#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/20/2212035.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212035_Fobs loop_ _publ_author_name 'Fu, Wei-Wei' 'Xie, Zai-Lai' 'Chen, Zhong-Ning' _publ_section_title ; catena-Poly[[[[\m-bis(diphenylphosphino)amine-\k^2^P:P']bis[acetonitrilecopper(I)]]-\m-(1,2-dicyanoethylene-1,2-dithiolato)-[(1,2-dicyanoethylene-1,2-dithiolato)molybdenate(IV)]-\m-1,2-dicyanoethylene-1,2-dithiolato] acetonitrile disolvate] ; _journal_coeditor_code BI2137 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m509 _journal_page_last m511 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 82.079 _cell_angle_beta 79.725 _cell_angle_gamma 88.113 _cell_length_a 12.6197 _cell_length_b 12.8711 _cell_length_c 23.4970 _exptl_crystal_F_000 1592.00 _reflns_d_resolution_high 0.8389 _[local]_cod_data_source_file bi2137Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' x in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 312.09 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 14761.46 7244.61 2310.12 o 2 0 0 150.29 308.75 15.21 o 3 0 0 10132.84 11834.33 213.47 o 4 0 0 1706.00 1704.92 52.86 o 5 0 0 46359.91 47569.78 847.73 o 6 0 0 6155.21 6290.23 140.16 o 7 0 0 403.77 394.63 20.42 o 8 0 0 44.60 -2.89 12.83 o 9 0 0 3167.22 3098.24 69.58 o 10 0 0 162.84 148.15 26.12 o 11 0 0 847.71 777.12 37.15 o 12 0 0 1007.65 863.09 54.67 o 13 0 0 117.88 88.91 39.82 o 14 0 0 1694.33 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