#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/05/2210560.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2210560_Fobs loop_ _publ_author_name 'Kawahata, Masatoshi' 'Ishikawa, Tsutomu' 'Yamaguchi, Kentaro' _publ_section_title ; 1,8-Bis(dimethylethyleneguanidino)naphthalene ; _journal_coeditor_code CV2111 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4549 _journal_page_last o4550 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.642 _cell_angle_gamma 90.000 _cell_length_a 8.4589 _cell_length_b 36.1680 _cell_length_c 17.9425 _exptl_crystal_F_000 2256.00 _reflns_d_resolution_high 0.7491 _[local]_cod_data_source_file cv2111Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 606IKWH IN P2(1)/N' _shelx_refln_list_code 4 _shelx_f_calc_maximum 889.75 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11388.30 10599.57 682.98 o 4 0 0 7849.03 7720.35 500.55 o 6 0 0 48.74 57.99 44.31 o 8 0 0 640.71 690.93 107.44 o 10 0 0 343.14 403.89 106.66 o 1 1 0 373.68 392.43 19.05 o 2 1 0 789.18 723.68 34.50 o 3 1 0 13906.43 14319.14 655.12 o 4 1 0 763.16 737.57 36.31 o 5 1 0 107.21 122.71 14.43 o 6 1 0 22.80 60.07 24.11 o 7 1 0 7.78 44.78 27.93 o 8 1 0 284.35 291.45 89.80 o 9 1 0 0.74 -42.35 50.46 o 10 1 0 82.18 160.05 66.76 o 0 2 0 8.21 3.14 3.14 o 1 2 0 26.81 6.35 4.83 o 2 2 0 5133.32 5047.95 230.92 o 3 2 0 6866.05 6548.83 300.04 o 4 2 0 4560.58 4276.46 197.35 o 5 2 0 420.85 354.25 20.95 o 6 2 0 696.46 756.36 44.02 o 7 2 0 22.60 18.60 27.66 o 8 2 0 183.75 179.31 47.91 o 9 2 0 16.46 -13.57 51.29 o 10 2 0 139.13 246.31 71.58 o 1 3 0 3856.95 3649.86 186.40 o 2 3 0 4194.45 4573.90 231.21 o 3 3 0 3462.79 3422.65 157.36 o 4 3 0 893.42 889.63 42.38 o 5 3 0 2629.54 2507.73 116.45 o 6 3 0 2024.80 1886.80 97.46 o 7 3 0 168.52 135.77 41.98 o 8 3 0 158.50 105.87 46.03 o 9 3 0 6.71 -36.94 51.24 o 10 3 0 234.42 266.42 75.68 o 0 4 0 504.81 554.47 72.15 o 1 4 0 362.44 365.15 19.83 o 2 4 0 34200.11 34806.66 1755.51 o 3 4 0 2071.72 2079.57 96.06 o 4 4 0 1932.30 1742.31 81.78 o 5 4 0 1071.30 1049.53 50.97 o 6 4 0 615.92 618.71 37.48 o 7 4 0 1081.48 1143.98 85.55 o 8 4 0 0.01 -8.93 65.09 o 9 4 0 266.98 306.90 61.82 o 10 4 0 3.60 -64.83 79.60 o 1 5 0 295.56 285.68 15.76 o 2 5 0 1460.79 1398.75 71.98 o 3 5 0 4255.47 4221.87 213.72 o 4 5 0 302.94 227.64 16.66 o 5 5 0 245.50 245.04 17.14 o 6 5 0 372.38 342.87 28.20 o 7 5 0 1891.55 1943.47 135.02 o 8 5 0 62.14 42.95 46.34 o 9 5 0 912.46 980.01 103.37 o 10 5 0 264.25 292.20 69.40 o 0 6 0 816.05 821.90 94.11 o 1 6 0 19311.74 18981.56 1060.82 o 2 6 0 18894.32 19546.29 985.84 o 3 6 0 5668.14 5743.39 288.29 o 4 6 0 845.48 1027.25 49.20 o 5 6 0 561.35 510.21 27.76 o 6 6 0 22.18 1.13 17.67 o 7 6 0 347.65 493.92 126.66 o 8 6 0 93.26 50.61 48.50 o 9 6 0 490.63 488.79 70.63 o 10 6 0 54.19 111.03 67.44 o 1 7 0 2146.51 2068.40 132.77 o 2 7 0 2851.36 2576.30 129.48 o 3 7 0 1289.13 1282.36 66.10 o 4 7 0 6.76 12.32 10.83 o 5 7 0 363.15 369.75 21.92 o 6 7 0 57.93 61.96 19.10 o 7 7 0 751.14 880.96 108.23 o 8 7 0 2314.99 2603.41 219.05 o 9 7 0 30.34 21.66 54.05 o 10 7 0 166.00 142.54 67.36 o 0 8 0 60698.42 57592.04 6397.98 o 1 8 0 802.42 682.51 56.56 o 2 8 0 4651.74 4282.94 215.62 o 3 8 0 758.96 843.99 44.69 o 4 8 0 602.55 656.93 37.43 o 5 8 0 2370.95 2446.81 113.73 o 6 8 0 302.65 306.27 27.91 o 7 8 0 45.85 100.64 49.41 o 8 8 0 88.66 35.74 45.69 o 9 8 0 167.24 228.50 63.45 o 10 8 0 506.16 552.50 84.29 o 1 9 0 4.08 12.02 11.05 o 2 9 0 2187.01 2098.57 116.63 o 3 9 0 835.17 871.47 45.71 o 4 9 0 8566.04 8950.00 453.20 o 5 9 0 4767.38 4833.75 245.79 o 6 9 0 44.94 -5.66 22.07 o 7 9 0 696.64 699.29 75.10 o 8 9 0 0.53 41.57 45.75 o 9 9 0 13.47 -50.54 75.29 o 10 9 0 758.64 838.22 102.99 o 0 10 0 81.24 134.11 24.31 o 1 10 0 185.04 215.34 23.53 o 2 10 0 659.40 503.12 31.46 o 3 10 0 210.05 210.72 17.24 o 4 10 0 395.08 368.30 23.76 o 5 10 0 749.55 869.69 54.24 o 6 10 0 88.95 81.06 24.72 o 7 10 0 2328.98 2351.12 196.03 o 8 10 0 1696.99 1718.42 151.67 o 9 10 0 7.14 107.51 165.48 o 10 10 0 15.83 -5.27 107.44 o 1 11 0 17.05 -0.21 12.16 o 2 11 0 13.27 16.24 13.73 o 3 11 0 1788.49 1751.25 101.56 o 4 11 0 449.71 455.21 30.52 o 5 11 0 0.73 8.86 19.45 o 6 11 0 19.84 -3.34 23.52 o 7 11 0 707.18 619.86 69.87 o 8 11 0 290.26 327.94 57.67 o 9 11 0 724.73 793.08 94.45 o 10 11 0 9.41 130.39 94.90 o 0 12 0 2583.04 2104.95 237.63 o 1 12 0 27.14 17.20 15.29 o 2 12 0 18.47 7.38 12.09 o 3 12 0 11447.87 11136.38 626.63 o 4 12 0 1384.53 1351.30 79.72 o 5 12 0 466.25 404.25 35.47 o 6 12 0 16.90 46.31 32.41 o 7 12 0 3023.08 3142.59 256.48 o 8 12 0 335.06 403.90 69.01 o 9 12 0 199.40 210.39 64.39 o 10 12 0 0.03 -19.16 91.37 o 1 13 0 3376.54 3442.79 272.84 o 2 13 0 15.02 -8.08 15.03 o 3 13 0 13574.96 13994.49 919.18 o 4 13 0 309.41 396.09 36.98 o 5 13 0 1975.29 2003.78 163.87 o 6 13 0 135.79 118.15 36.32 o 7 13 0 1732.78 1776.41 153.32 o 8 13 0 24.94 26.98 47.68 o 9 13 0 271.78 301.39 67.11 o 10 13 0 53.15 61.63 69.59 o 0 14 0 941.56 1007.77 117.64 o 1 14 0 68.19 77.44 17.16 o 2 14 0 1898.16 1764.66 119.91 o 3 14 0 3448.40 3536.00 234.68 o 4 14 0 177.29 175.01 21.35 o 5 14 0 386.49 418.16 48.24 o 6 14 0 194.44 187.10 43.53 o 7 14 0 925.77 1005.08 97.87 o 8 14 0 557.54 564.98 73.73 o 9 14 0 181.94 279.55 70.19 o 10 14 0 100.55 114.01 70.63 o 1 15 0 1800.45 1719.14 139.19 o 2 15 0 979.15 881.02 62.02 o 3 15 0 1.36 13.03 18.00 o 4 15 0 719.11 975.88 67.92 o 5 15 0 33.71 59.00 49.80 o 6 15 0 7.00 30.87 33.81 o 7 15 0 25.51 56.07 48.23 o 8 15 0 374.03 502.28 72.92 o 9 15 0 243.99 171.15 60.63 o 10 15 0 237.16 360.97 78.14 o 0 16 0 4982.66 4240.49 476.05 o 1 16 0 1683.30 1417.57 115.62 o 2 16 0 98.59 77.32 15.43 o 3 16 0 110.07 207.60 36.73 o 4 16 0 19.74 -0.11 16.74 o 5 16 0 1479.45 1640.03 165.09 o 6 16 0 892.95 1278.01 115.07 o 7 16 0 171.47 102.39 45.94 o 8 16 0 100.07 107.44 51.57 o 9 16 0 76.27 -3.97 55.94 o 10 16 0 81.65 110.19 77.03 o 1 17 0 69.42 47.50 23.53 o 2 17 0 3420.29 3311.05 220.34 o 3 17 0 1063.70 975.87 68.67 o 4 17 0 1335.69 1377.46 116.18 o 5 17 0 3188.90 3299.40 266.19 o 6 17 0 7.09 -11.76 51.76 o 7 17 0 230.82 172.65 47.97 o 8 17 0 646.53 570.64 75.97 o 9 17 0 2.13 -11.74 56.17 o 10 17 0 0.02 13.36 71.93 o 0 18 0 6693.37 6372.10 712.89 o 1 18 0 2676.21 2689.25 215.17 o 2 18 0 1041.03 1213.75 82.84 o 3 18 0 1541.77 1548.53 106.07 o 4 18 0 46.38 60.45 26.60 o 5 18 0 0.87 35.62 32.04 o 6 18 0 69.15 31.81 47.06 o 7 18 0 680.87 683.87 109.01 o 8 18 0 1203.97 1101.80 110.08 o 9 18 0 52.56 -46.71 65.37 o 10 18 0 40.08 108.32 77.64 o 1 19 0 3751.28 3857.79 307.22 o 2 19 0 1964.30 1993.38 160.82 o 3 19 0 57.50 50.01 18.46 o 4 19 0 277.02 308.44 75.68 o 5 19 0 236.25 210.27 38.77 o 6 19 0 784.37 948.65 89.56 o 7 19 0 13.54 7.03 41.19 o 8 19 0 116.99 78.43 78.43 o 9 19 0 14.35 7.84 90.97 o 0 20 0 781.39 864.25 106.66 o 1 20 0 1238.35 1448.78 119.23 o 2 20 0 3.81 -12.61 20.75 o 3 20 0 285.95 263.24 27.21 o 4 20 0 1045.10 1072.23 94.27 o 5 20 0 582.27 482.23 54.90 o 6 20 0 13.39 23.60 35.74 o 7 20 0 15.07 135.56 46.45 o 8 20 0 365.51 355.05 63.96 o 9 20 0 67.65 25.66 58.46 o 1 21 0 512.19 598.52 83.92 o 2 21 0 3854.70 4044.30 322.20 o 3 21 0 480.28 513.62 41.59 o 4 21 0 358.92 388.23 46.86 o 5 21 0 530.88 496.79 55.73 o 6 21 0 286.07 266.73 47.41 o 7 21 0 4850.00 4247.20 343.27 o 8 21 0 47.90 44.40 53.33 o 9 21 0 64.27 40.10 57.59 o 0 22 0 4234.47 4684.38 527.02 o 1 22 0 1849.90 1850.27 151.39 o 2 22 0 175.45 158.13 29.11 o 3 22 0 47.51 38.86 19.90 o 4 22 0 5038.82 4932.36 394.01 o 5 22 0 39.76 74.60 37.25 o 6 22 0 77.90 100.52 41.97 o 7 22 0 80.59 117.64 58.04 o 8 22 0 94.42 101.92 55.68 o 9 22 0 60.50 31.53 61.05 o 1 23 0 214.04 238.87 78.82 o 2 23 0 686.81 761.45 107.05 o 3 23 0 213.70 270.98 38.26 o 4 23 0 1001.02 1044.21 93.71 o 5 23 0 354.77 269.22 44.35 o 6 23 0 45.88 37.98 42.42 o 7 23 0 18.20 8.61 48.23 o 8 23 0 0.01 -8.24 52.81 o 9 23 0 190.50 159.74 66.52 o 0 24 0 2172.28 2037.50 235.28 o 1 24 0 2257.82 2193.68 178.29 o 2 24 0 1349.62 1391.14 118.12 o 3 24 0 860.27 871.89 80.13 o 4 24 0 90.61 106.42 35.48 o 5 24 0 0.12 26.91 46.27 o 6 24 0 101.02 240.26 66.66 o 7 24 0 596.41 600.92 124.70 o 8 24 0 414.83 450.07 72.15 o 9 24 0 26.17 76.84 65.51 o 1 25 0 234.65 261.97 75.68 o 2 25 0 639.05 673.31 64.59 o 3 25 0 1236.57 1364.12 151.75 o 4 25 0 41.58 42.64 32.93 o 5 25 0 276.33 317.02 86.66 o 6 25 0 769.16 703.28 135.28 o 7 25 0 6.00 70.58 49.36 o 8 25 0 16.03 15.94 56.92 o 9 25 0 20.04 -61.20 66.33 o 0 26 0 672.82 760.73 100.39 o 1 26 0 1.57 -15.26 27.41 o 2 26 0 64.15 93.99 32.44 o 3 26 0 21.65 22.54 31.60 o 4 26 0 3.21 -16.47 36.86 o 5 26 0 15.94 -5.95 40.00 o 6 26 0 63.64 61.49 45.88 o 7 26 0 27.07 18.76 50.38 o 8 26 0 71.67 -44.19 61.68 o 9 26 0 134.77 34.51 104.31 o 1 27 0 8.14 -9.88 33.33 o 2 27 0 744.42 899.16 83.72 o 3 27 0 379.27 446.52 104.70 o 4 27 0 442.04 512.11 65.88 o 5 27 0 20.36 -16.18 39.65 o 6 27 0 43.24 14.90 46.30 o 7 27 0 115.71 101.41 56.36 o 8 27 0 5.61 -26.12 61.44 o 0 28 0 1662.75 1708.12 202.34 o 1 28 0 573.75 777.60 91.37 o 2 28 0 770.28 691.49 68.74 o 3 28 0 487.18 532.25 58.16 o 4 28 0 584.49 622.81 130.97 o 5 28 0 12.58 100.72 45.13 o 6 28 0 447.12 508.42 68.20 o 7 28 0 895.15 1098.99 110.35 o 8 28 0 1.29 35.81 60.04 o 1 29 0 1173.69 1194.41 105.36 o 2 29 0 213.60 184.16 54.51 o 3 29 0 1103.28 1081.38 98.98 o 4 29 0 820.65 887.40 108.23 o 5 29 0 83.24 61.39 44.02 o 6 29 0 8.32 -45.51 46.57 o 7 29 0 352.24 398.96 121.17 o 8 29 0 10.07 -2.49 65.50 o 0 30 0 53.15 62.74 47.06 o 1 30 0 2.21 6.58 41.17 o 2 30 0 1566.73 1799.23 152.50 o 3 30 0 122.12 105.56 39.93 o 4 30 0 325.48 324.93 52.91 o 5 30 0 1158.43 1184.72 152.93 o 6 30 0 223.58 260.76 56.84 o 7 30 0 242.33 171.69 95.68 o 8 30 0 250.90 234.14 73.84 o 1 31 0 86.12 86.81 36.29 o 2 31 0 717.77 736.93 77.64 o 3 31 0 1995.03 2064.99 174.68 o 4 31 0 179.05 205.39 51.37 o 5 31 0 33.99 63.32 50.17 o 6 31 0 992.75 985.28 102.78 o 7 31 0 310.08 392.91 95.68 o 8 31 0 0.42 87.97 72.24 o 0 32 0 3714.02 3796.60 432.91 o 1 32 0 2762.03 2684.92 220.71 o 2 32 0 585.06 660.23 72.07 o 3 32 0 588.78 634.60 70.37 o 4 32 0 6.80 -15.81 51.76 o 5 32 0 93.95 96.86 49.36 o 6 32 0 4.36 -33.94 51.43 o 7 32 0 89.59 106.72 64.52 o 1 33 0 246.31 295.77 49.08 o 2 33 0 62.69 18.66 41.97 o 3 33 0 311.22 314.32 106.66 o 4 33 0 131.09 182.05 50.63 o 5 33 0 0.29 -6.04 46.89 o 6 33 0 26.42 69.76 55.63 o 7 33 0 277.08 232.64 67.88 o 0 34 0 3000.25 2791.96 324.68 o 1 34 0 626.97 792.54 82.62 o 2 34 0 31.14 -5.67 40.07 o 3 34 0 295.25 241.12 75.29 o 4 34 0 0.81 28.11 46.45 o 5 34 0 5.60 -52.39 52.39 o 6 34 0 7.17 -0.75 58.50 o 7 34 0 0.17 34.72 70.66 o 1 35 0 1395.34 1380.14 123.39 o 2 35 0 157.85 121.76 48.09 o 3 35 0 138.05 201.44 50.98 o 4 35 0 401.59 393.11 63.21 o 5 35 0 20.24 29.29 51.58 o 6 35 0 0.31 -50.75 58.10 o 7 35 0 82.05 57.38 69.03 o 0 36 0 1767.81 1744.98 214.89 o 1 36 0 35.71 32.15 43.81 o 2 36 0 577.35 864.89 90.61 o 3 36 0 1401.33 1499.91 135.59 o 4 36 0 172.34 230.64 102.35 o 5 36 0 94.11 96.08 86.66 o 6 36 0 165.32 243.90 71.38 o 1 37 0 692.77 766.20 138.81 o 2 37 0 5.55 1.46 44.88 o 3 37 0 726.62 786.10 116.07 o 4 37 0 148.31 127.32 58.46 o 5 37 0 32.09 -44.95 58.77 o 6 37 0 19.59 84.26 124.70 o 0 38 0 776.40 910.52 134.89 o 1 38 0 70.16 63.22 49.02 o 2 38 0 132.85 78.95 49.32 o 3 38 0 0.00 13.24 51.35 o 4 38 0 593.31 608.86 80.40 o 5 38 0 113.84 60.08 62.72 o 6 38 0 2.88 -25.33 68.18 o 1 39 0 101.54 158.44 54.89 o 2 39 0 16.74 20.38 50.98 o 3 39 0 553.18 556.35 75.95 o 4 39 0 54.03 93.86 62.96 o 5 39 0 276.58 261.17 69.34 o 0 40 0 282.96 255.67 83.92 o 1 40 0 465.55 658.78 81.17 o 2 40 0 32.21 -31.81 54.62 o 3 40 0 36.51 56.75 55.63 o 4 40 0 134.05 175.49 66.27 o 5 40 0 0.19 -1.12 65.82 o 1 41 0 97.33 150.58 67.45 o 2 41 0 50.39 81.58 68.62 o 3 41 0 113.53 126.49 63.52 o 4 41 0 371.00 506.73 82.32 o 5 41 0 4.68 50.66 65.43 o 0 42 0 23.67 174.11 91.76 o 1 42 0 35.94 74.99 59.06 o 2 42 0 8.05 2.77 60.01 o 3 42 0 715.90 969.35 108.12 o 4 42 0 38.00 75.31 66.13 o 1 43 0 191.79 289.50 69.87 o 2 43 0 102.26 162.46 66.74 o 3 43 0 41.94 113.27 68.74 o 4 43 0 147.69 170.34 119.99 o 0 44 0 124.78 60.39 89.41 o 1 44 0 28.90 27.55 89.01 o 2 44 0 35.90 29.67 63.77 o 3 44 0 255.78 345.11 95.29 o 1 45 0 21.07 42.58 70.92 o 2 45 0 65.73 37.78 80.78 o 0 46 0 74.23 67.45 105.87 o 1 46 0 151.47 132.58 73.84 o -9 0 1 900.47 1225.01 173.32 o -7 0 1 16.61 -22.92 34.86 o -5 0 1 1966.88 1805.41 121.21 o -3 0 1 2368.29 2110.14 135.97 o -1 0 1 93510.18 93677.64 7657.46 o 1 0 1 2130.13 2077.31 164.63 o 3 0 1 3053.92 2696.90 174.44 o 5 0 1 100.50 82.02 16.80 o 7 0 1 997.58 1272.85 160.77 o 9 0 1 107.50 25.10 81.56 o -10 1 1 30.46 -26.05 62.08 o -9 1 1 13.61 38.81 59.82 o -8 1 1 44.95 10.10 43.51 o -7 1 1 217.71 155.25 27.25 o -6 1 1 977.10 944.50 60.86 o -5 1 1 1849.99 1664.12 78.40 o -4 1 1 2372.91 2154.81 100.63 o -3 1 1 132.75 107.03 8.83 o -2 1 1 7140.98 7074.36 323.05 o -1 1 1 726.28 630.25 37.41 o 0 1 1 28.73 0.29 1.56 o 1 1 1 90.02 86.90 8.35 o 2 1 1 12170.68 12031.35 548.19 o 3 1 1 3857.72 3611.61 166.22 o 4 1 1 957.86 931.59 45.13 o 5 1 1 313.21 269.75 18.30 o 6 1 1 72.98 54.57 15.92 o 7 1 1 1230.78 1244.48 111.47 o 8 1 1 30.42 -9.25 45.87 o 9 1 1 140.22 245.28 63.45 o 10 1 1 381.46 458.05 81.87 o -10 2 1 317.57 395.73 96.46 o -9 2 1 538.35 452.33 70.51 o -8 2 1 78.02 58.98 83.52 o -7 2 1 10.17 -4.42 28.57 o -6 2 1 3352.82 3321.04 193.24 o -5 2 1 74.78 77.45 11.15 o -4 2 1 434.49 464.82 28.23 o -3 2 1 243.20 240.38 14.02 o -2 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