#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2212030.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212030_Fobs loop_ _publ_author_name 'Turner, David R.' 'Batten, Stuart R.' _publ_section_title ; catena-Poly[[copper(II)-bis(\m-3-carboxypyridine-2-carboxylato)-\k^3^N,O^2^:O^3^;\k^3^O^3^:N,O^2^] methanol disolvate] ; _journal_coeditor_code BI2129 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m452 _journal_page_last m454 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.136 _cell_angle_gamma 90.000 _cell_length_a 6.6850 _cell_length_b 9.7739 _cell_length_c 13.2657 _exptl_crystal_F_000 470.00 _reflns_d_resolution_high 0.8413 _[local]_cod_data_source_file bi2129Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' DT125AC in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 153.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 431.69 442.98 8.59 o 4 0 0 1650.03 1627.52 91.08 o 1 1 0 388.49 384.39 5.32 o 2 1 0 12.32 10.26 1.62 o 3 1 0 265.07 352.51 8.96 o 4 1 0 152.65 185.16 5.38 o 5 1 0 1122.97 1149.98 26.12 o 7 1 0 12.77 6.89 5.79 o 0 2 0 510.47 595.40 14.31 o 1 2 0 5728.16 5775.52 46.01 o 2 2 0 2245.92 2114.92 23.30 o 3 2 0 6.00 7.31 2.15 o 4 2 0 1794.34 1830.05 57.21 o 5 2 0 94.16 116.10 12.56 o 6 2 0 188.82 179.04 16.02 o 7 2 0 268.41 263.22 21.74 o 1 3 0 613.86 669.19 10.31 o 2 3 0 1557.09 1636.79 23.17 o 3 3 0 1544.40 1432.14 26.90 o 4 3 0 1194.27 1193.70 27.98 o 5 3 0 139.46 145.91 10.88 o 6 3 0 8.46 10.18 7.58 o 7 3 0 292.13 272.72 26.60 o 0 4 0 2356.67 2257.36 35.79 o 1 4 0 138.49 160.66 7.73 o 2 4 0 3819.35 3709.80 57.67 o 3 4 0 0.02 2.17 1.60 o 4 4 0 2381.20 2345.80 34.98 o 5 4 0 42.27 58.29 16.45 o 6 4 0 754.22 685.85 41.37 o 7 4 0 12.26 1.67 11.07 o 1 5 0 2724.27 2598.84 35.62 o 2 5 0 1.19 1.36 3.40 o 3 5 0 57.10 44.55 5.44 o 4 5 0 21.95 14.89 4.96 o 5 5 0 1061.90 1080.52 24.10 o 6 5 0 0.74 -5.30 6.94 o 7 5 0 322.16 324.46 35.75 o 0 6 0 348.46 310.80 33.39 o 1 6 0 492.75 507.00 18.60 o 2 6 0 1628.80 1473.16 39.50 o 3 6 0 64.80 60.39 8.05 o 4 6 0 995.16 991.64 25.38 o 5 6 0 19.31 26.38 4.95 o 6 6 0 42.58 47.38 13.64 o 1 7 0 64.93 53.92 4.52 o 2 7 0 0.15 -3.61 4.66 o 3 7 0 208.48 209.59 30.06 o 4 7 0 0.11 6.33 6.34 o 5 7 0 179.05 160.18 11.98 o 0 8 0 3274.70 3384.85 75.50 o 1 8 0 66.64 55.93 8.05 o 2 8 0 1186.02 1149.36 38.50 o 3 8 0 0.34 -2.23 8.07 o 4 8 0 929.55 880.05 31.73 o 5 8 0 17.94 16.12 5.77 o 1 9 0 369.53 386.11 22.62 o 2 9 0 2.10 12.20 7.22 o 3 9 0 25.64 15.52 8.54 o 4 9 0 33.16 29.40 8.60 o 5 9 0 219.15 236.47 17.48 o 0 10 0 1092.50 1080.39 58.81 o 1 10 0 85.81 82.08 17.65 o 2 10 0 250.87 247.18 21.62 o 3 10 0 8.24 14.57 7.55 o 4 10 0 243.28 250.26 21.01 o 1 11 0 118.54 129.51 27.77 o 2 11 0 32.67 23.24 17.96 o -7 0 1 3.00 3.09 4.00 o -5 0 1 1943.15 1870.77 54.03 o -3 0 1 729.94 619.46 21.13 o -1 0 1 8.49 17.33 7.37 o 1 0 1 1505.37 1595.77 17.76 o 3 0 1 130.07 105.49 5.18 o 5 0 1 673.89 683.29 22.09 o -7 1 1 72.96 56.43 10.92 o -6 1 1 664.77 672.24 28.71 o -5 1 1 38.49 47.04 4.19 o -4 1 1 1392.57 1365.00 34.52 o -3 1 1 7.24 18.23 1.89 o -2 1 1 24.26 48.02 2.31 o -1 1 1 0.25 9.16 1.45 o 0 1 1 6880.14 7426.43 87.46 o 1 1 1 144.21 124.24 2.86 o 2 1 1 2452.89 2301.47 24.02 o 3 1 1 6.52 14.20 2.26 o 4 1 1 613.60 624.72 9.66 o 5 1 1 2.33 22.39 5.26 o 6 1 1 797.76 763.66 44.39 o -7 2 1 1155.74 1135.20 50.10 o -6 2 1 110.07 107.15 14.45 o -5 2 1 1139.50 1135.02 25.65 o -4 2 1 8.02 8.29 3.34 o -3 2 1 2620.38 2545.19 37.63 o -2 2 1 7248.15 7349.05 67.01 o -1 2 1 23691.75 23329.21 261.24 o 0 2 1 46.84 44.99 1.90 o 1 2 1 2254.97 2223.51 24.44 o 2 2 1 38.69 34.99 3.04 o 3 2 1 4654.52 4826.12 59.99 o 4 2 1 450.26 486.84 14.96 o 5 2 1 4164.32 3995.60 84.91 o 6 2 1 103.45 110.90 10.95 o 7 2 1 179.49 162.38 17.81 o -7 3 1 471.18 396.01 31.43 o -6 3 1 574.48 620.88 36.71 o -5 3 1 12.63 8.24 5.66 o -4 3 1 173.01 163.50 7.02 o -3 3 1 24.34 21.76 2.73 o -2 3 1 4853.07 4830.87 57.12 o -1 3 1 8046.47 8166.12 106.30 o 0 3 1 39.31 32.05 2.35 o 1 3 1 45.51 50.51 2.92 o 2 3 1 5.39 15.59 2.84 o 3 3 1 61.04 54.01 4.92 o 4 3 1 2001.97 2069.80 33.40 o 5 3 1 407.00 454.80 15.14 o 6 3 1 3.52 4.51 7.88 o 7 3 1 23.64 18.70 10.38 o -7 4 1 450.71 464.24 37.96 o -6 4 1 0.26 5.35 8.10 o -5 4 1 353.30 376.82 34.95 o -4 4 1 60.74 68.85 8.55 o -3 4 1 109.06 80.38 5.01 o -2 4 1 228.29 248.87 16.21 o -1 4 1 3574.61 3396.65 51.92 o 0 4 1 6.15 4.09 2.40 o 1 4 1 3445.57 3169.06 42.54 o 2 4 1 24.53 37.15 3.30 o 3 4 1 1320.22 1267.47 19.58 o 4 4 1 51.22 65.74 4.58 o 5 4 1 472.65 511.41 17.26 o 6 4 1 0.04 2.13 6.97 o 7 4 1 810.05 953.12 52.75 o -7 5 1 90.16 128.49 25.22 o -6 5 1 691.69 655.11 44.46 o -5 5 1 197.24 188.93 13.96 o -4 5 1 6.08 14.16 3.40 o -3 5 1 74.33 77.55 23.52 o -2 5 1 1018.12 1010.55 28.25 o -1 5 1 1715.75 1801.99 29.31 o 0 5 1 1976.80 1984.71 30.08 o 1 5 1 119.25 112.88 7.93 o 2 5 1 42.37 69.25 6.12 o 3 5 1 168.86 178.54 11.61 o 4 5 1 259.70 284.71 9.45 o 5 5 1 238.10 241.80 9.06 o 6 5 1 313.62 340.31 33.79 o 7 5 1 7.97 5.72 8.49 o -5 6 1 1329.28 1236.23 33.06 o -4 6 1 149.06 127.20 10.76 o -3 6 1 749.38 750.54 20.28 o -2 6 1 111.27 116.35 10.84 o -1 6 1 3556.32 3469.53 49.84 o 0 6 1 110.07 124.00 7.03 o 1 6 1 2977.37 2809.06 49.18 o 2 6 1 197.27 202.81 20.90 o 3 6 1 820.19 857.48 20.79 o 4 6 1 18.23 22.65 3.65 o 5 6 1 1638.58 1637.07 77.66 o 6 6 1 0.01 2.77 7.88 o -5 7 1 56.19 38.28 7.26 o -4 7 1 107.45 105.58 11.26 o -3 7 1 0.10 2.04 4.88 o -2 7 1 515.94 476.79 17.26 o -1 7 1 13.61 11.45 4.43 o 0 7 1 1857.98 1867.70 33.99 o 1 7 1 123.57 130.34 7.61 o 2 7 1 55.91 34.85 11.15 o 3 7 1 1.71 0.03 4.81 o 4 7 1 701.23 685.92 22.19 o 5 7 1 1.92 5.13 4.66 o 6 7 1 419.13 389.66 40.63 o -5 8 1 460.76 458.90 21.94 o -4 8 1 268.19 302.03 22.32 o -3 8 1 596.36 551.06 24.94 o -2 8 1 737.97 723.38 29.47 o -1 8 1 191.31 190.00 16.42 o 0 8 1 0.33 1.32 3.76 o 1 8 1 457.51 428.68 22.25 o 2 8 1 176.48 188.43 16.50 o 3 8 1 512.77 534.63 28.52 o 4 8 1 604.25 608.00 25.85 o 5 8 1 110.89 122.94 21.49 o -5 9 1 78.80 75.34 11.05 o -4 9 1 381.15 343.40 33.72 o -3 9 1 44.02 37.26 8.95 o -2 9 1 187.97 205.69 25.58 o -1 9 1 146.10 142.07 16.11 o 0 9 1 368.48 355.88 22.02 o 1 9 1 144.88 166.80 19.47 o 2 9 1 561.76 547.01 27.06 o 3 9 1 110.67 114.53 14.44 o 4 9 1 346.76 341.81 21.33 o -4 10 1 36.41 29.21 9.58 o -3 10 1 206.06 194.12 19.43 o -2 10 1 1.32 -5.57 5.57 o -1 10 1 795.49 768.67 34.70 o 0 10 1 147.27 146.49 17.83 o 1 10 1 373.39 349.83 24.99 o 2 10 1 10.25 11.69 8.02 o 3 10 1 258.06 279.61 22.54 o -2 11 1 27.75 30.70 10.21 o -1 11 1 9.69 10.07 7.37 o 0 11 1 70.35 72.63 13.22 o 1 11 1 56.19 54.95 12.75 o 2 11 1 190.34 208.79 34.01 o -6 0 2 821.29 823.23 28.39 o -4 0 2 4.95 -0.88 3.19 o -2 0 2 322.69 342.98 7.80 o 0 0 2 13567.65 13686.07 205.47 o 2 0 2 8.30 11.17 1.67 o 4 0 2 1359.34 1357.88 25.93 o 6 0 2 2399.75 2434.21 92.30 o -7 1 2 657.42 624.37 33.20 o -6 1 2 32.73 38.23 9.15 o -5 1 2 1445.86 1445.98 26.52 o -4 1 2 227.66 289.41 9.10 o -3 1 2 2366.26 2375.43 30.85 o -2 1 2 259.79 277.77 5.61 o -1 1 2 8540.88 8551.02 99.86 o 0 1 2 191.36 198.22 7.11 o 1 1 2 3457.27 3541.12 29.65 o 2 1 2 206.03 195.40 4.20 o 3 1 2 1166.13 1171.44 13.87 o 4 1 2 289.99 327.15 6.44 o 5 1 2 1842.71 1903.80 44.32 o 6 1 2 182.74 168.56 17.42 o 7 1 2 113.54 102.95 20.90 o -7 2 2 2.46 3.31 8.71 o -6 2 2 231.33 250.51 21.35 o -4 2 2 45.78 45.44 4.20 o -3 2 2 4.40 21.24 3.07 o -2 2 2 2529.06 2428.68 31.00 o -1 2 2 5023.05 5063.66 59.51 o 0 2 2 241.02 209.81 5.14 o 1 2 2 44.58 52.89 2.68 o 2 2 2 137.70 104.93 3.91 o 3 2 2 111.86 118.47 6.57 o 4 2 2 1787.12 1771.95 34.45 o 5 2 2 857.28 834.16 20.18 o 6 2 2 80.92 77.55 21.95 o 7 2 2 2.24 -2.22 4.85 o -7 3 2 847.79 832.75 47.92 o -6 3 2 362.82 384.31 30.28 o -5 3 2 203.68 214.51 9.37 o -4 3 2 4.42 25.08 7.07 o -3 3 2 1210.73 1219.72 20.53 o -2 3 2 73.03 110.65 4.44 o -1 3 2 7974.30 8092.41 91.25 o 0 3 2 5652.86 5898.50 68.10 o 1 3 2 186.63 135.67 5.69 o 2 3 2 163.82 186.14 7.46 o 3 3 2 3499.03 3464.95 40.65 o 4 3 2 1.62 11.37 3.89 o 5 3 2 936.99 961.60 21.54 o 6 3 2 536.06 509.21 19.88 o 7 3 2 194.29 214.61 17.69 o -7 4 2 46.63 18.92 11.83 o -6 4 2 987.10 926.72 51.45 o -5 4 2 77.08 82.70 10.60 o -4 4 2 806.51 822.10 23.67 o -3 4 2 105.37 101.92 5.01 o -2 4 2 5702.08 5558.18 77.93 o -1 4 2 103.32 105.54 5.91 o 0 4 2 1404.19 1370.95 17.60 o 1 4 2 364.25 414.68 12.82 o 2 4 2 1415.78 1420.84 24.26 o 3 4 2 22.68 15.46 2.73 o 4 4 2 2972.51 2953.41 41.98 o 5 4 2 4.04 1.41 2.83 o 6 4 2 42.30 46.03 8.50 o 7 4 2 3.04 3.46 10.23 o -6 5 2 35.96 25.93 6.18 o -5 5 2 678.17 660.60 22.04 o -4 5 2 1.12 7.44 3.18 o -3 5 2 226.38 211.22 9.82 o -2 5 2 2295.44 2298.81 34.61 o -1 5 2 947.18 866.90 20.25 o 0 5 2 203.41 198.14 7.52 o 1 5 2 1369.17 1266.64 20.87 o 2 5 2 304.69 303.02 10.70 o 3 5 2 1215.28 1136.40 19.92 o 4 5 2 375.83 354.16 10.80 o 5 5 2 209.70 234.87 8.95 o 6 5 2 0.31 1.98 4.57 o 7 5 2 275.24 294.50 32.88 o -6 6 2 159.46 168.41 12.69 o -4 6 2 341.69 360.90 17.31 o -3 6 2 280.60 271.84 12.16 o -2 6 2 245.75 233.02 11.34 o -1 6 2 916.41 887.39 20.28 o 0 6 2 405.91 392.45 14.13 o 1 6 2 0.52 5.72 5.56 o 2 6 2 1287.29 1189.80 28.65 o 3 6 2 206.79 188.51 8.61 o 4 6 2 93.69 114.34 7.29 o 5 6 2 475.97 486.88 14.02 o 6 6 2 147.66 189.27 28.34 o -5 7 2 379.42 403.72 19.29 o -4 7 2 38.06 27.93 6.71 o -3 7 2 2651.12 2529.09 47.20 o -2 7 2 195.88 205.00 12.18 o -1 7 2 908.48 859.14 24.52 o 0 7 2 49.53 55.35 7.47 o 1 7 2 633.44 632.73 46.16 o 2 7 2 517.09 495.67 22.43 o 3 7 2 2051.40 2048.43 34.38 o 4 7 2 203.53 223.02 13.12 o 5 7 2 326.90 320.46 14.62 o 6 7 2 78.63 93.02 23.16 o -5 8 2 48.61 43.91 8.37 o -4 8 2 131.22 136.87 23.80 o -3 8 2 0.23 -0.72 8.93 o -2 8 2 463.85 477.60 38.69 o -1 8 2 98.00 86.86 12.07 o 0 8 2 630.47 645.26 28.01 o 1 8 2 2.69 -0.38 11.19 o 2 8 2 230.88 248.42 18.45 o 3 8 2 30.00 29.60 8.49 o 4 8 2 866.97 881.14 27.57 o 5 8 2 8.78 8.45 7.08 o -4 9 2 120.51 104.66 16.91 o -3 9 2 11.29 20.47 7.35 o -2 9 2 9.46 8.61 7.38 o -1 9 2 1555.73 1528.69 100.38 o 0 9 2 93.03 80.30 12.99 o 1 9 2 488.61 494.36 26.16 o 2 9 2 105.82 90.53 13.55 o 3 9 2 6.00 7.09 6.02 o 4 9 2 20.56 17.21 6.78 o -3 10 2 141.58 111.21 26.49 o -2 10 2 31.61 38.63 12.77 o -1 10 2 11.02 21.14 8.81 o 0 10 2 513.60 515.26 28.19 o 1 10 2 17.98 2.42 6.71 o 2 10 2 69.83 58.16 11.93 o 3 10 2 543.29 473.51 26.64 o -2 11 2 56.66 42.14 12.18 o -1 11 2 395.75 337.08 26.34 o 0 11 2 195.71 198.33 21.51 o 1 11 2 249.25 271.15 24.54 o 2 11 2 2.86 -0.71 6.90 o -7 0 3 137.16 158.97 16.61 o -5 0 3 346.52 293.43 27.70 o -3 0 3 4443.46 4612.59 62.75 o 1 0 3 2708.46 2781.49 50.07 o 3 0 3 2881.84 3002.57 38.21 o 5 0 3 161.10 172.94 9.33 o 7 0 3 445.59 418.83 37.76 o -7 1 3 542.29 519.36 29.92 o -6 1 3 728.47 737.21 35.75 o -5 1 3 83.34 127.86 8.40 o -4 1 3 2731.57 2772.90 42.74 o -3 1 3 1018.31 1152.32 18.01 o -2 1 3 933.39 902.94 13.39 o -1 1 3 3809.07 3856.31 46.45 o 0 1 3 4355.63 4134.83 59.89 o 1 1 3 1976.50 2038.20 22.29 o 2 1 3 7985.64 8023.98 76.23 o 3 1 3 869.55 1049.62 13.66 o 4 1 3 356.68 344.04 7.15 o 5 1 3 38.45 35.25 3.78 o 6 1 3 590.27 610.24 20.52 o 7 1 3 156.45 104.45 16.15 o -7 2 3 305.26 279.81 27.65 o -6 2 3 52.71 26.87 9.20 o -5 2 3 43.96 61.46 6.06 o -4 2 3 227.77 257.61 13.99 o -3 2 3 1002.17 1006.23 24.98 o -2 2 3 778.51 831.68 14.04 o -1 2 3 2044.75 2092.84 28.27 o 0 2 3 698.52 733.16 15.53 o 1 2 3 138.16 194.88 6.71 o 2 2 3 82.03 68.77 2.53 o 3 2 3 2056.76 2132.27 28.34 o 4 2 3 268.08 273.64 8.10 o 5 2 3 675.42 642.18 14.37 o 6 2 3 1.18 2.60 3.45 o 7 2 3 11.06 22.52 8.86 o -5 3 3 13.89 28.24 8.56 o -4 3 3 648.51 628.76 19.95 o -3 3 3 164.25 135.36 6.91 o -2 3 3 9824.77 10075.10 129.76 o -1 3 3 1212.13 1289.26 18.91 o 0 3 3 2792.71 2606.06 35.46 o 1 3 3 272.37 290.27 7.98 o 2 3 3 1229.54 1094.26 16.01 o 3 3 3 9.70 13.55 2.59 o 4 3 3 5775.57 5981.38 74.41 o 5 3 3 304.10 314.03 12.18 o 6 3 3 205.11 213.02 9.25 o 7 3 3 52.59 50.32 8.37 o -5 4 3 20.48 37.37 9.59 o -4 4 3 385.02 395.51 28.15 o -3 4 3 78.62 97.53 5.24 o -2 4 3 488.89 493.62 17.23 o -1 4 3 1234.46 1223.85 19.85 o 0 4 3 173.36 193.32 7.19 o 1 4 3 86.18 147.06 6.87 o 2 4 3 502.42 525.64 13.42 o 3 4 3 44.90 40.58 3.96 o 4 4 3 206.77 224.72 8.00 o 5 4 3 119.56 128.04 6.49 o 6 4 3 17.24 16.60 10.74 o 7 4 3 137.45 146.01 25.87 o -6 5 3 796.71 817.91 32.78 o -5 5 3 41.33 25.90 10.31 o -4 5 3 661.53 625.84 22.72 o -3 5 3 2.66 4.06 2.85 o -2 5 3 9050.55 8989.93 122.06 o -1 5 3 1103.78 1170.30 19.75 o 0 5 3 3779.95 3737.83 44.67 o 1 5 3 171.73 185.99 8.39 o 2 5 3 2820.25 2736.77 41.38 o 3 5 3 0.05 3.50 3.20 o 4 5 3 3361.74 3394.02 68.06 o 5 5 3 572.34 532.11 13.49 o 6 5 3 575.46 650.73 28.44 o -6 6 3 371.70 298.11 19.68 o -5 6 3 105.52 134.89 11.93 o -4 6 3 64.17 65.22 6.47 o -3 6 3 888.57 819.64 21.99 o -2 6 3 13.91 10.82 4.00 o -1 6 3 381.11 391.87 14.93 o 0 6 3 776.84 821.93 22.63 o 1 6 3 69.09 73.00 6.44 o 2 6 3 760.37 725.72 18.69 o 3 6 3 1482.95 1533.28 25.95 o 4 6 3 26.42 24.12 4.03 o 5 6 3 105.13 100.78 7.16 o 6 6 3 0.36 -0.81 8.44 o -6 7 3 160.45 177.03 15.78 o -5 7 3 138.05 118.47 8.79 o -4 7 3 19.83 31.44 5.58 o -3 7 3 1373.29 1276.72 33.98 o -2 7 3 1647.06 1509.33 55.64 o -1 7 3 113.60 107.53 9.84 o 0 7 3 412.32 442.50 17.14 o 1 7 3 161.12 161.53 14.74 o 2 7 3 59.45 42.68 9.03 o 3 7 3 446.09 420.09 21.28 o 4 7 3 796.99 790.05 19.81 o 5 7 3 46.75 33.61 5.95 o 6 7 3 116.46 122.02 24.83 o -5 8 3 142.07 129.81 17.27 o -4 8 3 53.84 51.77 9.82 o -3 8 3 230.30 274.03 20.77 o -2 8 3 10.32 14.70 6.47 o -1 8 3 395.42 401.31 22.10 o 0 8 3 84.73 63.34 10.59 o 1 8 3 551.84 517.14 25.17 o 2 8 3 335.08 315.46 19.74 o 3 8 3 141.49 140.97 12.32 o 4 8 3 37.44 47.86 9.43 o 5 8 3 214.63 222.69 14.05 o -4 9 3 1295.12 1268.66 43.97 o -3 9 3 0.85 7.86 9.99 o -2 9 3 129.74 144.46 16.68 o -1 9 3 0.02 -0.21 5.53 o 0 9 3 763.17 778.14 33.29 o 1 9 3 27.92 26.45 8.58 o 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