 8682.47 9311.12 309.89 o -9 3 1 23239.51 23254.83 565.15 o -8 3 1 6469.46 6255.77 285.49 o -7 3 1 77101.38 78199.78 1814.14 o -6 3 1 30412.98 31712.42 744.52 o -5 3 1 41971.33 40506.86 845.31 o -4 3 1 997.15 907.37 55.33 o -3 3 1 1862.89 1701.19 100.63 o -2 3 1 31328.97 32062.58 745.37 o -1 3 1 73665.41 77068.05 1582.15 o 0 3 1 15445.67 15767.06 299.41 o 1 3 1 70826.48 71614.24 1473.40 o 2 3 1 39293.41 39426.53 1054.12 o 3 3 1 1795.85 1689.06 133.68 o 4 3 1 888.98 772.12 47.60 o 5 3 1 28669.36 28386.43 670.46 o 6 3 1 12766.30 12379.11 307.20 o 7 3 1 19274.03 19108.29 465.23 o 8 3 1 9938.78 10020.37 348.84 o 9 3 1 3578.43 3372.37 205.15 o 10 3 1 7218.01 6753.08 239.49 o 11 3 1 1702.08 2096.57 146.07 o 12 3 1 2123.95 1920.80 152.95 o 13 3 1 3142.42 2871.98 189.24 o 14 3 1 627.34 417.34 162.14 o 15 3 1 91.60 457.68 293.39 o 16 3 1 371.79 -50.63 325.91 o -16 4 1 429.23 237.06 325.24 o -15 4 1 134.31 251.11 207.20 o -14 4 1 1371.95 1369.01 205.93 o -13 4 1 1.28 4.36 173.36 o -12 4 1 289.29 330.46 122.39 o -11 4 1 586.74 660.51 156.17 o -10 4 1 426.04 349.75 103.43 o -9 4 1 3496.70 3788.66 162.16 o -8 4 1 67.67 41.33 62.14 o -7 4 1 3355.01 3357.68 166.97 o -6 4 1 850.11 908.91 59.61 o -5 4 1 3700.99 3558.54 95.22 o -4 4 1 69.34 32.03 30.03 o -3 4 1 4809.07 4890.52 115.89 o -2 4 1 3047.61 3296.98 103.84 o -1 4 1 297.02 439.60 89.36 o 0 4 1 3213.95 3387.23 97.34 o 1 4 1 14018.23 14142.27 299.51 o 2 4 1 5216.41 5165.63 160.53 o 3 4 1 6592.76 6329.61 194.19 o 4 4 1 1456.26 1287.87 100.32 o 5 4 1 20808.12 19598.76 471.69 o 6 4 1 10365.44 10062.82 302.90 o 7 4 1 12293.32 11828.83 299.68 o 8 4 1 12464.54 12794.60 384.82 o 9 4 1 9453.65 8722.91 406.02 o 10 4 1 3427.99 3681.46 172.88 o 11 4 1 7735.26 7375.61 268.64 o 12 4 1 2759.75 2868.59 215.94 o 13 4 1 3634.55 3847.20 262.14 o 14 4 1 1291.10 1378.80 261.03 o 15 4 1 3735.96 3984.81 293.37 o -15 5 1 2581.67 2626.35 317.69 o -14 5 1 9229.21 9279.39 426.91 o -13 5 1 6018.96 6066.12 601.19 o -12 5 1 7292.34 7489.72 725.25 o -11 5 1 8358.00 8322.25 361.92 o -10 5 1 8478.87 9033.41 308.71 o -9 5 1 11736.72 11872.17 368.33 o -8 5 1 28890.83 28202.47 787.15 o -7 5 1 18324.55 18557.26 455.44 o -6 5 1 84286.86 86638.94 1799.27 o -5 5 1 28437.66 27838.61 659.70 o -4 5 1 46386.41 45444.01 950.89 o -3 5 1 12211.04 12032.50 259.40 o -2 5 1 32782.38 32288.71 673.45 o -1 5 1 32573.12 32862.34 625.52 o 0 5 1 60779.07 60159.55 1132.78 o 1 5 1 1729.01 1576.03 123.08 o 2 5 1 19403.97 18582.75 394.93 o 3 5 1 4428.36 4163.99 209.92 o 4 5 1 29844.04 28930.29 790.25 o 5 5 1 568.87 560.12 54.79 o 6 5 1 38289.55 38779.64 910.76 o 7 5 1 312.44 329.65 77.87 o 8 5 1 15703.86 15148.27 447.29 o 9 5 1 85.84 231.92 101.53 o 10 5 1 3050.05 3429.37 226.91 o 11 5 1 107.14 173.65 114.51 o 12 5 1 1824.49 1720.45 245.44 o 13 5 1 308.32 -25.71 195.65 o 14 5 1 1397.53 1317.35 216.54 o 15 5 1 0.09 -93.40 222.30 o -15 6 1 43.41 10.57 206.77 o -14 6 1 2368.64 2144.96 349.38 o -13 6 1 55.53 16.60 178.76 o -12 6 1 726.67 604.43 190.62 o -11 6 1 59.77 47.58 227.83 o -10 6 1 233.62 111.21 136.82 o -9 6 1 1413.09 1269.86 146.04 o -8 6 1 1689.41 1780.34 115.14 o -7 6 1 5755.42 5887.58 271.36 o -6 6 1 2524.34 2967.57 176.94 o -5 6 1 10462.40 11381.59 287.86 o -4 6 1 95.04 231.90 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