#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2211516.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2211516_Fobs loop_ _publ_author_name 'Bai, Guo-Yi' 'Simpson, Jim' 'Chen, Yong' 'Li, Jiang-Sheng' 'Ning, Hui-Sen' _publ_section_title ; 2,6-Di-tert-butyl-4-(hydroxymethyl)phenol ; _journal_coeditor_code LH2244 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o5719 _journal_page_last o5721 _journal_volume 62 _journal_year 2006 _space_group_IT_number 31 _symmetry_space_group_name_Hall 'P 2ac -2' _symmetry_space_group_name_H-M 'P m n 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 18.9010 _cell_length_b 6.2580 _cell_length_c 6.2670 _exptl_crystal_F_000 260.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file lh2244Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 60104B in Pmn2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 48.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y, z+1/2' '-x, y, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 12.83 7.56 0.40 o 6 0 0 1781.36 1641.42 31.39 o 8 0 0 129.05 98.43 2.47 o 10 0 0 42.52 48.57 1.17 o 12 0 0 4.70 2.71 0.50 o 14 0 0 1224.23 1173.50 22.10 o 16 0 0 169.03 177.10 4.08 o 18 0 0 1.42 1.38 0.55 o 20 0 0 91.91 90.50 2.64 o 22 0 0 0.01 0.74 0.52 o 2 1 0 165.45 114.13 3.63 o 3 1 0 2324.90 1934.78 79.55 o 4 1 0 384.80 340.50 3.25 o 5 1 0 1.69 1.72 0.19 o 6 1 0 842.65 822.71 18.43 o 7 1 0 1.44 2.99 0.67 o 8 1 0 808.11 752.19 9.96 o 9 1 0 2.87 2.58 0.44 o 10 1 0 17.44 30.43 0.52 o 11 1 0 59.79 54.18 0.76 o 12 1 0 12.02 6.38 0.34 o 13 1 0 75.93 83.39 1.28 o 14 1 0 0.00 1.04 0.37 o 15 1 0 274.91 271.84 4.07 o 16 1 0 35.11 42.40 1.09 o 17 1 0 21.01 20.81 0.77 o 18 1 0 14.21 14.53 0.68 o 19 1 0 0.01 0.19 0.31 o 20 1 0 1.53 2.43 0.43 o 21 1 0 3.01 2.44 0.62 o 22 1 0 15.54 16.12 0.76 o 0 2 0 696.02 543.79 11.57 o 1 2 0 2.86 1.66 0.18 o 2 2 0 24.66 36.50 0.62 o 3 2 0 593.50 464.95 4.05 o 4 2 0 8.12 16.03 0.30 o 5 2 0 58.75 59.83 0.64 o 6 2 0 1.10 1.28 0.16 o 7 2 0 798.53 964.70 10.44 o 8 2 0 1.02 1.22 0.18 o 9 2 0 133.13 185.08 1.94 o 10 2 0 15.45 14.78 0.40 o 11 2 0 17.57 25.37 0.53 o 12 2 0 36.80 33.30 0.62 o 13 2 0 7.39 16.20 0.47 o 14 2 0 34.86 28.41 0.60 o 15 2 0 13.78 10.61 0.43 o 16 2 0 3.16 3.51 0.34 o 17 2 0 6.16 5.37 0.49 o 18 2 0 19.49 14.34 0.66 o 19 2 0 0.19 0.05 0.29 o 20 2 0 2.25 3.47 0.44 o 21 2 0 14.52 17.50 0.77 o 0 3 0 137.09 97.52 1.56 o 1 3 0 63.14 112.94 1.25 o 2 3 0 40.10 54.72 0.71 o 3 3 0 556.89 512.49 4.47 o 4 3 0 19.89 23.56 0.36 o 5 3 0 12.79 11.82 0.27 o 6 3 0 9.81 10.05 0.27 o 7 3 0 197.17 197.61 2.84 o 8 3 0 76.59 69.60 0.79 o 9 3 0 0.04 0.90 0.20 o 10 3 0 0.07 0.73 0.21 o 11 3 0 55.09 47.48 0.75 o 12 3 0 3.37 2.57 0.41 o 13 3 0 22.53 17.21 0.49 o 14 3 0 3.59 4.13 0.32 o 15 3 0 23.26 15.89 0.49 o 16 3 0 8.94 9.29 0.41 o 17 3 0 23.81 24.93 0.67 o 18 3 0 2.36 3.90 0.37 o 19 3 0 0.76 1.45 0.39 o 20 3 0 2.95 3.48 1.13 o 0 4 0 663.44 679.42 9.23 o 1 4 0 17.32 20.39 0.91 o 2 4 0 81.63 71.06 1.14 o 3 4 0 54.16 53.13 0.96 o 4 4 0 20.09 22.79 0.49 o 5 4 0 69.13 59.91 0.85 o 6 4 0 51.16 51.43 0.78 o 7 4 0 98.62 111.55 1.37 o 8 4 0 21.83 26.94 0.67 o 9 4 0 17.23 17.65 0.59 o 10 4 0 68.92 62.31 1.08 o 11 4 0 70.07 67.04 1.15 o 12 4 0 17.21 19.32 0.62 o 13 4 0 3.12 3.03 0.37 o 14 4 0 97.74 96.70 1.51 o 15 4 0 0.03 0.41 0.30 o 16 4 0 8.38 6.64 0.64 o 17 4 0 1.18 2.04 0.38 o 18 4 0 0.73 0.87 0.35 o 0 5 0 19.29 25.20 0.82 o 1 5 0 21.85 29.18 0.61 o 2 5 0 35.85 39.54 0.88 o 3 5 0 19.60 22.10 0.69 o 4 5 0 56.01 62.04 1.13 o 5 5 0 8.37 10.99 0.56 o 6 5 0 66.36 71.26 1.48 o 7 5 0 1.01 1.95 0.51 o 8 5 0 105.56 108.45 4.70 o 9 5 0 15.30 15.84 0.80 o 10 5 0 8.82 9.41 0.70 o 11 5 0 1.39 1.92 0.57 o 12 5 0 0.00 -0.20 0.47 o 13 5 0 7.85 6.39 0.65 o 14 5 0 0.01 0.20 0.47 o 15 5 0 1.68 1.16 0.50 o 16 5 0 12.18 9.56 0.71 o 0 6 0 1.83 1.50 0.45 o 1 6 0 0.18 1.19 0.31 o 2 6 0 6.69 6.37 0.40 o 3 6 0 10.79 16.15 0.50 o 4 6 0 0.97 1.58 0.48 o 5 6 0 52.50 52.95 1.32 o 6 6 0 2.77 4.38 0.59 o 7 6 0 141.15 142.34 4.76 o 8 6 0 14.64 19.09 1.14 o 9 6 0 91.51 80.54 2.46 o 10 6 0 0.12 1.74 0.56 o 11 6 0 13.53 9.69 0.73 o 12 6 0 3.75 4.54 0.66 o 13 6 0 0.00 -0.27 0.51 o 0 7 0 0.20 0.28 0.41 o 1 7 0 3.40 2.78 0.36 o 2 7 0 1.63 3.08 0.45 o 3 7 0 2.23 2.78 0.45 o 4 7 0 0.03 -0.14 0.44 o 5 7 0 2.32 1.53 0.53 o 6 7 0 15.07 17.07 0.87 o 7 7 0 52.66 48.32 4.02 o 1 0 1 2075.10 1735.18 33.07 o 3 0 1 1949.97 1865.23 65.93 o 5 0 1 30.91 23.04 0.39 o 7 0 1 1082.20 1191.66 10.32 o 9 0 1 18.50 24.91 0.37 o 11 0 1 85.91 67.99 0.88 o 13 0 1 79.63 85.81 1.87 o 15 0 1 286.52 291.87 6.53 o 17 0 1 44.99 43.71 1.12 o 19 0 1 5.12 4.17 0.48 o 21 0 1 15.46 16.48 0.76 o 1 1 1 1740.57 1473.49 11.38 o 2 1 1 590.53 629.24 4.80 o 3 1 1 494.71 460.01 4.38 o 4 1 1 617.77 594.37 6.09 o 5 1 1 115.10 104.76 0.83 o 6 1 1 583.98 573.94 5.88 o 7 1 1 1019.23 1111.78 21.07 o 8 1 1 607.09 595.52 6.20 o 9 1 1 39.03 54.35 0.86 o 10 1 1 8.79 7.19 0.20 o 11 1 1 62.17 54.03 0.58 o 12 1 1 26.29 25.51 0.40 o 13 1 1 74.19 81.29 0.87 o 14 1 1 217.82 210.97 3.46 o 15 1 1 76.81 83.51 1.17 o 16 1 1 69.81 72.04 1.96 o 17 1 1 31.56 30.76 0.66 o 18 1 1 2.17 2.66 0.29 o 19 1 1 6.99 6.36 0.38 o 20 1 1 14.04 15.89 0.52 o 21 1 1 13.64 14.95 0.52 o 22 1 1 11.94 14.09 0.52 o 0 2 1 1240.54 1101.39 31.02 o 1 2 1 514.48 438.23 6.67 o 2 2 1 57.01 90.44 1.96 o 3 2 1 95.10 104.93 1.79 o 4 2 1 24.13 21.72 0.34 o 5 2 1 121.78 115.46 1.67 o 6 2 1 38.50 47.93 0.95 o 7 2 1 108.55 108.98 1.37 o 8 2 1 215.78 218.75 2.71 o 9 2 1 96.66 85.31 1.11 o 10 2 1 5.07 13.05 0.28 o 11 2 1 75.32 66.94 0.87 o 12 2 1 13.44 10.05 0.27 o 13 2 1 21.73 22.36 0.40 o 14 2 1 23.62 24.41 0.42 o 15 2 1 48.00 41.91 0.61 o 16 2 1 7.81 9.93 0.36 o 17 2 1 0.66 0.80 0.21 o 18 2 1 0.15 -0.01 0.19 o 19 2 1 1.53 2.04 0.27 o 20 2 1 1.11 0.93 0.24 o 21 2 1 4.03 4.68 0.53 o 0 3 1 625.79 632.71 15.33 o 1 3 1 95.38 124.96 1.71 o 2 3 1 76.56 67.48 0.71 o 3 3 1 320.26 320.26 4.00 o 4 3 1 162.31 184.42 1.87 o 5 3 1 7.26 9.40 0.19 o 6 3 1 25.57 28.25 0.31 o 7 3 1 75.22 86.95 1.11 o 8 3 1 28.19 30.25 0.35 o 9 3 1 13.16 22.20 0.34 o 10 3 1 84.21 83.59 1.20 o 11 3 1 2.96 2.83 0.19 o 12 3 1 3.79 4.13 0.22 o 13 3 1 5.78 3.58 0.22 o 14 3 1 57.28 48.73 0.58 o 15 3 1 5.51 6.09 0.26 o 16 3 1 10.59 10.18 0.30 o 17 3 1 22.67 19.85 0.54 o 18 3 1 4.21 4.98 0.40 o 19 3 1 5.29 5.60 0.52 o 20 3 1 3.23 3.07 0.37 o 0 4 1 7.44 7.62 0.56 o 1 4 1 67.58 81.33 0.67 o 2 4 1 30.07 28.81 0.34 o 3 4 1 51.98 38.86 0.41 o 4 4 1 89.91 95.57 1.12 o 5 4 1 3.38 1.95 0.18 o 6 4 1 48.80 44.19 0.50 o 7 4 1 44.27 46.38 0.68 o 8 4 1 115.53 99.71 1.02 o 9 4 1 9.59 9.05 0.29 o 10 4 1 29.64 27.39 0.55 o 11 4 1 13.60 16.06 0.41 o 12 4 1 5.68 6.18 0.32 o 13 4 1 25.43 24.53 0.49 o 14 4 1 1.57 1.93 0.25 o 15 4 1 6.63 6.17 0.33 o 16 4 1 2.85 2.28 0.26 o 17 4 1 10.78 10.57 0.39 o 18 4 1 7.00 5.29 0.42 o 0 5 1 25.39 25.54 0.57 o 1 5 1 20.10 24.89 0.44 o 2 5 1 46.88 44.99 0.58 o 3 5 1 2.30 1.41 0.21 o 4 5 1 27.60 23.40 0.49 o 5 5 1 9.96 14.15 0.42 o 6 5 1 90.71 92.68 1.45 o 7 5 1 206.34 218.24 4.57 o 8 5 1 71.01 75.14 1.79 o 9 5 1 16.30 14.77 0.70 o 10 5 1 17.59 19.21 0.58 o 11 5 1 1.56 1.98 0.37 o 12 5 1 14.53 15.86 0.55 o 13 5 1 8.55 7.45 0.58 o 14 5 1 3.61 3.54 0.41 o 15 5 1 7.79 7.91 0.66 o 16 5 1 6.64 7.60 0.47 o 0 6 1 49.52 56.32 1.28 o 1 6 1 7.94 6.54 0.40 o 2 6 1 7.51 9.26 0.50 o 3 6 1 9.36 9.68 0.40 o 4 6 1 3.45 3.79 0.41 o 5 6 1 1.45 1.19 0.32 o 6 6 1 26.94 25.50 0.81 o 7 6 1 3.96 3.58 0.41 o 8 6 1 50.37 48.71 1.43 o 9 6 1 1.94 2.30 0.39 o 10 6 1 17.93 19.99 0.63 o 11 6 1 0.94 0.50 0.37 o 12 6 1 0.66 0.48 0.36 o 0 7 1 11.59 11.00 1.00 o 1 7 1 8.77 9.82 0.54 o 2 7 1 2.53 2.51 0.46 o 3 7 1 1.48 1.43 0.52 o 4 7 1 3.82 3.15 0.34 o 5 7 1 7.25 7.52 1.07 o 6 7 1 11.17 11.16 1.33 o 7 7 1 23.79 22.73 1.44 o 0 0 2 1445.92 1310.45 24.45 o 2 0 2 330.31 337.03 9.18 o 4 0 2 250.87 307.65 12.14 o 6 0 2 367.55 382.31 3.69 o 8 0 2 768.89 813.78 7.68 o 10 0 2 152.19 132.71 1.46 o 12 0 2 110.19 101.65 1.22 o 14 0 2 50.71 36.57 0.99 o 16 0 2 1.64 2.24 0.41 o 18 0 2 19.88 15.54 1.12 o 20 0 2 3.18 3.58 0.48 o 0 1 2 913.54 1006.87 11.32 o 1 1 2 62.18 84.90 0.88 o 2 1 2 148.24 198.52 2.30 o 3 1 2 135.83 90.73 1.66 o 4 1 2 285.31 288.69 3.30 o 5 1 2 13.44 10.95 0.21 o 6 1 2 8.31 7.67 0.22 o 7 1 2 169.26 192.76 1.75 o 8 1 2 39.12 50.27 0.53 o 9 1 2 5.05 8.53 0.24 o 10 1 2 95.78 101.57 0.92 o 11 1 2 9.44 8.84 0.27 o 12 1 2 2.62 3.14 0.21 o 13 1 2 0.74 0.09 0.22 o 14 1 2 35.44 36.10 0.58 o 15 1 2 65.90 59.43 0.81 o 16 1 2 13.20 13.95 0.44 o 17 1 2 0.99 1.51 0.23 o 18 1 2 0.58 0.54 0.24 o 19 1 2 1.70 1.79 0.34 o 20 1 2 1.80 2.37 0.29 o 21 1 2 3.18 5.22 0.37 o 0 2 2 889.59 1045.13 13.01 o 1 2 2 115.97 121.58 0.88 o 2 2 2 817.02 934.03 6.05 o 3 2 2 10.29 15.30 0.25 o 4 2 2 417.64 421.17 2.77 o 5 2 2 70.54 68.66 0.56 o 6 2 2 30.20 32.96 0.34 o 7 2 2 15.74 20.47 0.29 o 8 2 2 18.55 15.16 0.26 o 9 2 2 9.78 8.73 0.26 o 10 2 2 73.94 68.98 0.96 o 11 2 2 8.22 8.30 0.27 o 12 2 2 18.94 18.18 0.36 o 13 2 2 10.75 16.98 0.36 o 14 2 2 64.26 53.47 1.05 o 15 2 2 45.41 52.67 0.75 o 16 2 2 127.71 124.47 2.87 o 17 2 2 1.68 1.52 0.23 o 18 2 2 19.63 20.25 0.49 o 19 2 2 2.38 3.40 0.27 o 20 2 2 0.35 0.63 0.25 o 0 3 2 415.11 379.70 7.11 o 1 3 2 146.69 153.23 1.83 o 2 3 2 32.84 18.86 0.27 o 3 3 2 3.66 3.52 0.17 o 4 3 2 2.41 3.23 0.14 o 5 3 2 21.68 16.52 0.23 o 6 3 2 15.01 12.07 0.22 o 7 3 2 14.21 12.56 0.23 o 8 3 2 82.01 67.88 1.03 o 9 3 2 11.04 12.01 0.28 o 10 3 2 3.18 3.04 0.20 o 11 3 2 6.53 7.11 0.27 o 12 3 2 12.91 15.81 0.39 o 13 3 2 13.64 12.59 0.52 o 14 3 2 33.70 36.31 0.81 o 15 3 2 38.24 32.41 1.20 o 16 3 2 5.48 5.43 0.33 o 17 3 2 4.00 4.20 0.39 o 18 3 2 7.05 5.87 0.46 o 19 3 2 0.53 0.90 0.24 o 0 4 2 19.19 16.96 0.70 o 1 4 2 22.34 18.64 0.39 o 2 4 2 5.03 3.32 0.21 o 3 4 2 36.15 40.06 0.53 o 4 4 2 23.13 18.48 0.32 o 5 4 2 61.41 58.83 0.72 o 6 4 2 41.39 40.36 0.61 o 7 4 2 430.06 418.38 4.82 o 8 4 2 42.02 47.01 0.59 o 9 4 2 102.20 109.06 2.07 o 10 4 2 32.96 34.72 0.64 o 11 4 2 4.26 5.69 0.29 o 12 4 2 5.55 6.13 0.33 o 13 4 2 11.44 10.41 0.36 o 14 4 2 5.83 6.61 0.52 o 15 4 2 4.16 4.60 0.79 o 16 4 2 0.06 0.11 0.65 o 17 4 2 3.79 3.56 0.44 o 0 5 2 46.88 45.44 2.65 o 1 5 2 15.97 12.17 0.55 o 2 5 2 2.93 3.18 0.37 o 3 5 2 15.99 15.78 0.65 o 4 5 2 4.77 5.34 0.32 o 5 5 2 9.61 8.51 0.38 o 6 5 2 51.10 48.57 1.07 o 7 5 2 9.81 11.81 0.41 o 8 5 2 62.20 59.71 1.95 o 9 5 2 21.26 20.96 0.70 o 10 5 2 4.78 4.84 0.42 o 11 5 2 10.92 9.88 0.47 o 12 5 2 2.42 3.01 0.48 o 13 5 2 0.92 1.41 0.62 o 14 5 2 8.50 10.56 1.17 o 15 5 2 3.65 5.03 0.93 o 0 6 2 23.80 23.97 1.03 o 1 6 2 48.90 44.15 2.98 o 2 6 2 0.94 1.72 0.52 o 3 6 2 4.19 4.32 0.59 o 4 6 2 3.28 3.44 0.43 o 5 6 2 0.56 0.70 0.34 o 6 6 2 2.60 3.06 0.38 o 7 6 2 1.46 1.47 0.34 o 8 6 2 0.63 0.62 0.39 o 9 6 2 0.85 0.41 0.32 o 10 6 2 1.33 1.09 0.53 o 11 6 2 0.14 0.31 0.33 o 0 7 2 8.44 8.97 2.34 o 1 7 2 2.28 0.90 0.52 o 2 7 2 3.03 3.91 1.20 o 3 7 2 0.60 1.55 0.56 o 4 7 2 0.42 -0.17 0.54 o 1 0 3 302.25 254.05 8.62 o 3 0 3 626.22 685.27 12.80 o 5 0 3 56.44 55.62 2.09 o 7 0 3 158.27 192.32 2.41 o 9 0 3 3.64 4.95 0.29 o 11 0 3 90.31 63.54 1.08 o 13 0 3 13.33 13.50 0.51 o 15 0 3 29.98 25.29 1.44 o 17 0 3 52.13 50.42 1.70 o 19 0 3 2.13 2.02 0.42 o 0 1 3 635.77 793.17 14.18 o 1 1 3 74.25 98.80 1.11 o 2 1 3 8.11 11.07 0.33 o 3 1 3 187.91 230.02 2.30 o 4 1 3 56.88 55.38 1.03 o 5 1 3 97.93 113.65 1.11 o 6 1 3 56.97 44.37 0.70 o 7 1 3 18.33 18.14 0.42 o 8 1 3 179.36 165.36 1.38 o 9 1 3 68.28 67.11 0.75 o 10 1 3 12.12 16.46 0.33 o 11 1 3 36.62 37.68 0.50 o 12 1 3 6.89 4.92 0.25 o 13 1 3 14.83 13.14 0.34 o 14 1 3 78.46 68.30 1.08 o 15 1 3 1.64 2.13 0.26 o 16 1 3 9.46 8.88 0.39 o 17 1 3 8.07 7.19 0.42 o 18 1 3 3.56 3.60 0.60 o 19 1 3 1.91 1.57 0.27 o 20 1 3 4.49 3.91 0.57 o 0 2 3 93.73 119.35 1.39 o 1 2 3 408.86 392.73 3.09 o 2 2 3 6.85 3.62 0.21 o 3 2 3 25.28 22.51 0.34 o 4 2 3 7.46 7.14 0.22 o 5 2 3 8.33 6.81 0.22 o 6 2 3 3.21 3.43 0.17 o 7 2 3 48.02 47.86 0.51 o 8 2 3 3.84 5.41 0.22 o 9 2 3 10.64 8.60 0.27 o 10 2 3 8.50 11.46 0.30 o 11 2 3 16.80 12.75 0.32 o 12 2 3 8.92 10.52 0.30 o 13 2 3 23.19 25.29 0.43 o 14 2 3 9.60 9.09 0.32 o 15 2 3 75.96 68.19 1.73 o 16 2 3 0.47 0.98 0.21 o 17 2 3 8.51 7.58 0.57 o 18 2 3 2.53 2.52 0.28 o 19 2 3 5.51 5.07 0.51 o 0 3 3 472.25 499.22 5.07 o 1 3 3 126.13 105.70 0.91 o 2 3 3 85.37 93.58 0.90 o 3 3 3 25.88 23.06 0.34 o 4 3 3 44.89 36.19 0.46 o 5 3 3 43.25 39.17 0.43 o 6 3 3 120.10 106.26 0.91 o 7 3 3 137.97 144.01 1.27 o 8 3 3 149.42 145.32 2.10 o 9 3 3 107.99 116.33 1.78 o 10 3 3 73.18 78.25 1.18 o 11 3 3 21.59 23.70 0.55 o 12 3 3 15.99 19.42 0.44 o 13 3 3 7.45 10.26 0.47 o 14 3 3 83.15 82.99 2.09 o 15 3 3 46.81 50.67 1.01 o 16 3 3 17.63 19.00 0.49 o 17 3 3 0.73 0.29 0.32 o 18 3 3 0.19 0.46 0.25 o 0 4 3 119.40 117.65 3.53 o 1 4 3 19.09 22.94 0.45 o 2 4 3 8.04 5.51 0.29 o 3 4 3 25.80 26.77 0.43 o 4 4 3 4.31 3.46 0.27 o 5 4 3 4.85 5.42 0.24 o 6 4 3 86.66 88.38 1.12 o 7 4 3 51.01 52.00 0.63 o 8 4 3 126.92 126.90 1.99 o 9 4 3 5.01 4.72 0.33 o 10 4 3 4.95 6.34 0.36 o 11 4 3 4.02 3.55 0.60 o 12 4 3 6.62 8.68 0.68 o 13 4 3 13.66 13.88 0.78 o 14 4 3 16.38 17.71 0.81 o 15 4 3 5.24 5.46 0.73 o 16 4 3 12.30 13.80 0.99 o 0 5 3 32.43 25.29 3.43 o 1 5 3 36.22 28.43 1.20 o 2 5 3 9.61 7.49 0.56 o 3 5 3 3.53 5.39 0.35 o 4 5 3 3.16 3.66 0.37 o 5 5 3 5.86 5.56 0.82 o 6 5 3 0.75 0.77 0.39 o 7 5 3 48.68 49.20 1.92 o 8 5 3 5.57 4.06 0.58 o 9 5 3 4.73 6.64 0.92 o 10 5 3 0.78 0.80 0.30 o 11 5 3 1.16 1.24 0.45 o 12 5 3 1.96 1.61 1.12 o 13 5 3 8.31 10.62 1.15 o 0 6 3 22.86 21.99 2.30 o 1 6 3 0.42 1.06 0.59 o 2 6 3 2.15 2.40 0.66 o 3 6 3 2.05 3.25 0.92 o 4 6 3 0.10 0.09 0.42 o 5 6 3 0.26 0.58 0.35 o 6 6 3 2.77 2.75 0.59 o 7 6 3 5.95 5.81 1.33 o 8 6 3 2.74 3.75 1.34 o 9 6 3 0.40 0.74 0.83 o 0 0 4 369.35 481.96 9.37 o 2 0 4 5.78 10.69 0.48 o 4 0 4 154.22 139.66 2.22 o 6 0 4 57.61 54.11 3.31 o 8 0 4 87.65 78.10 1.97 o 10 0 4 83.33 89.72 1.68 o 12 0 4 12.99 13.37 0.51 o 14 0 4 82.47 86.01 1.78 o 16 0 4 5.96 5.02 0.58 o 18 0 4 3.08 3.40 0.46 o 0 1 4 12.01 8.82 0.44 o 1 1 4 112.79 105.16 1.24 o 2 1 4 68.68 62.16 1.07 o 3 1 4 64.11 78.58 1.01 o 4 1 4 31.06 31.05 0.56 o 5 1 4 26.58 27.80 1.18 o 6 1 4 6.05 7.28 0.49 o 7 1 4 185.48 187.55 3.21 o 8 1 4 3.45 4.18 0.24 o 9 1 4 11.18 8.60 0.33 o 10 1 4 26.44 27.38 0.53 o 11 1 4 46.97 45.73 0.91 o 12 1 4 7.95 7.91 0.36 o 13 1 4 21.41 20.40 0.55 o 14 1 4 0.83 0.82 0.23 o 15 1 4 10.41 8.55 0.36 o 16 1 4 7.28 6.87 0.56 o 17 1 4 4.42 3.06 0.46 o 18 1 4 7.62 5.74 1.06 o 0 2 4 30.64 34.66 0.77 o 1 2 4 1.34 0.16 0.13 o 2 2 4 1.18 1.41 0.16 o 3 2 4 35.63 43.45 0.66 o 4 2 4 0.34 0.19 0.15 o 5 2 4 13.04 13.50 0.42 o 6 2 4 325.01 322.40 4.03 o 7 2 4 41.16 48.50 0.60 o 8 2 4 367.84 380.80 2.95 o 9 2 4 22.59 24.59 0.43 o 10 2 4 4.59 5.85 0.27 o 11 2 4 11.07 10.70 0.31 o 12 2 4 11.08 9.64 0.30 o 13 2 4 2.95 2.61 0.24 o 14 2 4 15.81 14.77 0.51 o 15 2 4 7.52 8.45 0.36 o 16 2 4 4.13 4.67 0.50 o 17 2 4 4.98 5.01 0.51 o 0 3 4 186.58 200.09 2.45 o 1 3 4 37.82 35.94 0.52 o 2 3 4 15.44 21.50 0.40 o 3 3 4 18.12 14.55 0.36 o 4 3 4 18.02 18.60 0.46 o 5 3 4 7.66 8.01 0.28 o 6 3 4 12.25 12.90 0.33 o 7 3 4 133.49 128.26 1.29 o 8 3 4 36.33 38.26 0.58 o 9 3 4 15.44 12.93 0.36 o 10 3 4 12.03 13.86 0.37 o 11 3 4 3.77 5.14 0.33 o 12 3 4 3.85 5.25 0.41 o 13 3 4 11.76 11.72 0.37 o 14 3 4 34.02 37.88 0.88 o 15 3 4 5.39 5.97 0.57 o 16 3 4 11.59 12.54 0.91 o 0 4 4 43.69 40.72 0.92 o 1 4 4 169.92 151.77 1.87 o 2 4 4 0.36 0.91 0.29 o 3 4 4 16.87 16.45 0.42 o 4 4 4 10.56 10.59 0.41 o 5 4 4 6.73 5.88 0.29 o 6 4 4 9.44 8.73 0.35 o 7 4 4 16.44 17.34 0.66 o 8 4 4 4.55 5.15 0.58 o 9 4 4 1.07 1.50 0.25 o 10 4 4 9.45 8.16 0.36 o 11 4 4 2.04 1.37 0.26 o 12 4 4 0.46 0.17 0.34 o 13 4 4 18.26 21.26 1.15 o 14 4 4 12.39 13.69 1.08 o 0 5 4 37.49 34.92 2.83 o 1 5 4 16.51 18.21 1.07 o 2 5 4 5.82 3.34 0.87 o 3 5 4 5.42 4.54 0.53 o 4 5 4 4.86 3.37 0.53 o 5 5 4 1.68 1.85 0.35 o 6 5 4 3.87 4.42 0.49 o 7 5 4 3.86 3.38 0.90 o 8 5 4 2.77 1.64 0.45 o 9 5 4 6.86 8.07 0.99 o 10 5 4 1.73 3.70 1.02 o 11 5 4 3.82 4.83 1.52 o 0 6 4 7.67 6.47 3.25 o 1 6 4 1.85 4.00 1.09 o 2 6 4 0.70 2.09 0.56 o 3 6 4 4.89 5.21 0.92 o 4 6 4 0.54 0.81 0.43 o 5 6 4 5.55 6.22 1.35 o 1 0 5 89.86 111.55 1.95 o 3 0 5 58.45 58.30 1.76 o 5 0 5 13.22 14.07 0.85 o 7 0 5 82.41 87.75 7.29 o 9 0 5 12.25 11.84 0.60 o 11 0 5 6.19 5.82 0.51 o 13 0 5 5.31 5.09 0.41 o 15 0 5 11.25 7.58 0.56 o 0 1 5 3.64 4.71 0.75 o 1 1 5 13.07 10.43 0.37 o 2 1 5 24.72 28.13 0.58 o 3 1 5 0.04 0.01 0.22 o 4 1 5 17.83 15.86 0.45 o 5 1 5 30.73 34.31 1.19 o 6 1 5 86.27 97.20 1.87 o 7 1 5 75.25 85.12 2.09 o 8 1 5 109.61 117.66 3.14 o 9 1 5 31.11 32.12 0.60 o 10 1 5 7.54 8.07 0.34 o 11 1 5 5.37 5.26 0.31 o 12 1 5 11.00 10.12 0.38 o 13 1 5 1.88 1.29 0.36 o 14 1 5 1.71 0.75 0.31 o 15 1 5 4.34 4.56 0.52 o 16 1 5 6.40 6.09 0.35 o 0 2 5 23.02 30.62 0.82 o 1 2 5 10.96 9.08 0.32 o 2 2 5 3.12 2.38 0.23 o 3 2 5 31.65 32.03 0.66 o 4 2 5 7.20 6.71 0.30 o 5 2 5 9.78 8.92 0.34 o 6 2 5 7.51 8.14 0.27 o 7 2 5 111.91 114.92 1.57 o 8 2 5 10.40 11.66 0.38 o 9 2 5 24.58 25.42 0.53 o 10 2 5 5.44 5.76 0.33 o 11 2 5 12.23 11.82 0.40 o 12 2 5 2.77 2.98 0.28 o 13 2 5 7.39 7.01 0.58 o 14 2 5 9.75 10.25 0.47 o 15 2 5 1.69 2.41 0.53 o 0 3 5 41.22 30.91 0.94 o 1 3 5 64.08 55.83 1.15 o 2 3 5 12.99 10.01 0.41 o 3 3 5 0.60 0.39 0.22 o 4 3 5 1.66 1.63 0.26 o 5 3 5 3.14 3.07 0.31 o 6 3 5 24.60 25.59 0.57 o 7 3 5 6.47 6.16 0.36 o 8 3 5 20.86 22.15 0.61 o 9 3 5 0.31 -0.19 0.21 o 10 3 5 0.21 0.04 0.23 o 11 3 5 0.63 0.80 0.30 o 12 3 5 0.99 0.31 0.29 o 13 3 5 6.24 7.00 1.17 o 14 3 5 6.15 7.51 0.51 o 0 4 5 67.30 65.70 2.06 o 1 4 5 3.22 2.76 0.36 o 2 4 5 4.32 4.20 0.32 o 3 4 5 6.63 5.20 0.34 o 4 4 5 0.69 0.30 0.23 o 5 4 5 0.32 0.13 0.21 o 6 4 5 0.40 0.31 0.22 o 7 4 5 5.05 4.96 0.62 o 8 4 5 2.34 3.24 0.48 o 9 4 5 2.84 3.11 0.48 o 10 4 5 1.68 1.72 0.51 o 11 4 5 1.06 1.69 0.86 o 0 5 5 12.87 8.81 1.05 o 1 5 5 20.01 20.54 1.18 o 2 5 5 9.07 7.42 0.49 o 3 5 5 1.11 1.31 0.44 o 4 5 5 6.34 5.33 0.68 o 5 5 5 2.14 1.63 0.32 o 6 5 5 6.56 7.30 1.12 o 7 5 5 5.98 6.56 1.15 o 0 0 6 10.37 9.06 0.79 o 2 0 6 8.91 9.82 0.57 o 4 0 6 23.50 30.68 2.37 o 6 0 6 58.09 74.89 10.34 o 8 0 6 105.18 107.38 5.28 o 10 0 6 32.94 31.90 1.00 o 12 0 6 2.94 2.98 0.81 o 0 1 6 21.05 20.80 0.76 o 1 1 6 11.88 17.16 0.49 o 2 1 6 1.96 2.14 0.27 o 3 1 6 5.62 5.17 0.34 o 4 1 6 1.58 0.79 0.25 o 5 1 6 2.09 1.29 0.25 o 6 1 6 18.69 23.93 1.78 o 7 1 6 38.23 40.47 0.91 o 8 1 6 19.60 22.31 0.53 o 9 1 6 19.93 20.87 0.52 o 10 1 6 4.12 4.20 0.47 o 11 1 6 1.47 1.72 0.26 o 12 1 6 0.66 0.17 0.32 o 13 1 6 1.36 0.84 0.30 o 0 2 6 11.17 11.72 0.59 o 1 2 6 49.87 48.66 0.76 o 2 2 6 2.79 2.94 0.26 o 3 2 6 3.65 2.68 0.26 o 4 2 6 0.16 -0.20 0.19 o 5 2 6 4.37 4.10 0.35 o 6 2 6 1.44 1.50 0.25 o 7 2 6 0.29 0.01 0.31 o 8 2 6 5.27 6.20 0.49 o 9 2 6 0.76 0.36 0.25 o 10 2 6 0.40 0.25 0.24 o 11 2 6 0.26 -0.17 0.32 o 0 3 6 17.46 18.14 1.40 o 1 3 6 0.18 0.03 0.25 o 2 3 6 0.75 0.78 0.27 o 3 3 6 0.84 0.58 0.26 o 4 3 6 0.20 0.06 0.25 o 5 3 6 0.50 0.28 0.26 o 6 3 6 5.50 5.30 0.46 o 7 3 6 0.57 0.05 0.43 o 8 3 6 6.73 7.14 0.49 o 9 3 6 1.52 0.75 0.34 o 0 4 6 1.62 2.03 0.45 o 1 4 6 5.52 5.15 0.38 o 2 4 6 0.01 -0.34 0.23 o 3 4 6 1.12 0.71 0.27 o 4 4 6 3.14 3.62 0.36 o 5 4 6 0.53 0.40 0.30 o 1 0 7 0.35 -0.52 0.64 o 3 0 7 0.86 1.98 0.76 o 5 0 7 7.62 8.65 1.15 o 7 0 7 87.66 121.05 32.71 o 0 1 7 4.99 4.82 0.52 o 1 1 7 9.68 9.55 0.45 o 2 1 7 1.05 0.46 0.27 o 3 1 7 1.97 1.36 0.29 o 4 1 7 2.36 2.84 0.35 o 5 1 7 1.23 1.97 0.33 o 6 1 7 20.58 28.68 3.61 o 7 1 7 7.16 12.09 2.71 o 0 2 7 17.62 17.66 1.10 o 1 2 7 0.71 1.01 0.48 o 2 2 7 2.61 2.21 0.38 o 3 2 7 3.96 5.94 0.40 o 4 2 7 0.22 -0.38 0.25 o