#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:22:51 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181034 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/14/2211423.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211423_Fobs loop_ _publ_author_name 'Hu, Man-Cheng' 'Wei, Xiao-Yun' 'Li, Shu-Ni' _publ_section_title ; Bis[N-(2-aminoethyl)-4-methylbenzenesulfonamidato]copper(II) ; _journal_coeditor_code HB2192 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3265 _journal_page_last m3266 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 73.020 _cell_angle_beta 84.913 _cell_angle_gamma 69.454 _cell_length_a 5.6497 _cell_length_b 7.8410 _cell_length_c 13.2882 _exptl_crystal_F_000 255.00 _reflns_d_resolution_high 0.8378 _cod_data_source_file hb2192Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 86.05 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1093.44 1085.50 27.97 o 2 0 0 185.18 202.60 5.29 o 3 0 0 1244.49 1252.07 15.79 o 4 0 0 1.22 0.00 0.56 o 5 0 0 164.54 138.15 5.51 o 6 0 0 91.87 97.01 4.99 o -6 1 0 35.17 40.67 3.31 o -5 1 0 1.97 1.57 1.01 o -4 1 0 156.84 169.05 3.85 o -3 1 0 77.90 62.19 1.82 o -2 1 0 152.85 164.60 4.26 o -1 1 0 1851.63 851.42 19.58 o 0 1 0 166.88 149.97 2.49 o 1 1 0 162.41 194.94 4.72 o 2 1 0 1262.13 1320.01 30.08 o 3 1 0 500.29 514.93 12.91 o 4 1 0 1.36 0.65 0.33 o 5 1 0 171.70 165.46 6.08 o 6 1 0 4.31 5.77 1.52 o -5 2 0 70.21 69.89 3.91 o -4 2 0 286.74 290.34 5.90 o -3 2 0 0.46 0.53 1.20 o -2 2 0 356.06 328.56 5.88 o -1 2 0 90.01 85.51 1.90 o 0 2 0 12.96 16.16 0.72 o 1 2 0 2571.27 2766.37 41.43 o 2 2 0 485.39 433.15 10.33 o 3 2 0 219.89 213.23 6.06 o 4 2 0 850.68 982.87 23.71 o 5 2 0 10.63 12.38 1.60 o 6 2 0 12.79 7.46 1.52 o -5 3 0 76.79 78.28 4.33 o -4 3 0 27.53 28.71 1.58 o -3 3 0 86.83 82.66 2.44 o -2 3 0 476.72 486.08 8.43 o -1 3 0 258.41 297.57 5.32 o 0 3 0 264.22 249.13 6.13 o 1 3 0 168.63 119.21 3.28 o 2 3 0 48.61 52.48 1.27 o 3 3 0 1005.49 946.30 21.94 o 4 3 0 869.02 901.14 21.66 o 5 3 0 20.96 21.70 1.96 o 6 3 0 122.73 109.63 4.87 o -4 4 0 9.04 8.31 1.05 o -3 4 0 424.51 438.61 9.69 o -2 4 0 227.84 244.61 5.00 o -1 4 0 220.28 205.57 4.13 o 0 4 0 735.22 697.23 11.19 o 1 4 0 38.71 50.40 2.06 o 2 4 0 1246.56 1303.67 19.98 o 3 4 0 1746.82 1928.12 30.15 o 4 4 0 71.32 63.91 1.85 o -3 5 0 29.66 34.10 1.75 o -2 5 0 1.27 1.60 0.58 o -1 5 0 228.59 228.01 4.68 o 0 5 0 174.61 183.64 5.45 o 1 5 0 14.38 17.84 1.42 o 2 5 0 688.04 626.75 14.26 o 3 5 0 17.97 14.44 1.31 o 4 5 0 2.12 2.79 0.81 o 5 5 0 276.08 282.15 7.83 o 6 5 0 15.72 13.61 1.43 o -3 6 0 0.69 -0.11 1.07 o -2 6 0 174.74 185.57 6.45 o -1 6 0 37.61 41.67 2.65 o 0 6 0 27.96 26.46 1.99 o 1 6 0 877.63 831.52 18.84 o 2 6 0 158.65 143.95 4.70 o 3 6 0 202.92 195.24 5.85 o 4 6 0 346.35 387.55 10.20 o 5 6 0 7.10 7.41 1.29 o 6 6 0 91.21 89.84 3.90 o -2 7 0 114.46 129.00 5.56 o -1 7 0 6.87 8.56 1.59 o 0 7 0 63.75 61.05 3.29 o 1 7 0 204.38 192.54 6.13 o 2 7 0 2.45 1.90 0.88 o 3 7 0 170.02 175.18 5.80 o 4 7 0 156.46 149.97 5.32 o 5 7 0 12.13 13.22 1.73 o 0 8 0 81.36 83.44 4.19 o 1 8 0 26.47 27.07 2.28 o 2 8 0 22.48 23.89 2.12 o 3 8 0 60.93 61.16 3.33 o 4 8 0 5.01 8.12 1.50 o -4 -8 1 10.73 9.16 1.64 o -3 -8 1 40.51 37.60 2.67 o -2 -8 1 133.38 133.48 5.19 o -1 -8 1 0.39 0.53 0.91 o 0 -8 1 108.51 107.18 4.82 o -5 -7 1 54.06 54.56 3.29 o -4 -7 1 63.77 65.73 3.40 o -3 -7 1 299.93 307.44 8.80 o -2 -7 1 25.38 31.72 2.26 o -1 -7 1 98.62 97.55 4.00 o 0 -7 1 96.89 93.33 4.12 o 1 -7 1 0.24 -1.11 0.74 o -6 -6 1 100.42 101.63 4.31 o -5 -6 1 5.68 4.87 1.15 o -4 -6 1 268.59 312.24 8.83 o -3 -6 1 221.47 235.99 6.93 o -2 -6 1 9.08 8.08 1.13 o -1 -6 1 450.40 423.23 10.67 o 0 -6 1 25.81 24.40 1.91 o 1 -6 1 2.78 1.92 0.99 o 2 -6 1 40.66 43.13 2.87 o 3 -6 1 1.65 1.94 1.28 o -6 -5 1 1.29 0.70 0.68 o -5 -5 1 98.69 93.52 3.68 o -4 -5 1 149.00 164.88 5.36 o -3 -5 1 101.95 113.35 4.01 o -2 -5 1 645.43 581.49 13.36 o -1 -5 1 422.36 369.59 9.18 o 0 -5 1 8.64 7.69 1.07 o 1 -5 1 381.91 380.08 9.88 o 2 -5 1 410.75 410.48 7.81 o 3 -5 1 50.39 59.82 2.32 o -5 -4 1 807.73 810.14 19.88 o -4 -4 1 166.93 192.39 3.99 o -3 -4 1 224.45 227.33 4.33 o -2 -4 1 1454.25 1570.70 24.02 o -1 -4 1 61.31 80.38 1.82 o 0 -4 1 1183.12 1156.51 18.04 o 1 -4 1 416.29 403.66 7.16 o 2 -4 1 2.84 4.24 0.67 o 3 -4 1 219.00 218.46 4.86 o 4 -4 1 0.73 0.81 0.88 o -6 -3 1 158.63 137.56 5.46 o -5 -3 1 31.61 32.46 2.23 o -4 -3 1 2.25 2.87 0.81 o -3 -3 1 1470.93 1602.30 36.41 o -2 -3 1 185.32 223.64 6.08 o -1 -3 1 6.27 19.91 0.92 o 0 -3 1 741.16 691.81 10.96 o 1 -3 1 37.05 38.79 1.28 o 2 -3 1 131.65 123.03 2.90 o 3 -3 1 299.64 293.48 5.82 o 4 -3 1 0.53 0.51 0.81 o 5 -3 1 63.59 65.13 3.93 o -6 -2 1 23.11 21.29 2.19 o -5 -2 1 44.73 39.05 2.60 o -4 -2 1 1156.49 1248.56 29.55 o -3 -2 1 55.68 72.47 2.78 o -2 -2 1 1036.22 1105.15 25.13 o -1 -2 1 3040.39 3116.88 46.55 o 0 -2 1 3.07 4.44 0.32 o 1 -2 1 319.65 322.58 5.51 o 2 -2 1 334.08 331.48 6.24 o 3 -2 1 1.58 0.48 0.40 o 4 -2 1 83.09 93.37 2.72 o 5 -2 1 41.77 46.58 3.24 o -6 -1 1 7.61 7.65 1.57 o -5 -1 1 72.61 70.82 3.63 o -4 -1 1 110.97 117.48 4.44 o -3 -1 1 104.15 137.88 4.52 o -2 -1 1 1724.17 1749.73 39.55 o -1 -1 1 1878.55 2010.59 44.76 o 0 -1 1 1360.02 1451.12 21.79 o 1 -1 1 3420.90 3596.88 53.67 o 2 -1 1 120.60 136.92 2.15 o 3 -1 1 17.47 22.09 1.03 o 4 -1 1 525.26 485.22 8.64 o 5 -1 1 45.52 38.77 2.85 o -6 0 1 10.22 12.21 1.99 o -5 0 1 173.92 162.72 6.18 o -4 0 1 5.29 5.53 1.09 o -3 0 1 1554.66 1551.89 35.92 o -2 0 1 379.09 321.31 5.47 o -1 0 1 2251.55 2507.86 37.53 o 0 0 1 4195.32 1856.72 42.10 o 1 0 1 2569.45 2769.77 40.57 o 2 0 1 103.31 125.39 2.15 o 3 0 1 308.26 246.93 3.64 o 4 0 1 52.20 51.74 2.83 o 5 0 1 0.75 0.60 0.89 o 6 0 1 58.66 59.03 3.79 o -6 1 1 52.15 44.52 3.35 o -5 1 1 57.51 54.74 3.39 o -4 1 1 40.16 44.19 2.26 o -3 1 1 244.00 201.32 4.30 o -2 1 1 463.67 506.17 9.98 o -1 1 1 37.69 24.30 2.93 o 0 1 1 4159.78 4767.13 72.70 o 1 1 1 107.16 119.94 2.02 o 2 1 1 2519.95 2756.89 61.63 o 3 1 1 2862.25 3283.45 50.70 o 4 1 1 0.70 1.15 0.54 o 5 1 1 211.13 201.53 6.94 o 6 1 1 25.48 24.10 2.47 o -5 2 1 37.49 35.96 2.83 o -4 2 1 421.36 427.85 8.03 o -3 2 1 70.40 80.99 2.29 o -2 2 1 827.76 936.82 14.90 o -1 2 1 276.43 274.09 4.77 o 0 2 1 2.53 3.47 0.83 o 1 2 1 6277.54 7242.47 145.43 o 2 2 1 615.17 718.11 16.60 o 3 2 1 9.56 6.57 0.83 o 4 2 1 413.41 373.40 6.86 o 5 2 1 114.80 110.28 4.54 o 6 2 1 1.54 -0.01 0.92 o -5 3 1 62.08 59.59 3.77 o -4 3 1 44.73 54.47 2.51 o -3 3 1 7.51 3.98 0.69 o -2 3 1 684.24 658.27 10.98 o -1 3 1 677.05 683.47 11.04 o 0 3 1 131.62 149.10 3.84 o 1 3 1 265.79 209.70 5.14 o 2 3 1 685.99 796.33 12.33 o 3 3 1 488.93 513.65 8.44 o 4 3 1 1656.16 1730.16 39.89 o 5 3 1 15.75 18.56 1.74 o 6 3 1 43.84 47.28 3.03 o -4 4 1 0.18 -0.44 0.54 o -3 4 1 82.82 71.12 2.38 o -2 4 1 422.61 410.50 7.50 o -1 4 1 410.29 394.68 6.96 o 0 4 1 459.95 429.06 7.18 o 1 4 1 113.86 82.32 2.83 o 2 4 1 37.93 37.41 1.69 o 3 4 1 784.71 818.44 12.94 o 4 4 1 55.42 57.12 1.73 o 5 4 1 28.23 27.85 1.73 o -4 5 1 0.23 0.25 0.68 o -3 5 1 116.49 120.95 3.41 o -2 5 1 2.52 1.87 0.61 o -1 5 1 198.92 192.18 4.09 o 0 5 1 755.70 744.31 16.88 o 1 5 1 74.83 71.80 2.84 o 2 5 1 836.12 841.08 18.47 o 3 5 1 160.07 147.12 4.52 o 4 5 1 0.78 4.59 0.91 o 5 5 1 619.03 675.11 15.73 o -3 6 1 0.29 1.20 1.15 o -2 6 1 98.42 98.57 4.40 o -1 6 1 333.80 345.66 9.57 o 0 6 1 0.95 2.66 0.97 o 1 6 1 62.85 66.28 2.90 o 2 6 1 396.47 373.86 9.49 o 3 6 1 166.12 159.49 5.05 o 4 6 1 371.41 399.34 10.25 o 5 6 1 49.15 48.92 2.74 o -2 7 1 90.46 101.16 4.82 o -1 7 1 30.14 28.76 2.49 o 0 7 1 4.65 2.88 1.09 o 1 7 1 488.50 446.84 11.45 o 2 7 1 22.20 19.43 1.73 o 3 7 1 58.57 63.09 3.03 o 4 7 1 91.47 94.70 3.99 o 5 7 1 0.44 0.53 0.78 o 0 8 1 103.12 105.77 4.72 o 1 8 1 140.62 134.47 5.17 o 2 8 1 15.17 16.33 1.74 o 3 8 1 96.66 104.21 4.42 o 4 8 1 40.43 38.58 2.65 o 5 8 1 27.70 29.31 2.50 o 2 9 1 140.84 132.19 5.33 o 3 9 1 20.90 20.42 2.18 o -4 -8 2 56.09 62.31 3.70 o -3 -8 2 14.92 14.71 1.84 o -2 -8 2 60.61 57.83 3.31 o -1 -8 2 0.36 0.30 0.89 o 0 -8 2 31.69 31.28 2.69 o -5 -7 2 157.31 165.09 6.24 o -4 -7 2 0.62 -0.23 0.70 o -3 -7 2 316.43 309.78 8.97 o -2 -7 2 242.32 234.26 7.19 o -1 -7 2 2.57 2.55 1.03 o 0 -7 2 172.85 165.96 5.83 o 1 -7 2 6.35 5.01 1.36 o -5 -6 2 5.86 6.13 1.27 o -4 -6 2 216.80 245.47 7.56 o -3 -6 2 287.51 294.92 8.34 o -2 -6 2 22.71 21.05 1.75 o -1 -6 2 383.94 352.02 9.33 o 0 -6 2 130.65 127.77 4.63 o 1 -6 2 33.78 33.56 2.43 o 2 -6 2 96.23 93.37 4.24 o -6 -5 2 40.47 36.12 2.28 o -5 -5 2 59.94 56.28 2.85 o -4 -5 2 194.61 219.27 6.66 o -3 -5 2 8.04 7.85 1.13 o -2 -5 2 274.14 266.53 7.20 o -1 -5 2 1602.20 1555.82 32.95 o 0 -5 2 57.14 54.81 2.60 o 1 -5 2 19.86 19.07 1.14 o 2 -5 2 80.02 78.66 2.54 o 3 -5 2 4.12 2.97 1.13 o -5 -4 2 369.73 370.42 10.26 o -4 -4 2 34.41 31.52 1.78 o -3 -4 2 19.36 18.81 1.20 o -2 -4 2 1425.13 1397.79 21.62 o -1 -4 2 18.71 20.50 1.03 o 0 -4 2 15.23 24.19 1.02 o 1 -4 2 359.12 364.44 6.64 o 2 -4 2 28.95 19.38 1.17 o 3 -4 2 44.95 39.91 2.14 o 4 -4 2 64.93 69.56 3.93 o -6 -3 2 209.50 239.83 8.20 o -5 -3 2 397.33 411.91 11.35 o -4 -3 2 7.14 7.65 1.00 o -3 -3 2 1554.72 1621.05 36.95 o -2 -3 2 1390.24 1509.99 23.10 o -1 -3 2 120.38 121.87 2.46 o 0 -3 2 1996.50 1985.03 30.10 o 1 -3 2 120.88 122.03 2.69 o 2 -3 2 52.74 53.20 1.72 o 3 -3 2 846.20 864.48 14.36 o 4 -3 2 2.49 0.98 0.88 o 5 -3 2 3.26 2.21 1.25 o -6 -2 2 55.91 48.84 3.12 o -5 -2 2 2.90 2.58 0.98 o -4 -2 2 756.35 739.04 18.29 o -3 -2 2 152.53 132.20 4.17 o -2 -2 2 2.04 0.64 0.38 o -1 -2 2 826.16 837.17 13.13 o 0 -2 2 144.05 134.54 2.54 o 1 -2 2 328.57 330.76 5.65 o 2 -2 2 474.97 456.16 7.77 o 3 -2 2 3.01 1.21 1.06 o 4 -2 2 0.33 1.03 0.87 o 5 -2 2 76.06 81.90 4.40 o -6 -1 2 0.39 0.31 0.95 o -5 -1 2 23.71 28.57 2.33 o -4 -1 2 283.27 299.69 8.75 o -3 -1 2 5.82 1.89 0.64 o -2 -1 2 2449.44 2648.17 59.29 o -1 -1 2 1406.57 1398.75 31.43 o 0 -1 2 89.15 92.59 2.40 o 1 -1 2 5843.40 6238.38 93.10 o 2 -1 2 637.00 604.43 8.01 o 3 -1 2 183.63 200.10 3.13 o 4 -1 2 303.63 309.24 9.48 o 5 -1 2 21.61 18.80 2.13 o -6 0 2 1.47 0.84 1.19 o -5 0 2 103.82 113.04 4.90 o -4 0 2 130.27 98.60 4.11 o -3 0 2 361.66 361.48 9.76 o -2 0 2 200.20 183.21 5.21 o -1 0 2 22.52 22.46 1.03 o 1 0 2 5392.07 5568.51 531.46 o 2 0 2 230.64 247.69 4.03 o 3 0 2 123.85 116.29 2.47 o 4 0 2 399.56 420.65 11.76 o 5 0 2 5.72 5.12 1.32 o 6 0 2 19.54 17.29 2.27 o -6 1 2 39.19 35.02 3.04 o -5 1 2 130.20 116.37 5.11 o -4 1 2 14.38 16.02 1.10 o -3 1 2 949.20 967.65 17.29 o -2 1 2 105.06 81.94 8.72 o -1 1 2 26.98 36.48 1.39 o 0 1 2 7404.72 8685.11 168.65 o 1 1 2 746.88 804.84 11.79 o 2 1 2 211.75 212.81 3.89 o 3 1 2 1044.44 1007.47 16.26 o 4 1 2 6.93 6.81 0.68 o 5 1 2 190.31 178.88 6.46 o 6 1 2 103.02 94.45 4.77 o -5 2 2 0.44 0.93 0.95 o -4 2 2 143.79 154.78 3.85 o -3 2 2 278.72 261.39 5.28 o -2 2 2 357.93 364.01 6.46 o -1 2 2 822.65 766.88 15.39 o 0 2 2 1215.02 1347.95 20.35 o 1 2 2 2455.88 2829.82 42.33 o 2 2 2 404.71 347.25 5.63 o 3 2 2 188.65 168.54 3.47 o 4 2 2 114.95 103.15 2.62 o 5 2 2 421.32 434.05 12.16 o 6 2 2 11.12 9.14 1.63 o -5 3 2 47.46 41.06 3.01 o -4 3 2 347.77 346.88 7.08 o -3 3 2 5.46 3.83 0.68 o -2 3 2 379.78 372.62 6.73 o -1 3 2 425.33 421.84 7.17 o 0 3 2 304.22 359.26 8.48 o 1 3 2 4123.13 4690.99 94.36 o 2 3 2 132.86 152.43 2.76 o 3 3 2 65.98 69.85 1.69 o 4 3 2 1698.08 1800.37 41.39 o 5 3 2 9.36 13.37 2.23 o 6 3 2 4.19 5.99 1.39 o -4 4 2 5.89 5.00 0.91 o -3 4 2 1.67 0.45 0.67 o -2 4 2 506.90 511.72 9.02 o -1 4 2 761.95 785.26 12.76 o 0 4 2 426.11 425.76 7.13 o 1 4 2 745.84 746.78 16.26 o 2 4 2 12.41 9.25 0.84 o 3 4 2 299.06 342.90 8.16 o 4 4 2 365.20 394.10 6.95 o 6 4 2 128.65 115.68 4.58 o -4 5 2 0.85 0.79 1.17 o -3 5 2 74.57 74.60 2.60 o -2 5 2 11.22 13.80 1.36 o -1 5 2 96.20 93.10 3.28 o 0 5 2 483.64 471.73 11.45 o 1 5 2 193.49 185.84 5.26 o 2 5 2 649.46 618.88 13.95 o 3 5 2 358.06 313.88 7.76 o 4 5 2 8.49 8.97 1.06 o 5 5 2 106.79 110.55 3.89 o 6 5 2 51.90 50.02 3.01 o -3 6 2 17.38 20.83 2.28 o -2 6 2 17.75 19.08 2.06 o -1 6 2 243.65 262.21 7.82 o 0 6 2 118.73 111.74 4.29 o 1 6 2 0.96 0.58 0.67 o 2 6 2 641.28 598.31 13.96 o 3 6 2 33.77 28.87 1.83 o 4 6 2 44.35 40.00 2.19 o 5 6 2 266.09 294.87 8.16 o -2 7 2 206.66 205.90 7.34 o -1 7 2 122.07 126.22 5.16 o 0 7 2 24.37 25.50 2.19 o 1 7 2 288.61 253.16 7.42 o 2 7 2 324.64 291.05 8.08 o 3 7 2 75.10 86.86 3.60 o 4 7 2 204.84 204.32 6.36 o 5 7 2 18.08 16.95 1.72 o -1 8 2 0.47 -0.13 1.07 o 0 8 2 53.59 55.23 3.36 o 1 8 2 144.86 149.71 5.59 o 2 8 2 4.93 4.78 1.13 o 3 8 2 61.65 61.12 3.16 o 4 8 2 54.89 61.68 3.24 o 5 8 2 2.57 3.02 1.09 o 1 9 2 4.02 4.13 1.43 o 2 9 2 111.42 106.68 4.66 o 3 9 2 121.16 114.63 4.77 o -3 -8 3 21.48 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