#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/30/2213029.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213029_Fobs loop_ _publ_author_name 'Swamy, G. Y. S. K.' 'Ravikumar, K.' 'Narender, P.' 'Rao, V. Jayathirtha' _publ_section_title ; Methyl 6-chloro-5-[hydroxy(5-oxocyclopent-1-enyl)methyl]pyridine-2-carboxylate ; _journal_coeditor_code SK3105 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1842 _journal_page_last o1843 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.671 _cell_angle_gamma 90.000 _cell_length_a 9.6954 _cell_length_b 11.0961 _cell_length_c 12.0810 _exptl_crystal_F_000 584.00 _reflns_d_resolution_high 0.7571 _[local]_cod_data_source_file sk3105Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' PU25m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 186.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 16196.01 14923.44 420.67 o 4 0 0 131.25 147.11 2.09 o 6 0 0 106.23 105.20 1.83 o 8 0 0 19.20 18.20 1.10 o 10 0 0 325.10 321.40 8.55 o 12 0 0 1.27 0.47 0.88 o 1 1 0 3777.97 4199.68 41.96 o 2 1 0 54.05 70.02 1.16 o 3 1 0 4195.03 4317.46 32.61 o 4 1 0 55.27 52.46 0.71 o 5 1 0 858.26 854.25 6.91 o 6 1 0 396.67 399.16 3.59 o 7 1 0 118.09 106.27 2.34 o 8 1 0 5.94 7.43 0.62 o 9 1 0 250.97 245.80 3.61 o 10 1 0 72.46 78.79 2.07 o 11 1 0 12.52 13.65 0.93 o 12 1 0 2.25 3.21 0.90 o 0 2 0 750.45 807.82 11.93 o 1 2 0 212.39 249.97 2.32 o 2 2 0 6012.24 6500.25 53.21 o 3 2 0 228.41 236.88 2.11 o 4 2 0 718.67 731.24 5.92 o 5 2 0 5.70 6.96 0.30 o 6 2 0 12.55 15.25 0.45 o 7 2 0 171.35 167.25 2.25 o 8 2 0 32.73 33.65 1.12 o 9 2 0 284.45 290.53 4.08 o 10 2 0 59.85 58.49 1.63 o 11 2 0 41.80 43.58 2.20 o 12 2 0 98.62 97.93 3.52 o 1 3 0 745.81 883.71 7.14 o 2 3 0 824.06 899.79 7.11 o 3 3 0 259.33 254.48 2.61 o 4 3 0 368.70 387.72 3.38 o 5 3 0 2400.93 2447.85 18.89 o 6 3 0 1363.57 1427.42 12.41 o 7 3 0 25.53 20.51 0.96 o 8 3 0 321.07 327.80 5.70 o 9 3 0 86.19 89.09 1.94 o 10 3 0 14.29 14.63 1.32 o 11 3 0 51.25 49.17 4.04 o 0 4 0 8548.30 9015.17 188.55 o 1 4 0 50.56 48.78 0.71 o 2 4 0 1114.05 1217.77 9.54 o 3 4 0 211.62 209.34 2.05 o 4 4 0 374.07 371.07 3.32 o 5 4 0 4.17 2.48 0.25 o 6 4 0 5.97 7.37 0.43 o 7 4 0 2.67 4.42 0.42 o 8 4 0 100.32 92.28 2.25 o 9 4 0 57.98 53.82 2.20 o 10 4 0 28.71 28.01 1.76 o 11 4 0 4.99 6.79 1.19 o 1 5 0 286.55 340.45 2.98 o 2 5 0 21.59 33.89 0.77 o 3 5 0 3395.45 3755.89 28.59 o 4 5 0 245.40 282.19 2.97 o 5 5 0 177.41 156.12 2.43 o 6 5 0 12.99 17.81 0.60 o 7 5 0 524.52 516.37 8.44 o 8 5 0 123.35 127.68 3.52 o 9 5 0 62.38 64.96 2.52 o 10 5 0 7.76 7.73 1.19 o 11 5 0 17.47 15.96 1.76 o 0 6 0 625.75 630.16 7.48 o 1 6 0 222.42 233.79 2.71 o 2 6 0 1055.22 1141.74 9.12 o 3 6 0 14.16 18.03 0.48 o 4 6 0 51.86 39.75 1.02 o 5 6 0 25.64 25.69 0.83 o 6 6 0 47.52 49.36 1.19 o 7 6 0 11.49 13.39 0.82 o 8 6 0 0.34 0.62 0.66 o 9 6 0 26.43 25.19 1.76 o 10 6 0 47.49 51.96 2.42 o 1 7 0 600.94 669.61 5.65 o 2 7 0 48.86 60.03 1.08 o 3 7 0 1.07 0.87 0.48 o 4 7 0 6.49 5.16 0.42 o 5 7 0 290.78 263.78 3.30 o 6 7 0 72.88 77.83 1.95 o 7 7 0 102.14 101.21 2.38 o 8 7 0 9.77 10.39 1.71 o 9 7 0 64.45 62.88 2.64 o 10 7 0 1.82 4.04 0.88 o 0 8 0 614.21 582.42 7.22 o 1 8 0 10.86 14.79 0.86 o 2 8 0 302.76 313.77 3.42 o 3 8 0 100.80 100.19 1.61 o 4 8 0 339.00 323.39 4.20 o 5 8 0 6.83 7.39 0.70 o 6 8 0 83.26 74.05 2.11 o 7 8 0 26.03 24.52 1.17 o 8 8 0 1.40 -0.16 0.78 o 9 8 0 27.35 31.77 1.98 o 1 9 0 104.95 98.37 2.13 o 2 9 0 4.63 5.57 0.44 o 3 9 0 206.72 202.66 2.64 o 4 9 0 0.44 0.16 0.31 o 5 9 0 195.80 196.07 3.07 o 6 9 0 71.20 66.69 1.66 o 7 9 0 68.26 72.90 2.09 o 8 9 0 1.86 3.30 0.88 o 9 9 0 31.59 35.25 2.08 o 0 10 0 536.16 539.30 10.11 o 1 10 0 17.34 16.37 0.78 o 2 10 0 250.14 228.99 3.33 o 3 10 0 104.79 87.08 2.15 o 4 10 0 24.35 17.85 0.84 o 5 10 0 85.13 73.40 2.47 o 6 10 0 161.51 156.75 3.29 o 7 10 0 13.04 12.74 1.01 o 8 10 0 26.92 25.27 3.11 o 1 11 0 0.38 -0.19 0.37 o 2 11 0 1.03 1.87 0.54 o 3 11 0 116.74 98.96 2.51 o 4 11 0 4.01 5.62 0.88 o 5 11 0 8.05 9.22 0.90 o 6 11 0 1.35 1.98 0.58 o 7 11 0 96.06 102.30 2.68 o 8 11 0 0.29 0.93 0.93 o 0 12 0 6.79 7.13 0.97 o 1 12 0 0.82 0.41 0.54 o 2 12 0 117.76 119.77 2.87 o 3 12 0 28.97 30.41 1.44 o 4 12 0 45.87 40.24 2.18 o 5 12 0 2.00 1.34 0.64 o 6 12 0 2.53 5.10 0.97 o 7 12 0 28.48 32.04 2.80 o 1 13 0 137.90 136.23 4.51 o 2 13 0 17.86 15.42 1.19 o 3 13 0 99.14 111.32 2.87 o 4 13 0 36.84 33.25 1.62 o 5 13 0 9.09 8.65 0.95 o 0 14 0 1.28 0.31 1.24 o 1 14 0 1.47 2.42 0.97 o 2 14 0 50.59 50.39 3.73 o 3 14 0 0.75 0.78 0.88 o -11 0 1 94.51 96.48 3.18 o -9 0 1 1321.98 1360.87 19.79 o -7 0 1 561.56 574.95 9.02 o -5 0 1 133.71 158.91 3.00 o -3 0 1 1803.94 2137.40 23.16 o -1 0 1 2835.76 3087.71 40.68 o 1 0 1 2578.12 2765.98 34.01 o 3 0 1 679.63 759.59 8.50 o 5 0 1 353.71 333.07 4.30 o 7 0 1 750.13 707.89 12.98 o 9 0 1 88.66 97.04 2.86 o 11 0 1 12.29 15.17 1.42 o -12 1 1 2.44 3.32 0.73 o -11 1 1 7.30 5.43 0.73 o -10 1 1 195.56 186.28 3.15 o -9 1 1 13.69 15.81 1.24 o -8 1 1 151.01 150.85 2.49 o -7 1 1 124.03 118.16 4.35 o -6 1 1 68.24 63.13 0.91 o -5 1 1 13.95 16.71 0.45 o -4 1 1 2297.69 2404.01 18.41 o -3 1 1 554.10 538.42 4.31 o -2 1 1 146.99 172.67 1.73 o -1 1 1 137.64 149.11 1.27 o 0 1 1 214.33 196.41 1.81 o 1 1 1 27.56 23.99 0.49 o 2 1 1 9342.03 9830.12 85.82 o 3 1 1 827.65 810.12 6.43 o 4 1 1 23.69 14.09 0.42 o 5 1 1 215.68 220.50 2.20 o 6 1 1 227.72 236.81 2.41 o 7 1 1 42.75 38.36 0.82 o 8 1 1 333.73 332.10 4.31 o 9 1 1 0.01 -0.31 0.31 o 10 1 1 70.31 76.46 1.86 o 11 1 1 12.65 13.69 1.13 o 12 1 1 11.63 15.55 2.49 o -12 2 1 1.68 2.80 1.10 o -11 2 1 105.38 113.99 2.48 o -10 2 1 0.69 1.32 0.47 o -9 2 1 56.50 52.92 1.43 o -8 2 1 47.80 45.29 1.28 o -7 2 1 363.13 350.24 4.97 o -6 2 1 9.19 9.58 0.41 o -5 2 1 13.11 16.42 0.52 o -4 2 1 3715.04 4097.36 31.04 o -3 2 1 4823.12 5189.51 39.12 o -2 2 1 15830.62 15806.97 145.22 o -1 2 1 169.40 148.41 1.29 o 0 2 1 7322.24 8000.41 77.38 o 1 2 1 24.29 22.80 0.37 o 2 2 1 22.08 22.65 0.40 o 3 2 1 36.66 38.65 0.58 o 4 2 1 10.85 11.45 0.38 o 5 2 1 3277.43 3308.02 25.31 o 6 2 1 210.05 219.91 2.30 o 7 2 1 1277.92 1319.47 10.68 o 8 2 1 17.44 17.02 0.81 o 9 2 1 0.07 -0.06 0.34 o 10 2 1 5.79 6.76 0.90 o 11 2 1 68.73 76.64 2.96 o -12 3 1 47.74 55.99 3.73 o -11 3 1 6.35 7.50 0.95 o -10 3 1 0.27 0.12 0.37 o -9 3 1 2.63 2.34 0.49 o -8 3 1 22.86 26.51 0.97 o -7 3 1 2.09 3.35 0.56 o -6 3 1 32.61 44.06 0.82 o -5 3 1 139.40 197.16 2.02 o -4 3 1 1050.83 1108.46 8.99 o -3 3 1 5053.18 5522.43 41.62 o -2 3 1 100.87 120.23 1.22 o -1 3 1 1548.54 1689.57 12.95 o 0 3 1 5348.95 5793.34 96.98 o 1 3 1 241.48 243.11 2.33 o 2 3 1 7137.90 7750.00 58.36 o 3 3 1 399.30 418.80 3.55 o 4 3 1 66.35 77.95 1.18 o 5 3 1 54.25 54.30 0.87 o 6 3 1 13.94 11.40 0.45 o 7 3 1 108.41 102.35 1.45 o 8 3 1 24.00 19.23 0.89 o 9 3 1 0.96 0.93 0.66 o 10 3 1 87.34 97.46 3.18 o 11 3 1 2.12 2.18 0.88 o -11 4 1 125.00 128.00 4.67 o -10 4 1 7.17 10.14 1.01 o -9 4 1 116.71 112.50 2.63 o -8 4 1 80.46 80.81 1.70 o -7 4 1 315.69 305.13 4.67 o -6 4 1 17.00 17.24 0.54 o -5 4 1 235.02 210.12 2.15 o -4 4 1 56.70 70.24 1.08 o -3 4 1 47.16 55.47 0.78 o -2 4 1 37.96 37.71 0.66 o -1 4 1 4.83 8.50 0.43 o 0 4 1 363.86 391.83 4.00 o 1 4 1 8.17 11.26 0.29 o 2 4 1 384.94 444.96 4.14 o 3 4 1 1418.28 1445.95 12.37 o 4 4 1 1.32 1.94 0.45 o 5 4 1 932.59 920.50 10.06 o 6 4 1 281.68 288.46 2.89 o 7 4 1 6.55 5.33 0.64 o 8 4 1 35.92 34.12 1.76 o 9 4 1 155.18 157.81 4.06 o 10 4 1 6.60 5.45 1.10 o 11 4 1 25.76 27.91 1.98 o -11 5 1 0.42 1.24 0.88 o -10 5 1 15.48 13.93 1.42 o -9 5 1 61.72 58.53 1.83 o -8 5 1 1.95 2.07 0.71 o -7 5 1 0.00 0.42 0.30 o -6 5 1 288.06 310.39 3.04 o -5 5 1 21.28 26.64 0.68 o -4 5 1 54.87 28.19 0.70 o -3 5 1 1033.30 1196.35 10.40 o -2 5 1 3090.48 3434.30 26.13 o -1 5 1 1372.94 1464.98 11.41 o 0 5 1 268.23 242.33 2.24 o 1 5 1 149.19 151.73 1.67 o 2 5 1 636.23 674.15 5.56 o 3 5 1 532.57 597.98 5.02 o 4 5 1 536.76 527.47 4.62 o 5 5 1 18.40 16.62 0.60 o 6 5 1 186.22 181.81 2.35 o 7 5 1 1.20 1.60 0.45 o 8 5 1 19.82 17.20 1.32 o 9 5 1 0.02 -0.62 0.62 o 10 5 1 0.07 0.13 0.75 o 11 5 1 26.60 25.50 2.80 o -10 6 1 2.01 2.18 0.88 o -9 6 1 77.00 73.43 2.74 o -8 6 1 58.84 55.02 1.73 o -7 6 1 116.31 122.42 2.16 o -6 6 1 109.75 99.33 1.85 o -5 6 1 135.25 132.84 1.86 o -4 6 1 155.63 160.44 1.81 o -3 6 1 391.82 378.69 3.47 o -2 6 1 10.44 9.68 0.35 o -1 6 1 52.01 42.69 0.93 o 0 6 1 246.35 257.28 2.45 o 1 6 1 78.37 68.79 0.95 o 2 6 1 456.34 488.66 4.20 o 3 6 1 204.79 187.47 2.27 o 4 6 1 1.33 1.24 0.28 o 5 6 1 779.21 797.88 9.09 o 6 6 1 13.51 13.65 0.69 o 7 6 1 238.84 231.70 4.69 o 8 6 1 38.50 40.38 2.02 o 9 6 1 60.66 61.43 2.64 o 10 6 1 3.75 5.15 1.24 o -10 7 1 18.06 19.19 1.76 o -9 7 1 3.08 4.93 0.97 o -8 7 1 0.73 1.41 2.64 o -7 7 1 85.53 80.26 1.96 o -6 7 1 26.64 33.81 1.03 o -5 7 1 2.72 1.24 0.28 o -4 7 1 246.63 260.53 3.03 o -3 7 1 40.05 31.37 0.97 o -2 7 1 4.74 10.39 0.43 o -1 7 1 679.06 751.39 6.28 o 0 7 1 2489.88 2684.00 21.05 o 1 7 1 131.69 165.16 2.30 o 2 7 1 333.57 278.72 5.91 o 3 7 1 60.23 56.23 1.23 o 4 7 1 151.00 164.22 2.18 o 5 7 1 1.56 1.30 0.36 o 6 7 1 113.64 109.92 2.78 o 7 7 1 0.05 0.04 0.60 o 8 7 1 30.39 28.16 1.76 o 9 7 1 24.50 27.22 1.76 o 10 7 1 104.88 125.06 7.15 o -10 8 1 0.00 0.00 0.93 o -9 8 1 150.62 150.31 4.40 o -8 8 1 19.14 20.55 1.54 o -7 8 1 58.35 71.44 2.98 o -6 8 1 0.71 0.23 0.31 o -5 8 1 158.16 138.30 2.32 o -4 8 1 204.22 174.91 2.38 o -3 8 1 39.96 36.68 0.91 o -2 8 1 6.55 7.05 0.42 o -1 8 1 0.00 0.49 0.21 o 0 8 1 510.56 532.73 5.20 o 1 8 1 13.01 10.61 0.52 o 2 8 1 85.98 87.64 2.25 o 3 8 1 247.80 244.50 3.27 o 4 8 1 74.14 74.01 1.59 o 5 8 1 219.04 210.80 4.13 o 6 8 1 35.29 32.43 1.16 o 7 8 1 158.21 153.40 3.22 o 8 8 1 29.85 30.32 1.80 o 9 8 1 75.24 79.73 3.18 o -9 9 1 5.53 6.94 1.19 o -8 9 1 0.73 0.31 0.66 o -7 9 1 3.01 5.14 0.72 o -6 9 1 116.79 112.46 2.57 o -5 9 1 35.30 30.96 1.00 o -4 9 1 96.50 96.37 1.69 o -3 9 1 192.64 181.90 2.45 o -2 9 1 301.64 306.07 3.93 o -1 9 1 0.37 0.86 0.31 o 0 9 1 171.52 169.79 2.60 o 1 9 1 70.57 70.96 1.47 o 2 9 1 83.98 73.52 1.33 o 3 9 1 94.36 80.22 1.67 o 4 9 1 165.47 160.13 2.68 o 5 9 1 1.23 0.84 0.37 o 6 9 1 0.64 0.06 0.49 o 7 9 1 25.46 25.62 1.31 o 8 9 1 22.34 24.94 1.97 o 9 9 1 1.10 3.42 1.24 o -9 10 1 34.47 45.41 3.42 o -8 10 1 16.32 19.98 1.64 o -7 10 1 122.31 113.69 4.80 o -6 10 1 29.12 30.62 1.37 o -5 10 1 6.89 9.71 0.76 o -4 10 1 5.76 6.71 0.62 o -3 10 1 81.91 76.04 1.71 o -2 10 1 0.09 -0.31 0.36 o -1 10 1 21.62 17.40 0.81 o 0 10 1 41.41 45.81 1.28 o 1 10 1 3.76 4.75 0.79 o 2 10 1 188.36 178.57 3.41 o 3 10 1 69.65 66.81 1.59 o 4 10 1 0.13 0.84 0.37 o 5 10 1 81.38 85.95 2.44 o 6 10 1 0.90 0.68 0.49 o 7 10 1 119.62 121.75 3.63 o 8 10 1 8.23 10.80 1.08 o -8 11 1 0.84 2.80 1.24 o -7 11 1 0.86 1.27 0.58 o -6 11 1 8.76 8.02 1.19 o -5 11 1 9.67 9.05 0.90 o -4 11 1 38.27 35.38 1.85 o -3 11 1 142.96 137.61 2.93 o -2 11 1 142.02 144.31 2.56 o -1 11 1 35.55 29.95 1.44 o 0 11 1 116.50 105.35 2.13 o 1 11 1 66.57 58.54 1.80 o 2 11 1 55.82 57.85 1.80 o 3 11 1 8.40 10.11 0.90 o 4 11 1 80.80 77.11 2.71 o 5 11 1 8.58 9.20 0.99 o 6 11 1 2.50 3.68 0.77 o 7 11 1 0.34 0.82 0.58 o -7 12 1 50.58 63.45 3.73 o -6 12 1 44.11 45.85 2.30 o -5 12 1 5.14 6.06 0.82 o -4 12 1 52.84 53.10 1.91 o -3 12 1 70.75 65.66 2.26 o -2 12 1 14.81 16.42 1.08 o -1 12 1 0.50 0.31 0.54 o 0 12 1 75.76 82.43 2.56 o 1 12 1 60.63 60.26 1.98 o 2 12 1 32.98 29.87 1.44 o 3 12 1 0.18 0.41 0.54 o 4 12 1 13.97 11.18 1.01 o 5 12 1 112.22 102.09 2.70 o 6 12 1 13.87 15.55 1.49 o -5 13 1 2.54 2.90 0.72 o -4 13 1 7.30 8.33 1.01 o -3 13 1 48.38 47.53 1.80 o -2 13 1 36.63 35.73 2.02 o -1 13 1 12.14 13.22 2.02 o 0 13 1 74.17 80.57 2.39 o 1 13 1 53.51 51.05 2.26 o 2 13 1 88.18 76.21 2.33 o 3 13 1 45.60 47.97 2.30 o 4 13 1 5.14 5.20 0.86 o 5 13 1 32.40 28.93 2.49 o -3 14 1 21.91 25.50 2.80 o -2 14 1 35.12 38.88 3.11 o -1 14 1 0.01 0.53 0.75 o 0 14 1 15.44 13.24 1.54 o 1 14 1 17.69 20.13 1.44 o 2 14 1 9.22 7.00 1.32 o 3 14 1 6.14 8.09 1.87 o -12 0 2 24.35 22.82 2.33 o -10 0 2 77.54 72.01 2.64 o -8 0 2 4.02 5.23 1.71 o -6 0 2 1918.28 2046.99 22.50 o -4 0 2 128.34 97.82 1.98 o -2 0 2 170.19 174.80 4.77 o 0 0 2 940.87 950.58 10.35 o 2 0 2 4157.76 4204.56 76.16 o 4 0 2 6.55 8.72 0.54 o 6 0 2 7.35 11.28 0.90 o 8 0 2 234.51 233.30 5.44 o 10 0 2 269.83 271.22 8.40 o -12 1 2 4.18 3.25 0.69 o -11 1 2 50.34 55.88 1.71 o -10 1 2 21.34 20.40 1.00 o -9 1 2 134.79 122.96 2.33 o -8 1 2 48.93 49.74 1.74 o -7 1 2 1070.95 1058.61 13.55 o -6 1 2 126.50 122.16 1.55 o -5 1 2 52.48 39.20 0.58 o -4 1 2 33.66 30.80 0.59 o -3 1 2 3.00 2.41 0.17 o -2 1 2 1989.05 2058.86 23.30 o -1 1 2 30.91 32.93 0.60 o 0 1 2 1150.47 1205.08 9.37 o 1 1 2 1715.11 1747.99 21.26 o 2 1 2 27.40 33.98 0.52 o 3 1 2 1946.79 1991.38 15.32 o 4 1 2 1738.78 1859.46 14.41 o 5 1 2 9.72 11.68 0.40 o 6 1 2 81.48 100.98 1.35 o 7 1 2 718.20 742.82 6.45 o 8 1 2 63.20 58.51 1.43 o 9 1 2 140.38 139.56 2.48 o 10 1 2 1.45 1.64 0.58 o 11 1 2 2.21 2.49 1.24 o -12 2 2 71.13 77.06 2.13 o -11 2 2 10.14 10.08 0.84 o -10 2 2 17.08 18.56 0.93 o -9 2 2 0.65 0.53 0.49 o -8 2 2 0.20 1.30 0.78 o -7 2 2 12.36 18.57 0.78 o -6 2 2 717.52 737.97 6.75 o -5 2 2 1086.21 1219.65 9.64 o -4 2 2 17.94 9.99 0.88 o -3 2 2 3629.91 3837.08 29.07 o -2 2 2 34739.03 31032.87 400.66 o -1 2 2 181.46 185.27 1.65 o 0 2 2 671.14 685.94 5.42 o 1 2 2 703.37 684.74 5.50 o 2 2 2 17.39 12.14 0.41 o 3 2 2 11.59 11.85 0.32 o 4 2 2 842.72 893.49 7.23 o 5 2 2 235.58 248.66 2.47 o 6 2 2 0.78 1.40 0.25 o 7 2 2 132.68 128.59 1.78 o 8 2 2 482.91 479.29 6.42 o 9 2 2 93.57 94.91 2.39 o 10 2 2 19.02 22.81 1.64 o 11 2 2 9.37 10.11 1.32 o -12 3 2 33.79 37.02 3.37 o -11 3 2 57.27 59.82 1.78 o -10 3 2 0.06 0.47 0.37 o -9 3 2 343.29 336.20 4.47 o -8 3 2 4.76 3.82 0.47 o -7 3 2 202.59 206.92 4.09 o -6 3 2 552.21 594.94 7.17 o -5 3 2 1863.83 2034.20 15.78 o -4 3 2 993.34 1095.55 9.57 o -3 3 2 0.72 1.30 0.16 o -2 3 2 22.83 23.16 0.44 o -1 3 2 2958.16 3308.90 25.05 o 0 3 2 272.67 272.86 2.34 o 1 3 2 241.64 244.24 2.41 o 2 3 2 246.07 261.05 2.76 o 3 3 2 177.02 177.11 1.79 o 4 3 2 70.31 73.40 1.07 o 5 3 2 1047.69 1122.28 9.05 o 6 3 2 1.72 1.09 0.25 o 7 3 2 541.05 535.60 4.88 o 8 3 2 24.91 22.88 1.56 o 9 3 2 19.47 20.71 1.54 o 10 3 2 32.68 32.25 1.86 o 11 3 2 2.65 4.07 1.10 o -11 4 2 5.84 7.23 1.01 o -10 4 2 18.13 18.02 1.18 o -9 4 2 1.99 1.24 0.47 o -8 4 2 76.52 64.52 1.47 o -7 4 2 129.37 124.46 2.10 o -6 4 2 6.42 5.55 0.37 o -5 4 2 212.37 243.77 2.43 o -4 4 2 4482.79 5014.95 37.98 o -3 4 2 1055.92 1195.64 9.44 o -2 4 2 28.97 13.74 0.38 o -1 4 2 28.68 26.07 0.48 o 0 4 2 305.05 348.57 2.98 o 1 4 2 996.79 1038.20 9.04 o 2 4 2 1463.74 1522.77 13.02 o 3 4 2 174.57 180.38 1.84 o 4 4 2 798.62 841.63 6.91 o 5 4 2 188.33 178.96 2.32 o 6 4 2 81.68 85.79 1.66 o 7 4 2 314.84 309.57 8.31 o 8 4 2 21.58 20.42 1.05 o 9 4 2 91.62 99.74 3.18 o 10 4 2 138.56 135.22 4.06 o -11 5 2 71.41 78.07 3.08 o -10 5 2 32.64 34.04 1.55 o -9 5 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