#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2212661.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212661_Fobs loop_ _publ_author_name 'Siero\'n, Les\/law' _publ_section_title ; trans-Bis(hydrogen maleato-\kO)bis(pyridine-2-carboxamide-\k^2^N^1^,O)copper(II) ; _journal_coeditor_code OM2103 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m862 _journal_page_last m864 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.190 _cell_angle_gamma 90.000 _cell_length_a 11.0611 _cell_length_b 12.6061 _cell_length_c 7.8818 _exptl_crystal_F_000 550.00 _reflns_d_resolution_high 0.8408 _[local]_cod_data_source_file om2103Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title t011008 _shelx_refln_list_code 4 _shelx_f_calc_maximum 265.34 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 2279.52 2108.93 12.34 o 4 0 0 3106.09 2926.05 16.79 o 5 0 0 3344.50 3323.87 23.62 o 6 0 0 6989.40 7258.92 23.85 o 7 0 0 1668.41 1657.03 12.49 o 8 0 0 262.95 256.99 4.70 o 9 0 0 957.08 974.81 14.50 o 10 0 0 1160.98 1224.60 11.44 o 11 0 0 75.83 70.02 4.00 o 12 0 0 0.85 0.28 1.02 o 13 0 0 5.12 4.92 5.31 o 2 1 0 3913.50 3950.85 27.62 o 3 1 0 839.38 858.78 10.32 o 4 1 0 178.92 182.04 1.86 o 5 1 0 111.45 117.68 1.54 o 6 1 0 249.76 255.94 4.80 o 7 1 0 223.38 212.79 3.21 o 8 1 0 0.01 0.00 0.92 o 9 1 0 142.38 145.95 3.43 o 10 1 0 42.57 44.81 2.36 o 11 1 0 152.11 148.58 3.43 o 12 1 0 17.12 16.20 2.67 o 13 1 0 45.71 42.79 3.16 o 0 2 0 427.15 459.48 5.26 o 1 2 0 5263.33 5406.42 36.64 o 2 2 0 1154.98 1211.26 8.04 o 3 2 0 34.88 38.13 0.93 o 4 2 0 70.31 102.40 1.44 o 5 2 0 872.19 790.83 3.20 o 6 2 0 647.60 604.73 8.36 o 7 2 0 674.04 622.59 6.35 o 8 2 0 426.03 417.13 4.83 o 9 2 0 453.59 474.66 5.17 o 10 2 0 43.50 42.72 2.73 o 11 2 0 154.40 161.09 3.85 o 12 2 0 11.85 12.80 3.00 o 13 2 0 67.39 66.48 4.12 o 1 3 0 35.05 39.14 1.09 o 2 3 0 481.85 472.54 3.34 o 3 3 0 432.22 448.07 2.16 o 4 3 0 1038.36 1079.33 3.97 o 5 3 0 751.68 799.21 5.11 o 6 3 0 2734.47 2942.18 26.93 o 7 3 0 141.83 153.74 3.89 o 8 3 0 77.28 79.81 3.61 o 9 3 0 6.25 5.11 3.48 o 10 3 0 0.53 1.60 1.26 o 11 3 0 1.52 0.42 2.96 o 12 3 0 58.09 59.52 3.21 o 0 4 0 8064.97 7642.68 30.41 o 1 4 0 328.98 298.76 2.38 o 2 4 0 186.28 161.35 1.59 o 3 4 0 1764.72 1784.45 9.05 o 4 4 0 1593.35 1573.73 6.67 o 5 4 0 861.09 827.64 4.47 o 6 4 0 1869.32 1859.32 13.64 o 7 4 0 247.58 225.69 4.62 o 8 4 0 801.92 775.96 7.95 o 9 4 0 913.96 929.18 9.17 o 10 4 0 322.23 337.69 6.37 o 11 4 0 35.54 35.85 3.40 o 12 4 0 87.93 87.08 3.54 o 1 5 0 7.31 15.73 1.00 o 2 5 0 3279.08 3482.04 17.62 o 3 5 0 538.94 600.18 3.38 o 4 5 0 174.51 197.29 1.89 o 5 5 0 77.92 81.69 1.57 o 6 5 0 18.01 22.99 1.73 o 7 5 0 46.17 48.56 2.51 o 8 5 0 317.43 315.60 5.70 o 9 5 0 91.24 92.99 4.20 o 10 5 0 23.46 25.01 3.53 o 11 5 0 1.91 3.01 5.60 o 12 5 0 1.00 0.00 0.07 o 0 6 0 4511.41 4518.61 26.47 o 1 6 0 6516.17 6745.53 28.43 o 2 6 0 2722.88 2709.78 20.15 o 3 6 0 1625.17 1570.29 4.89 o 4 6 0 2028.67 2006.44 6.67 o 5 6 0 1014.14 981.71 4.27 o 6 6 0 978.70 970.91 8.59 o 7 6 0 611.61 616.72 5.91 o 8 6 0 461.77 448.36 6.78 o 9 6 0 224.02 244.62 5.70 o 10 6 0 102.11 97.27 4.60 o 11 6 0 106.66 109.11 9.03 o 12 6 0 1.47 2.02 12.99 o 1 7 0 1421.56 1652.26 7.93 o 2 7 0 121.62 137.89 2.06 o 3 7 0 216.39 240.87 2.31 o 4 7 0 27.30 26.12 1.33 o 5 7 0 379.78 406.23 3.38 o 6 7 0 387.65 385.70 4.71 o 7 7 0 27.47 27.95 2.73 o 8 7 0 365.08 383.92 6.62 o 9 7 0 7.06 7.11 3.18 o 10 7 0 26.08 22.01 4.86 o 11 7 0 13.60 10.80 5.67 o 0 8 0 590.13 531.54 9.59 o 1 8 0 259.08 220.99 2.57 o 2 8 0 327.72 326.02 2.76 o 3 8 0 444.69 431.18 3.43 o 4 8 0 287.02 281.83 2.97 o 5 8 0 1487.03 1454.50 9.56 o 6 8 0 120.35 127.81 3.13 o 7 8 0 82.27 87.49 3.45 o 8 8 0 1.75 0.98 1.79 o 9 8 0 17.87 16.07 4.40 o 10 8 0 101.91 98.00 6.13 o 11 8 0 46.07 52.72 5.85 o 1 9 0 74.11 75.46 1.93 o 2 9 0 19.08 18.88 1.62 o 3 9 0 8.28 7.46 2.01 o 4 9 0 6.95 12.42 2.21 o 5 9 0 75.67 77.06 2.73 o 6 9 0 510.27 500.41 5.93 o 7 9 0 42.46 38.32 3.16 o 8 9 0 0.13 0.00 3.33 o 9 9 0 15.64 13.02 4.68 o 10 9 0 31.15 24.58 5.25 o 0 10 0 27.86 25.94 2.58 o 1 10 0 278.31 285.84 3.72 o 2 10 0 1093.19 1101.34 8.17 o 3 10 0 277.91 259.16 3.76 o 4 10 0 1501.25 1495.41 8.06 o 5 10 0 1151.11 1166.33 7.36 o 6 10 0 324.90 332.25 4.44 o 7 10 0 56.44 64.64 4.05 o 8 10 0 246.86 236.08 9.18 o 9 10 0 154.20 161.60 7.27 o 1 11 0 23.01 17.04 2.62 o 2 11 0 8.11 8.09 2.44 o 3 11 0 5.54 3.45 1.60 o 4 11 0 18.24 22.12 2.47 o 5 11 0 74.77 71.82 2.90 o 6 11 0 213.70 225.04 4.36 o 7 11 0 19.06 13.50 4.42 o 8 11 0 16.47 23.45 5.06 o 0 12 0 2.53 3.06 3.16 o 1 12 0 348.11 346.40 5.71 o 2 12 0 522.57 516.34 6.05 o 3 12 0 475.18 484.44 6.01 o 4 12 0 174.91 175.52 4.03 o 5 12 0 98.39 106.37 3.61 o 6 12 0 24.75 26.76 3.01 o 7 12 0 147.08 148.57 9.31 o 1 13 0 0.80 0.10 0.51 o 2 13 0 0.01 0.00 2.18 o 3 13 0 0.04 0.00 0.79 o 4 13 0 1.10 0.00 3.06 o 5 13 0 4.16 1.81 1.68 o 6 13 0 0.83 1.03 4.70 o 0 14 0 244.85 209.79 7.40 o 1 14 0 243.05 248.36 5.56 o 2 14 0 210.52 211.18 6.09 o 3 14 0 166.10 159.03 5.69 o 4 14 0 307.22 321.97 6.56 o -13 1 1 6.99 4.72 2.40 o -12 1 1 61.70 58.73 3.21 o -11 1 1 247.73 252.27 5.20 o -10 1 1 67.36 76.25 3.11 o -9 1 1 313.41 321.43 10.06 o -8 1 1 504.46 504.60 5.69 o -7 1 1 352.70 356.83 4.49 o -6 1 1 25.40 21.12 1.01 o -5 1 1 2312.51 2232.26 12.14 o -4 1 1 2429.65 2424.87 10.23 o -3 1 1 1054.89 1060.10 6.13 o -2 1 1 6230.00 6094.57 34.18 o -1 1 1 4140.71 4102.71 8.64 o 0 1 1 4879.58 5020.89 14.22 o 1 1 1 5284.96 5542.79 31.64 o 2 1 1 5524.89 5831.74 12.10 o 3 1 1 3721.25 3795.47 8.72 o 4 1 1 157.65 184.51 1.43 o 5 1 1 469.91 409.96 2.59 o 6 1 1 1734.45 1782.90 8.53 o 7 1 1 1270.09 1234.30 8.41 o 8 1 1 1073.93 1095.02 6.62 o 9 1 1 584.73 573.36 10.43 o 10 1 1 33.77 33.47 2.32 o 11 1 1 79.67 70.14 2.82 o 12 1 1 81.29 92.42 3.18 o 13 1 1 70.26 67.03 3.49 o -12 2 1 74.75 66.65 4.98 o -11 2 1 33.52 31.37 3.32 o -10 2 1 124.82 125.11 3.97 o -9 2 1 0.95 0.17 0.83 o -8 2 1 7.87 8.04 2.24 o -7 2 1 173.98 187.94 3.60 o -6 2 1 9.08 9.49 0.98 o -5 2 1 646.82 654.21 6.03 o -4 2 1 159.02 168.74 1.48 o -3 2 1 14.74 14.70 0.82 o -2 2 1 7047.05 7124.05 59.89 o -1 2 1 37.17 39.68 0.91 o 0 2 1 6591.85 6599.69 36.22 o 1 2 1 22.41 21.24 0.76 o 2 2 1 82.91 80.79 0.87 o 3 2 1 577.45 597.11 3.12 o 4 2 1 3016.94 3299.14 17.44 o 5 2 1 259.79 317.03 2.29 o 6 2 1 302.26 329.23 2.77 o 7 2 1 0.01 0.27 0.61 o 8 2 1 385.06 375.38 4.61 o 9 2 1 93.74 91.25 3.14 o 10 2 1 49.48 47.28 3.07 o 11 2 1 7.15 7.97 2.09 o 12 2 1 8.19 6.03 2.57 o -12 3 1 271.75 285.95 6.03 o -11 3 1 263.83 268.78 5.49 o -10 3 1 175.01 176.22 6.63 o -9 3 1 114.99 118.91 3.84 o -8 3 1 816.20 830.27 11.66 o -7 3 1 325.10 315.91 3.42 o -6 3 1 3760.68 3881.54 13.16 o -5 3 1 2095.45 2080.02 6.00 o -4 3 1 617.82 540.38 4.25 o -3 3 1 597.06 553.03 3.47 o -2 3 1 749.69 637.26 4.70 o -1 3 1 49.94 39.50 0.99 o 0 3 1 3696.71 3608.07 17.74 o 1 3 1 3816.27 3792.76 33.88 o 2 3 1 1380.43 1283.33 5.96 o 3 3 1 1043.17 1072.70 3.68 o 4 3 1 5156.48 5309.58 21.88 o 5 3 1 298.60 269.54 2.28 o 6 3 1 1180.29 1078.90 8.18 o 7 3 1 1231.72 1230.75 8.79 o 8 3 1 543.86 517.83 5.32 o 9 3 1 1271.34 1287.87 8.57 o 10 3 1 866.21 882.41 7.64 o 11 3 1 449.33 460.29 5.63 o 12 3 1 87.16 97.23 3.95 o -12 4 1 4.35 4.83 2.24 o -11 4 1 0.13 1.38 1.31 o -10 4 1 8.78 9.10 2.71 o -9 4 1 52.02 50.85 3.18 o -8 4 1 33.60 27.12 3.22 o -7 4 1 54.66 51.17 2.51 o -6 4 1 14.69 15.66 1.22 o -5 4 1 234.74 255.23 2.20 o -4 4 1 139.71 151.01 1.95 o -3 4 1 154.41 170.09 1.93 o -2 4 1 60.57 61.11 1.28 o -1 4 1 696.76 750.81 5.16 o 0 4 1 860.69 816.46 7.02 o 1 4 1 246.42 254.60 2.07 o 2 4 1 390.97 441.61 2.40 o 3 4 1 701.27 802.74 3.53 o 4 4 1 411.15 466.28 3.20 o 5 4 1 238.11 276.28 2.43 o 6 4 1 355.27 371.16 2.98 o 7 4 1 141.62 131.84 3.80 o 8 4 1 12.58 11.25 2.82 o 9 4 1 40.94 42.06 2.79 o 10 4 1 44.03 41.54 2.84 o 11 4 1 1.59 1.73 3.07 o 12 4 1 1.11 0.00 1.72 o -12 5 1 37.88 42.82 3.86 o -11 5 1 236.46 245.85 5.58 o -10 5 1 116.42 119.46 4.23 o -9 5 1 44.43 43.42 4.29 o -8 5 1 22.48 22.07 3.39 o -7 5 1 953.83 955.22 10.79 o -6 5 1 1200.60 1237.80 7.62 o -5 5 1 1756.41 1762.88 7.05 o -4 5 1 187.25 170.60 2.19 o -3 5 1 561.76 492.99 2.42 o -2 5 1 356.18 330.11 2.39 o -1 5 1 8257.09 8587.82 42.70 o 0 5 1 1109.26 1052.61 6.96 o 1 5 1 701.62 607.13 5.23 o 2 5 1 586.63 541.25 2.46 o 3 5 1 2607.76 2491.94 6.42 o 4 5 1 1150.92 1160.93 4.75 o 5 5 1 882.48 801.87 6.03 o 6 5 1 232.65 203.84 2.58 o 7 5 1 115.02 108.54 3.73 o 8 5 1 416.60 423.56 6.25 o 9 5 1 612.83 603.59 12.34 o 10 5 1 63.84 64.31 4.87 o 11 5 1 10.73 14.25 4.71 o 12 5 1 28.21 33.78 6.73 o -12 6 1 50.35 52.37 4.15 o -11 6 1 28.97 27.96 3.64 o -10 6 1 4.85 4.13 3.22 o -9 6 1 6.22 4.90 3.69 o -8 6 1 39.25 34.38 3.43 o -7 6 1 104.24 112.40 2.81 o -6 6 1 308.75 325.95 3.35 o -5 6 1 91.91 107.09 2.18 o -4 6 1 0.51 1.51 1.19 o -3 6 1 17.95 25.13 1.06 o -2 6 1 553.26 567.88 3.71 o -1 6 1 167.28 162.67 2.40 o 0 6 1 79.68 65.78 2.82 o 1 6 1 12.11 16.63 1.01 o 2 6 1 21.80 25.12 1.01 o 3 6 1 1442.16 1587.96 9.87 o 4 6 1 166.49 177.53 1.93 o 5 6 1 365.80 371.71 3.22 o 6 6 1 243.09 252.10 2.88 o 7 6 1 109.06 97.09 3.06 o 8 6 1 47.67 42.18 3.52 o 9 6 1 432.58 411.23 8.50 o 10 6 1 53.55 45.72 4.85 o 11 6 1 1.15 0.00 3.77 o -11 7 1 19.35 20.28 4.45 o -10 7 1 55.69 57.60 4.38 o -9 7 1 56.01 56.56 4.81 o -8 7 1 219.38 216.51 5.60 o -7 7 1 46.89 39.09 2.35 o -6 7 1 466.20 491.59 4.17 o -5 7 1 771.28 758.64 4.86 o -4 7 1 1076.85 1089.83 6.61 o -3 7 1 769.68 706.88 5.62 o -2 7 1 2005.01 1878.74 13.22 o -1 7 1 439.87 427.51 3.55 o 0 7 1 1572.11 1498.54 11.50 o 1 7 1 2092.90 1936.26 11.14 o 2 7 1 2699.07 2769.53 15.88 o 3 7 1 1099.43 1120.83 6.87 o 4 7 1 1742.88 1703.28 12.33 o 5 7 1 295.22 306.24 3.21 o 6 7 1 262.98 250.41 3.31 o 7 7 1 439.09 472.02 6.39 o 8 7 1 339.13 325.22 7.76 o 9 7 1 115.97 123.54 5.91 o 10 7 1 128.73 118.14 6.31 o 11 7 1 54.76 48.70 5.53 o -11 8 1 1.02 0.00 3.53 o -10 8 1 22.98 23.29 4.56 o -9 8 1 53.46 50.80 4.26 o -8 8 1 20.17 17.92 3.64 o -7 8 1 85.56 101.19 2.97 o -6 8 1 252.70 252.43 3.38 o -5 8 1 126.80 138.85 2.67 o -4 8 1 287.66 293.23 3.14 o -3 8 1 198.46 182.95 2.58 o -2 8 1 173.71 186.12 2.50 o -1 8 1 106.36 97.99 2.13 o 0 8 1 172.23 169.91 2.29 o 1 8 1 353.28 336.14 3.28 o 2 8 1 175.34 181.99 2.67 o 3 8 1 151.01 140.30 2.54 o 4 8 1 229.69 220.06 2.98 o 5 8 1 1435.46 1515.58 13.01 o 6 8 1 2.08 0.00 1.72 o 7 8 1 301.93 293.12 5.52 o 8 8 1 74.49 79.79 5.09 o 9 8 1 6.30 6.95 10.89 o 10 8 1 18.01 10.90 4.67 o 11 8 1 28.53 35.52 5.59 o -10 9 1 213.33 212.39 7.73 o -9 9 1 115.24 122.05 5.38 o -8 9 1 3.95 0.00 3.75 o -7 9 1 1039.08 1075.61 10.50 o -6 9 1 1206.74 1242.24 13.50 o -5 9 1 774.43 837.52 7.20 o -4 9 1 856.97 881.94 7.09 o -3 9 1 455.92 448.48 3.83 o -2 9 1 489.08 471.36 3.80 o -1 9 1 633.44 606.36 10.18 o 0 9 1 567.26 579.86 9.73 o 1 9 1 290.42 288.39 3.32 o 2 9 1 1031.03 1065.78 7.49 o 3 9 1 3527.60 3522.20 21.01 o 4 9 1 1008.38 1029.73 7.65 o 5 9 1 646.97 629.71 5.86 o 6 9 1 6.97 2.29 1.49 o 7 9 1 179.15 173.29 4.32 o 8 9 1 654.02 663.40 10.99 o 9 9 1 187.61 193.08 7.38 o 10 9 1 157.52 160.46 7.31 o -9 10 1 1.04 4.79 4.33 o -8 10 1 71.93 68.24 4.89 o -7 10 1 148.09 133.07 4.43 o -6 10 1 121.65 113.27 3.49 o -5 10 1 332.00 331.08 6.39 o -4 10 1 75.36 71.07 2.66 o -3 10 1 19.21 18.10 1.84 o -2 10 1 18.73 14.54 2.06 o -1 10 1 1.79 1.28 1.61 o 0 10 1 1.65 1.02 1.38 o 1 10 1 3.46 1.38 0.78 o 2 10 1 41.41 39.45 2.24 o 3 10 1 20.25 18.89 2.24 o 4 10 1 137.14 139.52 3.48 o 5 10 1 588.27 564.47 5.87 o 6 10 1 0.04 0.44 0.70 o 7 10 1 0.10 3.25 2.70 o 8 10 1 8.89 5.44 5.30 o 9 10 1 8.96 5.88 4.46 o -8 11 1 25.13 29.98 5.33 o -7 11 1 59.72 61.13 3.95 o -6 11 1 337.61 338.26 7.95 o -5 11 1 97.66 102.14 3.42 o -4 11 1 2.06 3.68 2.64 o -3 11 1 76.70 84.07 3.30 o -2 11 1 165.93 165.58 3.93 o -1 11 1 300.47 331.47 5.35 o 0 11 1 70.29 73.64 2.68 o 1 11 1 41.64 38.01 2.36 o 2 11 1 17.78 18.91 2.32 o 3 11 1 74.74 80.53 3.09 o 4 11 1 1075.73 1035.95 7.87 o 5 11 1 119.72 123.18 3.59 o 6 11 1 17.27 18.02 3.09 o 7 11 1 85.24 89.69 4.06 o 8 11 1 99.97 87.10 6.35 o -7 12 1 108.19 91.51 4.90 o -6 12 1 8.56 6.51 3.23 o -5 12 1 41.23 45.29 3.30 o -4 12 1 2.23 2.28 2.33 o -3 12 1 30.24 31.18 2.97 o -2 12 1 1.09 1.09 0.91 o -1 12 1 103.93 94.43 3.54 o 0 12 1 117.83 106.83 3.52 o 1 12 1 26.35 22.89 3.59 o 2 12 1 16.32 15.24 3.48 o 3 12 1 63.55 63.73 3.11 o 4 12 1 42.19 33.90 3.01 o 5 12 1 5.40 2.27 2.46 o 6 12 1 9.51 6.47 3.02 o 7 12 1 1.31 0.00 2.83 o -6 13 1 236.32 237.32 6.81 o -5 13 1 97.43 93.68 5.20 o -4 13 1 215.12 218.58 4.93 o -3 13 1 158.27 153.15 4.39 o -2 13 1 678.61 667.45 7.96 o -1 13 1 1656.39 1591.56 11.66 o 0 13 1 619.60 586.27 8.76 o 1 13 1 42.61 39.33 4.03 o 2 13 1 247.89 241.60 6.14 o 3 13 1 473.26 474.33 8.11 o 4 13 1 422.39 426.88 5.93 o 5 13 1 513.18 509.59 6.54 o 6 13 1 100.01 108.85 5.09 o -4 14 1 3.54 1.31 2.04 o -3 14 1 1.48 1.32 3.40 o -2 14 1 64.62 63.94 3.94 o -1 14 1 1.45 0.00 4.33 o 0 14 1 57.38 54.59 4.54 o 1 14 1 14.57 15.22 4.41 o 2 14 1 6.35 4.83 5.05 o 3 14 1 3.28 4.47 2.94 o 4 14 1 2.84 0.00 2.91 o -12 0 2 374.34 359.60 13.54 o -11 0 2 557.29 625.09 16.19 o -10 0 2 87.42 74.92 5.16 o -9 0 2 288.35 305.54 9.22 o -8 0 2 559.42 557.47 22.40 o -7 0 2 721.20 728.90 8.95 o -6 0 2 1081.69 1064.26 11.53 o -5 0 2 750.17 689.04 6.04 o -4 0 2 4637.03 4523.60 43.17 o -3 0 2 12414.55 12661.92 77.49 o -2 0 2 70404.50 70277.20 245.77 o -1 0 2 5924.74 5827.21 15.86 o 0 0 2 4719.41 4746.18 28.04 o 1 0 2 9127.04 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