#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2210100.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210100_Fobs loop_ _publ_author_name 'Michiue, Kenji' 'Steele, Ian M.' 'Jordan, Richard F.' _publ_section_title ; [Bis(3-mesitylpyrazol-1-yl)(5-mesitylpyrazol-1-yl)borohydrido]dichloro(5-mesitylpyrazole)titanium(III) toluene solvate ; _journal_coeditor_code BM2002 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2357 _journal_page_last m2358 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.820 _cell_angle_gamma 90.000 _cell_length_a 13.1370 _cell_length_b 17.2770 _cell_length_c 24.8240 _exptl_crystal_F_000 2036.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file bm2002Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Kenji09 in P2(1)/n P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 405.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2937.13 2203.55 681.96 o 3 0 0 33137.18 36728.11 1170.62 o 4 0 0 6292.56 7970.57 181.34 o 5 0 0 17658.13 18250.44 607.00 o 6 0 0 2781.03 2336.98 56.88 o 7 0 0 7172.55 7339.19 472.60 o 8 0 0 6465.75 6208.02 255.34 o 9 0 0 2448.24 2549.98 99.02 o 10 0 0 9078.31 8782.37 426.57 o 11 0 0 156.53 91.49 75.33 o 12 0 0 5.90 -83.17 83.17 o 13 0 0 146.58 56.84 91.46 o 14 0 0 0.84 -79.04 110.27 o 1 1 0 1309.57 1138.92 422.24 o 2 1 0 3696.62 2464.95 556.84 o 3 1 0 9864.06 10930.15 167.86 o 4 1 0 14073.87 13891.47 346.25 o 5 1 0 1.66 2.26 36.71 o 6 1 0 6.62 14.55 35.32 o 7 1 0 1465.83 1428.20 40.49 o 8 1 0 844.97 751.83 42.12 o 9 1 0 221.99 279.74 45.21 o 10 1 0 337.11 351.94 49.52 o 11 1 0 599.32 673.94 55.18 o 12 1 0 326.98 322.09 59.63 o 13 1 0 451.07 459.06 66.87 o 14 1 0 67.77 60.32 72.00 o 0 2 0 1608.42 1507.09 998.14 o 1 2 0 18103.44 13408.21 3829.98 o 2 2 0 965.92 668.31 195.83 o 3 2 0 4782.41 5417.73 223.64 o 4 2 0 55.62 105.71 35.85 o 5 2 0 913.10 1020.66 40.68 o 6 2 0 1456.75 1225.87 50.38 o 7 2 0 2816.20 2881.63 110.84 o 8 2 0 3848.91 3705.13 139.22 o 9 2 0 202.90 212.36 46.18 o 10 2 0 2597.73 2473.92 79.11 o 11 2 0 177.20 183.72 54.28 o 12 2 0 214.18 237.35 59.96 o 13 2 0 1721.74 1603.22 69.88 o 14 2 0 1028.07 923.75 74.79 o 1 3 0 5961.00 4943.41 1247.97 o 2 3 0 56.60 431.95 172.55 o 3 3 0 1.01 24.86 58.53 o 4 3 0 511.39 451.02 35.21 o 5 3 0 4627.54 4266.24 166.44 o 6 3 0 1826.17 1769.64 92.22 o 7 3 0 2.37 6.21 43.50 o 8 3 0 1679.17 1747.52 74.50 o 9 3 0 721.81 632.52 50.54 o 10 3 0 3055.42 2874.34 120.60 o 11 3 0 1719.49 1923.62 97.00 o 12 3 0 588.93 615.97 66.08 o 13 3 0 28.19 14.55 70.47 o 14 3 0 34.39 17.22 83.92 o 0 4 0 994.35 464.02 91.07 o 1 4 0 1700.91 1911.79 191.47 o 2 4 0 729.37 847.92 33.50 o 3 4 0 1629.47 1538.26 69.19 o 4 4 0 622.34 484.17 38.47 o 5 4 0 3807.31 4159.51 182.62 o 6 4 0 132.37 130.06 38.02 o 7 4 0 821.95 783.85 52.37 o 8 4 0 203.45 200.03 44.44 o 9 4 0 719.25 620.18 50.72 o 10 4 0 31.12 -18.54 53.83 o 11 4 0 473.82 530.03 61.23 o 12 4 0 392.31 440.89 67.38 o 13 4 0 692.97 664.20 73.82 o 14 4 0 981.33 867.52 95.03 o 1 5 0 2361.90 2281.81 256.78 o 2 5 0 741.95 952.17 66.57 o 3 5 0 12613.11 13007.06 289.74 o 4 5 0 5481.88 5646.89 230.49 o 5 5 0 167.65 232.19 59.69 o 6 5 0 1051.51 1073.00 42.64 o 7 5 0 543.54 469.46 42.50 o 8 5 0 31.47 62.24 45.80 o 9 5 0 0.92 -17.37 54.06 o 10 5 0 257.39 295.33 55.39 o 11 5 0 3346.59 3387.80 173.53 o 12 5 0 23.71 29.13 66.99 o 13 5 0 210.39 209.64 73.21 o 14 5 0 9.68 -22.37 102.14 o 0 6 0 11117.05 9859.31 994.35 o 1 6 0 363.55 707.22 237.89 o 2 6 0 171.25 409.77 185.51 o 3 6 0 201.66 341.75 56.01 o 4 6 0 280.53 256.53 40.23 o 5 6 0 0.45 41.40 41.95 o 6 6 0 4345.36 4010.12 126.63 o 7 6 0 8.25 -30.54 42.61 o 8 6 0 286.00 228.51 47.64 o 9 6 0 122.48 56.80 51.81 o 10 6 0 503.17 435.60 57.42 o 11 6 0 59.72 -53.67 60.98 o 12 6 0 832.98 846.47 71.36 o 13 6 0 304.11 284.75 74.80 o 1 7 0 1113.10 1225.31 268.99 o 2 7 0 560.54 737.53 91.45 o 3 7 0 7874.26 7806.26 124.72 o 4 7 0 1700.22 1797.19 99.78 o 5 7 0 140.78 168.81 42.44 o 6 7 0 31.53 59.81 45.16 o 7 7 0 1591.46 1617.66 51.00 o 8 7 0 696.56 777.38 51.21 o 9 7 0 559.87 578.08 54.88 o 10 7 0 279.80 298.50 59.12 o 11 7 0 31.13 48.49 63.60 o 12 7 0 3.35 -3.24 69.47 o 13 7 0 289.54 211.63 82.82 o 0 8 0 8467.27 7730.83 719.76 o 1 8 0 8482.13 8982.10 587.91 o 2 8 0 425.97 431.74 63.63 o 3 8 0 2511.76 2638.25 118.14 o 4 8 0 358.78 403.63 46.27 o 5 8 0 703.12 910.13 57.57 o 6 8 0 64.92 39.33 50.91 o 7 8 0 3946.16 3971.01 131.99 o 8 8 0 2400.21 2425.95 68.90 o 9 8 0 264.62 272.96 55.79 o 10 8 0 1267.17 1324.20 64.52 o 11 8 0 178.83 123.51 66.91 o 12 8 0 176.55 145.58 78.40 o 13 8 0 83.71 85.91 91.84 o 1 9 0 620.75 621.99 181.46 o 2 9 0 398.02 519.90 41.88 o 3 9 0 8.65 29.19 45.48 o 4 9 0 62.61 82.15 45.10 o 5 9 0 834.15 878.90 49.35 o 6 9 0 796.19 698.85 51.68 o 7 9 0 590.19 493.17 54.70 o 8 9 0 25.30 13.97 52.96 o 9 9 0 704.56 758.74 60.16 o 10 9 0 345.08 317.91 63.87 o 11 9 0 0.71 -25.02 68.28 o 12 9 0 123.93 52.20 74.82 o 13 9 0 0.40 125.53 104.79 o 0 10 0 18297.66 15641.10 1369.76 o 1 10 0 352.49 471.98 116.12 o 2 10 0 2604.72 2614.53 104.23 o 3 10 0 374.48 399.22 44.16 o 4 10 0 1062.36 1109.11 50.35 o 5 10 0 1.60 46.34 49.26 o 6 10 0 71.73 85.05 53.34 o 7 10 0 3717.63 3712.86 101.38 o 8 10 0 7680.60 7763.19 192.99 o 9 10 0 378.55 468.26 62.00 o 10 10 0 2369.14 2463.35 73.03 o 11 10 0 0.34 19.95 74.98 o 12 10 0 10.73 81.85 99.01 o 1 11 0 6316.74 6209.84 391.01 o 2 11 0 110.53 64.83 49.51 o 3 11 0 45.27 103.58 45.82 o 4 11 0 398.69 455.34 52.89 o 5 11 0 107.42 113.05 53.42 o 6 11 0 93.23 63.87 61.79 o 7 11 0 85.82 93.60 58.99 o 8 11 0 827.93 816.93 65.41 o 9 11 0 1381.53 1409.57 66.89 o 10 11 0 741.93 796.83 70.86 o 11 11 0 371.81 364.42 74.06 o 12 11 0 11.76 -2.11 92.48 o 0 12 0 1523.32 1031.11 114.85 o 1 12 0 681.96 589.88 49.64 o 2 12 0 516.80 580.72 55.71 o 3 12 0 419.51 492.07 51.79 o 4 12 0 8.05 6.84 50.69 o 5 12 0 4607.96 4390.03 182.12 o 6 12 0 3895.23 3798.82 111.52 o 7 12 0 273.81 344.07 63.62 o 8 12 0 1394.97 1374.33 70.87 o 9 12 0 655.92 693.34 68.56 o 10 12 0 805.71 808.81 73.42 o 11 12 0 0.33 -81.03 87.06 o 1 13 0 55.29 86.52 51.70 o 2 13 0 94.10 59.02 57.09 o 3 13 0 4730.53 4438.81 206.75 o 4 13 0 456.22 507.56 55.42 o 5 13 0 302.02 365.07 59.94 o 6 13 0 480.34 435.79 62.21 o 7 13 0 1190.66 1139.11 69.91 o 8 13 0 235.62 263.97 70.66 o 9 13 0 2057.88 2024.43 87.24 o 10 13 0 0.25 37.97 78.59 o 11 13 0 686.94 661.31 95.29 o 0 14 0 290.64 243.51 106.74 o 1 14 0 863.45 839.91 58.74 o 2 14 0 1.97 -0.24 67.97 o 3 14 0 5537.96 5434.39 235.87 o 4 14 0 768.36 793.88 61.03 o 5 14 0 431.72 438.09 61.64 o 6 14 0 0.38 74.02 70.25 o 7 14 0 543.88 550.82 77.74 o 8 14 0 329.17 280.27 74.92 o 9 14 0 0.64 90.23 83.49 o 10 14 0 217.56 231.24 91.93 o 1 15 0 408.27 354.59 59.40 o 2 15 0 560.66 684.13 68.55 o 3 15 0 778.06 777.61 69.99 o 4 15 0 626.22 602.05 70.82 o 5 15 0 0.65 57.20 70.96 o 6 15 0 363.31 284.20 68.49 o 7 15 0 296.38 288.34 72.16 o 8 15 0 116.66 156.68 83.31 o 9 15 0 411.31 509.85 133.40 o 0 16 0 4589.52 4283.03 350.81 o 1 16 0 289.55 395.67 63.81 o 2 16 0 1247.17 1222.56 99.78 o 3 16 0 416.33 492.83 73.49 o 4 16 0 1668.92 1647.47 79.14 o 5 16 0 1648.86 1701.12 76.50 o 6 16 0 158.96 118.06 70.89 o 7 16 0 181.91 171.53 74.72 o 8 16 0 75.54 146.37 84.77 o 9 16 0 1.92 67.39 102.98 o 1 17 0 811.59 622.60 68.52 o 2 17 0 104.96 132.69 76.56 o 3 17 0 3.92 -16.50 77.07 o 4 17 0 6.50 -31.05 78.68 o 5 17 0 26.96 -23.80 81.29 o 6 17 0 51.97 78.31 83.31 o 7 17 0 8.18 96.72 82.49 o 8 17 0 29.39 152.41 90.39 o 0 18 0 2920.48 3054.68 121.66 o 1 18 0 833.87 852.23 75.10 o 2 18 0 55.28 100.99 72.34 o 3 18 0 66.82 118.19 75.17 o 4 18 0 64.73 57.32 82.01 o 5 18 0 27.17 32.90 84.63 o 6 18 0 2.99 80.02 100.70 o 1 19 0 348.46 486.64 78.19 o 2 19 0 699.02 781.37 79.49 o 3 19 0 397.13 313.01 81.79 o 4 19 0 0.97 -40.19 98.20 o 5 19 0 207.17 169.85 102.42 o 0 20 0 932.65 1148.06 200.03 o 1 20 0 3.16 116.31 115.87 o 2 20 0 16.09 1.78 90.03 o 3 20 0 64.50 24.58 150.17 o -14 1 1 334.47 305.13 69.50 o -13 1 1 29.94 30.40 63.05 o -12 1 1 158.36 155.21 57.61 o -11 1 1 1172.34 1253.25 59.35 o -10 1 1 917.02 904.00 49.41 o -9 1 1 11545.56 11497.52 410.24 o -8 1 1 15.78 -0.16 38.89 o -7 1 1 353.41 187.31 36.15 o -6 1 1 3222.05 2907.21 61.21 o -5 1 1 985.99 1514.31 41.42 o -4 1 1 518.30 562.61 40.33 o -3 1 1 14579.60 14292.45 331.67 o -2 1 1 7139.59 8054.55 1437.84 o 1 1 1 84052.21 26093.04 18984.34 o 2 1 1 1161.75 1210.66 284.68 o 3 1 1 19947.66 20548.30 553.05 o 4 1 1 21876.90 21978.28 672.17 o 5 1 1 42.88 80.51 37.56 o 6 1 1 3753.64 4249.75 157.31 o 7 1 1 7351.76 7716.41 200.64 o 8 1 1 6059.74 6071.55 160.25 o 9 1 1 9306.80 9014.05 257.89 o 10 1 1 4635.07 4689.15 111.83 o 11 1 1 1350.57 1280.18 76.94 o 12 1 1 219.58 196.02 61.09 o 13 1 1 15.11 19.72 72.31 o 14 1 1 3.94 -4.20 77.23 o -14 2 1 472.41 445.57 75.84 o -13 2 1 2003.08 2119.43 70.18 o -12 2 1 1941.03 1965.44 72.96 o -11 2 1 581.22 525.32 53.89 o -10 2 1 2019.07 1834.67 53.40 o -9 2 1 150.61 93.33 43.78 o -8 2 1 53.79 37.93 42.52 o -7 2 1 331.09 325.35 36.89 o -6 2 1 1620.85 2156.73 84.95 o -5 2 1 0.55 6.71 38.28 o -4 2 1 4.29 -10.85 34.17 o -3 2 1 4723.95 4579.12 239.58 o -2 2 1 924.63 768.20 201.03 o -1 2 1 1240.14 1169.52 342.05 o 0 2 1 25390.80 10230.23 5601.45 o 1 2 1 12942.65 12430.49 3122.70 o 2 2 1 15341.06 14158.64 2793.37 o 3 2 1 7909.66 6993.17 211.68 o 4 2 1 892.48 831.00 39.59 o 5 2 1 4130.75 4885.02 132.83 o 6 2 1 1921.20 2083.31 61.43 o 7 2 1 16.86 50.42 39.01 o 8 2 1 780.48 758.49 43.45 o 9 2 1 730.75 740.40 49.95 o 10 2 1 82.13 77.17 54.26 o 11 2 1 2015.43 2049.45 101.80 o 12 2 1 361.77 422.32 62.85 o 13 2 1 47.07 69.70 66.79 o 14 2 1 7.20 60.22 83.53 o -14 3 1 196.84 241.76 77.00 o -13 3 1 64.11 28.94 68.30 o -12 3 1 985.27 1083.45 65.45 o -11 3 1 33.10 -4.95 56.44 o -10 3 1 1279.88 1325.27 55.58 o -9 3 1 286.47 286.40 47.23 o -8 3 1 21.35 86.81 42.94 o -7 3 1 1473.65 1644.02 76.55 o -6 3 1 86.49 140.72 36.73 o -5 3 1 268.94 238.00 35.61 o -4 3 1 1551.39 1592.78 85.02 o -3 3 1 1563.81 1464.96 49.70 o -2 3 1 1358.22 1348.59 139.29 o -1 3 1 1674.52 2109.90 599.92 o 0 3 1 994.79 1105.58 345.88 o 1 3 1 4640.94 4240.01 1064.03 o 2 3 1 31687.78 30659.88 877.35 o 3 3 1 2018.44 2178.36 86.58 o 4 3 1 1132.89 1129.60 66.18 o 5 3 1 115.30 30.97 36.76 o 6 3 1 48.37 24.51 36.22 o 7 3 1 934.08 1073.50 52.75 o 8 3 1 1180.07 1194.43 45.29 o 9 3 1 2029.12 1945.27 72.01 o 10 3 1 109.35 55.00 50.58 o 11 3 1 0.14 -37.79 55.74 o 12 3 1 832.26 893.21 69.56 o 13 3 1 21.61 23.29 72.97 o 14 3 1 272.16 207.49 93.52 o -14 4 1 2.92 29.99 77.51 o -13 4 1 1393.65 1512.39 88.26 o -12 4 1 1243.47 1216.50 66.88 o -11 4 1 1026.79 1041.26 60.53 o -10 4 1 1363.45 1317.52 73.58 o -9 4 1 284.81 283.85 48.58 o -8 4 1 1866.30 1731.42 80.09 o -7 4 1 138.88 118.08 39.60 o -6 4 1 11540.41 11172.32 297.92 o -5 4 1 3038.56 2797.10 157.63 o -4 4 1 4.54 368.42 187.11 o -3 4 1 13169.22 12264.46 459.79 o -2 4 1 1.03 235.64 90.91 o -1 4 1 3879.71 3012.01 270.78 o 0 4 1 6.68 1.69 47.17 o 1 4 1 542.63 651.86 101.04 o 2 4 1 13634.15 14000.74 397.54 o 3 4 1 291.36 738.48 111.04 o 4 4 1 8238.86 7170.02 301.08 o 5 4 1 3111.72 3112.70 102.90 o 6 4 1 987.17 805.85 40.54 o 7 4 1 424.73 485.09 43.31 o 8 4 1 449.98 480.18 47.09 o 9 4 1 290.51 246.04 51.29 o 10 4 1 37.71 63.04 55.68 o 11 4 1 1569.81 1490.23 65.35 o 12 4 1 1294.55 1299.37 71.92 o 13 4 1 5.51 -72.84 72.84 o 14 4 1 1160.74 1163.68 108.28 o -14 5 1 21.63 -1.40 89.97 o -13 5 1 76.24 70.31 70.21 o -12 5 1 21.47 -60.35 64.31 o -11 5 1 95.69 41.11 58.85 o -10 5 1 318.92 326.93 54.61 o -9 5 1 417.86 462.00 50.28 o -8 5 1 390.84 358.01 44.88 o -7 5 1 1175.50 1219.19 48.24 o -6 5 1 1668.81 1750.20 102.10 o -5 5 1 1136.55 1556.25 115.74 o -4 5 1 1761.18 1865.15 82.49 o -3 5 1 1971.30 1794.54 98.18 o -2 5 1 58.59 599.12 199.91 o -1 5 1 560.20 546.96 140.28 o 0 5 1 17.09 110.09 75.58 o 1 5 1 25.15 188.25 67.53 o 2 5 1 151.04 160.49 36.72 o 3 5 1 2279.57 1993.69 57.24 o 4 5 1 301.50 337.51 85.66 o 5 5 1 1307.83 1695.60 89.99 o 6 5 1 6808.03 6983.52 254.84 o 7 5 1 259.09 277.25 43.73 o 8 5 1 2.49 -9.47 50.32 o 9 5 1 636.21 657.67 53.22 o 10 5 1 395.46 383.75 57.04 o 11 5 1 2.32 14.31 61.58 o 12 5 1 1.66 14.42 72.57 o 13 5 1 41.70 -22.31 74.60 o -14 6 1 4.62 -1.72 102.29 o -13 6 1 272.30 272.90 73.02 o -12 6 1 1862.90 1827.10 84.48 o -11 6 1 77.32 58.44 63.73 o -10 6 1 712.19 697.14 56.39 o -9 6 1 4.25 -21.93 49.90 o -8 6 1 63.80 61.05 45.66 o -7 6 1 1037.18 994.94 55.54 o -6 6 1 4286.51 3924.93 135.10 o -5 6 1 3.71 50.94 40.28 o -4 6 1 585.90 504.88 48.16 o -3 6 1 4145.40 4286.93 89.08 o -2 6 1 7310.20 6830.00 400.49 o -1 6 1 1163.60 1070.39 131.79 o 0 6 1 4879.14 3493.64 217.69 o 1 6 1 12280.52 11302.14 649.51 o 2 6 1 15758.22 15876.11 316.75 o 3 6 1 388.23 376.93 61.38 o 4 6 1 2827.02 3093.40 84.82 o 5 6 1 458.74 378.57 43.03 o 6 6 1 1257.09 1062.31 59.45 o 7 6 1 0.23 27.44 44.22 o 8 6 1 0.73 -48.73 53.33 o 9 6 1 46.43 101.04 53.73 o 10 6 1 663.88 675.09 60.22 o 11 6 1 1171.44 1171.99 67.30 o 12 6 1 1107.96 1197.67 74.22 o 13 6 1 145.88 92.31 81.76 o -13 7 1 0.13 11.00 81.43 o -12 7 1 3.30 35.78 68.51 o -11 7 1 1.37 -36.79 68.79 o -10 7 1 147.42 165.34 56.12 o -9 7 1 1506.23 1431.83 80.10 o -8 7 1 1170.30 1159.77 51.41 o -7 7 1 2541.04 2435.75 88.77 o -6 7 1 960.84 1036.69 46.99 o -5 7 1 172.50 167.09 42.32 o -4 7 1 6538.43 7034.64 111.88 o -3 7 1 466.09 673.87 94.89 o -2 7 1 43.85 140.57 45.22 o -1 7 1 54.17 46.35 92.96 o 0 7 1 890.28 825.52 93.89 o 1 7 1 4892.11 4611.17 231.25 o 2 7 1 0.19 363.22 228.78 o 3 7 1 5545.82 5567.94 99.41 o 4 7 1 698.25 704.82 44.16 o 5 7 1 949.18 834.56 45.43 o 6 7 1 184.86 194.60 42.85 o 7 7 1 1077.74 1099.78 51.46 o 8 7 1 2352.80 2340.42 98.82 o 9 7 1 100.59 50.72 54.59 o 10 7 1 0.31 -48.57 59.59 o 11 7 1 1953.01 1917.97 71.67 o 12 7 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