#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2210010.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210010_Fobs loop_ _publ_author_name 'Kareev, Ivan E.' 'Shustova, Natalia B.' 'Newell, Brian S.' 'Miller, Susie M.' 'Anderson, Oren P.' 'Strauss, Steven H.' 'Boltalina, Olga V.' _publ_section_title ; 1,6,11,18,24,27,52,55-Octakis(trifluoromethyl)-1,6,11,18,24,27,52,55-octahydro(C~60~-I~h~)[5,6]fullerene ; _journal_coeditor_code TK2058 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3154 _journal_page_last o3156 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.589 _cell_angle_gamma 90.000 _cell_length_a 17.4108 _cell_length_b 9.7708 _cell_length_c 24.5142 _exptl_crystal_F_000 2496.00 _reflns_d_resolution_high 0.7494 _[local]_cod_data_source_file tk2058Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ss157 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 320.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 8.12 -2.83 2.83 o 2 0 0 2168.66 2316.31 40.00 o 3 0 0 2180.68 2138.89 42.86 o 4 0 0 1266.63 1300.87 42.40 o 5 0 0 937.50 814.74 54.12 o 6 0 0 20850.56 20962.11 215.74 o 7 0 0 1635.29 1231.64 46.62 o 8 0 0 2893.13 2976.93 67.31 o 9 0 0 300.29 232.54 32.28 o 10 0 0 83.14 33.35 29.18 o 11 0 0 4141.93 3871.18 87.29 o 12 0 0 4568.52 4462.47 97.01 o 13 0 0 198.88 127.22 38.21 o 14 0 0 3757.78 3941.63 121.04 o 15 0 0 2837.28 2771.98 109.85 o 16 0 0 1388.15 1227.50 104.76 o 17 0 0 7911.64 7784.93 229.84 o 18 0 0 141.20 221.98 77.86 o 19 0 0 280.36 355.75 112.20 o 20 0 0 195.96 146.18 104.14 o 21 0 0 20.79 247.22 117.06 o 22 0 0 170.38 149.06 198.75 o 23 0 0 172.79 83.11 196.80 o 1 1 0 20392.19 20491.04 219.72 o 2 1 0 235.25 225.40 11.90 o 3 1 0 40349.89 40785.90 288.79 o 4 1 0 91921.99 94640.02 650.82 o 5 1 0 385.87 412.11 19.25 o 6 1 0 12846.84 12089.32 97.51 o 7 1 0 3193.67 3464.27 56.21 o 8 1 0 4063.46 3826.64 51.12 o 9 1 0 3925.62 3605.97 52.19 o 10 1 0 401.90 420.02 25.23 o 11 1 0 5071.55 5328.43 68.97 o 12 1 0 620.78 665.57 32.17 o 13 1 0 1757.89 1766.49 51.39 o 14 1 0 146.64 106.75 33.06 o 15 1 0 329.08 250.58 52.54 o 16 1 0 1774.54 1608.55 74.19 o 17 1 0 965.92 1062.36 68.13 o 18 1 0 77.97 14.78 60.78 o 19 1 0 0.03 -53.69 55.67 o 20 1 0 283.64 411.93 83.81 o 21 1 0 3.84 -37.71 68.39 o 22 1 0 3.24 25.89 69.24 o 23 1 0 983.33 1104.55 138.16 o 0 2 0 11016.77 12855.97 157.80 o 1 2 0 1797.38 1713.92 30.43 o 2 2 0 6857.87 7689.38 77.72 o 3 2 0 628.92 716.14 34.10 o 4 2 0 16211.84 15919.50 123.78 o 5 2 0 2034.36 2066.47 33.12 o 6 2 0 17.73 -14.91 14.91 o 7 2 0 775.24 822.30 33.61 o 8 2 0 4898.99 4250.51 56.69 o 9 2 0 2848.32 2940.07 49.03 o 10 2 0 0.63 -15.70 18.39 o 11 2 0 49.68 20.68 21.12 o 12 2 0 363.84 462.46 29.03 o 13 2 0 3947.03 3966.46 74.76 o 14 2 0 1042.65 1052.37 57.81 o 15 2 0 9618.56 8762.67 145.05 o 16 2 0 351.64 287.05 49.64 o 17 2 0 137.55 94.51 66.54 o 18 2 0 1427.40 1259.23 95.32 o 19 2 0 39.80 75.43 54.90 o 20 2 0 53.54 125.83 74.06 o 21 2 0 2774.07 2751.74 178.95 o 22 2 0 797.38 952.17 130.77 o 1 3 0 16984.42 17610.07 171.26 o 2 3 0 369.00 344.57 19.36 o 3 3 0 11944.61 12270.98 107.05 o 4 3 0 3301.85 3383.53 50.99 o 5 3 0 0.00 -18.09 18.09 o 6 3 0 4014.30 4148.30 58.41 o 7 3 0 15521.08 16305.64 132.75 o 8 3 0 6012.98 5838.44 65.61 o 9 3 0 1550.00 1621.29 32.92 o 10 3 0 288.40 275.16 20.99 o 11 3 0 458.49 439.99 26.80 o 12 3 0 335.19 319.86 29.78 o 13 3 0 3831.07 3909.70 73.98 o 14 3 0 428.10 325.99 36.95 o 15 3 0 1040.99 1037.54 71.40 o 16 3 0 1352.42 1278.75 76.26 o 17 3 0 2365.53 2585.61 117.92 o 18 3 0 274.16 273.95 65.95 o 19 3 0 961.65 919.13 87.49 o 20 3 0 3468.20 3360.70 265.39 o 21 3 0 1323.65 990.37 109.05 o 22 3 0 100.50 25.07 93.75 o 0 4 0 2159.96 2438.56 77.35 o 1 4 0 429.94 519.09 25.09 o 2 4 0 3802.20 3775.09 51.99 o 3 4 0 528.66 501.10 21.28 o 4 4 0 275.02 199.96 18.80 o 5 4 0 4373.45 4642.73 72.65 o 6 4 0 342.33 343.99 24.42 o 7 4 0 4093.29 4345.19 71.49 o 8 4 0 4923.35 4939.11 80.09 o 9 4 0 53.50 53.57 25.09 o 10 4 0 9.85 7.09 21.06 o 11 4 0 770.57 855.85 36.32 o 12 4 0 1020.72 893.92 48.99 o 13 4 0 2821.58 2773.30 76.66 o 14 4 0 120.93 44.50 42.34 o 15 4 0 0.55 4.83 44.58 o 16 4 0 234.56 226.92 58.33 o 17 4 0 737.83 680.62 74.96 o 18 4 0 48.47 -26.66 57.06 o 19 4 0 380.44 227.41 69.78 o 20 4 0 199.71 147.14 70.39 o 21 4 0 218.35 291.15 85.48 o 22 4 0 131.93 82.55 86.21 o 1 5 0 1646.06 1667.36 41.38 o 2 5 0 24881.35 26884.14 246.48 o 3 5 0 93.17 171.40 18.57 o 4 5 0 5431.28 5405.56 75.53 o 5 5 0 41.47 11.69 18.35 o 6 5 0 55.66 49.22 19.20 o 7 5 0 352.56 427.32 29.30 o 8 5 0 221.77 201.34 29.55 o 9 5 0 266.24 308.06 33.60 o 10 5 0 374.64 353.44 40.68 o 11 5 0 1266.59 1435.47 66.18 o 12 5 0 620.35 556.29 64.72 o 13 5 0 1077.71 1082.65 63.09 o 14 5 0 103.93 83.38 47.50 o 15 5 0 0.00 42.89 47.09 o 16 5 0 105.48 60.51 51.76 o 17 5 0 526.75 607.55 75.90 o 18 5 0 118.07 134.60 63.64 o 19 5 0 248.04 259.98 71.63 o 20 5 0 18.86 79.80 69.65 o 21 5 0 66.14 -41.43 70.37 o 0 6 0 1670.36 1996.15 141.06 o 1 6 0 97.31 51.52 24.30 o 2 6 0 4003.99 4188.32 63.92 o 3 6 0 26.24 78.11 22.64 o 4 6 0 13.45 -17.59 17.59 o 5 6 0 221.40 297.34 26.86 o 6 6 0 21.14 6.52 20.48 o 7 6 0 5420.53 5059.24 80.62 o 8 6 0 106.29 96.04 29.96 o 9 6 0 2930.04 2966.84 76.90 o 10 6 0 0.59 8.98 37.00 o 11 6 0 146.29 156.00 47.89 o 12 6 0 1450.11 1552.44 150.40 o 13 6 0 1.67 12.94 51.53 o 14 6 0 709.12 805.20 65.23 o 15 6 0 508.79 622.60 72.40 o 16 6 0 541.97 675.12 72.17 o 17 6 0 221.05 246.29 69.32 o 18 6 0 139.99 157.19 72.49 o 19 6 0 52.71 -60.19 67.30 o 20 6 0 169.21 223.42 81.65 o 1 7 0 431.29 447.84 39.06 o 2 7 0 9.81 -27.36 27.36 o 3 7 0 62.59 80.02 20.83 o 4 7 0 394.90 427.50 30.58 o 5 7 0 918.02 865.02 41.81 o 6 7 0 26.30 65.78 39.84 o 7 7 0 760.03 758.55 50.55 o 8 7 0 174.48 177.67 39.71 o 9 7 0 1150.41 1193.78 77.32 o 10 7 0 271.98 194.38 49.91 o 11 7 0 1590.97 1639.74 98.32 o 12 7 0 1109.26 1049.15 91.62 o 13 7 0 3884.38 3774.09 143.29 o 14 7 0 921.76 925.35 87.93 o 15 7 0 203.73 200.08 56.14 o 16 7 0 419.16 410.79 66.34 o 17 7 0 267.31 231.82 65.90 o 18 7 0 30.45 -61.56 64.26 o 19 7 0 5.62 -69.58 71.75 o 0 8 0 783.54 768.57 86.16 o 1 8 0 7960.79 7455.44 159.95 o 2 8 0 455.60 361.44 57.27 o 3 8 0 178.55 273.36 37.54 o 4 8 0 644.04 815.64 55.72 o 5 8 0 667.37 628.27 48.29 o 6 8 0 236.34 272.00 44.19 o 7 8 0 282.58 281.17 51.19 o 8 8 0 1576.29 1647.27 87.25 o 9 8 0 3490.28 3453.30 143.21 o 10 8 0 1366.75 1250.30 84.48 o 11 8 0 576.37 600.85 67.87 o 12 8 0 0.19 -13.88 52.08 o 13 8 0 15.88 19.45 59.37 o 14 8 0 753.91 705.06 83.65 o 15 8 0 340.04 400.19 84.89 o 16 8 0 139.47 200.93 70.36 o 17 8 0 8.55 31.24 65.03 o 18 8 0 113.80 125.52 73.80 o 1 9 0 626.92 454.19 74.42 o 2 9 0 432.64 243.88 58.66 o 3 9 0 801.48 670.19 68.03 o 4 9 0 7138.58 6405.46 162.83 o 5 9 0 687.11 711.84 102.54 o 6 9 0 751.24 905.46 93.70 o 7 9 0 760.83 743.15 91.22 o 8 9 0 2070.54 2066.46 132.73 o 9 9 0 32.13 37.69 69.73 o 10 9 0 1030.37 956.64 110.94 o 11 9 0 275.29 213.28 89.68 o 12 9 0 297.96 294.13 95.01 o 13 9 0 9.11 18.68 87.95 o 14 9 0 27.83 82.03 92.99 o 15 9 0 0.24 -9.80 93.68 o 16 9 0 2.72 -79.78 155.62 o 0 10 0 197.68 128.51 95.30 o 1 10 0 2206.23 1926.88 158.34 o 2 10 0 914.04 1009.11 69.13 o 3 10 0 202.43 223.45 47.70 o 4 10 0 44.33 -49.85 55.16 o 5 10 0 280.78 272.95 70.64 o 6 10 0 193.56 147.11 70.07 o 7 10 0 708.04 939.59 102.29 o 8 10 0 319.01 331.36 84.99 o 9 10 0 1467.96 1305.31 125.37 o 10 10 0 308.77 389.92 98.80 o 11 10 0 458.13 468.67 103.20 o 12 10 0 23.86 118.40 98.59 o 13 10 0 2.28 311.75 109.09 o 14 10 0 92.87 156.09 108.01 o 1 11 0 167.87 139.93 62.97 o 2 11 0 16.22 0.94 54.64 o 3 11 0 93.08 22.71 80.29 o 4 11 0 278.18 220.90 72.11 o 5 11 0 182.02 309.98 76.87 o 6 11 0 21.99 107.99 94.45 o 7 11 0 16.62 -43.63 71.74 o 8 11 0 35.81 118.21 82.94 o 9 11 0 15.80 76.91 86.07 o 10 11 0 3.49 92.98 88.22 o 11 11 0 351.44 289.05 106.03 o 12 11 0 895.33 1100.52 172.14 o 0 12 0 950.10 584.49 204.60 o 1 12 0 113.15 296.24 126.07 o 2 12 0 82.45 63.57 58.58 o 3 12 0 379.47 323.30 77.66 o 4 12 0 2078.12 2037.29 197.08 o 5 12 0 484.32 593.82 94.47 o 6 12 0 21.13 8.87 75.63 o 7 12 0 60.09 115.88 83.40 o 8 12 0 343.62 162.92 87.91 o 9 12 0 21.79 84.36 167.43 o 1 13 0 576.83 735.82 178.63 o -23 1 1 0.70 9.77 86.56 o -22 1 1 2.47 24.75 77.05 o -21 1 1 45.73 132.10 69.05 o -20 1 1 13.89 1.64 58.88 o -19 1 1 4.50 -4.20 57.73 o -18 1 1 884.69 742.03 68.04 o -17 1 1 14.04 9.47 43.27 o -16 1 1 2666.81 3020.20 91.63 o -15 1 1 1972.46 2088.36 84.50 o -14 1 1 1205.18 1359.12 55.79 o -13 1 1 110.76 120.38 27.67 o -12 1 1 3017.74 2957.36 55.29 o -11 1 1 1166.66 1166.45 38.14 o -10 1 1 2871.53 3200.70 56.65 o -9 1 1 1552.27 1788.04 39.54 o -8 1 1 9588.25 10438.42 92.50 o -7 1 1 37.49 16.68 16.25 o -6 1 1 539.50 494.34 21.23 o -5 1 1 110.63 125.28 15.75 o -4 1 1 698.66 584.79 23.84 o -3 1 1 7614.97 7249.22 64.83 o -2 1 1 5457.18 5476.37 50.02 o -1 1 1 2195.58 2206.40 28.24 o 0 1 1 6162.92 6002.50 66.73 o 1 1 1 500.55 479.36 20.90 o 2 1 1 172.00 114.26 12.12 o 3 1 1 640.34 746.57 41.77 o 4 1 1 3200.14 3426.09 55.10 o 5 1 1 615.20 523.47 20.84 o 6 1 1 75.97 26.08 15.09 o 7 1 1 16863.34 17308.15 128.94 o 8 1 1 571.70 514.04 23.19 o 9 1 1 6539.91 7738.87 78.32 o 10 1 1 90.26 82.70 20.55 o 11 1 1 9549.74 9990.93 98.67 o 12 1 1 900.30 968.56 36.71 o 13 1 1 1483.74 1489.23 48.28 o 14 1 1 1127.42 1168.88 52.22 o 15 1 1 1749.88 1677.20 70.72 o 16 1 1 36.44 -37.53 37.53 o 17 1 1 3325.99 2859.16 114.98 o 18 1 1 57.77 37.01 52.90 o 19 1 1 0.03 -1.54 57.36 o 20 1 1 2.88 18.44 66.73 o 21 1 1 1.86 137.99 75.95 o 22 1 1 891.64 1103.84 113.01 o 23 1 1 48.67 95.70 98.36 o -22 2 1 1001.84 1038.72 132.63 o -21 2 1 802.13 701.19 99.88 o -20 2 1 1493.13 1522.50 134.72 o -19 2 1 1661.01 1580.08 92.07 o -18 2 1 48.17 80.60 50.60 o -17 2 1 62.40 188.67 51.50 o -16 2 1 2181.65 2387.73 83.80 o -15 2 1 168.02 97.72 37.85 o -14 2 1 1020.72 896.98 57.57 o -13 2 1 24.64 -27.03 27.03 o -12 2 1 540.93 556.41 30.91 o -11 2 1 204.65 201.60 23.84 o -10 2 1 918.00 1115.33 37.49 o -9 2 1 3669.29 3665.85 53.83 o -8 2 1 1928.11 1734.31 36.72 o -7 2 1 3389.75 3449.45 43.96 o -6 2 1 0.01 -0.30 14.68 o -5 2 1 10.65 -3.71 14.20 o -4 2 1 423.63 390.74 20.13 o -3 2 1 4580.54 4283.50 47.70 o -2 2 1 30731.15 31013.49 223.61 o -1 2 1 48078.39 50798.00 406.79 o 0 2 1 2877.02 3257.19 43.73 o 1 2 1 128.72 154.89 22.36 o 2 2 1 49.49 18.61 13.90 o 3 2 1 23745.50 23221.93 190.21 o 4 2 1 2373.66 2080.43 38.51 o 5 2 1 24985.56 23756.69 165.14 o 6 2 1 2007.69 2067.16 36.86 o 7 2 1 3540.56 3434.58 47.35 o 8 2 1 10882.60 10425.00 92.92 o 9 2 1 1370.22 1350.49 35.43 o 10 2 1 3336.05 3288.88 51.48 o 11 2 1 6812.07 6546.81 76.31 o 12 2 1 3877.75 3739.31 73.99 o 13 2 1 7310.50 7399.38 101.42 o 14 2 1 855.74 958.96 49.36 o 15 2 1 1203.51 1244.98 92.40 o 16 2 1 159.38 170.80 50.94 o 17 2 1 393.82 261.96 56.91 o 18 2 1 2351.12 2324.82 105.02 o 19 2 1 8.18 -0.20 58.08 o 20 2 1 434.49 516.24 97.75 o 21 2 1 9.39 13.63 88.07 o 22 2 1 412.50 454.44 113.28 o -22 3 1 236.77 103.64 84.95 o -21 3 1 784.60 888.42 136.22 o -20 3 1 1708.02 1731.10 128.10 o -19 3 1 0.14 -7.88 59.21 o -18 3 1 5178.06 4836.70 155.94 o -17 3 1 26.22 -23.23 51.46 o -16 3 1 1164.11 1321.74 88.14 o -15 3 1 257.07 343.00 45.36 o -14 3 1 382.60 506.06 39.75 o -13 3 1 3121.34 3131.39 66.24 o -12 3 1 2113.72 2190.49 52.30 o -11 3 1 2423.87 2499.18 56.87 o -10 3 1 527.34 622.61 26.36 o -9 3 1 1898.44 1850.93 37.18 o -8 3 1 789.29 848.29 30.24 o -7 3 1 14.50 43.96 17.44 o -6 3 1 0.68 15.20 16.17 o -5 3 1 399.62 427.32 20.60 o -4 3 1 326.41 472.90 23.81 o -3 3 1 3186.22 3271.54 47.13 o -2 3 1 13374.28 13441.91 125.99 o -1 3 1 4827.19 5004.05 63.42 o 0 3 1 4936.36 5093.75 63.59 o 1 3 1 7799.02 7939.72 96.65 o 2 3 1 1339.90 1528.16 38.46 o 3 3 1 1168.20 1039.73 34.27 o 4 3 1 18321.12 17902.64 150.04 o 5 3 1 1326.46 1124.23 35.54 o 6 3 1 20592.00 20598.07 170.03 o 7 3 1 9754.36 10112.05 88.27 o 8 3 1 157.60 287.09 20.77 o 9 3 1 8799.58 9053.17 88.88 o 10 3 1 269.52 228.86 22.48 o 11 3 1 3247.64 3263.87 55.00 o 12 3 1 59.72 30.01 25.08 o 13 3 1 1870.27 1806.68 58.58 o 14 3 1 393.27 377.11 42.53 o 15 3 1 5310.56 5382.29 123.51 o 16 3 1 1285.00 1516.53 77.69 o 17 3 1 258.75 227.26 62.18 o 18 3 1 166.84 60.67 69.19 o 19 3 1 90.45 178.11 66.54 o 20 3 1 0.04 0.16 73.51 o 21 3 1 726.79 625.73 101.46 o 22 3 1 50.94 94.12 91.62 o -22 4 1 33.85 43.32 82.57 o -21 4 1 218.28 133.02 76.52 o -20 4 1 0.06 0.16 63.57 o -19 4 1 5.15 -27.29 58.95 o -18 4 1 1383.64 1259.29 94.19 o -17 4 1 317.73 323.65 67.46 o -16 4 1 3.05 -23.15 51.47 o -15 4 1 41.09 -26.49 44.17 o -14 4 1 725.26 617.54 53.34 o -13 4 1 1514.53 1626.66 65.25 o -12 4 1 268.39 339.07 35.36 o -11 4 1 654.17 665.91 33.27 o -10 4 1 254.58 224.61 24.82 o -9 4 1 5103.11 5453.82 73.93 o -8 4 1 0.06 -23.27 23.27 o -7 4 1 2894.44 2457.99 55.71 o -6 4 1 7859.19 7379.98 91.92 o -5 4 1 22416.80 21525.01 193.55 o -4 4 1 12457.44 12696.73 117.66 o -3 4 1 192.72 224.99 17.70 o -2 4 1 21238.30 21285.43 198.25 o -1 4 1 39.67 13.18 15.39 o 0 4 1 2474.00 2804.48 46.60 o 1 4 1 9.99 1.99 14.72 o 2 4 1 111.47 177.79 21.07 o 3 4 1 7915.54 8086.36 93.14 o 4 4 1 3955.29 3924.85 51.81 o 5 4 1 248.53 317.09 21.74 o 6 4 1 215.16 364.27 24.37 o 7 4 1 9532.23 9088.00 102.62 o 8 4 1 42.55 15.70 24.32 o 9 4 1 202.98 229.76 28.32 o 10 4 1 610.20 534.07 35.24 o 11 4 1 2218.34 2020.97 72.02 o 12 4 1 1.76 8.31 31.15 o 13 4 1 12.33 -2.83 35.37 o 14 4 1 441.39 358.48 50.20 o 15 4 1 597.70 669.41 62.27 o 16 4 1 42.80 51.58 53.56 o 17 4 1 195.39 180.80 61.93 o 18 4 1 99.37 64.34 59.85 o 19 4 1 278.35 270.66 70.60 o 20 4 1 77.17 66.61 66.84 o 21 4 1 4.62 -63.79 69.58 o 22 4 1 108.72 161.93 98.49 o -21 5 1 32.66 -67.66 67.66 o -20 5 1 185.83 242.54 75.59 o -19 5 1 28.69 95.31 65.66 o -18 5 1 141.66 96.20 62.53 o -17 5 1 0.34 39.52 56.16 o -16 5 1 148.39 85.07 54.33 o -15 5 1 889.87 1042.09 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