#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/33/2213330.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213330_Fobs loop_ _publ_author_name 'Kasyan, Oleg' 'Kalchenko, Vitaly' 'B\"ohmer, Volker' 'Bolte, Michael' _publ_section_title ; 25-Decyloxy-26,27,28-trihydroxy-5,11,17-tris(4-nitrophenyldiazenyl)-2,8,14,20-thiacalix[4]arene toluene hemisolvate ; _journal_coeditor_code HB2337 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2346 _journal_page_last o2348 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 69.893 _cell_angle_beta 65.769 _cell_angle_gamma 76.226 _cell_length_a 14.0437 _cell_length_b 14.6038 _cell_length_c 16.0762 _exptl_crystal_F_000 1178.00 _reflns_d_resolution_high 0.8201 _[local]_cod_data_source_file hb2337IIsup2.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' boeh41 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 228.84 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 16.69 33.07 47.98 o 4 0 0 36.19 106.33 41.03 o 5 0 0 5508.94 5584.79 195.02 o 6 0 0 709.47 1014.06 43.35 o 7 0 0 1963.03 1785.63 50.32 o 8 0 0 715.68 704.59 34.00 o 9 0 0 306.09 184.66 32.04 o 10 0 0 442.00 593.82 35.98 o 11 0 0 319.90 370.40 32.12 o 12 0 0 45.62 33.41 30.03 o 13 0 0 61.07 57.80 32.73 o 14 0 0 88.13 101.95 34.62 o 15 0 0 42.69 64.48 35.56 o -15 1 0 59.45 85.85 32.90 o -14 1 0 135.71 118.44 35.90 o -13 1 0 0.29 45.17 30.78 o -12 1 0 5.94 20.84 30.73 o -11 1 0 267.26 260.58 33.27 o -10 1 0 2041.58 1963.09 48.87 o -9 1 0 1335.27 1426.61 50.07 o -8 1 0 207.60 227.70 31.28 o -7 1 0 4829.57 5439.43 111.07 o -6 1 0 5515.52 5822.71 119.20 o -5 1 0 5357.98 5387.15 98.54 o -4 1 0 719.04 1037.22 44.72 o -3 1 0 5000.77 5374.39 154.85 o -2 1 0 1703.26 909.49 49.49 o 3 1 0 958.32 1785.53 77.24 o 4 1 0 2469.24 3218.75 76.54 o 5 1 0 108.66 22.05 34.27 o 6 1 0 893.60 1087.44 43.53 o 7 1 0 235.71 221.65 33.83 o 8 1 0 1325.75 1433.82 40.92 o 9 1 0 48.18 84.36 31.98 o 10 1 0 141.19 100.25 33.73 o 11 1 0 13.34 51.64 35.31 o 12 1 0 9.57 -2.95 30.82 o 13 1 0 128.68 123.20 34.42 o 14 1 0 215.14 169.98 35.54 o 15 1 0 20.68 8.13 39.08 o -15 2 0 20.92 61.05 32.50 o -14 2 0 22.66 56.94 33.48 o -13 2 0 7.62 49.29 31.71 o -12 2 0 95.47 151.56 34.10 o -11 2 0 190.91 194.92 35.83 o -10 2 0 920.92 1029.63 35.76 o -9 2 0 275.52 384.32 29.78 o -8 2 0 29.06 41.29 27.86 o -7 2 0 328.93 358.58 26.54 o -6 2 0 4956.00 5159.86 86.30 o -5 2 0 1164.15 999.19 37.81 o -4 2 0 1103.61 1207.97 38.24 o -3 2 0 750.07 637.81 37.06 o -2 2 0 2076.75 1607.71 50.26 o -1 2 0 4975.24 3662.05 90.62 o 2 2 0 6885.16 4841.94 258.21 o 3 2 0 1643.93 1749.52 86.38 o 4 2 0 54.18 66.81 57.40 o 5 2 0 0.05 26.76 53.81 o 6 2 0 80.42 37.24 52.48 o 7 2 0 937.11 1224.24 45.45 o 8 2 0 123.78 47.22 35.48 o 9 2 0 1773.77 1448.25 39.97 o 10 2 0 74.16 176.72 36.07 o 11 2 0 133.59 131.92 34.52 o 12 2 0 301.48 352.52 34.43 o 13 2 0 1.86 -8.60 32.59 o 14 2 0 83.82 68.71 42.18 o 15 2 0 2.17 7.95 41.71 o -14 3 0 3.36 -34.76 36.14 o -13 3 0 2.59 28.06 26.83 o -12 3 0 144.29 148.50 32.49 o -11 3 0 1.57 -3.35 30.37 o -10 3 0 0.58 26.48 26.59 o -9 3 0 14.26 41.80 23.23 o -8 3 0 303.19 377.93 26.82 o -7 3 0 169.48 178.14 22.99 o -6 3 0 0.88 13.76 27.37 o -5 3 0 329.97 496.61 28.03 o -4 3 0 575.67 506.94 30.35 o -3 3 0 777.71 728.31 34.84 o -2 3 0 20625.68 18026.60 389.27 o -1 3 0 1521.97 942.71 42.77 o 0 3 0 6215.51 5338.21 211.11 o 1 3 0 7274.90 7482.88 209.96 o 2 3 0 3078.07 2880.73 148.77 o 3 3 0 662.33 541.26 61.72 o 4 3 0 6410.68 5861.98 508.30 o 5 3 0 370.61 369.51 52.91 o 6 3 0 1065.47 1016.83 152.24 o 7 3 0 323.16 227.48 47.85 o 8 3 0 543.27 669.51 43.93 o 9 3 0 1623.39 2083.29 53.68 o 10 3 0 51.19 24.45 57.38 o 11 3 0 365.73 325.39 43.10 o 12 3 0 4.90 55.59 38.75 o 13 3 0 80.54 91.21 47.22 o 14 3 0 142.06 153.52 39.92 o 15 3 0 3.72 32.56 48.27 o -14 4 0 27.45 -7.44 37.73 o -13 4 0 10.59 34.74 28.90 o -12 4 0 69.94 55.79 33.12 o -11 4 0 31.55 28.98 27.99 o -10 4 0 529.40 515.67 27.34 o -9 4 0 412.69 367.08 28.02 o -8 4 0 781.66 704.13 28.21 o -7 4 0 1367.41 1383.15 53.08 o -6 4 0 682.26 805.46 29.83 o -5 4 0 591.29 606.91 28.58 o -4 4 0 38.66 93.61 27.81 o -3 4 0 314.36 305.31 31.42 o -2 4 0 11095.95 10156.28 142.42 o -1 4 0 211.45 1887.84 656.04 o 0 4 0 2398.47 2269.17 49.84 o 1 4 0 235.97 124.79 44.82 o 2 4 0 553.11 359.52 57.32 o 3 4 0 537.59 582.32 58.64 o 4 4 0 3427.50 3411.62 100.93 o 5 4 0 796.66 750.95 56.72 o 6 4 0 247.35 264.40 59.15 o 7 4 0 350.07 413.19 60.74 o 8 4 0 187.91 135.88 55.46 o 9 4 0 1269.90 1156.38 80.41 o 10 4 0 773.23 651.79 52.29 o 11 4 0 91.39 73.18 46.22 o 12 4 0 385.37 363.46 44.90 o 13 4 0 269.38 334.91 37.70 o 14 4 0 32.67 118.08 41.31 o 15 4 0 0.66 -20.25 48.04 o -14 5 0 35.31 42.50 37.29 o -13 5 0 172.18 207.03 35.94 o -12 5 0 880.43 841.33 60.89 o -11 5 0 30.36 10.19 32.46 o -10 5 0 112.95 65.23 22.90 o -9 5 0 68.00 101.48 23.61 o -8 5 0 39.20 42.60 25.20 o -7 5 0 596.23 652.89 26.77 o -6 5 0 472.89 483.97 27.78 o -5 5 0 204.15 201.60 24.61 o -4 5 0 2055.71 2305.05 76.54 o -3 5 0 76.83 73.46 27.42 o -2 5 0 42.51 49.70 25.66 o -1 5 0 4.66 -8.46 28.65 o 0 5 0 2088.75 2327.33 44.49 o 1 5 0 1914.26 1516.18 57.24 o 2 5 0 2.49 68.23 59.25 o 3 5 0 87.26 76.82 50.84 o 4 5 0 7058.88 6989.61 153.41 o 5 5 0 27.43 53.17 43.74 o 6 5 0 16.99 39.93 51.09 o 7 5 0 37.82 -57.95 57.95 o 8 5 0 281.76 370.55 46.64 o 9 5 0 584.26 567.41 61.75 o 10 5 0 2312.38 2174.76 73.73 o 11 5 0 418.41 366.98 45.76 o 12 5 0 465.43 487.73 48.71 o 13 5 0 67.86 130.47 42.09 o 14 5 0 133.82 97.74 42.00 o 15 5 0 12.40 -25.17 36.67 o -13 6 0 98.40 83.64 33.10 o -12 6 0 315.94 193.07 40.58 o -11 6 0 4.17 19.29 26.01 o -10 6 0 102.55 118.23 27.00 o -9 6 0 193.15 179.78 22.68 o -8 6 0 320.62 391.93 36.37 o -7 6 0 228.09 219.73 24.14 o -6 6 0 113.97 140.07 25.38 o -5 6 0 386.32 374.46 26.28 o -4 6 0 700.22 711.49 30.02 o -3 6 0 1320.61 1260.89 58.32 o -2 6 0 42.89 25.20 26.70 o -1 6 0 12.91 -0.52 26.62 o 0 6 0 251.69 169.97 30.28 o 1 6 0 2083.63 2132.18 56.17 o 2 6 0 227.38 125.28 44.06 o 3 6 0 144.59 178.79 52.74 o 4 6 0 121.58 160.01 39.36 o 5 6 0 4260.11 4473.65 107.72 o 6 6 0 101.15 143.68 42.22 o 7 6 0 64.98 44.51 42.22 o 8 6 0 34.70 11.89 44.73 o 9 6 0 777.24 728.58 53.88 o 10 6 0 558.43 477.53 51.06 o 11 6 0 197.19 185.82 47.89 o 12 6 0 174.13 143.43 39.39 o 13 6 0 19.66 6.97 37.56 o 14 6 0 221.22 290.32 40.33 o 15 6 0 30.19 31.10 114.82 o -13 7 0 15.16 32.81 35.74 o -12 7 0 25.17 1.82 44.22 o -11 7 0 30.88 53.48 35.14 o -10 7 0 0.07 47.00 26.75 o -9 7 0 9.88 5.50 26.70 o -8 7 0 173.16 226.72 29.17 o -7 7 0 485.43 458.44 30.91 o -6 7 0 128.94 119.35 30.56 o -5 7 0 1068.27 1035.41 47.09 o -4 7 0 698.55 696.32 32.78 o -3 7 0 2.99 30.22 26.34 o -2 7 0 1717.46 1673.53 85.27 o -1 7 0 2914.54 3015.67 82.89 o 0 7 0 8354.79 8590.59 272.32 o 1 7 0 0.43 1.60 26.80 o 2 7 0 1004.84 960.40 41.86 o 3 7 0 178.54 126.70 39.07 o 4 7 0 517.30 553.29 45.06 o 5 7 0 3181.47 2903.65 134.76 o 6 7 0 262.80 296.81 47.77 o 7 7 0 0.90 13.04 48.56 o 8 7 0 257.18 246.44 40.48 o 9 7 0 1351.32 1535.13 75.63 o 10 7 0 0.16 -0.69 43.71 o 11 7 0 386.06 388.71 48.61 o 12 7 0 57.25 111.18 41.23 o 13 7 0 7.96 57.87 41.96 o 14 7 0 21.91 54.16 52.89 o -12 8 0 392.93 367.36 36.39 o -11 8 0 10.04 46.99 29.11 o -10 8 0 15.58 39.21 30.36 o -9 8 0 42.02 10.21 32.31 o -8 8 0 4.15 16.93 27.07 o -7 8 0 1096.34 1143.07 61.23 o -6 8 0 508.77 508.36 29.54 o -5 8 0 2224.11 2327.83 46.26 o -4 8 0 164.44 195.60 26.59 o -3 8 0 186.01 238.71 26.49 o -2 8 0 1561.94 1760.71 73.78 o -1 8 0 2316.19 2221.81 63.47 o 0 8 0 4213.61 4434.59 102.28 o 1 8 0 271.01 311.55 33.42 o 2 8 0 70.07 85.85 23.93 o 3 8 0 716.92 712.44 50.93 o 4 8 0 283.82 287.76 38.57 o 5 8 0 1738.09 1716.75 56.26 o 6 8 0 0.08 -35.46 35.46 o 7 8 0 166.46 242.97 54.54 o 8 8 0 493.56 550.30 87.00 o 9 8 0 539.32 580.24 56.67 o 10 8 0 117.05 114.73 37.73 o 11 8 0 7.82 13.93 45.00 o 12 8 0 5.24 15.01 85.26 o 13 8 0 0.47 3.48 42.46 o 14 8 0 0.95 95.85 43.02 o -12 9 0 285.61 269.40 62.41 o -11 9 0 6.59 14.23 30.01 o -10 9 0 35.22 74.54 27.16 o -9 9 0 1.93 2.25 31.70 o -8 9 0 175.82 184.40 26.16 o -7 9 0 898.43 786.14 53.84 o -6 9 0 275.42 280.03 28.94 o -5 9 0 1548.22 1580.53 53.20 o -4 9 0 2.33 40.88 23.87 o -3 9 0 1693.09 1579.40 34.06 o -2 9 0 67.75 51.44 25.90 o -1 9 0 109.41 154.66 24.78 o 0 9 0 2131.84 2154.94 55.81 o 1 9 0 2931.28 3147.48 123.86 o 2 9 0 82.53 93.47 29.60 o 3 9 0 556.58 695.24 31.86 o 4 9 0 23.99 7.27 31.34 o 5 9 0 181.98 129.07 37.86 o 6 9 0 156.48 190.97 43.61 o 7 9 0 31.77 38.03 38.50 o 8 9 0 574.09 604.56 52.47 o 9 9 0 1.20 -7.62 70.62 o 10 9 0 135.16 59.05 76.90 o 11 9 0 103.17 149.19 73.29 o 12 9 0 0.06 -0.77 43.84 o 13 9 0 7.50 5.31 43.29 o -11 10 0 49.65 5.56 33.44 o -10 10 0 9.02 2.25 34.98 o -9 10 0 44.55 -1.88 29.43 o -8 10 0 344.43 365.33 28.48 o -7 10 0 304.54 321.82 23.27 o -6 10 0 49.03 34.42 23.57 o -5 10 0 118.41 163.40 23.14 o -4 10 0 6.77 20.17 23.69 o -3 10 0 58.62 88.99 25.64 o -2 10 0 119.38 147.01 26.26 o -1 10 0 37.31 -13.43 28.75 o 0 10 0 163.31 163.41 31.64 o 1 10 0 7.17 27.30 28.43 o 2 10 0 102.79 101.27 31.42 o 3 10 0 131.92 96.63 27.59 o 4 10 0 8.31 25.88 27.26 o 5 10 0 0.80 -2.89 28.62 o 6 10 0 100.08 103.69 42.40 o 7 10 0 238.00 247.33 49.46 o 8 10 0 21.85 21.47 50.32 o 9 10 0 16.14 10.83 73.49 o 10 10 0 33.09 53.63 74.90 o 11 10 0 124.59 73.83 79.71 o 12 10 0 13.81 132.54 77.51 o 13 10 0 1.81 9.94 52.37 o -10 11 0 27.07 78.60 32.59 o -9 11 0 3.59 11.14 29.48 o -8 11 0 366.85 325.15 43.66 o -7 11 0 508.65 559.05 32.83 o -6 11 0 41.31 109.44 32.26 o -5 11 0 7.46 61.30 25.26 o -4 11 0 0.08 32.48 25.47 o -3 11 0 448.75 646.73 38.66 o -2 11 0 396.18 406.02 30.05 o -1 11 0 232.10 248.38 32.86 o 0 11 0 282.37 264.02 32.75 o 1 11 0 82.11 9.22 36.85 o 2 11 0 1109.44 1118.94 58.46 o 3 11 0 2.31 -9.52 30.78 o 4 11 0 88.50 80.65 25.07 o 5 11 0 262.29 290.90 31.28 o 6 11 0 164.44 194.47 30.65 o 7 11 0 605.51 597.77 41.53 o 8 11 0 0.22 46.90 38.71 o 9 11 0 24.64 -1.45 53.73 o 10 11 0 21.91 45.39 57.51 o 11 11 0 0.12 -16.98 54.06 o 12 11 0 37.38 -10.48 68.91 o -9 12 0 26.35 8.72 28.99 o -8 12 0 150.79 132.36 33.23 o -7 12 0 45.10 12.31 26.06 o -6 12 0 20.79 27.57 25.74 o -5 12 0 335.93 379.42 30.48 o -4 12 0 120.10 111.83 25.82 o -3 12 0 341.61 280.89 26.68 o -2 12 0 47.07 18.30 28.12 o -1 12 0 7.38 10.47 25.69 o 0 12 0 173.25 202.28 30.27 o 1 12 0 187.34 186.13 43.83 o 2 12 0 483.82 501.37 38.42 o 3 12 0 60.52 58.32 28.18 o 4 12 0 57.83 85.42 26.72 o 5 12 0 4.80 20.32 26.48 o 6 12 0 76.28 105.29 33.76 o 7 12 0 31.63 57.54 33.03 o 8 12 0 32.46 32.39 33.01 o 9 12 0 5.12 -14.84 45.76 o 10 12 0 135.18 216.77 46.83 o 11 12 0 0.02 33.83 66.41 o -8 13 0 11.62 34.79 31.48 o -7 13 0 55.48 63.09 29.63 o -6 13 0 72.37 70.36 29.75 o -5 13 0 145.21 97.71 25.26 o -4 13 0 0.64 11.66 23.87 o -3 13 0 12.36 31.07 30.21 o -2 13 0 1.21 16.68 26.49 o -1 13 0 22.81 56.65 29.67 o 0 13 0 0.13 54.68 38.45 o 1 13 0 390.04 417.63 34.83 o 2 13 0 1.69 -0.80 28.45 o 3 13 0 150.07 206.76 26.01 o 4 13 0 75.95 55.18 25.99 o 5 13 0 310.07 381.18 33.26 o 6 13 0 97.94 160.17 28.46 o 7 13 0 32.02 9.06 33.31 o 8 13 0 156.59 155.30 32.94 o 9 13 0 359.55 272.73 36.61 o 10 13 0 23.67 75.57 61.64 o 11 13 0 205.81 88.41 64.33 o -6 14 0 1.02 10.39 33.13 o -5 14 0 16.01 36.57 36.53 o -4 14 0 114.26 132.48 34.63 o -3 14 0 74.93 60.41 30.44 o -2 14 0 75.71 68.98 28.94 o -1 14 0 48.42 66.11 39.90 o 0 14 0 56.77 71.17 30.14 o 1 14 0 101.03 72.30 33.67 o 2 14 0 4.18 1.51 32.70 o 3 14 0 175.22 221.54 29.43 o 4 14 0 1635.40 1379.88 35.75 o 5 14 0 1072.67 905.93 55.95 o 6 14 0 36.84 6.80 32.15 o 7 14 0 96.36 79.85 33.22 o 8 14 0 33.67 96.51 33.76 o 9 14 0 93.17 80.73 36.81 o -5 15 0 113.74 76.19 36.60 o -4 15 0 57.61 69.71 34.12 o -3 15 0 6.33 81.77 34.42 o -2 15 0 26.94 56.57 34.90 o -1 15 0 224.43 255.85 29.49 o 0 15 0 300.71 316.98 33.47 o 1 15 0 11.77 18.32 38.43 o 2 15 0 65.05 132.02 31.87 o 3 15 0 64.63 45.87 29.44 o 4 15 0 129.62 185.01 29.33 o 5 15 0 172.41 112.78 35.67 o 6 15 0 36.94 68.02 30.00 o 7 15 0 54.64 2.09 36.08 o 8 15 0 0.13 -1.43 36.72 o -2 16 0 31.10 -7.39 32.87 o -1 16 0 0.13 34.55 31.20 o 0 16 0 36.43 38.61 32.46 o 1 16 0 5.84 35.35 32.48 o 2 16 0 5.83 98.20 42.17 o 3 16 0 12.01 26.21 34.62 o 4 16 0 198.56 241.42 35.30 o 5 16 0 31.87 55.76 30.64 o 6 16 0 30.61 14.18 87.07 o -4 -16 1 0.27 -35.44 35.44 o -3 -16 1 103.98 92.69 37.26 o -2 -16 1 5.23 -11.40 44.35 o -1 -16 1 26.72 32.69 30.36 o 0 -16 1 14.38 6.41 39.20 o 1 -16 1 1.33 5.19 35.97 o -7 -15 1 2.25 -10.02 36.37 o -6 -15 1 158.44 160.80 36.28 o -5 -15 1 248.31 286.36 33.69 o -4 -15 1 111.14 82.04 31.97 o -3 -15 1 0.74 37.44 35.07 o -2 -15 1 185.63 160.63 37.79 o -1 -15 1 256.61 213.55 32.67 o 0 -15 1 48.52 56.42 45.67 o 1 -15 1 39.18 48.92 37.55 o 2 -15 1 0.04 -6.32 36.81 o 3 -15 1 2.96 39.38 35.77 o 4 -15 1 24.93 78.20 39.92 o -9 -14 1 39.10 50.92 58.82 o -8 -14 1 95.13 75.53 40.61 o -7 -14 1 33.55 27.65 33.20 o -6 -14 1 0.03 -29.29 29.51 o -5 -14 1 105.41 112.18 31.04 o -4 -14 1 299.17 222.59 30.42 o -3 -14 1 520.13 632.80 39.74 o -2 -14 1 133.65 127.96 35.14 o -1 -14 1 271.81 236.64 40.11 o 0 -14 1 109.92 64.05 34.66 o 1 -14 1 360.99 281.16 40.76 o 2 -14 1 5.75 47.50 31.03 o 3 -14 1 0.93 21.03 25.28 o 4 -14 1 3.92 12.46 26.77 o 5 -14 1 1.98 62.50 31.07 o 6 -14 1 100.01 127.45 30.82 o -10 -13 1 0.03 -6.14 68.16 o -9 -13 1 7.92 64.06 38.34 o -8 -13 1 35.21 -22.19 36.54 o -7 -13 1 21.38 37.38 30.43 o -6 -13 1 7.04 33.22 28.86 o -5 -13 1 40.12 20.59 32.04 o -4 -13 1 378.93 460.32 29.52 o -3 -13 1 12.72 5.99 27.95 o -2 -13 1 91.30 82.40 36.97 o -1 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367.93 73.96 o -7 -9 2 275.48 377.76 51.35 o -6 -9 2 37.97 45.22 47.99 o -5 -9 2 17.93 41.66 46.75 o -4 -9 2 768.61 826.22 53.60 o -3 -9 2 289.43 245.33 30.47 o -2 -9 2 86.72 120.41 32.53 o -1 -9 2 621.88 622.57 37.28 o 0 -9 2 960.71 1122.95 40.57 o 1 -9 2 342.30 349.42 29.75 o 2 -9 2 156.52 102.93 28.61 o 3 -9 2 5.36 32.18 26.17 o 4 -9 2 383.22 377.76 26.12 o 5 -9 2 25.02 26.52 25.88 o 6 -9 2 5850.28 6603.69 293.98 o 7 -9 2 3424.47 3202.47 67.55 o 8 -9 2 114.32 149.81 30.74 o 9 -9 2 2.88 12.44 23.03 o 10 -9 2 0.50 -3.71 32.01 o 11 -9 2 143.48 197.74 32.94 o 12 -9 2 22.91 11.42 30.74 o -13 -8 2 0.76 -7.87 55.07 o -12 -8 2 7.80 131.69 55.72 o -11 -8 2 1069.41 1068.94 61.23 o -10 -8 2 65.20 157.30 59.88 o -9 -8 2 32.19 -38.52 71.62 o -8 -8 2 659.50 644.52 82.39 o -7 -8 2 70.16 109.81 57.37 o -6 -8 2 15.30 16.40 45.91 o -5 -8 2 2.88 70.03 62.19 o -4 -8 2 854.20 843.36 65.15 o -3 -8 2 466.58 443.02 36.87 o -2 -8 2 2010.81 1999.26 80.99 o -1 -8 2 1446.35 1579.07 44.38 o 0 -8 2 137.96 199.09 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25.11 o 10 -7 2 666.28 558.71 33.97 o 11 -7 2 8.79 10.18 29.70 o 12 -7 2 3.56 -4.06 28.46 o 13 -7 2 232.12 233.53 30.40 o -14 -6 2 76.12 124.17 59.21 o -13 -6 2 108.75 206.82 47.49 o -12 -6 2 0.00 -41.97 56.61 o -11 -6 2 553.16 466.44 41.07 o -10 -6 2 22.59 28.28 36.27 o -9 -6 2 119.33 223.81 106.76 o -8 -6 2 31.87 16.25 81.55 o -7 -6 2 18.72 45.16 64.87 o -6 -6 2 493.54 410.72 48.44 o -5 -6 2 67.31 59.47 39.52 o -4 -6 2 0.00 7.26 40.88 o -3 -6 2 0.06 -7.08 38.46 o -2 -6 2 56.65 113.76 35.71 o -1 -6 2 563.21 540.88 41.42 o 0 -6 2 123.18 212.02 32.42 o 1 -6 2 115.30 202.87 31.34 o 2 -6 2 828.33 1019.30 31.67 o 3 -6 2 3221.00 3343.74 45.44 o 4 -6 2 2936.44 2696.63 39.53 o 5 -6 2 20.22 46.43 27.39 o 6 -6 2 531.90 597.82 27.73 o 7 -6 2 101.69 98.21 28.00 o 8 -6 2 164.60 159.36 28.35 o 9 -6 2 1168.29 1234.24 43.78 o 10 -6 2 90.79 123.63 25.40 o 11 -6 2 6.76 11.93 28.17 o 12 -6 2 14.11 15.83 31.35 o 13 -6 2 380.43 378.07 37.61 o 14 -6 2 59.19 70.59 38.99 o -14 -5 2 4.85 21.99 40.71 o -13 -5 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432.15 444.01 47.26 o 9 6 19 6.83 44.31 31.52 o 10 6 19 3.88 7.17 34.92 o 4 7 19 74.41 77.23 37.78 o 5 7 19 37.64 44.81 45.18 o 6 7 19 0.29 1.00 39.56 o 7 7 19 45.43 116.74 40.75 o 8 7 19 269.95 199.62 38.11 o 9 7 19 10.61 6.88 37.91 o 10 7 19 12.53 11.40 40.51 o 4 8 19 42.18 35.18 56.44 o 5 8 19 30.60 46.77 45.71 o 6 8 19 46.42 58.59 48.01 o 7 8 19 11.17 55.05 40.35 o 8 8 19 1.58 -28.66 39.49 o 9 8 19 6.30 70.94 46.27 o 10 8 19 20.94 65.54 59.65 o 6 9 19 126.53 28.13 60.69 o 7 9 19 1.92 -8.70 46.59 o 8 9 19 68.19 65.12 42.63 o 9 9 19 3.12 33.49 48.09 o