#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2213118.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213118_Fobs loop_ _publ_author_name 'Weinmann, Markus' 'Nuss, J\"urgen' 'Jansen, Martin' _publ_section_title ; N,N-Dimethylguanidinium chloride ; _journal_coeditor_code BH2085 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2767 _journal_page_last o2769 _journal_volume 63 _journal_year 2007 _space_group_IT_number 70 _symmetry_space_group_name_Hall '-F 2uv 2vw' _symmetry_space_group_name_H-M 'F d d d :2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.7568 _cell_length_b 15.7317 _cell_length_c 23.3640 _exptl_crystal_F_000 1056.00 _reflns_d_resolution_high 0.8016 _[local]_cod_data_source_file bh2085Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wei6_m in Fddd' _shelx_refln_list_code 4 _shelx_f_calc_maximum 515.37 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+3/4, -y+3/4, z' '-x+3/4, y, -z+3/4' 'x, -y+3/4, -z+3/4' 'x, y+1/2, z+1/2' '-x+3/4, -y+5/4, z+1/2' '-x+3/4, y+1/2, -z+5/4' 'x, -y+5/4, -z+5/4' 'x+1/2, y, z+1/2' '-x+5/4, -y+3/4, z+1/2' '-x+5/4, y, -z+5/4' 'x+1/2, -y+3/4, -z+5/4' 'x+1/2, y+1/2, z' '-x+5/4, -y+5/4, z' '-x+5/4, y+1/2, -z+3/4' 'x+1/2, -y+5/4, -z+3/4' '-x, -y, -z' 'x-3/4, y-3/4, -z' 'x-3/4, -y, z-3/4' '-x, y-3/4, z-3/4' '-x, -y+1/2, -z+1/2' 'x-3/4, y-1/4, -z+1/2' 'x-3/4, -y+1/2, z-1/4' '-x, y-1/4, z-1/4' '-x+1/2, -y, -z+1/2' 'x-1/4, y-3/4, -z+1/2' 'x-1/4, -y, z-1/4' '-x+1/2, y-3/4, z-1/4' '-x+1/2, -y+1/2, -z' 'x-1/4, y-1/4, -z' 'x-1/4, -y+1/2, z-3/4' '-x+1/2, y-1/4, z-3/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 113207.96 117557.91 862.73 o 8 0 0 11785.77 12404.26 454.32 o 2 2 0 2554.87 2181.54 57.07 o 6 2 0 213.40 213.79 39.52 o 0 4 0 13997.86 16781.75 206.86 o 4 4 0 11175.07 11161.96 136.32 o 8 4 0 2363.48 2828.74 179.64 o 2 6 0 51265.81 56025.61 589.97 o 6 6 0 7591.22 7395.68 184.19 o 0 8 0 19059.76 18598.02 262.56 o 4 8 0 9095.27 9246.05 189.08 o 2 10 0 25815.22 25149.42 300.03 o 6 10 0 5410.25 5513.87 170.02 o 0 12 0 4400.28 4529.27 138.25 o 4 12 0 2709.11 2583.56 119.03 o 2 14 0 3858.78 3856.12 151.14 o 0 16 0 24027.09 24171.38 708.14 o 4 16 0 13540.43 13876.74 567.04 o 2 18 0 1416.36 1972.51 188.75 o 1 1 1 5275.82 6197.17 45.97 o 3 1 1 5559.86 5349.02 58.44 o 5 1 1 2956.39 2813.16 52.79 o 7 1 1 876.57 873.86 60.16 o 1 3 1 26487.18 29816.69 138.57 o 3 3 1 7482.51 7592.33 74.48 o 5 3 1 4765.36 4567.52 80.25 o 7 3 1 1218.87 1199.19 58.90 o 1 5 1 77040.95 83250.25 292.74 o 3 5 1 23363.37 23638.83 154.09 o 5 5 1 9317.10 9160.00 132.30 o 7 5 1 2775.90 2806.41 77.96 o 1 7 1 320.18 519.79 22.18 o 3 7 1 1.74 32.95 17.37 o 5 7 1 5.32 -16.39 28.70 o 7 7 1 239.67 313.19 45.17 o 1 9 1 10704.18 12317.49 96.26 o 3 9 1 8647.38 8654.34 124.21 o 5 9 1 2789.67 2754.87 84.87 o 7 9 1 2191.96 2170.18 85.00 o 1 11 1 5529.64 5212.61 67.67 o 3 11 1 5073.75 4837.38 102.06 o 5 11 1 2091.07 2146.45 80.32 o 1 13 1 4066.00 3849.22 89.19 o 3 13 1 3064.40 2845.18 86.04 o 5 13 1 2115.17 2107.13 84.43 o 1 15 1 4901.60 4689.82 111.79 o 3 15 1 3423.50 3396.99 93.68 o 5 15 1 1674.52 1635.90 89.92 o 1 17 1 110.09 280.06 64.46 o 3 17 1 103.49 347.58 44.72 o 1 19 1 2517.02 2309.01 147.53 o 2 0 2 265603.91 285560.66 1338.67 o 6 0 2 17928.51 17582.37 254.53 o 0 2 2 26994.77 26502.92 188.01 o 2 2 2 1566.95 1360.85 27.77 o 4 2 2 2847.46 2671.66 49.62 o 6 2 2 550.48 516.23 34.52 o 8 2 2 136.93 176.42 45.67 o 2 4 2 2558.40 2574.61 44.98 o 4 4 2 591.22 535.51 28.64 o 6 4 2 1432.93 1392.73 64.48 o 8 4 2 75.73 160.67 40.98 o 0 6 2 21265.61 23369.57 295.52 o 2 6 2 100.14 85.78 18.30 o 4 6 2 7910.47 7699.51 103.78 o 6 6 2 2.60 10.88 38.18 o 8 6 2 504.86 695.64 69.34 o 2 8 2 2780.31 2621.85 50.72 o 4 8 2 7.99 37.32 26.73 o 6 8 2 1087.74 1132.91 63.83 o 0 10 2 11298.30 11262.23 173.20 o 2 10 2 16.82 6.58 18.00 o 4 10 2 3448.58 3024.56 86.19 o 6 10 2 84.75 71.34 31.33 o 2 12 2 589.44 482.49 44.86 o 4 12 2 18.40 22.59 28.70 o 6 12 2 491.22 471.90 47.96 o 0 14 2 239.32 387.83 54.32 o 2 14 2 67.85 106.04 28.76 o 4 14 2 97.60 109.35 34.33 o 2 16 2 8989.93 9115.68 149.01 o 4 16 2 51.59 66.17 40.49 o 0 18 2 89.60 186.74 90.26 o 2 18 2 13.91 78.51 38.95 o 1 1 3 3396.58 3352.79 34.31 o 3 1 3 114.84 91.52 17.34 o 5 1 3 203.43 261.04 22.50 o 7 1 3 23.80 52.83 31.08 o 1 3 3 0.16 3.68 12.74 o 3 3 3 1226.62 1183.19 35.16 o 5 3 3 161.14 132.98 21.88 o 7 3 3 315.26 324.49 40.34 o 1 5 3 4378.39 4127.22 52.74 o 3 5 3 2635.99 2403.45 50.08 o 5 5 3 34.58 43.04 22.72 o 7 5 3 282.92 277.23 39.12 o 1 7 3 4852.12 5147.71 55.00 o 3 7 3 4154.48 4095.52 70.22 o 5 7 3 263.10 320.31 41.68 o 7 7 3 1069.58 1053.95 66.07 o 1 9 3 1036.42 1289.40 32.35 o 3 9 3 2.09 58.21 20.66 o 5 9 3 1221.67 1150.75 65.23 o 7 9 3 23.72 151.67 39.57 o 1 11 3 30.44 20.55 16.29 o 3 11 3 239.22 202.95 37.21 o 5 11 3 23.32 22.53 27.30 o 1 13 3 6.01 29.70 25.15 o 3 13 3 74.58 82.49 30.06 o 5 13 3 1.20 32.91 27.73 o 1 15 3 99.46 102.20 32.10 o 3 15 3 32.41 59.93 27.01 o 5 15 3 43.37 114.74 33.62 o 1 17 3 566.67 611.81 67.64 o 3 17 3 421.10 410.02 37.83 o 1 19 3 0.15 95.67 54.76 o 0 0 4 26278.32 25610.31 206.54 o 4 0 4 2637.37 2586.76 67.50 o 8 0 4 215.51 488.22 108.36 o 2 2 4 53628.75 57086.82 220.44 o 4 2 4 2421.58 2166.67 43.46 o 6 2 4 7366.33 6845.51 106.14 o 8 2 4 639.32 796.02 159.96 o 0 4 4 10450.36 11189.51 100.47 o 2 4 4 1140.64 1098.34 34.99 o 4 4 4 2414.20 2213.10 48.34 o 6 4 4 500.23 479.27 39.11 o 8 4 4 194.50 266.50 48.42 o 2 6 4 2875.16 2625.16 50.54 o 4 6 4 16.95 35.66 21.26 o 6 6 4 1072.31 985.63 64.77 o 0 8 4 9469.04 10609.73 123.22 o 2 8 4 16.91 8.75 14.30 o 4 8 4 3190.07 2923.87 79.28 o 6 8 4 31.74 66.43 31.54 o 2 10 4 3632.35 3570.42 66.85 o 4 10 4 167.51 152.61 36.09 o 6 10 4 1447.73 1447.63 79.67 o 0 12 4 1491.38 1548.91 71.03 o 2 12 4 1.71 11.80 25.75 o 4 12 4 733.32 677.82 53.27 o 6 12 4 122.81 144.56 43.28 o 2 14 4 6518.00 6523.26 121.73 o 4 14 4 578.55 559.16 48.84 o 0 16 4 86.22 134.27 87.57 o 2 16 4 74.53 46.30 27.81 o 4 16 4 66.81 81.38 31.07 o 2 18 4 1707.04 1632.63 81.98 o 1 1 5 20777.79 23012.59 138.09 o 3 1 5 13295.14 13209.82 96.52 o 5 1 5 3723.43 3365.62 63.50 o 7 1 5 2056.39 2062.83 78.01 o 1 3 5 6201.20 6633.28 57.62 o 3 3 5 8571.71 8056.90 72.28 o 5 3 5 507.19 484.35 35.51 o 7 3 5 1962.00 2054.09 110.60 o 1 5 5 18802.96 19972.41 131.36 o 3 5 5 12013.49 11817.75 110.30 o 5 5 5 2757.60 2476.23 66.91 o 7 5 5 2279.99 2329.46 89.26 o 1 7 5 11541.32 11480.65 95.04 o 3 7 5 4701.08 4455.26 74.62 o 5 7 5 6697.40 6641.00 119.51 o 7 7 5 519.45 528.05 52.34 o 1 9 5 3120.81 2809.06 51.56 o 3 9 5 263.67 229.42 29.73 o 5 9 5 2518.97 2300.79 85.49 o 7 9 5 15.20 33.89 34.13 o 1 11 5 11753.91 12071.58 124.06 o 3 11 5 6588.28 6499.38 118.43 o 5 11 5 4747.68 4886.63 124.76 o 1 13 5 2331.61 2295.41 67.60 o 3 13 5 2115.21 2116.48 77.82 o 5 13 5 636.97 678.98 60.08 o 1 15 5 2528.59 2437.06 83.80 o 3 15 5 1831.47 1865.56 73.26 o 5 15 5 1316.95 1319.91 78.22 o 1 17 5 2511.32 2399.03 90.96 o 3 17 5 1841.51 1818.31 82.12 o 1 19 5 1702.64 1990.28 125.51 o 2 0 6 26882.07 26420.96 184.80 o 6 0 6 2324.34 2376.26 103.90 o 0 2 6 74435.16 84193.01 551.29 o 2 2 6 1659.01 1636.39 34.82 o 4 2 6 23920.24 24462.13 163.51 o 6 2 6 1050.32 1047.16 63.47 o 8 2 6 4261.82 4280.82 170.20 o 2 4 6 11014.90 10623.08 93.47 o 4 4 6 691.90 696.11 36.86 o 6 4 6 2699.26 2733.32 92.48 o 8 4 6 231.41 376.98 83.62 o 0 6 6 28252.91 29346.69 209.86 o 2 6 6 54.37 3.29 16.65 o 4 6 6 11957.61 11994.46 126.07 o 6 6 6 0.41 32.72 28.40 o 2 8 6 19099.10 19099.42 147.23 o 4 8 6 51.76 64.56 24.85 o 6 8 6 4184.49 4283.19 113.62 o 0 10 6 27719.72 28636.46 239.64 o 2 10 6 10.33 51.53 18.94 o 4 10 6 12918.35 13091.41 170.15 o 6 10 6 135.44 180.82 53.32 o 2 12 6 1057.20 984.34 48.74 o 4 12 6 103.23 105.74 38.29 o 6 12 6 360.08 410.49 46.97 o 0 14 6 18188.38 18872.37 289.40 o 2 14 6 237.81 242.58 37.91 o 4 14 6 10064.84 10408.41 179.82 o 2 16 6 5708.93 5976.59 130.50 o 4 16 6 111.21 152.77 47.04 o 0 18 6 3119.63 2991.38 177.03 o 2 18 6 25.06 85.58 33.26 o 1 1 7 12438.11 13125.92 93.29 o 3 1 7 7325.21 7230.69 70.14 o 5 1 7 4724.84 4404.19 85.82 o 7 1 7 1061.49 1063.23 74.99 o 1 3 7 5336.46 4936.07 53.22 o 3 3 7 659.12 570.67 23.59 o 5 3 7 2195.67 2037.78 68.81 o 7 3 7 113.23 99.81 45.65 o 1 5 7 42891.63 46049.33 212.70 o 3 5 7 18861.21 19344.19 147.52 o 5 5 7 7931.66 7674.00 126.55 o 7 5 7 2168.03 2168.43 96.70 o 1 7 7 1373.61 1193.92 36.47 o 3 7 7 3603.33 3356.11 64.89 o 5 7 7 413.33 426.97 43.20 o 7 7 7 1648.13 1602.61 102.68 o 1 9 7 529.21 444.84 27.70 o 3 9 7 1579.26 1447.33 54.30 o 5 9 7 1.33 112.19 38.54 o 7 9 7 745.32 736.05 106.66 o 1 11 7 13895.82 14162.48 137.39 o 3 11 7 11252.21 11546.33 142.58 o 5 11 7 5350.35 5250.28 128.09 o 1 13 7 1621.11 1571.45 59.82 o 3 13 7 934.70 932.48 58.94 o 5 13 7 750.17 828.26 65.38 o 1 15 7 3036.95 2915.68 97.98 o 3 15 7 2155.84 2060.31 81.67 o 5 15 7 1232.75 1383.49 79.39 o 1 17 7 782.58 734.91 79.04 o 3 17 7 526.65 531.46 57.39 o 0 0 8 61194.97 64154.96 917.18 o 4 0 8 5207.99 4924.24 111.59 o 8 0 8 254.19 352.76 132.27 o 2 2 8 5617.68 5815.18 65.55 o 4 2 8 322.96 435.49 24.86 o 6 2 8 2104.62 2078.04 82.97 o 8 2 8 184.40 198.14 66.85 o 0 4 8 1262.38 1384.24 47.11 o 2 4 8 4.25 5.04 15.19 o 4 4 8 32.46 -10.59 24.50 o 6 4 8 196.36 238.36 39.86 o 2 6 8 6885.90 6387.29 81.67 o 4 6 8 3.95 2.42 23.19 o 6 6 8 1739.81 1732.77 82.80 o 0 8 8 4811.93 4715.57 92.99 o 2 8 8 64.73 54.36 18.31 o 4 8 8 1895.00 1794.85 69.34 o 6 8 8 24.48 34.74 37.67 o 2 10 8 12757.13 12639.97 129.76 o 4 10 8 9.73 21.76 33.47 o 6 10 8 3402.93 3265.08 118.02 o 0 12 8 3847.78 3704.02 120.52 o 2 12 8 46.87 33.10 25.02 o 4 12 8 1759.23 1740.45 81.25 o 6 12 8 64.69 131.81 44.29 o 2 14 8 6002.88 6078.97 127.66 o 4 14 8 278.51 344.96 42.19 o 0 16 8 3882.58 3858.94 214.71 o 2 16 8 20.86 58.59 35.78 o 4 16 8 2032.96 2126.92 101.52 o 2 18 8 1.01 111.19 36.44 o 1 1 9 232.55 239.03 23.87 o 3 1 9 23.13 56.66 13.02 o 5 1 9 16.84 29.98 25.67 o 7 1 9 11.36 103.08 93.67 o 1 3 9 5750.17 6528.07 66.93 o 3 3 9 2049.62 1933.07 41.96 o 5 3 9 1054.09 961.11 59.42 o 7 3 9 140.19 193.28 60.53 o 1 5 9 18605.25 20242.10 128.86 o 3 5 9 4990.25 4766.32 72.06 o 5 5 9 1965.07 1888.36 83.87 o 7 5 9 565.37 522.07 63.09 o 1 7 9 2707.74 2597.16 50.21 o 3 7 9 3193.25 3036.23 72.99 o 5 7 9 382.03 382.25 53.46 o 7 7 9 311.55 264.48 50.90 o 1 9 9 3537.28 3324.25 65.41 o 3 9 9 2433.90 2321.18 65.84 o 5 9 9 560.23 537.02 52.43 o 7 9 9 734.63 616.59 112.99 o 1 11 9 3722.34 3521.45 74.48 o 3 11 9 2785.14 2701.12 78.72 o 5 11 9 1460.94 1432.85 76.07 o 1 13 9 695.67 764.78 48.51 o 3 13 9 482.65 419.34 55.57 o 5 13 9 278.99 262.37 56.21 o 1 15 9 36.71 62.58 27.11 o 3 15 9 45.52 35.37 39.31 o 1 17 9 850.62 786.32 76.93 o 3 17 9 524.10 489.55 50.10 o 2 0 10 111.12 67.46 29.48 o 6 0 10 583.86 525.28 79.00 o 0 2 10 9303.58 8519.45 100.94 o 2 2 10 0.47 -13.01 13.01 o 4 2 10 3794.78 3508.50 74.58 o 6 2 10 11.53 104.97 35.12 o 2 4 10 23016.56 24228.66 147.47 o 4 4 10 10.04 -18.53 29.05 o 6 4 10 4372.76 4268.56 112.07 o 0 6 10 3876.68 4028.63 78.26 o 2 6 10 4.54 9.25 14.18 o 4 6 10 897.90 828.44 49.01 o 6 6 10 27.15 20.16 34.93 o 2 8 10 4176.03 4005.87 70.88 o 4 8 10 11.24 3.90 26.48 o 6 8 10 1407.26 1485.89 96.11 o 0 10 10 589.39 666.18 56.00 o 2 10 10 15.98 -20.40 20.40 o 4 10 10 41.36 26.69 26.78 o 6 10 10 12.35 -45.29 45.29 o 2 12 10 24103.36 24327.40 225.60 o 4 12 10 20.58 27.85 30.81 o 6 12 10 6750.08 6973.44 179.46 o 0 14 10 80.35 86.55 39.01 o 2 14 10 1.76 31.41 29.59 o 4 14 10 33.51 104.17 31.10 o 2 16 10 42.67 120.59 42.54 o 0 18 10 5166.19 5052.73 425.92 o 1 1 11 9738.51 9099.56 90.56 o 3 1 11 4560.66 4406.63 72.39 o 5 1 11 2088.14 2138.04 78.43 o 7 1 11 1291.17 1170.17 86.87 o 1 3 11 26272.48 28626.82 162.29 o 3 3 11 13324.72 13909.60 126.97 o 5 3 11 7046.20 7088.68 129.35 o 7 3 11 1795.27 1887.95 109.45 o 1 5 11 387.13 618.74 25.48 o 3 5 11 117.10 142.12 25.35 o 5 5 11 183.45 207.58 42.96 o 7 5 11 16.14 28.15 35.95 o 1 7 11 14433.81 14152.23 128.25 o 3 7 11 9986.36 9930.60 126.53 o 5 7 11 4274.39 4354.50 117.28 o 7 7 11 2022.34 2247.40 119.95 o 1 9 11 14422.23 14648.14 147.45 o 3 9 11 10927.43 11108.40 140.76 o 5 9 11 4145.50 4311.56 119.17 o 1 11 11 1.93 13.82 25.43 o 3 11 11 15.24 63.13 39.34 o 5 11 11 31.06 114.41 62.26 o 1 13 11 6589.42 6460.64 118.90 o 3 13 11 4198.71 4180.78 110.06 o 5 13 11 2923.40 2873.37 124.29 o 1 15 11 1328.93 1381.76 88.19 o 3 15 11 1134.66 1112.08 98.50 o 1 17 11 4283.37 4422.10 131.28 o 0 0 12 10772.68 10879.48 227.72 o 4 0 12 6696.87 6392.62 136.66 o 2 2 12 15058.16 14146.23 137.29 o 4 2 12 363.09 355.16 42.27 o 6 2 12 3235.81 3280.03 112.57 o 0 4 12 41551.30 44596.84 298.77 o 2 4 12 113.67 107.16 16.49 o 4 4 12 16023.71 17223.37 193.84 o 6 4 12 69.59 183.96 37.23 o 2 6 12 10152.94 9812.13 117.10 o 4 6 12 15.71 11.34 32.88 o 6 6 12 2713.14 2755.67 94.02 o 0 8 12 16232.06 16727.86 180.35 o 2 8 12 1.23 21.43 22.59 o 4 8 12 7893.02 7724.26 134.39 o 6 8 12 3.54 -14.06 37.56 o 2 10 12 1255.38 1178.58 55.52 o 4 10 12 77.02 134.77 44.61 o 6 10 12 517.46 649.50 69.80 o 0 12 12 32922.19 34406.72 390.73 o 2 12 12 0.64 4.61 23.99 o 4 12 12 17805.59 18111.07 267.21 o 2 14 12 2050.24 1958.70 78.22 o 4 14 12 162.57 271.72 43.86 o 0 16 12 2219.75 2148.02 98.58 o 2 16 12 13.68 34.86 30.19 o 1 1 13 4081.17 3923.80 63.98 o 3 1 13 2997.27 2782.28 62.92 o 5 1 13 1561.51 1636.83 102.02 o 7 1 13 688.88 761.83 70.20 o 1 3 13 16456.37 17548.71 127.98 o 3 3 13 12163.45 12181.58 197.86 o 5 3 13 2948.73 2795.23 86.90 o 7 3 13 2742.43 2802.63 143.59 o 1 5 13 128.33 64.81 16.30 o 3 5 13 427.57 383.71 44.93 o 5 5 13 86.42 95.29 37.17 o 7 5 13 399.49 499.35 83.52 o 1 7 13 6607.84 6546.56 90.99 o 3 7 13 3504.76 3421.28 90.27 o 5 7 13 3773.77 3562.72 106.76 o 1 9 13 10862.62 10854.19 131.15 o 3 9 13 4822.74 4490.23 93.28 o 5 9 13 5458.98 5544.19 134.17 o 1 11 13 140.78 167.40 34.41 o 3 11 13 105.21 98.65 27.90 o 5 11 13 81.97 94.07 45.29 o 1 13 13 4614.10 4566.94 107.58 o 3 13 13 4007.70 3801.52 94.37 o 5 13 13 1620.39 1722.49 104.63 o 1 15 13 1050.50 1096.95 68.44 o 3 15 13 688.58 805.56 86.62 o 1 17 13 2500.22 2622.43 145.22 o 2 0 14 8117.50 7780.06 136.70 o 6 0 14 2383.55 2514.19 154.21 o 0 2 14 205.34 174.17 26.82 o 2 2 14 256.54 274.38 28.55 o 4 2 14 193.46 149.44 41.68 o 6 2 14 659.26 685.08 65.79 o 2 4 14 4374.74 4407.75 73.56 o 4 4 14 196.99 146.44 40.01 o 6 4 14 1450.50 1335.03 77.03 o 0 6 14 2329.16 2228.79 66.90 o 2 6 14 0.44 8.02 20.09 o 4 6 14 1019.76 915.06 62.93 o 6 6 14 14.30 84.22 42.09 o 2 8 14 2811.77 2718.76 71.33 o 4 8 14 17.95 55.60 31.98 o 6 8 14 844.67 896.60 60.84 o 0 10 14 7.49 122.09 42.31 o 2 10 14 16.24 114.09 27.82 o 4 10 14 5.65 66.74 35.14 o 6 10 14 96.88 104.32 51.52 o 2 12 14 5989.20 5586.25 112.40 o 4 12 14 49.12 24.56 36.49 o 0 14 14 26.84 94.11 66.03 o 2 14 14 174.33 234.37 49.65 o 4 14 14 9.66 78.81 33.71 o 2 16 14 820.90 892.34 67.40 o 1 1 15 889.63 882.23 38.64 o 3 1 15 600.25 512.41 38.11 o 5 1 15 114.07 77.42 55.68 o 7 1 15 124.67 118.24 54.16 o 1 3 15 1097.47 1126.59 42.84 o 3 3 15 50.22 87.13 28.46 o 5 3 15 573.23 560.84 54.01 o 7 3 15 40.92 115.18 48.59 o 1 5 15 292.19 359.09 28.75 o 3 5 15 275.72 309.33 45.28 o 5 5 15 19.96 74.42 41.91 o 1 7 15 918.14 898.46 44.27 o 3 7 15 34.63 18.86 34.84 o 5 7 15 820.52 808.59 63.08 o 1 9 15 113.26 47.86 26.11 o 3 9 15 741.95 766.28 58.84 o 5 9 15 36.26 105.67 38.08 o 1 11 15 735.93 666.75 50.57 o 3 11 15 461.71 492.42 51.23 o 5 11 15 332.52 398.65 69.68 o 1 13 15 150.64 229.62 33.78 o 3 13 15 27.60 40.09 35.17 o 1 15 15 109.12 146.10 40.51 o 3 15 15 81.17 66.90 58.73 o 0 0 16 2053.85 2087.32 116.30 o 4 0 16 444.04 418.33 63.83 o 2 2 16 14428.04 14589.76 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21 10.46 14.07 36.88 o 3 1 21 4.24 69.01 32.05 o 5 1 21 25.58 -20.59 77.73 o 1 3 21 83.87 89.50 36.18 o 3 3 21 71.04 44.80 44.98 o 5 3 21 111.83 175.25 82.49 o 1 5 21 1974.00 1980.16 88.66 o 3 5 21 1130.20 1142.44 66.52 o 5 5 21 783.89 889.76 55.99 o 1 7 21 880.67 699.46 76.14 o 3 7 21 563.49 519.92 51.42 o 5 7 21 462.77 636.54 51.42 o 1 9 21 221.68 214.51 52.93 o 3 9 21 335.31 347.08 42.87 o 1 11 21 106.38 263.50 67.55 o 3 11 21 17.41 58.81 36.04 o 1 13 21 60.26 90.48 34.74 o 2 0 22 21392.68 22360.67 329.16 o 0 2 22 62.72 70.32 53.39 o 2 2 22 17.50 16.87 37.62 o 4 2 22 27.09 79.88 43.81 o 2 4 22 2369.12 2323.75 102.33 o 4 4 22 3.32 63.51 30.52 o 0 6 22 4711.47 4205.93 182.63 o 2 6 22 20.06 92.80 40.23 o 4 6 22 2367.47 2468.86 128.11 o 2 8 22 1073.71 1088.65 79.46 o 4 8 22 0.00 39.33 46.25 o 0 10 22 3743.38 3795.43 219.83 o 2 10 22 17.74 34.06 35.63 o 2 12 22 913.58 1241.71 92.93 o 1 1 23 2614.96 2599.77 85.70 o 3 1 23 1795.39 1713.40 112.61 o 5 1 23 1152.51 1218.45 140.06 o 1 3 23 2624.56 2566.73 93.84 o 3 3 23 2718.35 2673.13 103.09 o 5 3 23 858.37 1163.43 96.90 o 1 5 23 4428.29 4174.04 115.48 o 3 5 23 3653.67 3812.81 107.85 o 1 7 23 916.93 1072.51 92.08 o 3 7 23 324.60 305.67 56.37 o 1 9 23 3912.13 3599.84 134.40 o 3 9 23 1984.52 1771.24 107.77 o 1 11 23 1143.33 1200.71 106.11 o 0 0 24 18434.61 19273.82 576.59 o 4 0 24 10016.38 9918.07 380.62 o 2 2 24 1124.87 1183.49 77.03 o 4 2 24 206.07 180.56 58.83 o 0 4 24 8322.73 8161.26 253.10 o 2 4 24 13.01 34.68 53.99 o 4 4 24 4736.54 5015.87 174.42 o 2 6 24 5816.10 5717.96 148.90 o 4 6 24 10.82 77.24 36.80 o 0 8 24 2644.91 2582.44 183.85 o 2 8 24 2.28 154.15 58.56 o 2 10 24 3857.29 3660.27 133.35 o 1 1 25 1779.51 1915.51 80.91 o 3 1 25 1202.53 1237.55 129.45 o 1 3 25 2018.62 2134.99 92.18 o 3 3 25 933.71 966.07 102.08 o 1 5 25 1077.48 1022.96 89.77 o 3 5 25 622.76 734.22 64.56 o 1 7 25 958.07 965.38 90.85 o 3 7 25 1386.65 1539.51 92.38 o 1 9 25 2502.63 2403.49 119.59 o 2 0 26 1259.90 1102.80 221.96 o 0 2 26 4.46 83.11 65.41 o 2 2 26 85.26 104.23 34.37 o 2 4 26 2041.35 2112.24 97.46 o 0 6 26 588.82 669.13 99.84 o 2 6 26 0.65 74.21 65.75 o 1 1 27 42.24 0.99 33.80 o 3 1 27 4.65 140.09 56.51 o 1 3 27 14.84 -33.80 33.80 o 1 5 27 1008.93 1171.40 96.02 o 1 7 27 35.57 106.05 52.89 o 0 0 28 2948.65 3256.79 260.63 o 2 2 28 2122.19 2214.04 114.72 o 0 4 28 206.20 300.39 66.23 o