#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:26:43 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181046 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/26/2212669.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212669_Fobs loop_ _publ_author_name 'Lough, Alan J.' 'Allen, Anna' 'Tam, William' _publ_section_title ; Cyclodimerization product of benzooxanorbornadiene ; _journal_coeditor_code PV2004 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1462 _journal_page_last o1463 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 86.098 _cell_angle_beta 80.700 _cell_angle_gamma 81.639 _cell_length_a 10.3040 _cell_length_b 10.9700 _cell_length_c 25.6730 _exptl_crystal_F_000 1216.00 _reflns_d_resolution_high 0.7704 _cod_data_source_file pv2004IIsup2.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' k0694 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 245.56 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 19755.06 15577.77 3888.22 o 3 0 0 116.55 109.63 8.85 o 4 0 0 4.69 3.80 8.50 o 5 0 0 531.79 476.76 24.93 o 6 0 0 806.96 689.42 48.11 o 7 0 0 215.46 201.21 22.58 o 8 0 0 134.23 108.05 19.28 o 9 0 0 187.02 186.09 24.17 o 10 0 0 193.86 205.91 26.09 o 11 0 0 581.40 582.61 51.64 o 12 0 0 188.29 239.42 54.21 o 13 0 0 12.71 11.96 66.31 o -12 1 0 1.02 16.36 27.03 o -11 1 0 0.18 0.33 24.69 o -10 1 0 500.29 473.18 44.38 o -9 1 0 1119.14 1196.11 55.21 o -8 1 0 104.99 82.05 18.25 o -7 1 0 2.55 11.70 11.47 o -6 1 0 30.29 25.57 6.94 o -5 1 0 812.38 758.41 27.27 o -4 1 0 739.40 621.57 15.95 o -3 1 0 1713.12 1579.64 26.19 o -2 1 0 21559.68 20522.00 332.86 o -1 1 0 492.54 268.53 72.60 o 1 1 0 1065.05 889.82 25.75 o 2 1 0 2524.11 2145.79 58.38 o 3 1 0 878.95 813.71 32.22 o 4 1 0 293.53 273.54 35.85 o 5 1 0 893.41 847.58 36.76 o 6 1 0 37.46 26.02 11.40 o 7 1 0 49.39 32.22 14.93 o 8 1 0 1.52 12.46 13.75 o 9 1 0 122.59 95.75 21.72 o 10 1 0 90.91 100.82 22.44 o 11 1 0 193.24 208.36 32.62 o 12 1 0 12.38 16.21 29.41 o 13 1 0 0.28 -0.87 42.27 o -12 2 0 26.37 11.42 32.90 o -11 2 0 11.48 35.17 29.20 o -10 2 0 186.49 206.48 35.20 o -9 2 0 6.54 -18.67 18.67 o -8 2 0 611.17 641.37 20.23 o -7 2 0 576.73 626.48 20.51 o -6 2 0 229.41 247.27 12.45 o -5 2 0 1192.11 1254.32 29.41 o -4 2 0 3481.21 3664.98 56.83 o -3 2 0 250.74 241.90 10.27 o -2 2 0 3547.40 3420.16 57.61 o -1 2 0 876.89 866.98 21.20 o 1 2 0 151.85 131.57 8.14 o 2 2 0 56.27 52.90 11.08 o 3 2 0 399.17 409.67 15.62 o 4 2 0 482.32 438.62 16.42 o 5 2 0 669.69 650.59 24.77 o 6 2 0 2750.89 3001.38 109.90 o 7 2 0 30.22 4.29 20.36 o 8 2 0 629.86 595.45 33.64 o 9 2 0 7.82 12.54 17.22 o 10 2 0 162.70 181.59 27.80 o 11 2 0 6.48 31.25 24.61 o 12 2 0 1.56 -19.12 25.07 o 13 2 0 5.97 21.84 29.27 o -12 3 0 233.85 223.71 41.75 o -11 3 0 359.23 392.54 43.46 o -10 3 0 411.78 440.25 36.52 o -9 3 0 385.11 415.87 30.70 o -8 3 0 1.53 4.49 12.92 o -7 3 0 4.37 0.21 7.25 o -6 3 0 262.50 293.51 12.15 o -5 3 0 2087.94 2217.08 46.46 o -4 3 0 3225.61 3165.09 65.38 o -3 3 0 133.36 116.41 6.45 o -2 3 0 2164.60 2144.04 39.82 o -1 3 0 140.44 151.05 9.32 o 0 3 0 1074.64 952.38 31.83 o 1 3 0 8.97 9.64 6.60 o 2 3 0 1003.30 966.31 49.30 o 3 3 0 1642.49 1509.17 57.21 o 4 3 0 228.36 212.73 15.13 o 5 3 0 4.16 -3.53 11.34 o 6 3 0 29.03 26.97 8.25 o 7 3 0 615.47 635.55 34.94 o 8 3 0 85.63 97.24 29.55 o 9 3 0 133.90 105.87 20.85 o 10 3 0 379.66 436.24 73.01 o 11 3 0 4.60 0.15 26.00 o 12 3 0 39.95 97.55 31.52 o 13 3 0 0.35 -13.61 29.05 o -12 4 0 108.59 148.95 51.04 o -11 4 0 185.83 250.18 46.33 o -10 4 0 123.21 113.76 27.58 o -9 4 0 24.11 19.84 11.42 o -8 4 0 422.76 460.84 24.77 o -7 4 0 1.67 -3.71 8.16 o -6 4 0 304.85 333.63 16.80 o -5 4 0 205.23 192.32 11.58 o -4 4 0 768.60 742.65 27.61 o -3 4 0 6.56 16.32 6.09 o -2 4 0 6220.26 6532.25 166.28 o -1 4 0 258.96 261.17 14.49 o 0 4 0 14167.42 13758.06 343.29 o 1 4 0 43.71 42.43 8.99 o 2 4 0 571.33 494.29 36.56 o 3 4 0 214.91 208.14 15.53 o 4 4 0 909.12 917.36 34.68 o 5 4 0 85.97 87.82 11.72 o 6 4 0 2178.81 2316.59 134.82 o 7 4 0 144.56 158.41 14.18 o 8 4 0 209.89 247.11 12.75 o 9 4 0 35.40 58.41 33.33 o 10 4 0 49.74 65.90 20.68 o 11 4 0 97.85 77.70 24.80 o 12 4 0 117.01 100.13 29.47 o 13 4 0 0.57 2.50 34.13 o -11 5 0 155.21 150.20 30.76 o -10 5 0 220.34 236.98 21.55 o -9 5 0 93.32 73.13 35.86 o -8 5 0 231.87 291.22 33.03 o -7 5 0 40.61 24.12 10.03 o -6 5 0 339.12 348.44 15.57 o -5 5 0 802.65 810.60 51.53 o -4 5 0 8.76 5.61 6.87 o -3 5 0 1.31 -7.62 11.31 o -2 5 0 1199.38 1467.35 45.23 o -1 5 0 11.32 -1.03 8.79 o 0 5 0 276.44 257.89 20.37 o 1 5 0 1352.69 1377.51 53.82 o 2 5 0 41.94 40.68 12.66 o 3 5 0 2564.73 2621.35 84.16 o 4 5 0 36.32 33.68 12.03 o 5 5 0 757.25 825.62 34.19 o 6 5 0 142.67 129.12 15.98 o 7 5 0 0.16 17.95 9.42 o 8 5 0 142.43 151.76 34.36 o 9 5 0 60.67 35.92 22.33 o 10 5 0 392.58 359.01 49.50 o 11 5 0 69.58 70.50 25.92 o 12 5 0 22.56 13.18 40.64 o -11 6 0 1.44 -8.72 25.05 o -10 6 0 23.41 24.54 31.18 o -9 6 0 100.83 103.99 23.79 o -8 6 0 521.35 624.62 32.61 o -7 6 0 245.05 232.03 30.56 o -6 6 0 18.72 18.04 11.15 o -5 6 0 60.83 41.76 10.07 o -4 6 0 15.09 0.45 11.83 o -3 6 0 4.37 8.63 7.56 o -2 6 0 2100.20 2421.19 51.46 o -1 6 0 167.92 184.32 21.09 o 0 6 0 4831.82 5281.07 154.00 o 1 6 0 255.19 252.13 22.54 o 2 6 0 0.01 2.89 12.72 o 3 6 0 1148.94 1196.68 61.28 o 4 6 0 262.76 250.81 20.61 o 5 6 0 30.15 6.98 18.38 o 6 6 0 20.64 7.19 20.36 o 7 6 0 0.32 -10.14 10.14 o 8 6 0 2.27 -11.00 11.00 o 9 6 0 270.79 253.10 19.81 o 10 6 0 16.84 14.79 18.86 o 11 6 0 78.36 41.55 29.89 o 12 6 0 246.29 210.34 67.40 o -9 7 0 2.88 24.05 31.95 o -8 7 0 59.29 81.62 33.94 o -7 7 0 31.12 41.96 16.38 o -6 7 0 487.15 476.23 48.00 o -5 7 0 43.15 32.44 9.99 o -4 7 0 674.16 693.63 40.27 o -3 7 0 22.34 32.52 8.72 o -2 7 0 10.25 -0.08 7.87 o -1 7 0 804.78 918.66 36.61 o 0 7 0 164.19 183.86 30.84 o 1 7 0 93.37 56.19 15.85 o 2 7 0 39.55 -13.58 20.33 o 3 7 0 145.12 148.63 29.30 o 4 7 0 0.71 -5.90 16.92 o 5 7 0 139.54 180.67 23.63 o 6 7 0 17.28 27.59 13.00 o 7 7 0 58.48 42.43 15.46 o 8 7 0 12.37 14.76 18.64 o 9 7 0 413.82 504.42 33.54 o 10 7 0 0.67 6.14 19.00 o 11 7 0 14.92 22.85 32.64 o 12 7 0 49.52 50.77 42.33 o -9 8 0 30.96 15.98 25.94 o -8 8 0 177.00 143.12 35.74 o -7 8 0 115.89 162.63 26.96 o -6 8 0 636.97 620.25 45.95 o -5 8 0 0.75 -4.55 10.85 o -4 8 0 77.03 55.24 14.89 o -3 8 0 2.59 0.85 9.72 o -2 8 0 553.83 592.67 24.24 o -1 8 0 255.87 260.88 23.84 o 0 8 0 798.51 872.54 49.78 o 1 8 0 51.61 42.13 29.89 o 2 8 0 18.61 18.49 20.10 o 3 8 0 387.27 370.68 77.78 o 4 8 0 60.89 69.74 19.54 o 5 8 0 87.63 73.12 21.39 o 6 8 0 736.32 606.17 43.57 o 7 8 0 605.53 601.17 42.50 o 8 8 0 36.44 14.26 20.44 o 9 8 0 144.30 140.94 23.28 o 10 8 0 41.04 62.54 22.13 o 11 8 0 59.53 107.37 53.60 o -8 9 0 3.90 7.90 33.84 o -7 9 0 4.56 15.98 28.00 o -6 9 0 3.30 -24.97 24.97 o -5 9 0 8.01 2.41 21.79 o -4 9 0 105.36 120.81 16.80 o -3 9 0 37.67 23.34 11.67 o -2 9 0 2.75 -8.03 8.03 o -1 9 0 1023.98 1200.88 50.56 o 0 9 0 5.21 12.54 19.73 o 1 9 0 1898.06 2096.73 95.24 o 2 9 0 222.91 250.88 42.01 o 3 9 0 375.61 389.00 39.08 o 4 9 0 0.18 -6.11 33.84 o 5 9 0 107.08 81.97 32.73 o 6 9 0 20.11 16.42 20.25 o 7 9 0 1.91 -16.66 23.44 o 8 9 0 18.91 18.50 26.46 o 9 9 0 563.94 670.69 64.97 o 10 9 0 104.44 82.46 32.13 o 11 9 0 238.98 315.64 65.12 o -8 10 0 25.79 -13.91 40.03 o -7 10 0 23.78 14.09 50.16 o -6 10 0 149.00 182.29 42.61 o -5 10 0 0.03 -4.12 34.87 o -4 10 0 394.40 377.20 60.97 o -3 10 0 71.40 63.61 15.32 o -2 10 0 161.33 142.29 17.57 o -1 10 0 626.97 705.35 42.38 o 0 10 0 729.14 746.44 45.61 o 1 10 0 49.84 22.55 23.98 o 2 10 0 21.30 -3.41 40.03 o 3 10 0 332.93 342.29 47.60 o 4 10 0 104.49 74.60 29.13 o 5 10 0 29.66 45.73 27.49 o 6 10 0 424.13 413.88 40.97 o 7 10 0 149.65 102.50 33.48 o 8 10 0 2.69 12.37 30.92 o 9 10 0 71.18 37.45 35.39 o -6 11 0 80.48 62.88 46.73 o -5 11 0 44.77 162.17 67.69 o -4 11 0 48.95 66.48 43.64 o -3 11 0 7.20 16.30 25.54 o -2 11 0 40.79 63.08 20.77 o -1 11 0 1.29 18.09 14.75 o 0 11 0 5.66 54.90 22.87 o 1 11 0 2.73 0.00 52.22 o 2 11 0 1.50 13.06 37.11 o 3 11 0 0.98 6.53 45.69 o 4 11 0 5.78 28.00 38.82 o 5 11 0 29.22 49.30 55.66 o 6 11 0 13.26 21.13 40.20 o 7 11 0 1.75 -27.14 52.22 o 8 11 0 175.75 176.62 41.58 o 9 11 0 1.04 -10.48 50.16 o -5 12 0 11.69 4.12 49.30 o -4 12 0 122.21 91.57 68.72 o -3 12 0 139.70 111.67 52.57 o -2 12 0 17.77 57.55 44.66 o -1 12 0 56.49 70.95 51.54 o 0 12 0 69.18 2.23 43.29 o 1 12 0 25.98 25.77 28.90 o 2 12 0 6.47 67.51 45.69 o 3 12 0 4.29 -2.23 39.17 o 4 12 0 140.49 170.95 67.18 o 5 12 0 1.66 -47.24 47.24 o 6 12 0 13.07 51.02 42.43 o 7 12 0 7.96 8.42 44.15 o 8 12 0 0.04 -23.02 41.92 o -3 13 0 46.08 58.92 52.57 o -2 13 0 21.31 -31.95 46.73 o -1 13 0 95.50 139.50 75.08 o 0 13 0 12.50 -41.06 41.06 o 1 13 0 0.14 -26.11 43.46 o 2 13 0 5.78 49.99 56.52 o 3 13 0 0.02 -43.46 43.46 o 4 13 0 49.70 56.35 47.59 o 5 13 0 65.14 84.01 51.71 o 6 13 0 0.10 -10.65 51.19 o 0 14 0 4.30 -75.41 75.41 o 1 14 0 0.52 -56.35 56.35 o 2 14 0 8.97 78.16 84.69 o 3 14 0 0.29 52.22 82.63 o -3 -14 1 34.84 78.51 65.45 o -2 -14 1 12.35 56.69 58.92 o -1 -14 1 26.00 54.46 58.75 o 0 -14 1 4.46 97.23 60.47 o -6 -13 1 9.22 125.75 76.79 o -5 -13 1 31.64 23.71 71.12 o -4 -13 1 86.62 95.52 58.58 o -3 -13 1 4.35 -52.39 63.22 o -2 -13 1 0.54 -21.82 67.68 o 0 -13 1 0.03 -21.64 45.52 o 1 -13 1 72.47 232.27 62.36 o 2 -13 1 324.40 225.45 76.64 o -8 -12 1 0.17 14.60 41.74 o -7 -12 1 5.65 -2.06 41.92 o -6 -12 1 80.94 148.60 44.67 o -5 -12 1 61.42 55.83 42.95 o -4 -12 1 4.83 52.05 49.82 o -3 -12 1 102.20 137.44 45.87 o -2 -12 1 0.30 56.86 50.33 o -1 -12 1 3.37 -13.06 41.57 o 0 -12 1 1.81 -52.22 58.58 o 1 -12 1 20.30 6.53 62.53 o 2 -12 1 185.80 108.76 55.50 o 3 -12 1 26.66 58.92 48.44 o 4 -12 1 9.04 -22.85 39.34 o 5 -12 1 5.55 0.00 53.08 o -9 -11 1 11.45 -29.38 39.68 o -8 -11 1 61.90 29.03 39.34 o -7 -11 1 30.32 18.73 35.56 o -6 -11 1 452.10 479.85 63.59 o -5 -11 1 144.54 96.39 45.01 o -4 -11 1 243.45 272.69 47.60 o -3 -11 1 72.40 58.93 39.17 o 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40.11 o -2 -9 1 415.79 373.61 35.86 o -1 -9 1 253.40 229.81 37.03 o 0 -9 1 306.83 331.94 36.46 o 1 -9 1 0.02 9.36 7.27 o 2 -9 1 1752.98 2027.51 61.59 o 3 -9 1 50.42 43.23 12.64 o 4 -9 1 630.35 578.60 58.92 o 5 -9 1 36.90 36.84 20.35 o 6 -9 1 458.84 529.88 43.53 o 7 -9 1 18.19 7.90 41.57 o 8 -9 1 7.00 -5.84 41.40 o 9 -9 1 133.67 35.74 29.72 o -11 -8 1 177.95 152.36 38.09 o -9 -8 1 35.67 35.28 23.36 o -8 -8 1 534.27 584.13 44.52 o -7 -8 1 1.72 -28.10 67.34 o -6 -8 1 4.54 -14.70 15.16 o -5 -8 1 200.02 171.04 26.03 o -4 -8 1 584.66 680.20 63.35 o -3 -8 1 17.34 -11.92 18.98 o -2 -8 1 168.33 174.98 24.29 o -1 -8 1 881.44 911.32 51.96 o 0 -8 1 25.33 11.92 16.82 o 1 -8 1 1.77 6.30 21.85 o 2 -8 1 30.75 5.96 9.65 o 3 -8 1 2.97 17.49 12.94 o 4 -8 1 0.89 -0.80 11.13 o 5 -8 1 5.47 20.29 21.30 o 6 -8 1 31.13 11.34 15.99 o 7 -8 1 165.13 170.85 32.03 o 8 -8 1 24.32 45.35 25.60 o 9 -8 1 3.60 -9.96 37.62 o -12 -7 1 1.93 -22.45 29.55 o -11 -7 1 33.34 76.49 50.16 o -10 -7 1 37.85 48.54 23.45 o -9 -7 1 34.85 27.79 15.63 o -8 -7 1 17.31 4.74 13.84 o -7 -7 1 207.59 166.18 19.99 o -6 -7 1 47.79 74.40 20.22 o -5 -7 1 228.01 171.54 36.17 o -4 -7 1 835.36 907.98 43.72 o -3 -7 1 1952.57 1952.90 83.66 o -2 -7 1 22.37 -21.25 24.31 o -1 -7 1 17.76 35.04 34.01 o 0 -7 1 12.92 -8.55 18.30 o 1 -7 1 2.84 -8.00 41.92 o 2 -7 1 91.79 115.42 11.38 o 3 -7 1 31.31 31.92 9.39 o 4 -7 1 9.35 2.84 8.81 o 5 -7 1 55.15 63.06 16.69 o 6 -7 1 257.97 267.95 25.47 o 7 -7 1 436.69 448.94 34.67 o 8 -7 1 26.67 50.25 19.67 o 9 -7 1 47.61 33.67 23.88 o -12 -6 1 0.01 -13.20 25.66 o -11 -6 1 20.72 17.07 31.18 o -10 -6 1 49.16 39.24 19.91 o -9 -6 1 296.77 300.89 21.32 o -8 -6 1 140.91 126.51 37.71 o -7 -6 1 131.64 109.69 16.26 o -6 -6 1 293.63 267.29 28.18 o -5 -6 1 809.19 864.87 88.58 o -4 -6 1 485.76 556.84 29.52 o -3 -6 1 587.97 670.70 33.60 o -2 -6 1 97.12 106.33 16.78 o -1 -6 1 1758.47 1932.21 72.41 o 0 -6 1 153.53 137.39 20.07 o 1 -6 1 286.64 253.50 45.46 o 2 -6 1 25.41 22.46 7.70 o 3 -6 1 220.94 194.62 15.25 o 4 -6 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