#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:23:09 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181035 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/15/2211515.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211515_Fobs loop_ _publ_author_name 'Sonar, Vijayakumar N.' 'Venkataraj, M.' 'Parkin, Sean' 'Crooks, Peter A.' _publ_section_title ; (Z)-2-(Cyclohexylidene)-1-azabicyclo[2.2.2]octan-3-one ; _journal_coeditor_code LH2243 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o5576 _journal_page_last o5577 _journal_volume 62 _journal_year 2006 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.524 _cell_angle_gamma 90.000 _cell_length_a 9.2795 _cell_length_b 6.7778 _cell_length_c 9.8401 _exptl_crystal_F_000 240.00 _reflns_d_resolution_high .7702 _cod_data_source_file lh2243Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' k05305 - P21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 40.89 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 762.11 718.06 32.92 o 3 0 0 52.70 49.16 .71 o 4 0 0 31.49 33.29 .54 o 5 0 0 38.14 40.01 .71 o 6 0 0 37.56 33.26 .91 o 7 0 0 26.97 26.77 .81 o 8 0 0 .01 .41 .30 o 9 0 0 3.53 3.68 .51 o 10 0 0 2.03 3.00 .61 o 11 0 0 46.05 45.11 2.63 o 1 1 0 314.04 283.20 3.01 o 2 1 0 712.20 669.21 6.95 o 3 1 0 410.89 390.74 3.44 o 4 1 0 246.90 257.71 2.40 o 5 1 0 307.44 325.62 5.22 o 6 1 0 58.06 59.91 .86 o 7 1 0 18.37 17.97 .61 o 8 1 0 55.98 50.53 1.33 o 9 1 0 52.14 49.23 1.13 o 10 1 0 116.99 114.16 2.97 o 11 1 0 13.54 12.40 .87 o 0 2 0 13.59 13.47 .25 o 1 2 0 138.25 126.91 1.40 o 2 2 0 23.68 24.95 .29 o 3 2 0 25.11 27.18 .31 o 4 2 0 74.93 78.61 .77 o 5 2 0 215.99 209.08 2.47 o 6 2 0 37.00 38.67 .65 o 7 2 0 80.68 80.41 1.21 o 8 2 0 10.64 8.39 .41 o 9 2 0 70.37 67.49 1.80 o 10 2 0 27.01 32.79 1.29 o 11 2 0 19.45 18.83 1.11 o 1 3 0 104.17 105.37 1.05 o 2 3 0 85.65 86.00 .91 o 3 3 0 118.25 121.99 1.30 o 4 3 0 107.07 103.39 1.16 o 5 3 0 36.60 39.10 .57 o 6 3 0 118.84 113.33 1.71 o 7 3 0 30.17 29.27 .62 o 8 3 0 42.73 39.03 .99 o 9 3 0 23.67 24.51 1.22 o 10 3 0 1.70 1.64 .56 o 11 3 0 3.15 3.22 .76 o 0 4 0 302.38 287.12 5.02 o 1 4 0 180.46 185.78 2.21 o 2 4 0 83.87 84.59 .95 o 3 4 0 38.58 35.88 .49 o 4 4 0 18.92 17.84 .38 o 5 4 0 303.64 304.11 4.01 o 6 4 0 30.27 31.93 .72 o 7 4 0 .09 .05 .19 o 8 4 0 60.47 66.26 1.40 o 9 4 0 10.84 10.45 .79 o 10 4 0 10.27 10.94 .99 o 1 5 0 103.94 103.84 1.50 o 2 5 0 152.65 147.68 1.74 o 3 5 0 245.47 254.43 3.33 o 4 5 0 213.63 215.78 3.97 o 5 5 0 28.99 26.54 .66 o 6 5 0 89.49 88.63 1.71 o 7 5 0 16.22 15.71 .65 o 8 5 0 15.44 13.03 .71 o 9 5 0 18.08 16.59 .95 o 0 6 0 45.05 39.54 1.45 o 1 6 0 144.86 150.27 2.73 o 2 6 0 124.03 127.08 2.11 o 3 6 0 48.95 46.46 .93 o 4 6 0 6.41 4.53 .35 o 5 6 0 3.58 2.91 .33 o 6 6 0 4.15 3.28 .57 o 7 6 0 14.72 12.92 .75 o 8 6 0 7.32 7.56 .77 o 1 7 0 119.78 125.87 2.77 o 2 7 0 12.58 10.12 .58 o 3 7 0 144.20 143.12 3.43 o 4 7 0 2.29 1.71 .47 o 5 7 0 21.57 22.38 .92 o 6 7 0 13.36 13.74 .75 o 7 7 0 5.61 4.86 .66 o 0 8 0 7.72 7.66 1.11 o 1 8 0 4.59 4.68 .66 o 2 8 0 17.57 16.78 1.09 o 3 8 0 18.35 17.39 1.64 o 4 8 0 .17 .90 .67 o -11 0 1 .02 -.78 .78 o -10 0 1 26.45 26.23 1.08 o -9 0 1 29.78 28.87 1.05 o -8 0 1 1.73 1.25 .34 o -7 0 1 18.03 18.13 .64 o -6 0 1 74.90 80.53 1.76 o -5 0 1 518.45 540.83 8.17 o -4 0 1 690.32 698.57 10.03 o -3 0 1 144.57 137.32 2.06 o -2 0 1 18.95 16.95 .30 o -1 0 1 21.43 23.70 .34 o 0 0 1 66.98 69.45 1.28 o 1 0 1 536.59 507.10 8.78 o 3 0 1 20.94 21.20 .37 o 4 0 1 94.11 101.63 1.42 o 5 0 1 1.86 1.65 .14 o 6 0 1 67.62 68.44 1.28 o 7 0 1 .99 2.03 .14 o 8 0 1 19.17 15.06 .71 o 9 0 1 45.53 43.56 1.42 o 10 0 1 6.39 5.98 .88 o 11 0 1 13.74 14.92 1.28 o -11 1 1 41.23 44.26 1.68 o -10 1 1 11.56 9.72 .53 o -9 1 1 15.32 14.54 .53 o -8 1 1 36.61 39.25 .87 o -7 1 1 87.84 82.62 1.65 o -6 1 1 92.00 90.79 1.19 o -5 1 1 49.21 54.74 .63 o -4 1 1 23.60 23.05 .27 o -3 1 1 394.96 386.75 3.77 o -2 1 1 832.84 796.64 9.17 o 0 1 1 523.89 480.90 5.01 o 2 1 1 1017.88 939.01 12.60 o 3 1 1 14.53 12.66 .30 o 4 1 1 25.42 28.43 .33 o 5 1 1 55.56 55.86 1.32 o 6 1 1 90.05 88.88 1.11 o 7 1 1 68.25 68.56 .88 o 8 1 1 76.42 77.17 1.42 o 9 1 1 18.27 15.96 .70 o 10 1 1 23.55 25.03 .94 o 11 1 1 19.49 19.64 1.20 o -11 2 1 38.13 39.45 1.72 o -10 2 1 9.87 9.99 .74 o -9 2 1 125.87 128.06 4.02 o -8 2 1 11.58 11.73 .62 o -7 2 1 5.70 4.56 .29 o -6 2 1 62.68 68.59 1.40 o -5 2 1 29.21 32.03 .46 o -4 2 1 1224.11 1224.12 25.21 o -3 2 1 310.36 322.06 3.09 o -2 2 1 314.66 327.49 3.33 o -1 2 1 523.31 528.35 5.37 o 0 2 1 175.64 173.32 3.21 o 1 2 1 317.03 309.53 3.13 o 2 2 1 506.73 489.26 7.70 o 3 2 1 203.68 204.91 2.00 o 4 2 1 320.14 324.61 3.42 o 5 2 1 130.76 139.66 1.79 o 6 2 1 77.72 79.14 1.13 o 7 2 1 27.30 29.50 .56 o 8 2 1 12.24 10.36 .81 o 9 2 1 44.54 44.08 1.44 o 10 2 1 .44 .59 .47 o 11 2 1 32.72 31.38 1.60 o -11 3 1 2.78 1.00 .58 o -10 3 1 23.05 22.98 1.99 o -9 3 1 15.75 15.79 .66 o -8 3 1 143.71 139.17 3.26 o -7 3 1 22.89 20.95 .53 o -6 3 1 340.98 339.25 6.90 o -5 3 1 14.33 15.38 .33 o -4 3 1 148.40 143.47 1.69 o -3 3 1 44.02 41.90 .52 o -2 3 1 58.87 57.53 .62 o -1 3 1 322.74 331.64 3.22 o 0 3 1 44.65 41.65 .57 o 1 3 1 604.92 624.16 7.48 o 2 3 1 68.92 70.81 .78 o 3 3 1 66.22 64.68 .81 o 4 3 1 6.11 3.81 .15 o 5 3 1 58.28 59.18 1.05 o 6 3 1 129.92 125.95 1.87 o 7 3 1 49.25 51.96 2.26 o 8 3 1 75.76 68.30 1.65 o 9 3 1 7.47 8.08 1.23 o 10 3 1 14.62 14.47 1.23 o -10 4 1 22.91 18.44 1.59 o -9 4 1 1.21 1.57 .56 o -8 4 1 27.73 24.88 .96 o -7 4 1 83.20 84.75 1.66 o -6 4 1 119.17 117.75 1.92 o -5 4 1 371.47 367.16 8.24 o -4 4 1 151.39 145.63 2.46 o -3 4 1 52.08 50.92 .88 o -2 4 1 117.10 108.88 1.50 o -1 4 1 3.38 3.12 .20 o 0 4 1 4.73 5.19 .19 o 1 4 1 130.80 126.25 1.43 o 2 4 1 33.89 30.64 .44 o 3 4 1 24.37 19.84 .57 o 4 4 1 41.66 36.68 .63 o 5 4 1 173.86 165.92 2.49 o 6 4 1 3.55 2.95 .26 o 7 4 1 276.13 279.79 5.23 o 8 4 1 3.01 1.93 .33 o 9 4 1 65.58 64.19 1.97 o 10 4 1 33.13 36.32 1.74 o -9 5 1 11.07 11.25 .91 o -8 5 1 5.79 4.46 .50 o -7 5 1 3.09 2.23 .42 o -6 5 1 39.16 38.32 .87 o -5 5 1 32.62 33.57 .77 o -4 5 1 87.31 86.92 1.36 o -3 5 1 409.50 400.06 5.13 o -2 5 1 68.79 69.10 1.01 o -1 5 1 147.09 150.85 3.46 o 0 5 1 79.06 75.37 1.54 o 1 5 1 3.45 3.26 .37 o 2 5 1 13.09 11.62 .27 o 3 5 1 19.33 17.36 .39 o 4 5 1 4.04 3.31 .28 o 5 5 1 58.24 60.84 1.10 o 6 5 1 34.46 35.77 .81 o 7 5 1 31.47 33.89 .91 o 8 5 1 16.62 16.12 .97 o 9 5 1 9.32 9.06 1.20 o -8 6 1 7.52 8.72 .75 o -7 6 1 50.92 49.60 2.30 o -6 6 1 1.51 2.07 .34 o -5 6 1 34.33 36.66 .98 o -4 6 1 39.60 39.49 .88 o -3 6 1 201.74 199.74 3.14 o -2 6 1 222.09 221.16 3.59 o -1 6 1 22.69 23.12 .63 o 0 6 1 11.96 11.75 .41 o 1 6 1 38.02 35.70 1.50 o 2 6 1 149.97 142.74 2.35 o 3 6 1 11.51 10.70 .61 o 4 6 1 35.22 33.45 1.43 o 5 6 1 55.48 55.47 2.65 o 6 6 1 1.71 1.65 .35 o 7 6 1 8.98 8.10 .93 o 8 6 1 9.06 9.02 1.74 o -7 7 1 1.65 1.69 .73 o -6 7 1 4.68 4.19 .52 o -5 7 1 .12 .84 .52 o -4 7 1 22.37 23.25 1.06 o -3 7 1 28.16 24.30 1.02 o -2 7 1 38.80 36.36 1.10 o -1 7 1 48.25 48.08 1.84 o 0 7 1 38.35 36.63 1.18 o 1 7 1 59.88 58.09 1.58 o 2 7 1 104.26 111.05 2.65 o 3 7 1 3.40 3.01 .48 o 4 7 1 2.06 2.11 .45 o 5 7 1 4.83 4.38 .59 o 6 7 1 25.76 30.84 1.86 o -5 8 1 7.57 3.95 .91 o -4 8 1 2.57 2.12 .63 o -3 8 1 19.84 20.87 1.11 o -2 8 1 8.54 7.55 .86 o -1 8 1 8.39 8.59 .80 o 0 8 1 6.85 5.89 .93 o 1 8 1 46.66 50.72 3.22 o 2 8 1 41.36 45.18 1.62 o 3 8 1 12.97 14.17 .90 o 4 8 1 54.32 54.89 2.31 o -12 0 2 16.16 15.33 1.45 o -11 0 2 .82 1.11 .68 o -10 0 2 .34 .68 .54 o -9 0 2 23.92 24.61 .88 o -8 0 2 161.01 161.53 3.71 o -7 0 2 46.63 42.95 1.18 o -6 0 2 115.16 119.15 2.46 o -5 0 2 6.78 4.25 .14 o -4 0 2 3.54 3.17 .14 o -3 0 2 8.85 11.18 .24 o -2 0 2 15.66 15.33 .24 o -1 0 2 143.30 132.62 1.72 o 1 0 2 857.00 775.99 17.25 o 2 0 2 312.07 336.22 5.81 o 3 0 2 2.56 3.00 .14 o 4 0 2 34.73 36.30 .64 o 5 0 2 52.36 54.90 .91 o 6 0 2 23.70 27.62 .61 o 7 0 2 177.55 178.64 3.38 o 8 0 2 32.44 30.96 1.18 o 9 0 2 3.57 2.50 .44 o 10 0 2 .46 1.32 .68 o 11 0 2 .73 -.14 .71 o -11 1 2 4.62 5.63 .86 o -10 1 2 85.87 84.39 3.83 o -9 1 2 27.00 26.28 .78 o -8 1 2 46.42 43.38 .92 o -7 1 2 21.48 22.11 .64 o -6 1 2 61.37 63.37 .89 o -5 1 2 256.92 279.98 3.14 o -4 1 2 73.54 76.84 .83 o -3 1 2 450.36 470.93 4.64 o -2 1 2 812.06 807.31 8.87 o -1 1 2 292.17 298.27 2.89 o 0 1 2 55.67 52.01 .54 o 1 1 2 1150.95 1101.22 18.47 o 2 1 2 450.50 441.20 4.30 o 3 1 2 562.08 582.76 5.67 o 4 1 2 172.97 176.86 1.84 o 5 1 2 86.33 90.66 1.07 o 6 1 2 12.95 14.50 .29 o 7 1 2 73.37 71.80 1.04 o 8 1 2 65.82 63.19 1.25 o 9 1 2 4.11 3.12 .42 o 10 1 2 16.58 15.62 .76 o 11 1 2 4.27 3.43 .78 o -11 2 2 1.50 1.05 .62 o -10 2 2 6.35 6.00 .62 o -9 2 2 143.32 153.35 3.33 o -8 2 2 18.43 19.70 .64 o -7 2 2 44.38 44.55 .85 o -6 2 2 131.05 135.18 1.94 o -5 2 2 18.40 19.51 .44 o -4 2 2 148.13 149.65 1.50 o -3 2 2 196.32 205.44 2.21 o -2 2 2 1671.99 1661.40 38.46 o -1 2 2 550.23 552.16 5.54 o 0 2 2 1384.57 1363.66 23.32 o 1 2 2 50.86 51.15 .56 o 2 2 2 109.48 109.61 1.12 o 3 2 2 791.81 849.75 8.65 o 4 2 2 8.57 6.80 .16 o 5 2 2 57.71 53.38 .69 o 6 2 2 44.81 43.56 .72 o 7 2 2 174.52 176.38 2.85 o 8 2 2 81.35 83.38 1.75 o 9 2 2 16.15 17.93 .79 o 10 2 2 48.75 47.42 1.72 o -11 3 2 .18 .86 .69 o -10 3 2 16.49 15.97 .89 o -9 3 2 50.12 48.96 1.52 o -8 3 2 8.23 8.52 .41 o -7 3 2 220.51 217.13 5.08 o -6 3 2 229.97 218.99 2.96 o -5 3 2 47.47 48.09 .66 o -4 3 2 302.31 319.57 5.77 o -3 3 2 359.73 368.38 3.88 o -2 3 2 353.35 383.09 4.02 o -1 3 2 148.60 154.79 1.63 o 0 3 2 34.41 37.61 .46 o 1 3 2 258.55 276.25 3.66 o 2 3 2 77.68 84.16 .94 o 3 3 2 68.08 74.81 .83 o 4 3 2 20.00 18.62 .32 o 5 3 2 8.43 7.43 .26 o 6 3 2 101.04 101.15 1.58 o 7 3 2 68.78 62.44 2.40 o 8 3 2 88.01 89.28 1.84 o 9 3 2 84.17 89.56 3.09 o 10 3 2 21.30 23.42 2.80 o -10 4 2 27.52 29.30 1.38 o -9 4 2 7.66 7.79 .66 o -8 4 2 17.10 16.38 .76 o -7 4 2 32.41 29.98 .74 o -6 4 2 125.29 115.52 2.11 o -5 4 2 251.15 251.95 3.18 o -4 4 2 78.22 72.87 1.00 o -3 4 2 36.75 38.35 .57 o -2 4 2 50.46 41.75 .91 o -1 4 2 17.67 18.63 .36 o 0 4 2 154.88 170.93 2.19 o 1 4 2 134.72 133.34 1.71 o 2 4 2 79.64 83.59 1.94 o 3 4 2 104.55 100.93 1.87 o 4 4 2 109.80 111.11 1.67 o 5 4 2 4.73 5.37 .28 o 6 4 2 90.76 88.53 1.43 o 7 4 2 6.18 6.37 .36 o 8 4 2 54.11 55.95 2.04 o 9 4 2 33.85 33.87 1.26 o -9 5 2 2.37 2.14 .60 o -8 5 2 2.77 3.88 1.32 o -7 5 2 36.91 35.19 1.28 o -6 5 2 48.81 45.64 1.45 o -5 5 2 65.94 65.84 1.14 o -4 5 2 156.30 147.48 2.26 o -3 5 2 151.52 147.01 1.87 o -2 5 2 89.42 90.85 1.30 o -1 5 2 146.67 138.09 2.11 o 0 5 2 50.84 50.76 .98 o 1 5 2 60.54 60.07 1.03 o 2 5 2 35.62 32.32 .64 o 3 5 2 63.15 61.41 .88 o 4 5 2 58.60 53.30 1.92 o 5 5 2 42.88 38.49 .80 o 6 5 2 6.51 7.18 .37 o 7 5 2 10.10 10.66 .53 o 8 5 2 11.55 10.92 1.06 o 9 5 2 19.29 18.83 1.15 o -8 6 2 5.02 5.75 .78 o -7 6 2 17.07 14.99 .95 o -6 6 2 4.18 3.74 .44 o -5 6 2 40.51 42.32 1.13 o -4 6 2 32.69 29.46 .82 o -3 6 2 15.83 13.75 .45 o -2 6 2 97.70 100.21 1.96 o -1 6 2 37.12 34.05 1.54 o 0 6 2 70.81 63.81 1.27 o 1 6 2 28.42 26.17 .69 o 2 6 2 10.81 9.34 .83 o 3 6 2 22.15 22.05 .66 o 4 6 2 1.44 1.55 .35 o 5 6 2 23.53 26.51 1.01 o 6 6 2 30.75 31.31 .86 o 7 6 2 .34 .01 .48 o 8 6 2 51.13 58.58 2.48 o -7 7 2 .81 .61 .54 o -6 7 2 1.10 .95 .76 o -5 7 2 3.25 3.02 .54 o -4 7 2 15.44 15.41 .79 o -3 7 2 32.44 31.74 1.21 o -2 7 2 21.20 21.22 1.28 o -1 7 2 59.10 58.83 1.63 o 0 7 2 8.16 6.84 .49 o 1 7 2 122.10 122.73 2.91 o 2 7 2 64.02 67.62 1.84 o 3 7 2 64.27 70.68 1.73 o 4 7 2 115.33 123.66 3.18 o 5 7 2 3.48 3.98 .61 o 6 7 2 45.61 49.20 2.73 o -4 8 2 5.58 6.35 .89 o -3 8 2 2.16 2.30 1.60 o -2 8 2 1.15 1.01 .58 o -1 8 2 8.84 9.46 .76 o 0 8 2 14.71 14.54 .90 o 1 8 2 51.11 54.26 1.90 o 2 8 2 27.24 25.78 1.33 o 3 8 2 47.71 49.91 1.74 o 4 8 2 8.43 5.60 .99 o -12 0 3 24.63 28.19 2.03 o -11 0 3 22.84 24.88 1.69 o -10 0 3 17.12 16.11 .91 o -9 0 3 6.28 6.11 .51 o -8 0 3 .38 -.03 .30 o -7 0 3 107.15 104.20 2.30 o -6 0 3 82.51 78.33 1.32 o -5 0 3 17.26 14.69 .34 o -4 0 3 21.97 17.69 .34 o -3 0 3 14.30 15.84 .30 o -2 0 3 268.17 260.86 3.51 o -1 0 3 10.74 12.73 .27 o 0 0 3 268.68 260.12 5.64 o 1 0 3 344.50 326.70 5.87 o 2 0 3 1287.40 1309.90 44.57 o 3 0 3 15.31 18.40 .41 o 4 0 3 29.44 42.85 .81 o 5 0 3 73.63 72.49 1.38 o 6 0 3 272.82 270.79 5.17 o 7 0 3 115.39 113.31 2.33 o 8 0 3 18.22 17.56 .71 o 9 0 3 22.63 22.86 1.15 o 10 0 3 17.69 18.40 1.35 o -11 1 3 5.38 5.15 .88 o -10 1 3 31.59 29.24 1.09 o -9 1 3 7.21 6.91 .44 o -8 1 3 92.05 90.15 3.43 o -7 1 3 141.14 146.05 2.37 o -6 1 3 95.15 94.73 1.32 o -5 1 3 198.14 202.55 2.59 o -4 1 3 29.32 29.56 .38 o -3 1 3 1188.97 1194.38 15.77 o -2 1 3 293.04 277.07 2.89 o -1 1 3 943.21 921.93 12.21 o 0 1 3 3.42 2.98 .27 o 1 1 3 73.22 79.87 1.10 o 2 1 3 736.88 762.09 9.24 o 3 1 3 122.55 129.14 1.40 o 4 1 3 220.27 234.72 2.68 o 5 1 3 74.26 78.39 1.03 o 6 1 3 181.61 177.81 3.16 o 7 1 3 189.69 190.08 2.55 o 8 1 3 118.18 115.14 1.92 o 9 1 3 9.99 9.49 .54 o 10 1 3 28.37 29.11 1.15 o -11 2 3 3.62 2.83 .62 o -10 2 3 10.29 11.49 .86 o -9 2 3 62.25 58.58 1.94 o -8 2 3 111.77 113.20 2.48 o -7 2 3 54.04 48.95 1.37 o -6 2 3 20.29 18.30 .42 o -5 2 3 344.47 342.31 4.61 o -4 2 3 284.00 311.57 3.33 o -3 2 3 1202.00 1245.00 16.99 o -2 2 3 395.70 422.69 4.14 o -1 2 3 279.94 310.36 2.89 o 0 2 3 91.99 99.42 1.05 o 1 2 3 181.48 181.50 2.06 o 2 2 3 167.80 176.53 1.92 o 3 2 3 55.47 60.75 .68 o 4 2 3 7.83 11.15 .23 o 5 2 3 24.70 29.11 .47 o 6 2 3 50.11 45.64 .72 o 7 2 3 52.84 48.55 1.18 o 8 2 3 91.76 90.67 1.91 o 9 2 3 31.99 29.92 1.27 o 10 2 3 17.76 17.03 .97 o -11 3 3 6.23 7.33 .80 o -10 3 3 10.68 8.56 .74 o -9 3 3 7.07 5.65 .57 o -8 3 3 15.67 14.16 .55 o -7 3 3 125.75 120.25 2.15 o -6 3 3 41.35 41.14 .74 o -5 3 3 75.92 69.32 .96 o -4 3 3 131.98 135.90 1.79 o -3 3 3 523.45 549.75 6.39 o -2 3 3 218.39 221.29 2.31 o -1 3 3 590.05 651.50 6.49 o 0 3 3 58.00 60.92 .74 o 1 3 3 207.59 234.00 3.09 o 2 3 3 305.29 322.59 3.69 o 3 3 3 12.49 11.53 .24 o 4 3 3 40.81 44.12 .63 o 5 3 3 61.91 65.12 .95 o 6 3 3 57.59 62.13 1.05 o 7 3 3 26.97 20.91 .62 o 8 3 3 16.47 13.74 .93 o 9 3 3 20.67 22.07 2.70 o 10 3 3 35.24 36.71 1.50 o -10 4 3 11.72 12.24 1.27 o -9 4 3 9.56 9.29 .78 o -8 4 3 59.51 60.55 1.54 o -7 4 3 1.18 .76 .26 o -6 4 3 33.98 32.48 .79 o -5 4 3 64.59 64.75 1.07 o -4 4 3 558.26 550.80 8.57 o -3 4 3 8.24 7.34 .20 o -2 4 3 18.43 20.90 .34 o -1 4 3 121.96 119.92 1.69 o 0 4 3 98.28 96.33 1.28 o 1 4 3 121.63 123.79 2.68 o 2 4 3 19.14 20.16 .39 o 3 4 3 27.06 28.26 .49 o 4 4 3 .01 .20 .14 o 5 4 3 29.42 28.00 .62 o 6 4 3 42.07 35.66 .76 o 7 4 3 27.46 25.05 .68 o 8 4 3 58.19 61.19 1.57 o 9 4 3 12.34 12.03 1.57 o -9 5 3 12.88 12.41 1.11 o -8 5 3 8.80 8.50 .66 o -7 5 3 11.11 10.82 .95 o -6 5 3 5.63 5.13 .52 o -5 5 3 143.17 140.43 2.57 o -4 5 3 12.40 12.52 .44 o -3 5 3 123.04 125.55 1.92 o -2 5 3 83.44 77.83 1.19 o -1 5 3 64.58 61.10 1.12 o 0 5 3 38.18 41.61 1.03 o 1 5 3 68.07 62.18 1.55 o 2 5 3 85.76 81.43 1.36 o 3 5 3 19.07 18.39 .64 o 4 5 3 43.29 37.69 .78 o 5 5 3 23.67 23.26 .62 o 6 5 3 4.25 3.02 .49 o 7 5 3 23.37 25.93 .82 o 8 5 3 22.29 24.66 1.07 o -8 6 3 22.17 20.46 1.94 o -7 6 3 69.31 78.55 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