#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2213326.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213326_Fobs loop_ _publ_author_name 'Mersmann, Klaus' 'N\"ather, Christian' 'Tuczek, Felix' _publ_section_title ; Chloridobis[1,2-bis(diphenylphosphino)ethane](ethylimido)molybdenum(IV) tetraphenylborate acetonitrile disolvate ; _journal_coeditor_code GW2011 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1476 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.387 _cell_angle_gamma 90.000 _cell_length_a 15.3299 _cell_length_b 21.5840 _cell_length_c 21.3439 _exptl_crystal_F_000 2864.00 _reflns_d_resolution_high 0.7826 _[local]_cod_data_source_file gw2011Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' (Felix28)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 305.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 25555.57 27728.15 615.09 o 4 0 0 918.16 845.44 93.37 o 6 0 0 18855.47 20362.99 228.60 o 8 0 0 17757.18 17695.42 452.71 o 10 0 0 5957.07 6250.42 246.75 o 12 0 0 2122.62 2474.18 106.07 o 14 0 0 1881.35 1971.99 74.39 o 16 0 0 58.22 90.34 72.45 o 18 0 0 1079.39 960.55 127.56 o 2 1 0 6275.34 7527.23 108.05 o 3 1 0 30820.33 30621.32 288.35 o 4 1 0 57005.34 61355.09 683.20 o 5 1 0 7337.90 7454.67 73.06 o 6 1 0 10.50 -16.01 41.12 o 7 1 0 16697.52 16496.54 420.15 o 8 1 0 10310.13 11584.92 276.01 o 9 1 0 23039.51 25186.76 446.71 o 10 1 0 0.82 7.42 34.96 o 11 1 0 1456.78 1410.16 52.00 o 12 1 0 2413.33 2509.56 154.23 o 13 1 0 5369.46 5550.48 74.72 o 14 1 0 994.02 932.05 55.47 o 15 1 0 5.61 6.20 60.16 o 16 1 0 11.21 5.90 60.83 o 17 1 0 82.73 105.04 59.76 o 18 1 0 0.40 13.63 87.81 o 19 1 0 1462.69 1374.43 155.51 o 1 2 0 2156.11 2181.30 93.32 o 2 2 0 8592.18 7695.76 129.52 o 3 2 0 32253.63 33841.82 226.93 o 4 2 0 15898.87 16104.19 231.12 o 5 2 0 6023.93 6006.53 139.72 o 6 2 0 407.11 361.52 47.58 o 7 2 0 4150.68 4441.38 79.44 o 8 2 0 19516.98 20060.62 237.24 o 9 2 0 6785.07 6815.45 140.79 o 10 2 0 11.64 104.65 35.36 o 11 2 0 329.31 301.69 45.35 o 12 2 0 358.44 424.69 68.94 o 13 2 0 164.62 190.51 48.28 o 14 2 0 148.25 197.56 54.49 o 15 2 0 4276.94 4461.49 256.74 o 16 2 0 1270.83 1326.58 90.02 o 17 2 0 118.04 151.58 61.22 o 18 2 0 1770.59 1713.64 150.24 o 19 2 0 27.23 30.75 87.53 o 1 3 0 791.48 739.90 100.07 o 2 3 0 207.47 15.74 60.89 o 3 3 0 7399.30 7534.02 92.17 o 4 3 0 11081.82 10501.70 167.70 o 5 3 0 983.65 640.13 48.91 o 6 3 0 6413.79 6836.68 91.38 o 7 3 0 8.86 59.74 33.42 o 8 3 0 2054.18 2420.82 40.62 o 9 3 0 182.88 263.38 34.75 o 10 3 0 113.98 95.92 39.15 o 11 3 0 2234.91 2198.90 55.58 o 12 3 0 17.56 5.12 67.96 o 13 3 0 1834.11 1875.89 73.83 o 14 3 0 705.82 806.03 55.86 o 15 3 0 527.80 498.10 63.45 o 16 3 0 4.84 233.58 73.71 o 17 3 0 22.32 -49.33 60.67 o 18 3 0 18.60 120.28 71.69 o 19 3 0 243.04 261.37 72.25 o 0 4 0 92.41 210.79 125.58 o 1 4 0 158.63 82.60 76.10 o 2 4 0 30241.47 30674.44 927.94 o 3 4 0 2672.01 1882.81 69.07 o 4 4 0 25398.58 26227.60 487.44 o 5 4 0 7548.95 7618.07 195.53 o 6 4 0 38286.48 40827.36 754.28 o 7 4 0 7483.77 8123.67 172.59 o 8 4 0 5974.75 5809.39 95.00 o 9 4 0 77.16 35.49 32.29 o 10 4 0 6548.51 6647.46 151.74 o 11 4 0 1317.80 1359.72 75.25 o 12 4 0 303.78 348.52 57.54 o 13 4 0 2721.47 2628.24 64.71 o 14 4 0 1850.52 1985.61 87.82 o 15 4 0 171.75 197.66 49.76 o 16 4 0 420.74 581.43 63.12 o 17 4 0 252.06 204.09 74.61 o 18 4 0 136.53 199.32 72.80 o 19 4 0 64.59 172.65 78.57 o 2 5 0 3990.50 4521.11 133.58 o 3 5 0 44759.76 51937.12 235.89 o 4 5 0 1204.34 1329.61 61.59 o 5 5 0 68940.70 75657.07 2070.50 o 6 5 0 3595.61 3896.69 71.95 o 7 5 0 4028.85 3476.91 68.37 o 8 5 0 6433.60 6416.94 244.76 o 9 5 0 1145.34 1302.23 50.04 o 10 5 0 26.30 66.65 55.11 o 11 5 0 2025.69 2065.02 78.17 o 12 5 0 3447.90 3221.27 69.95 o 13 5 0 4336.85 4293.04 90.52 o 14 5 0 90.67 94.77 50.61 o 15 5 0 2520.90 2863.78 77.09 o 16 5 0 349.65 319.44 62.57 o 17 5 0 1821.01 1668.73 134.97 o 18 5 0 0.18 75.72 87.05 o 19 5 0 278.89 380.76 87.59 o 1 6 0 17410.39 18786.62 518.73 o 2 6 0 40239.66 42796.81 315.63 o 3 6 0 7416.49 8605.18 130.12 o 4 6 0 63037.35 71259.02 839.82 o 5 6 0 7548.98 7867.19 161.71 o 6 6 0 6238.49 5626.16 123.17 o 7 6 0 38.67 15.66 40.96 o 8 6 0 924.56 822.53 50.74 o 9 6 0 10940.41 11365.81 331.72 o 10 6 0 4318.03 4615.21 265.92 o 11 6 0 1764.64 1892.56 75.22 o 12 6 0 4474.82 4263.61 76.98 o 13 6 0 3613.42 3633.91 67.35 o 14 6 0 3864.10 3901.07 176.80 o 15 6 0 1313.48 1242.64 65.59 o 16 6 0 2049.31 2065.31 69.27 o 17 6 0 322.22 334.53 92.74 o 18 6 0 529.96 384.72 73.39 o 1 7 0 8198.18 7561.44 228.24 o 2 7 0 758.71 553.65 89.39 o 3 7 0 31670.18 31928.53 249.39 o 4 7 0 128.53 40.97 64.43 o 5 7 0 23321.59 25383.80 962.64 o 6 7 0 332.09 329.29 48.25 o 7 7 0 4365.82 4625.29 144.62 o 8 7 0 2372.51 2657.96 72.68 o 9 7 0 706.23 854.33 43.68 o 10 7 0 907.10 793.10 58.31 o 11 7 0 1668.60 1719.50 95.42 o 12 7 0 1617.98 1702.92 63.19 o 13 7 0 1732.38 1789.03 279.52 o 14 7 0 85.15 33.38 50.26 o 15 7 0 316.18 341.27 62.27 o 16 7 0 0.49 -55.30 72.72 o 17 7 0 854.87 958.48 77.96 o 18 7 0 191.09 123.02 72.48 o 0 8 0 1053.07 948.27 106.76 o 1 8 0 9.63 31.67 58.16 o 2 8 0 250.48 330.82 70.52 o 3 8 0 5297.45 5598.67 129.82 o 4 8 0 5.86 88.83 50.75 o 5 8 0 3515.67 4076.84 83.90 o 6 8 0 438.15 547.83 58.65 o 7 8 0 226.42 293.46 45.50 o 8 8 0 74.40 94.18 45.50 o 9 8 0 1023.30 973.62 50.56 o 10 8 0 27.80 235.70 69.67 o 11 8 0 4260.79 4257.86 81.17 o 12 8 0 25.73 -12.99 55.13 o 13 8 0 0.61 58.27 62.09 o 14 8 0 793.47 746.98 53.30 o 15 8 0 17.36 22.43 73.05 o 16 8 0 6.89 -33.54 73.43 o 17 8 0 11.09 104.55 61.65 o 18 8 0 8.20 167.66 114.80 o 1 9 0 16027.79 17511.07 548.04 o 2 9 0 427.89 519.82 63.95 o 3 9 0 12718.27 12925.29 148.47 o 4 9 0 537.94 697.01 89.72 o 5 9 0 7083.46 7284.64 205.32 o 6 9 0 1773.94 1651.35 65.70 o 7 9 0 2881.48 3205.55 132.23 o 8 9 0 1282.35 1274.13 67.21 o 9 9 0 883.40 785.59 50.22 o 10 9 0 550.96 623.35 89.60 o 11 9 0 3778.31 3837.94 73.92 o 12 9 0 165.37 223.27 66.79 o 13 9 0 2281.53 2404.86 214.06 o 14 9 0 146.75 115.87 52.52 o 15 9 0 71.98 106.24 73.25 o 16 9 0 1410.83 1274.94 102.97 o 17 9 0 724.83 1040.66 77.37 o 18 9 0 163.30 156.70 89.42 o 0 10 0 11392.28 10274.44 384.14 o 1 10 0 595.52 696.58 58.07 o 2 10 0 18354.28 18168.31 489.02 o 3 10 0 2713.60 3539.83 92.97 o 4 10 0 21566.05 21750.33 185.85 o 5 10 0 673.89 576.48 83.40 o 6 10 0 6283.80 7142.80 171.19 o 7 10 0 224.11 138.70 63.65 o 8 10 0 1598.21 1490.73 54.94 o 9 10 0 2154.45 2210.99 85.84 o 10 10 0 8780.42 8911.84 455.38 o 11 10 0 1451.89 1568.49 135.94 o 12 10 0 4176.64 3840.79 120.34 o 13 10 0 1128.67 1146.68 90.50 o 14 10 0 4.00 -82.99 105.31 o 15 10 0 396.59 397.61 75.07 o 16 10 0 833.77 840.39 63.86 o 17 10 0 2496.84 2161.92 98.09 o 18 10 0 4492.17 4096.81 109.66 o 1 11 0 21211.76 22040.54 737.58 o 2 11 0 947.27 850.47 64.99 o 3 11 0 24297.84 26137.50 197.27 o 4 11 0 3040.57 3264.89 83.12 o 5 11 0 10765.27 11337.14 137.60 o 6 11 0 4624.40 5204.81 330.90 o 7 11 0 3691.64 3816.77 72.21 o 8 11 0 1036.81 947.05 65.90 o 9 11 0 19420.47 21114.23 1147.88 o 10 11 0 376.19 300.88 61.65 o 11 11 0 7868.02 8214.46 353.83 o 12 11 0 4002.42 3950.56 130.41 o 13 11 0 15.73 58.61 64.23 o 14 11 0 1175.00 1112.68 65.19 o 15 11 0 2.48 17.13 73.48 o 16 11 0 77.83 70.92 63.26 o 17 11 0 3126.57 2836.03 100.66 o 0 12 0 21889.35 21772.11 1421.81 o 1 12 0 178.78 276.44 55.98 o 2 12 0 17781.45 18813.87 587.30 o 3 12 0 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