#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:28:51 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181053 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/33/2213329.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213329_Fobs loop_ _publ_author_name 'Ho, Soo Yei' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; {(Z)-O-Ethyl N-[4-(methoxycarbonyl)phenyl]thiocarbamato-\kS}(tricyclohexylphosphine-\kP)gold(I) ; _journal_coeditor_code HB2336 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1211 _journal_page_last m1213 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.837 _cell_angle_gamma 90.000 _cell_length_a 15.2963 _cell_length_b 9.1081 _cell_length_c 22.2657 _exptl_crystal_F_000 1440.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file hb2336Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n, -50C' _shelx_refln_list_code 4 _shelx_f_calc_maximum 457.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 43.24 -19.19 12.79 o 4 0 0 125802.17 126528.15 6077.36 o 6 0 0 300.65 310.91 34.55 o 8 0 0 26984.23 26612.46 1296.08 o 10 0 0 173.65 139.46 42.22 o 12 0 0 23379.51 23534.24 814.16 o 14 0 0 1827.41 1465.14 91.43 o 16 0 0 9173.65 9447.91 361.80 o 18 0 0 588.60 616.69 130.50 o 1 1 0 10388.80 12137.50 288.28 o 2 1 0 97311.63 104334.39 2865.29 o 3 1 0 42880.64 48129.64 1321.06 o 4 1 0 6030.72 5830.54 166.04 o 5 1 0 8719.07 8239.16 233.41 o 6 1 0 20125.42 19325.21 537.94 o 7 1 0 3014.92 2730.09 87.10 o 8 1 0 46.45 31.55 21.21 o 9 1 0 2563.12 2343.17 108.68 o 10 1 0 18111.88 18386.88 520.47 o 11 1 0 1825.28 1686.73 71.58 o 12 1 0 384.76 393.53 50.49 o 13 1 0 2408.19 2306.17 125.31 o 14 1 0 8586.23 8500.74 263.12 o 15 1 0 2353.30 2297.14 104.46 o 16 1 0 8.51 -10.89 41.49 o 17 1 0 299.79 396.15 65.03 o 18 1 0 2920.90 2849.96 131.31 o 19 1 0 665.95 701.71 98.91 o 0 2 0 103272.31 104996.93 2872.87 o 1 2 0 65146.12 74165.21 1568.12 o 2 2 0 6958.78 7392.61 180.19 o 3 2 0 38858.17 40310.89 1097.21 o 4 2 0 6612.21 6254.80 441.41 o 5 2 0 58031.82 62041.89 1704.55 o 6 2 0 2064.93 2225.00 72.17 o 7 2 0 8232.10 7518.87 217.38 o 8 2 0 3413.08 3189.44 126.11 o 9 2 0 7566.40 7850.56 231.63 o 10 2 0 719.67 666.88 39.93 o 11 2 0 9006.47 8822.70 313.11 o 12 2 0 3299.21 3089.40 225.82 o 13 2 0 9457.77 8878.53 457.40 o 14 2 0 598.43 556.01 66.38 o 15 2 0 3205.54 3327.51 291.71 o 16 2 0 1280.82 1318.34 101.82 o 17 2 0 4464.80 4248.03 164.46 o 18 2 0 3.75 2.08 49.77 o 19 2 0 241.56 211.70 79.17 o 1 3 0 29752.11 31006.46 603.30 o 2 3 0 1255.52 1386.71 37.58 o 3 3 0 27407.59 26970.05 642.71 o 4 3 0 2556.18 2811.02 117.63 o 5 3 0 31917.01 32697.04 1103.71 o 6 3 0 35.05 34.55 34.55 o 7 3 0 11622.20 11757.03 353.99 o 8 3 0 55.17 38.67 18.03 o 9 3 0 13264.17 13341.58 381.64 o 10 3 0 78.67 153.37 39.68 o 11 3 0 6793.05 6285.91 346.73 o 12 3 0 1295.94 1196.88 179.76 o 13 3 0 5542.74 5152.20 421.58 o 14 3 0 6.12 -0.15 48.56 o 15 3 0 5324.23 4886.88 217.47 o 16 3 0 1.31 -7.02 56.07 o 17 3 0 1277.24 1288.67 106.56 o 18 3 0 32.98 67.76 70.90 o 19 3 0 1916.61 1747.32 109.69 o 0 4 0 33468.45 35607.94 982.86 o 1 4 0 7925.95 8120.02 180.82 o 2 4 0 9904.96 10172.68 233.36 o 3 4 0 16877.06 16971.55 367.15 o 4 4 0 14094.22 14373.40 350.81 o 5 4 0 9210.67 9043.91 261.82 o 6 4 0 23.15 49.62 29.39 o 7 4 0 9727.15 9104.53 327.95 o 8 4 0 7523.84 7322.25 271.87 o 9 4 0 9358.28 8704.82 321.46 o 10 4 0 188.21 228.01 47.49 o 11 4 0 2917.07 2802.68 137.97 o 12 4 0 4994.56 4596.43 197.23 o 13 4 0 5376.91 5347.31 271.88 o 14 4 0 9.22 -60.23 51.82 o 15 4 0 1003.64 930.64 91.99 o 16 4 0 1637.23 1865.87 151.61 o 17 4 0 853.45 663.36 90.20 o 18 4 0 243.47 101.58 152.89 o 1 5 0 1114.94 1197.27 84.97 o 2 5 0 24697.21 24849.02 489.35 o 3 5 0 3662.97 3582.40 81.32 o 4 5 0 1043.22 1096.57 51.52 o 5 5 0 5747.83 6059.50 160.35 o 6 5 0 21750.12 20566.46 710.19 o 7 5 0 7203.32 6683.58 253.67 o 8 5 0 8.17 52.63 43.50 o 9 5 0 1390.25 1384.33 99.80 o 10 5 0 13403.21 14043.19 706.25 o 11 5 0 4578.57 4252.88 187.17 o 12 5 0 35.95 110.41 50.16 o 13 5 0 287.76 244.59 136.26 o 14 5 0 2481.49 2415.62 137.04 o 15 5 0 671.52 672.84 85.89 o 16 5 0 37.11 -2.81 67.94 o 17 5 0 143.91 188.21 79.29 o 0 6 0 21211.66 22805.14 639.79 o 1 6 0 809.73 854.78 31.53 o 2 6 0 12.96 38.74 15.98 o 3 6 0 1538.89 1430.84 73.53 o 4 6 0 25454.84 26693.22 579.99 o 5 6 0 303.09 357.44 34.29 o 6 6 0 812.79 711.52 51.48 o 7 6 0 109.10 195.52 88.28 o 8 6 0 25672.18 25605.53 1237.22 o 9 6 0 63.85 14.33 47.44 o 10 6 0 148.42 182.27 51.63 o 11 6 0 336.68 368.47 114.51 o 12 6 0 7490.43 6970.73 426.69 o 13 6 0 0.54 -60.58 52.47 o 14 6 0 324.55 340.14 75.42 o 15 6 0 116.21 174.12 100.44 o 16 6 0 2418.73 2442.38 157.70 o 17 6 0 75.77 -18.15 101.72 o 1 7 0 5968.56 5465.46 122.50 o 2 7 0 12463.80 12495.11 256.80 o 3 7 0 693.53 727.71 40.18 o 4 7 0 114.59 121.63 28.04 o 5 7 0 7172.14 6590.74 308.12 o 6 7 0 14222.35 13790.50 388.00 o 7 7 0 1252.83 1286.01 102.36 o 8 7 0 176.26 162.47 52.10 o 9 7 0 1503.44 1549.87 110.67 o 10 7 0 8935.99 8148.78 486.83 o 11 7 0 1024.09 969.97 90.52 o 12 7 0 608.10 556.69 80.46 o 13 7 0 445.90 396.06 80.88 o 14 7 0 907.42 961.21 101.93 o 15 7 0 932.21 958.88 108.12 o 0 8 0 1755.24 1873.48 103.83 o 1 8 0 3628.97 3385.19 125.88 o 2 8 0 63.56 59.59 34.36 o 3 8 0 8535.06 8089.36 195.82 o 4 8 0 1912.04 2083.06 73.56 o 5 8 0 4727.44 4642.37 178.28 o 6 8 0 97.60 142.00 50.92 o 7 8 0 5761.44 5666.17 170.60 o 8 8 0 1172.51 1170.66 82.92 o 9 8 0 5322.02 5127.59 330.10 o 10 8 0 14.22 77.25 109.39 o 11 8 0 1354.67 1488.26 182.32 o 12 8 0 516.25 668.54 88.83 o 13 8 0 2661.45 2810.50 164.65 o 14 8 0 176.42 132.75 78.37 o 1 9 0 6150.94 6007.16 175.52 o 2 9 0 426.38 347.17 38.72 o 3 9 0 4324.27 4224.43 120.13 o 4 9 0 414.66 388.05 41.74 o 5 9 0 6322.29 6428.36 253.80 o 6 9 0 252.34 261.11 41.80 o 7 9 0 4097.24 4088.31 139.77 o 8 9 0 101.19 70.82 50.97 o 9 9 0 1238.75 1453.97 170.81 o 10 9 0 391.28 326.94 64.32 o 11 9 0 2630.25 2690.17 250.18 o 12 9 0 24.27 5.53 70.97 o 0 10 0 1916.86 1823.67 123.04 o 1 10 0 2458.06 2497.93 118.93 o 2 10 0 492.82 482.66 55.96 o 3 10 0 965.92 989.63 67.07 o 4 10 0 2379.69 2421.96 89.02 o 5 10 0 1598.56 1577.24 84.58 o 6 10 0 111.85 194.71 50.25 o 7 10 0 485.37 524.35 62.67 o 8 10 0 2682.97 2455.03 172.44 o 9 10 0 720.03 706.33 84.76 o 10 10 0 431.80 488.45 88.13 o 1 11 0 581.31 578.17 75.97 o 2 11 0 3925.34 3930.01 183.85 o 3 11 0 921.41 1108.29 89.00 o 4 11 0 0.59 9.42 59.65 o 5 11 0 13.61 -24.89 77.94 o 6 11 0 1843.15 2035.39 116.67 o 7 11 0 129.82 128.96 83.60 o -19 0 1 901.68 825.24 149.70 o -17 0 1 4586.16 5019.26 322.42 o -15 0 1 1785.51 1664.53 148.42 o -13 0 1 29667.04 29144.48 1434.26 o -11 0 1 2697.29 2414.31 152.25 o -9 0 1 25347.95 25087.36 1224.43 o -7 0 1 11733.67 11745.31 580.87 o -5 0 1 46836.42 46089.45 2223.68 o -3 0 1 22430.08 21312.36 697.94 o 1 0 1 7923.96 9456.38 469.56 o 3 0 1 95761.19 97001.13 4664.86 o 5 0 1 11787.80 12763.74 624.37 o 7 0 1 17884.53 17944.21 877.70 o 9 0 1 295.93 321.82 33.70 o 11 0 1 16285.16 14836.24 1375.40 o 13 0 1 606.21 622.44 83.80 o 15 0 1 12359.05 12091.78 479.79 o 17 0 1 0.31 -14.07 89.56 o 19 0 1 3678.46 4414.08 313.46 o -19 1 1 1430.49 1492.80 127.52 o -18 1 1 84.93 73.86 48.40 o -17 1 1 1025.02 966.18 74.59 o -16 1 1 3274.67 3312.62 135.26 o -15 1 1 8020.88 7451.43 332.66 o -14 1 1 545.09 513.48 48.10 o -13 1 1 1606.36 1493.47 72.23 o -12 1 1 7189.02 7119.58 219.17 o -11 1 1 16679.52 15760.67 451.76 o -10 1 1 3600.74 3432.91 122.47 o -9 1 1 3256.15 2884.53 95.72 o -8 1 1 8704.93 8573.98 248.06 o -7 1 1 9964.74 9586.24 273.76 o -6 1 1 3441.01 3384.69 103.33 o -5 1 1 119.36 135.69 21.40 o -4 1 1 15633.45 14666.04 408.03 o -3 1 1 60468.49 63365.82 1689.36 o -2 1 1 10272.58 10740.33 257.02 o -1 1 1 5875.02 5334.64 104.12 o 0 1 1 61602.00 58944.19 1248.27 o 1 1 1 79619.86 80311.45 1700.88 o 2 1 1 37256.12 39785.62 1921.73 o 3 1 1 62249.21 68040.61 1866.86 o 4 1 1 14841.05 15686.37 435.54 o 5 1 1 42226.18 44072.83 1212.78 o 6 1 1 10488.94 10861.62 307.02 o 7 1 1 110.70 104.10 16.54 o 8 1 1 7065.88 7031.31 206.47 o 9 1 1 11806.00 11440.21 329.17 o 10 1 1 1825.80 1687.99 68.83 o 11 1 1 23.63 18.18 26.38 o 12 1 1 3809.85 3746.22 129.13 o 13 1 1 10681.91 10701.85 377.43 o 14 1 1 973.17 890.98 91.04 o 15 1 1 9.53 -1.55 38.92 o 16 1 1 1340.34 1280.77 79.73 o 17 1 1 5865.36 5987.26 209.93 o 18 1 1 896.05 829.09 88.97 o 19 1 1 22.03 4.79 111.31 o -19 2 1 182.65 153.43 63.59 o -18 2 1 3377.20 3587.52 160.75 o -17 2 1 1035.71 875.72 92.54 o -16 2 1 600.92 624.81 78.37 o -15 2 1 132.93 135.46 57.78 o -14 2 1 7791.81 7588.90 631.41 o -13 2 1 3156.89 2754.13 136.42 o -12 2 1 3349.34 3134.60 153.79 o -11 2 1 2025.43 1986.52 104.23 o -10 2 1 11767.61 12006.85 346.74 o -9 2 1 4216.13 4028.07 243.28 o -8 2 1 5940.89 5513.58 165.74 o -7 2 1 6388.91 6769.32 197.49 o -6 2 1 22322.57 23544.71 652.84 o -5 2 1 20806.31 22233.19 616.48 o -4 2 1 1107.51 1119.42 38.39 o -3 2 1 17.45 35.99 18.13 o -2 2 1 52461.66 54870.74 1162.95 o -1 2 1 16012.57 17344.65 338.65 o 0 2 1 11658.86 11453.00 225.46 o 1 2 1 580.41 615.03 18.30 o 2 2 1 59289.72 61812.73 1182.46 o 3 2 1 5076.75 5259.96 207.22 o 4 2 1 14473.60 14854.80 578.30 o 5 2 1 14574.00 14880.94 519.67 o 6 2 1 26303.53 27579.01 764.16 o 7 2 1 5615.50 5714.62 168.80 o 8 2 1 8376.69 8343.61 242.49 o 9 2 1 24.63 38.01 21.33 o 10 2 1 8092.55 7866.79 234.54 o 11 2 1 5678.21 5463.87 190.74 o 12 2 1 2409.11 2284.61 110.56 o 13 2 1 6.31 -16.63 42.49 o 14 2 1 5380.78 5210.19 220.74 o 15 2 1 1731.76 1727.42 236.70 o 16 2 1 2248.58 2181.90 340.33 o 17 2 1 7.79 0.24 48.56 o 18 2 1 1917.83 1955.09 106.38 o 19 2 1 835.27 928.92 84.62 o -19 3 1 5.43 -55.59 75.01 o -18 3 1 352.68 347.33 83.61 o -17 3 1 278.33 324.70 75.34 o -16 3 1 6559.69 6713.24 580.23 o -15 3 1 368.37 343.56 66.09 o -14 3 1 1314.49 1239.91 93.37 o -13 3 1 139.27 103.61 98.52 o -12 3 1 19261.80 18200.11 918.64 o -11 3 1 1060.99 771.97 65.97 o -10 3 1 2633.86 2327.59 86.28 o -9 3 1 714.77 689.13 37.62 o -8 3 1 28565.21 28620.71 796.20 o -7 3 1 1268.74 1250.11 47.74 o -6 3 1 2125.31 1875.59 83.22 o -5 3 1 2055.55 2098.67 120.91 o -4 3 1 34310.05 34858.48 1167.07 o -3 3 1 956.65 903.11 55.93 o -2 3 1 9594.30 9972.07 216.89 o -1 3 1 1525.12 1391.40 34.39 o 0 3 1 52786.02 55858.60 1083.04 o 1 3 1 1156.27 1348.24 33.25 o 2 3 1 39231.86 42260.41 898.65 o 3 3 1 880.11 748.26 30.19 o 4 3 1 38342.16 37941.59 1154.32 o 5 3 1 5914.49 5888.03 480.43 o 6 3 1 7402.08 7437.55 741.44 o 7 3 1 17.28 34.64 14.88 o 8 3 1 23917.88 25017.00 698.77 o 9 3 1 108.52 94.10 30.93 o 10 3 1 6239.35 4415.36 255.89 o 11 3 1 383.50 276.49 50.16 o 12 3 1 8827.55 8657.53 508.58 o 13 3 1 95.65 124.08 53.10 o 14 3 1 3617.43 3464.16 162.58 o 15 3 1 244.50 153.83 58.06 o 16 3 1 3569.38 3064.33 268.68 o 17 3 1 165.53 181.61 68.99 o 18 3 1 1437.56 1454.78 96.26 o -18 4 1 2107.58 2019.50 141.54 o -17 4 1 810.99 770.73 112.59 o -16 4 1 156.91 146.49 68.49 o -15 4 1 872.03 967.69 93.40 o -14 4 1 3019.91 2901.93 206.63 o -13 4 1 3100.70 2678.23 139.90 o -12 4 1 420.78 434.59 58.62 o -11 4 1 50.65 34.43 80.61 o -10 4 1 21138.35 20682.54 721.04 o -9 4 1 4998.94 4739.56 189.96 o -8 4 1 1462.91 1368.55 86.36 o -7 4 1 310.45 425.95 53.74 o -6 4 1 32044.11 33910.04 1149.53 o -5 4 1 3962.26 3789.27 120.61 o -4 4 1 10042.99 10266.38 253.94 o -3 4 1 4861.77 4753.15 109.69 o -2 4 1 12931.31 12740.27 253.95 o -1 4 1 12793.31 13633.81 269.94 o 0 4 1 16505.81 16828.21 332.03 o 1 4 1 7245.37 8085.36 164.13 o 2 4 1 9037.75 8995.72 182.06 o 3 4 1 26942.14 29044.43 622.00 o 4 4 1 10840.92 11060.04 299.94 o 5 4 1 35.90 53.32 27.87 o 6 4 1 23698.18 23362.82 799.41 o 7 4 1 14216.04 14335.07 510.50 o 8 4 1 7318.74 6940.86 401.75 o 9 4 1 3141.10 2723.02 125.60 o 10 4 1 5737.14 5385.15 432.45 o 11 4 1 2629.65 2338.91 121.66 o 12 4 1 7580.92 7413.69 288.45 o 13 4 1 1047.38 980.78 163.77 o 14 4 1 1531.21 1439.30 103.44 o 15 4 1 1793.60 1611.12 113.84 o 16 4 1 1102.70 1007.48 95.87 o 17 4 1 1.62 -5.78 63.92 o 18 4 1 1162.83 1170.09 115.78 o -17 5 1 620.72 764.15 118.35 o -16 5 1 677.14 727.86 112.59 o -15 5 1 3655.65 3537.93 184.07 o -14 5 1 79.33 194.12 94.68 o -13 5 1 1168.23 1203.03 99.80 o -12 5 1 1686.91 1677.90 105.33 o -11 5 1 7352.50 7584.63 294.40 o -10 5 1 7.84 5.02 39.53 o -9 5 1 443.90 523.91 133.06 o -8 5 1 5980.88 5505.30 217.11 o -7 5 1 25231.31 25702.68 883.87 o -6 5 1 95.23 128.71 30.80 o -5 5 1 2480.25 2349.92 81.87 o -4 5 1 4967.07 4861.46 114.95 o -3 5 1 35589.89 37118.25 727.05 o -2 5 1 7765.11 7950.50 164.04 o -1 5 1 464.01 460.21 21.02 o 0 5 1 772.07 770.58 27.39 o 1 5 1 15374.60 15936.80 326.24 o 2 5 1 3799.78 3888.72 86.25 o 3 5 1 1539.58 1561.86 43.15 o 4 5 1 5059.45 4990.61 134.64 o 5 5 1 24799.24 26526.09 662.05 o 6 5 1 1192.42 1046.27 68.45 o 7 5 1 795.38 700.14 58.47 o 8 5 1 4840.31 4492.05 195.75 o 9 5 1 13845.73 13260.92 953.19 o 10 5 1 3581.09 3190.26 226.46 o 11 5 1 1549.60 1412.50 94.38 o 12 5 1 710.71 616.11 105.55 o 13 5 1 4827.98 4531.10 204.73 o 14 5 1 836.81 933.49 95.32 o 15 5 1 112.41 40.94 61.20 o 16 5 1 173.20 236.07 75.07 o 17 5 1 2327.01 2408.73 153.38 o -17 6 1 2947.64 3274.37 195.32 o -16 6 1 127.64 181.57 83.77 o -15 6 1 741.14 679.11 154.17 o -14 6 1 81.96 119.98 65.46 o -13 6 1 4170.27 3808.24 185.46 o -12 6 1 31.54 12.93 81.24 o -11 6 1 2162.59 2177.27 122.52 o -10 6 1 7.98 36.51 48.45 o -9 6 1 12305.36 12340.88 451.12 o -8 6 1 94.52 118.47 92.12 o -7 6 1 6185.93 5704.75 226.04 o -6 6 1 56.11 135.71 47.63 o -5 6 1 40505.68 42358.95 1014.57 o -4 6 1 27.09 37.30 22.48 o -3 6 1 908.79 892.79 32.78 o -2 6 1 2371.73 2403.33 64.37 o -1 6 1 24515.26 25008.65 493.52 o 0 6 1 29.34 44.96 16.19 o 1 6 1 1029.53 1021.05 35.30 o 2 6 1 2217.83 2310.05 59.68 o 3 6 1 19768.36 20143.11 402.33 o 4 6 1 15.89 32.05 22.32 o 5 6 1 2409.98 2299.93 79.80 o 6 6 1 186.77 161.18 35.64 o 7 6 1 43257.46 42581.36 1450.86 o 8 6 1 807.21 812.77 72.72 o 9 6 1 799.91 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209.19 o 1 3 27 19.91 -47.06 64.30 o 2 3 27 3342.18 3460.63 198.53 o -4 4 27 2184.88 2153.17 169.53 o -3 4 27 1808.56 1857.97 140.19 o -2 4 27 2388.57 2492.82 282.76 o -1 4 27 476.31 571.77 94.94 o 0 4 27 2075.83 2222.20 280.20 o -6 0 28 636.64 513.06 127.94 o -4 0 28 3489.70 3762.85 290.43 o -2 0 28 1068.59 939.11 158.65 o 0 0 28 3539.01 3714.23 292.99 o 2 0 28 1629.95 1697.82 198.31 o -6 1 28 2433.56 2572.05 165.56 o -5 1 28 123.21 177.27 88.92 o -4 1 28 502.23 573.91 143.94 o -3 1 28 900.95 935.27 110.36 o -2 1 28 3224.02 3498.16 200.82 o -1 1 28 70.04 291.92 86.31 o 0 1 28 587.78 675.74 103.59 o 1 1 28 1848.95 1779.87 144.73 o 2 1 28 4458.90 4858.33 249.69 o -5 2 28 3075.16 3040.84 182.72 o -4 2 28 942.37 1069.81 116.57 o -3 2 28 317.62 435.71 89.44 o -2 2 28 28.90 10.04 70.38 o -1 2 28 3213.58 3364.77 264.85 o 0 2 28 1439.34 1511.52 130.61 o 1 2 28 206.11 359.38 87.78 o