#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/01/2210104.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210104_Fobs loop_ _publ_author_name 'Bhattacharyya, Kinkini' 'Kar, Tanusree' 'Bocelli, Gabriele' 'Banerjee, Sukdeb' 'Mondal, Nirup Bikash' _publ_section_title ; Farnesiaside, a new diterpene glycoside ; _journal_coeditor_code BT2140 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4007 _journal_page_last o4009 _journal_volume 62 _journal_year 2006 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 114.820 _cell_angle_gamma 90.000 _cell_length_a 11.6910 _cell_length_b 9.3360 _cell_length_c 12.3700 _exptl_crystal_F_000 548.00 _reflns_d_resolution_high 0.8199 _[local]_cod_data_source_file bt2140Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'Novel diterpene glycoside,Farnesiaside' _shelx_refln_list_code 4 _shelx_f_calc_maximum 140.16 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 9 -4 0 26.34 23.97 1.31 o 10 -4 0 117.98 105.81 2.32 o 11 -4 0 31.75 32.45 1.28 o 12 -4 0 21.56 23.17 0.91 o 7 -3 0 118.92 119.82 2.28 o 8 -3 0 158.23 145.56 2.66 o 9 -3 0 192.17 181.95 3.09 o 10 -3 0 15.01 14.11 1.10 o 11 -3 0 1.89 1.53 0.67 o 12 -3 0 7.08 8.22 0.76 o 5 -2 0 308.67 343.84 2.97 o 6 -2 0 164.63 182.88 2.41 o 7 -2 0 59.12 56.92 1.61 o 8 -2 0 259.78 265.68 3.45 o 9 -2 0 205.81 200.62 3.16 o 10 -2 0 39.31 42.04 1.60 o 11 -2 0 60.72 57.60 1.71 o 12 -2 0 17.64 17.52 0.94 o 3 -1 0 2300.64 2360.47 5.64 o 4 -1 0 402.26 393.48 2.63 o 5 -1 0 187.48 207.16 2.21 o 6 -1 0 28.15 26.77 1.01 o 7 -1 0 700.86 692.26 4.95 o 8 -1 0 391.16 400.19 4.13 o 9 -1 0 133.29 123.78 2.49 o 10 -1 0 27.81 19.98 1.22 o 11 -1 0 20.23 17.21 1.14 o 12 -1 0 77.11 79.74 1.75 o 1 0 0 239.07 243.81 0.98 o 2 0 0 1012.34 917.54 2.72 o 3 0 0 8.91 8.82 0.47 o 4 0 0 160.92 205.54 1.88 o 5 0 0 59.08 64.08 1.27 o 6 0 0 137.04 143.41 2.06 o 7 0 0 1622.07 1553.06 7.36 o 8 0 0 817.02 810.36 5.82 o 9 0 0 227.62 199.45 3.11 o 10 0 0 60.01 59.98 1.87 o 11 0 0 0.56 0.42 0.66 o 12 0 0 7.65 6.71 0.80 o 2 1 0 723.03 654.48 7.45 o 3 1 0 2295.39 2166.10 5.39 o 4 1 0 391.37 354.01 2.50 o 5 1 0 189.43 201.26 2.17 o 6 1 0 28.93 25.62 1.00 o 7 1 0 699.99 676.60 4.90 o 8 1 0 391.44 394.82 4.12 o 9 1 0 133.54 122.46 2.50 o 10 1 0 28.03 21.23 1.22 o 11 1 0 20.44 17.35 1.11 o 12 1 0 78.50 79.25 1.83 o 0 2 0 1244.83 1331.96 3.50 o 1 2 0 213.49 226.67 12.21 o 2 2 0 127.36 135.73 5.78 o 3 2 0 1115.10 1101.32 14.52 o 4 2 0 73.33 68.65 0.86 o 5 2 0 307.21 323.85 2.85 o 6 2 0 162.63 168.01 2.34 o 7 2 0 60.87 56.60 1.57 o 8 2 0 259.25 251.58 3.37 o 9 2 0 206.69 192.24 3.08 o 10 2 0 39.22 39.04 1.57 o 11 2 0 60.00 55.59 1.70 o 12 2 0 17.21 16.92 1.01 o 1 3 0 859.57 892.49 42.94 o 3 3 0 438.63 478.53 20.70 o 4 3 0 463.22 464.83 9.54 o 5 3 0 768.23 779.07 9.84 o 6 3 0 157.54 151.14 1.65 o 7 3 0 121.22 114.89 2.24 o 8 3 0 158.09 135.20 2.60 o 9 3 0 192.77 179.66 3.05 o 10 3 0 15.39 15.55 1.07 o 11 3 0 1.78 1.79 0.68 o 12 3 0 7.09 5.48 0.71 o 1 4 0 1035.24 1160.67 45.69 o 2 4 0 960.06 1077.33 80.28 o 3 4 0 1177.42 1198.39 27.14 o 4 4 0 46.42 46.45 8.10 o 5 4 0 66.62 64.19 1.10 o 6 4 0 26.59 24.25 0.81 o 7 4 0 745.98 698.95 4.55 o 8 4 0 111.47 102.96 2.10 o 9 4 0 25.72 22.80 1.34 o 10 4 0 117.77 108.65 2.34 o 11 4 0 31.63 32.68 1.25 o 12 4 0 21.43 24.58 0.90 o 1 5 0 535.83 659.99 20.54 o 2 5 0 306.69 330.44 20.41 o 3 5 0 764.06 809.10 62.16 o 4 5 0 113.53 111.46 6.03 o 5 5 0 176.42 177.80 9.22 o 6 5 0 19.56 21.39 0.84 o 7 5 0 156.50 152.51 5.73 o 8 5 0 183.51 181.35 2.15 o 9 5 0 15.02 13.46 0.76 o 10 5 0 5.54 6.47 0.56 o 11 5 0 44.34 50.00 0.97 o 0 6 0 974.89 1161.16 6.24 o 1 6 0 21.72 20.34 0.75 o 2 6 0 35.10 48.00 2.86 o 3 6 0 200.94 212.53 16.01 o 4 6 0 132.62 132.35 9.11 o 5 6 0 0.81 0.84 0.53 o 6 6 0 308.90 288.34 11.89 o 7 6 0 9.11 6.06 0.67 o 8 6 0 4.54 4.25 0.62 o 9 6 0 2.22 2.14 0.67 o 10 6 0 28.33 30.86 1.10 o 1 7 0 91.93 101.56 3.44 o 2 7 0 176.94 191.17 6.50 o 3 7 0 24.31 23.22 2.29 o 4 7 0 17.45 16.59 1.41 o 5 7 0 272.38 244.06 10.72 o 6 7 0 61.70 60.04 2.08 o 7 7 0 81.12 77.53 1.87 o 8 7 0 76.14 77.92 2.56 o 9 7 0 1.58 1.64 0.45 o 10 7 0 12.15 11.67 0.58 o 0 8 0 1165.57 1217.98 7.58 o 1 8 0 168.91 154.14 3.45 o 2 8 0 513.41 503.81 21.69 o 3 8 0 4.97 2.58 0.69 o 4 8 0 18.41 19.60 2.30 o 5 8 0 49.38 45.37 2.00 o 6 8 0 20.23 19.96 0.86 o 7 8 0 8.10 8.72 0.62 o 8 8 0 18.99 16.32 1.83 o 9 8 0 27.75 27.17 1.56 o 1 9 0 216.64 213.58 4.51 o 2 9 0 19.90 19.85 0.90 o 3 9 0 60.71 73.39 5.18 o 4 9 0 4.98 6.29 2.09 o 5 9 0 45.65 46.58 2.88 o 6 9 0 0.42 0.74 0.65 o 7 9 0 50.85 52.86 2.82 o 0 10 0 212.98 206.28 2.99 o 1 10 0 31.40 31.11 0.98 o 2 10 0 10.48 11.39 0.94 o 3 10 0 38.40 42.97 3.85 o 4 10 0 5.99 4.32 0.55 o 5 10 0 24.07 23.23 1.69 o 6 10 0 3.97 4.37 0.94 o 1 11 0 13.51 13.01 0.58 o 2 11 0 15.97 18.12 1.02 o 3 11 0 17.95 19.18 0.94 o 11 -5 1 31.37 29.86 1.00 o 9 -4 1 50.04 46.18 1.64 o 10 -4 1 20.84 18.24 1.13 o 11 -4 1 39.13 41.09 1.30 o 7 -3 1 502.34 506.36 4.66 o 8 -3 1 193.60 190.22 3.05 o 9 -3 1 85.17 85.15 2.10 o 10 -3 1 92.87 94.49 2.17 o 11 -3 1 20.62 21.82 1.10 o 12 -3 1 0.94 1.61 0.41 o 4 -2 1 432.17 531.27 3.43 o 5 -2 1 1080.83 1091.20 5.49 o 6 -2 1 517.17 551.19 4.33 o 7 -2 1 155.00 161.42 2.57 o 8 -2 1 16.25 16.39 1.08 o 9 -2 1 158.96 140.22 2.72 o 10 -2 1 29.67 28.25 1.33 o 11 -2 1 11.03 11.57 0.94 o 12 -2 1 21.49 25.67 0.95 o 2 -1 1 404.04 407.76 2.14 o 3 -1 1 940.12 934.26 3.77 o 4 -1 1 1317.11 1351.12 5.20 o 5 -1 1 3435.13 3616.03 9.84 o 6 -1 1 327.35 316.72 3.22 o 7 -1 1 354.83 370.65 3.82 o 8 -1 1 40.42 38.86 1.45 o 9 -1 1 6.86 6.60 0.91 o 10 -1 1 79.70 75.92 2.01 o 11 -1 1 15.63 15.21 0.94 o 12 -1 1 0.10 0.50 0.45 o -13 0 1 24.93 28.38 1.02 o -12 0 1 2.00 0.84 0.64 o -11 0 1 1.12 0.81 0.72 o -10 0 1 112.08 111.95 2.48 o -9 0 1 524.85 513.99 4.86 o -8 0 1 0.93 1.36 0.65 o -7 0 1 24.43 24.81 1.03 o -6 0 1 1653.77 1491.87 6.25 o -5 0 1 1700.32 1660.45 5.83 o -4 0 1 1085.27 1054.99 4.02 o -3 0 1 1596.45 1443.00 4.02 o -2 0 1 5752.84 5501.03 6.75 o -1 0 1 1215.49 1057.62 2.12 o 0 0 1 416.96 395.80 1.21 o 1 0 1 122.17 97.89 0.84 o 2 0 1 133.88 128.80 1.18 o 3 0 1 2261.98 2195.89 5.70 o 4 0 1 3106.19 3124.44 7.90 o 5 0 1 0.42 0.11 0.45 o 6 0 1 8.57 10.66 0.79 o 7 0 1 270.14 261.93 3.17 o 8 0 1 6.47 7.04 0.83 o 9 0 1 118.49 112.81 2.42 o 10 0 1 53.08 51.86 1.77 o 11 0 1 92.11 96.01 2.08 o 12 0 1 0.08 -0.12 0.48 o -13 1 1 0.68 0.76 0.42 o -12 1 1 16.37 15.61 0.95 o -11 1 1 68.55 67.90 1.92 o -10 1 1 179.41 172.55 2.97 o -9 1 1 802.02 759.79 5.91 o -8 1 1 55.17 55.46 1.60 o -7 1 1 88.10 76.00 1.68 o -6 1 1 1176.44 1107.93 5.44 o -5 1 1 485.19 475.83 3.18 o -4 1 1 683.93 675.20 3.30 o -3 1 1 6201.58 6148.20 9.03 o -2 1 1 17713.19 18003.55 14.76 o -1 1 1 2794.07 2897.49 4.34 o 0 1 1 3767.25 3988.19 5.07 o 1 1 1 1406.94 1403.41 3.35 o -13 2 1 0.09 0.20 0.40 o -12 2 1 8.24 8.42 0.78 o -11 2 1 31.97 28.51 1.35 o -10 2 1 103.02 107.43 2.36 o -9 2 1 36.13 30.15 1.38 o -8 2 1 203.92 199.96 2.92 o -7 2 1 188.25 181.01 2.57 o -6 2 1 238.80 269.25 2.81 o -5 2 1 493.03 468.41 3.32 o -4 2 1 557.92 530.70 3.14 o -3 2 1 2000.61 1969.34 5.44 o -2 2 1 1193.96 1188.27 3.76 o -1 2 1 1485.96 1602.38 4.02 o 0 2 1 403.95 415.37 2.02 o 1 2 1 220.78 227.76 1.61 o 2 2 1 1735.02 1720.49 4.95 o 3 2 1 1094.30 1110.05 4.42 o -12 3 1 11.94 12.45 0.87 o -11 3 1 39.34 36.05 1.47 o -10 3 1 77.72 72.36 2.00 o -9 3 1 76.36 70.60 1.95 o -8 3 1 74.15 65.87 1.83 o -7 3 1 49.93 45.02 1.41 o -6 3 1 141.84 137.28 2.14 o -5 3 1 232.83 240.74 2.56 o -4 3 1 362.82 370.60 2.87 o -3 3 1 685.20 640.99 3.45 o -2 3 1 1337.73 1420.58 4.79 o -1 3 1 1560.63 1745.90 5.10 o 0 3 1 798.07 857.32 3.53 o 1 3 1 247.72 234.50 1.93 o 2 3 1 1202.67 1192.24 4.64 o 3 3 1 81.39 80.47 1.36 o 4 3 1 771.45 775.10 4.48 o 5 3 1 156.28 146.05 2.15 o 6 3 1 405.10 412.91 3.92 o -12 4 1 54.86 64.84 1.50 o -11 4 1 4.78 3.83 0.72 o -10 4 1 45.11 41.71 1.53 o -9 4 1 83.09 80.78 2.11 o -8 4 1 88.09 84.44 2.07 o -7 4 1 71.77 68.35 1.82 o -6 4 1 1766.83 1745.80 7.99 o -5 4 1 130.92 131.90 2.06 o -4 4 1 873.27 919.24 5.00 o -3 4 1 234.22 285.78 2.64 o -2 4 1 955.53 1050.84 4.76 o -1 4 1 11.78 10.84 0.64 o 0 4 1 1357.23 1456.94 5.41 o 1 4 1 442.94 473.74 3.17 o 2 4 1 758.89 793.64 4.31 o 3 4 1 92.60 85.38 1.55 o 4 4 1 94.81 89.10 1.71 o 5 4 1 362.01 369.33 3.65 o 6 4 1 503.13 472.13 4.40 o 7 4 1 96.41 86.03 2.08 o 8 4 1 51.28 50.71 1.70 o -11 5 1 23.14 24.83 1.14 o -10 5 1 76.23 77.39 2.02 o -9 5 1 135.91 133.09 2.61 o -8 5 1 26.10 27.48 1.33 o -7 5 1 28.37 29.33 1.35 o -6 5 1 35.78 39.60 1.43 o -5 5 1 38.52 36.19 1.30 o -4 5 1 43.48 53.30 1.45 o -3 5 1 832.03 970.21 5.41 o -1 5 1 1099.85 1259.80 5.80 o 0 5 1 331.15 409.24 3.31 o 1 5 1 213.29 230.99 2.55 o 2 5 1 712.93 757.38 4.74 o 3 5 1 77.32 81.33 1.71 o 4 5 1 25.81 19.84 1.04 o 5 5 1 229.89 222.91 3.05 o 6 5 1 11.32 9.76 0.99 o 7 5 1 416.35 404.53 4.42 o 8 5 1 109.95 113.61 2.45 o 9 5 1 11.08 11.00 0.97 o 10 5 1 6.36 5.59 0.72 o -11 6 1 54.51 60.29 1.42 o -10 6 1 42.68 46.33 1.45 o -9 6 1 18.72 14.92 1.11 o -8 6 1 20.39 19.41 1.22 o -7 6 1 27.34 23.94 1.31 o -6 6 1 85.32 81.93 2.04 o -5 6 1 19.23 15.69 1.06 o -4 6 1 35.40 41.53 1.49 o -3 6 1 67.50 87.56 1.91 o -2 6 1 23.57 30.15 1.22 o -1 6 1 300.70 336.21 3.46 o 0 6 1 397.94 426.73 3.82 o 1 6 1 72.64 78.22 1.73 o 2 6 1 10.59 10.14 0.83 o 3 6 1 305.11 290.98 3.40 o 4 6 1 162.77 168.42 2.73 o 5 6 1 742.54 717.65 5.73 o 6 6 1 346.19 321.67 3.95 o 7 6 1 57.99 56.01 1.82 o 8 6 1 14.30 13.16 0.99 o 9 6 1 81.36 82.96 1.89 o 10 6 1 17.56 13.92 0.87 o -10 7 1 15.12 16.14 0.83 o -9 7 1 7.44 7.12 0.77 o -8 7 1 39.58 45.03 1.58 o -7 7 1 88.06 89.97 2.17 o -6 7 1 296.84 294.32 3.81 o -5 7 1 17.26 20.51 1.34 o -4 7 1 276.41 281.65 3.70 o -3 7 1 477.05 509.51 4.80 o -2 7 1 206.34 220.08 3.14 o -1 7 1 366.74 425.28 4.26 o 0 7 1 53.16 55.91 1.67 o 1 7 1 137.92 135.68 2.51 o 2 7 1 57.77 60.56 1.77 o 3 7 1 489.36 472.92 4.65 o 4 7 1 322.32 298.40 3.79 o 5 7 1 404.66 356.15 4.18 o 6 7 1 72.83 63.89 1.96 o 7 7 1 16.15 16.11 1.10 o 8 7 1 3.96 2.39 0.77 o 9 7 1 2.07 1.87 0.52 o -9 8 1 50.21 60.96 1.43 o -8 8 1 6.33 6.39 0.80 o -7 8 1 33.37 34.39 1.43 o -6 8 1 18.20 26.69 1.37 o -5 8 1 239.00 241.65 3.48 o -4 8 1 53.98 61.72 1.88 o -3 8 1 142.25 145.77 2.78 o -2 8 1 153.25 154.66 2.84 o -1 8 1 7.46 6.89 1.06 o 0 8 1 176.17 174.98 2.97 o 1 8 1 31.80 32.22 1.50 o 2 8 1 137.17 130.50 2.66 o 3 8 1 110.28 101.28 2.39 o 4 8 1 1.79 3.03 0.96 o 5 8 1 118.77 111.92 2.43 o 6 8 1 67.56 58.21 1.76 o 7 8 1 98.32 93.67 1.97 o 8 8 1 3.22 3.26 0.64 o -8 9 1 14.28 14.45 0.78 o -7 9 1 32.04 32.10 1.22 o -6 9 1 2.31 1.56 0.75 o -5 9 1 78.71 82.53 2.10 o -4 9 1 66.70 64.95 1.94 o -3 9 1 265.64 252.38 3.55 o -2 9 1 37.73 36.64 1.61 o -1 9 1 114.93 92.93 2.26 o 0 9 1 26.26 21.35 1.36 o 1 9 1 28.86 31.34 1.58 o 2 9 1 32.60 29.56 1.45 o 3 9 1 20.26 19.84 1.27 o 4 9 1 54.02 49.59 1.67 o 5 9 1 112.47 101.27 2.14 o 6 9 1 20.52 18.57 1.01 o 7 9 1 3.65 4.69 0.59 o -6 10 1 0.84 1.06 0.53 o -5 10 1 2.75 2.69 0.66 o -4 10 1 18.72 17.99 1.04 o -3 10 1 17.03 16.52 1.07 o -2 10 1 4.32 5.35 0.87 o -1 10 1 12.26 11.90 1.05 o 0 10 1 34.35 37.12 1.41 o 1 10 1 39.42 35.59 1.45 o 2 10 1 57.67 59.47 1.70 o 3 10 1 9.42 9.07 0.84 o 4 10 1 1.26 1.79 0.64 o 5 10 1 9.31 9.00 0.71 o -3 11 1 30.83 32.67 1.04 o -2 11 1 60.44 64.48 1.45 o -1 11 1 14.11 12.12 0.85 o 0 11 1 12.21 13.24 0.82 o 1 11 1 18.23 19.64 0.93 o 2 11 1 13.54 12.26 0.79 o 8 -4 2 45.61 45.23 1.64 o 9 -4 2 45.16 50.89 1.66 o 10 -4 2 54.87 63.25 1.61 o 11 -4 2 2.01 1.70 0.46 o 6 -3 2 93.35 92.92 1.99 o 7 -3 2 166.97 160.46 2.78 o 8 -3 2 161.49 157.65 2.81 o 9 -3 2 11.36 14.02 1.03 o 10 -3 2 80.37 91.57 2.05 o 11 -3 2 51.15 49.53 1.32 o 4 -2 2 749.10 775.82 4.43 o 5 -2 2 341.66 383.92 3.46 o 6 -2 2 340.17 341.79 3.57 o 7 -2 2 11.20 13.64 0.93 o 8 -2 2 191.70 199.28 3.13 o 9 -2 2 26.82 26.20 1.30 o 10 -2 2 4.73 2.84 0.72 o 11 -2 2 18.51 21.65 0.98 o 2 -1 2 2707.01 2818.83 6.42 o 3 -1 2 1270.83 1288.52 4.86 o 4 -1 2 1507.31 1540.15 6.00 o 5 -1 2 802.85 780.18 4.76 o 6 -1 2 257.26 242.35 2.95 o 7 -1 2 200.65 187.75 2.85 o 8 -1 2 203.43 185.11 2.96 o 9 -1 2 21.21 17.20 1.19 o 10 -1 2 19.26 16.82 1.09 o 11 -1 2 48.36 53.76 1.45 o -13 0 2 7.13 7.74 0.71 o -12 0 2 158.63 151.88 2.63 o -11 0 2 420.52 391.39 4.39 o -10 0 2 43.06 49.45 1.73 o -9 0 2 363.24 324.71 3.81 o -8 0 2 1.63 1.51 0.61 o -7 0 2 12.17 12.90 0.81 o -6 0 2 1055.15 1006.97 5.01 o -5 0 2 1872.15 1745.31 5.86 o -4 0 2 1545.67 1633.00 5.00 o -3 0 2 2014.40 1873.78 4.64 o -2 0 2 19644.02 19024.24 15.26 o -1 0 2 6084.67 6079.30 6.96 o 0 0 2 1189.51 1099.10 2.88 o 1 0 2 3854.92 3815.46 6.34 o 2 0 2 11.45 11.18 0.52 o 3 0 2 701.82 727.87 3.57 o 4 0 2 260.09 219.26 2.24 o 5 0 2 878.71 852.55 4.92 o 6 0 2 194.72 185.17 2.58 o 7 0 2 34.79 34.55 1.33 o 8 0 2 27.21 23.39 1.25 o 9 0 2 30.38 30.86 1.37 o 10 0 2 7.30 5.70 0.83 o 11 0 2 4.99 6.45 0.72 o 12 0 2 3.56 4.46 0.47 o -13 1 2 12.60 15.48 0.82 o -12 1 2 108.64 104.98 2.16 o -11 1 2 16.42 14.02 1.07 o -10 1 2 0.11 0.45 0.65 o -9 1 2 37.49 37.92 1.42 o -8 1 2 143.98 141.14 2.38 o -7 1 2 70.38 65.38 1.53 o -6 1 2 550.61 522.76 3.66 o -5 1 2 749.47 747.54 3.90 o -4 1 2 869.45 850.51 3.67 o -3 1 2 441.03 420.29 2.26 o -2 1 2 1717.40 1601.79 3.94 o -1 1 2 2102.83 2124.41 4.24 o 0 1 2 1951.81 1991.71 4.22 o 1 1 2 939.70 902.64 3.14 o -13 2 2 9.45 9.55 0.72 o -12 2 2 14.83 14.28 0.97 o -11 2 2 26.91 29.32 1.35 o -10 2 2 245.76 237.99 3.41 o -9 2 2 260.17 229.05 3.26 o -8 2 2 29.03 28.01 1.19 o -7 2 2 224.90 209.97 2.69 o -6 2 2 208.69 210.66 2.44 o -5 2 2 104.15 90.82 1.47 o -4 2 2 53.06 54.39 1.04 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