#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2214415.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214415_Fobs loop_ _publ_author_name 'Srinivasan, Krishnan' 'Govindarajan, Subbaiah' 'Harrison, William T. A.' _publ_section_title ; catena-Poly[[dihydraziniummanganese(II)]-di-\m-sulfato-\k^4^O:O'] from synchrotron data ; _journal_coeditor_code WM2112 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i152 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 92.651 _cell_angle_beta 104.332 _cell_angle_gamma 99.249 _cell_length_a 5.3910 _cell_length_b 5.8678 _cell_length_c 7.3954 _exptl_crystal_F_000 159.00 _reflns_d_resolution_high 0.6962 _[local]_cod_data_source_file wm2112Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SRINI KS10 MN/hydrazine/sulfate Daresbury data ssf1249' _shelx_refln_list_code 4 _shelx_f_calc_maximum 24.70 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 0.31 0.84 0.08 o 2 0 0 39.04 49.05 2.43 o 5 0 0 150.26 166.36 5.18 o 6 0 0 251.85 245.39 10.48 o 7 0 0 22.08 21.22 1.01 o -7 1 0 1.02 1.27 0.39 o -6 1 0 5.97 7.06 0.51 o -4 1 0 3.65 2.99 0.27 o 5 1 0 14.25 12.15 1.06 o 6 1 0 226.78 254.01 7.58 o -7 2 0 243.09 273.19 8.14 o -6 2 0 18.24 15.87 0.81 o -5 2 0 1.60 1.76 0.23 o -3 2 0 0.83 0.74 0.12 o 5 2 0 4.32 3.13 0.29 o -7 3 0 72.19 53.72 3.08 o -5 3 0 15.43 16.65 0.85 o -4 3 0 95.76 102.53 3.95 o 1 3 0 80.39 64.15 3.28 o 2 3 0 19.15 13.72 0.53 o 3 3 0 2.93 4.02 0.33 o 6 3 0 2.09 2.75 0.50 o -6 4 0 261.18 361.13 11.81 o -4 4 0 19.30 26.28 1.15 o -2 4 0 154.23 164.23 5.18 o -1 4 0 62.22 91.16 3.13 o 1 4 0 23.90 21.22 0.95 o 2 4 0 3.60 4.13 0.50 o 5 4 0 85.84 90.13 4.45 o -6 5 0 0.37 0.25 0.21 o -4 5 0 2.09 2.44 0.30 o -3 5 0 105.94 80.19 2.77 o -1 5 0 26.78 35.77 1.47 o 0 5 0 136.39 154.06 5.45 o 2 5 0 1.03 1.16 0.23 o 3 5 0 287.51 289.03 12.28 o 4 5 0 82.91 85.20 4.27 o -5 6 0 5.65 5.72 0.64 o -4 6 0 419.17 335.01 13.75 o -3 6 0 3.39 2.48 0.40 o -2 6 0 116.48 92.17 4.52 o 0 6 0 7.21 4.86 0.52 o 1 6 0 253.72 258.62 11.13 o 2 6 0 103.39 110.55 3.80 o 3 6 0 4.78 5.50 0.46 o -4 7 0 4.62 4.25 0.54 o -3 7 0 58.53 86.80 4.44 o -2 7 0 7.74 10.81 0.68 o -1 7 0 111.81 108.08 3.67 o 0 7 0 37.65 24.14 2.65 o 1 7 0 119.56 129.36 4.33 o 2 7 0 126.76 101.50 9.63 o -3 8 0 36.21 51.94 3.00 o -2 8 0 28.79 34.91 1.55 o -1 8 0 1.64 1.21 0.60 o 0 8 0 144.23 147.44 6.78 o 0 -8 1 176.62 195.70 8.85 o 1 -8 1 93.03 85.97 4.39 o 2 -8 1 1.02 1.70 0.47 o -3 -7 1 0.16 0.00 0.23 o -2 -7 1 44.43 29.69 1.29 o -1 -7 1 25.18 28.14 1.29 o 0 -7 1 12.90 12.18 1.12 o 2 -7 1 38.74 56.72 2.49 o 3 -7 1 0.64 2.36 0.47 o 4 -7 1 243.68 217.50 9.50 o -3 -6 1 117.45 133.06 4.45 o -2 -6 1 8.63 7.74 0.52 o -1 -6 1 304.01 266.06 11.21 o 0 -6 1 1.97 1.99 0.65 o 1 -6 1 12.63 14.65 0.77 o 3 -6 1 51.56 58.75 3.15 o 4 -6 1 4.77 4.19 0.56 o 5 -6 1 88.95 87.92 3.08 o -5 -5 1 63.10 66.93 3.50 o -4 -5 1 46.60 54.47 2.98 o -2 -5 1 106.54 123.63 4.13 o -1 -5 1 4.83 3.87 0.42 o 1 -5 1 16.69 21.36 0.98 o 2 -5 1 50.87 50.09 1.53 o 4 -5 1 2.51 2.57 0.29 o 5 -5 1 76.61 81.45 2.88 o 6 -5 1 76.64 97.33 3.40 o -4 -4 1 44.96 52.95 2.09 o -3 -4 1 31.75 33.31 1.40 o -1 -4 1 1.61 1.43 0.19 o 2 -4 1 32.95 44.37 1.38 o 3 -4 1 150.67 152.05 4.81 o 4 -4 1 42.06 49.72 1.90 o 5 -4 1 19.48 21.57 0.99 o 6 -4 1 252.95 257.79 7.70 o -6 -3 1 0.80 0.47 0.33 o -5 -3 1 18.70 22.27 1.44 o -3 -3 1 13.93 10.64 0.46 o -2 -3 1 72.94 76.35 2.70 o 0 -3 1 2.01 2.28 0.16 o 5 -3 1 63.35 62.10 2.31 o 6 -3 1 58.73 63.84 2.42 o -6 -2 1 76.45 70.76 3.63 o -5 -2 1 1.82 1.42 0.23 o 3 -2 1 57.05 66.35 2.33 o 6 -2 1 13.33 15.78 0.81 o 7 -2 1 128.69 138.28 4.55 o -7 -1 1 18.81 20.05 1.01 o 1 -1 1 28.52 38.89 1.42 o 4 -1 1 20.67 20.90 0.90 o 7 -1 1 13.49 19.21 0.99 o -7 0 1 0.33 0.28 0.17 o -6 0 1 17.04 15.18 0.76 o -4 0 1 1.14 2.57 0.35 o -3 0 1 16.95 17.97 0.61 o -1 0 1 7.64 14.69 0.49 o 2 0 1 28.81 31.69 0.98 o 4 0 1 60.74 53.14 2.82 o 5 0 1 14.95 19.76 0.93 o 6 0 1 249.06 236.23 10.16 o 7 0 1 75.70 103.08 4.97 o -7 1 1 240.15 279.95 11.89 o -6 1 1 36.18 40.02 1.63 o -5 1 1 11.64 5.50 0.62 o -3 1 1 101.45 169.80 7.51 o 0 1 1 0.33 0.85 0.10 o 3 1 1 0.46 0.69 0.11 o 5 1 1 21.87 26.31 1.18 o 6 1 1 13.33 13.02 0.72 o -7 2 1 47.73 64.43 5.70 o -5 2 1 80.26 90.07 3.12 o -4 2 1 125.86 150.53 4.79 o 0 2 1 170.11 52.50 2.62 o 3 2 1 26.00 26.60 0.92 o 6 2 1 45.01 62.64 3.46 o -7 3 1 4.82 5.81 0.48 o -6 3 1 61.15 66.94 2.47 o -5 3 1 289.24 284.12 11.89 o -4 3 1 4.39 3.38 0.42 o -3 3 1 0.88 4.28 0.32 o 1 3 1 0.96 0.62 0.14 o 2 3 1 157.10 152.85 6.93 o 4 3 1 12.82 12.22 0.92 o 5 3 1 264.59 265.34 11.19 o -7 4 1 58.91 108.22 5.13 o -6 4 1 1.28 1.69 0.28 o -4 4 1 14.31 20.62 0.96 o -3 4 1 60.73 60.32 2.22 o 2 4 1 46.51 49.94 1.91 o 3 4 1 249.01 177.44 8.00 o 4 4 1 147.70 176.69 7.90 o 5 4 1 0.29 0.21 0.21 o -6 5 1 1.23 1.70 0.31 o -5 5 1 35.96 43.75 1.77 o -3 5 1 2.01 2.46 0.44 o -2 5 1 288.77 219.40 9.59 o 1 5 1 225.62 144.08 6.67 o 3 5 1 60.78 58.08 2.22 o 4 5 1 217.14 232.46 10.01 o -5 6 1 24.29 30.39 2.03 o -3 6 1 143.18 124.02 5.79 o -2 6 1 11.10 4.68 0.52 o 0 6 1 13.63 12.63 0.72 o 1 6 1 0.74 0.39 0.18 o 2 6 1 281.01 268.95 10.24 o 3 6 1 10.54 11.43 0.70 o -4 7 1 12.56 5.81 0.62 o -3 7 1 84.80 126.05 6.02 o -2 7 1 12.75 14.18 0.81 o -1 7 1 95.90 114.71 3.92 o 0 7 1 423.37 394.95 15.87 o 1 7 1 22.47 25.67 1.22 o 2 7 1 76.20 46.94 1.85 o -2 8 1 134.37 155.55 7.47 o -1 8 1 41.07 15.73 1.20 o 0 8 1 117.08 110.43 5.29 o 1 -8 2 315.35 377.01 15.54 o 2 -8 2 11.74 13.24 1.13 o -2 -7 2 0.31 0.01 0.31 o -1 -7 2 172.51 153.97 7.21 o 0 -7 2 2.06 3.96 0.61 o 1 -7 2 228.99 273.44 11.69 o -4 -6 2 14.19 13.11 1.18 o -3 -6 2 297.75 307.59 9.10 o -2 -6 2 69.34 51.45 2.00 o -1 -6 2 3.98 4.25 0.88 o 0 -6 2 218.32 308.87 12.96 o 1 -6 2 3.41 4.46 0.37 o 2 -6 2 78.18 107.14 3.66 o 4 -6 2 1.42 1.56 0.45 o 5 -6 2 164.51 184.29 5.73 o -4 -5 2 15.37 16.99 0.95 o -3 -5 2 0.38 0.46 0.28 o -1 -5 2 0.47 0.82 0.19 o 0 -5 2 152.25 138.14 10.41 o 2 -5 2 65.25 65.50 1.94 o 3 -5 2 169.18 122.80 7.06 o 4 -5 2 90.26 98.98 5.11 o 5 -5 2 18.20 17.80 0.88 o 6 -5 2 191.94 162.82 7.58 o -6 -4 2 4.04 4.79 0.69 o -5 -4 2 51.39 49.42 2.72 o -3 -4 2 1.75 1.12 0.21 o -2 -4 2 52.63 61.44 2.27 o 0 -4 2 11.08 9.53 0.86 o 2 -4 2 99.24 68.01 3.66 o 3 -4 2 84.65 83.21 4.10 o 5 -4 2 0.36 0.28 0.16 o 6 -4 2 4.46 3.56 0.35 o -6 -3 2 147.83 224.11 9.90 o -5 -3 2 11.80 10.86 0.85 o 3 -3 2 135.34 136.10 4.37 o 4 -3 2 256.63 329.03 13.65 o 5 -3 2 161.99 187.53 5.84 o 6 -3 2 101.01 111.22 3.77 o -6 -2 2 12.54 8.32 0.78 o -5 -2 2 31.69 42.01 1.69 o -4 -2 2 25.59 25.49 1.07 o 4 -2 2 0.89 1.00 0.19 o 5 -2 2 248.61 265.92 11.31 o 6 -2 2 97.86 129.53 4.26 o -7 -1 2 81.72 79.16 2.85 o -6 -1 2 2.32 2.32 0.27 o -4 -1 2 59.81 53.26 1.94 o -3 -1 2 25.59 26.74 0.88 o 5 -1 2 100.59 92.15 3.15 o 6 -1 2 263.72 259.57 22.55 o -7 0 2 349.23 474.24 20.28 o -6 0 2 28.93 26.73 1.17 o -5 0 2 133.58 121.99 3.98 o -2 0 2 1.08 2.17 0.14 o 3 0 2 29.99 41.37 2.53 o 5 0 2 116.43 64.44 3.23 o 6 0 2 56.44 46.09 3.59 o -7 1 2 70.60 65.08 2.41 o -5 1 2 37.41 38.76 1.66 o -2 1 2 84.03 64.90 4.04 o 1 1 2 69.24 88.05 4.19 o 3 1 2 2.02 1.43 0.18 o 5 1 2 137.84 228.46 11.11 o 6 1 2 63.86 29.53 1.85 o -7 2 2 30.79 10.70 0.95 o -6 2 2 123.59 126.34 4.15 o -5 2 2 21.48 21.85 1.46 o -4 2 2 165.22 67.29 3.36 o 1 2 2 30.13 38.46 1.18 o 2 2 2 186.24 196.61 8.54 o 4 2 2 8.06 6.83 0.62 o 6 2 2 32.71 47.34 2.80 o -7 3 2 21.88 22.58 1.31 o -4 3 2 36.34 15.86 1.14 o -1 3 2 28.67 39.64 1.22 o 2 3 2 8.44 9.45 0.54 o 4 3 2 0.38 0.49 0.22 o 5 3 2 1.79 1.46 0.33 o -7 4 2 55.05 62.29 3.26 o -6 4 2 9.94 10.83 0.64 o -3 4 2 28.63 28.69 0.98 o -2 4 2 68.40 68.41 3.32 o 0 4 2 3.47 3.53 0.30 o 3 4 2 68.74 66.91 2.47 o -6 5 2 243.26 269.67 8.04 o -5 5 2 245.38 244.17 10.07 o -2 5 2 209.57 94.15 4.61 o 0 5 2 59.15 62.85 2.31 o 1 5 2 28.99 8.78 0.74 o 3 5 2 11.29 14.54 1.70 o 4 5 2 187.35 184.91 8.23 o -5 6 2 61.88 55.97 3.05 o -4 6 2 12.12 9.64 0.84 o -2 6 2 57.14 61.59 2.32 o -1 6 2 48.92 46.95 1.86 o 0 6 2 180.77 247.55 10.75 o 1 6 2 5.82 5.91 0.45 o 2 6 2 69.18 60.52 2.29 o 3 6 2 42.57 34.64 3.41 o -4 7 2 17.94 27.65 1.90 o -3 7 2 53.82 64.76 3.43 o -2 7 2 173.02 181.42 5.77 o -1 7 2 6.33 8.96 1.00 o 0 7 2 376.66 258.67 11.20 o 1 7 2 60.40 44.62 2.68 o -2 8 2 162.05 178.09 8.22 o 1 -8 3 60.41 68.19 3.68 o -2 -7 3 0.80 1.14 0.41 o -1 -7 3 151.47 180.06 8.20 o 1 -7 3 22.06 27.65 1.79 o 2 -7 3 214.18 217.13 9.53 o -4 -6 3 32.63 33.71 2.14 o -3 -6 3 126.38 188.95 8.56 o -1 -6 3 22.52 24.90 1.68 o 1 -6 3 228.26 230.88 10.00 o 2 -6 3 6.84 7.52 0.74 o 4 -6 3 98.40 113.25 5.21 o 5 -6 3 49.04 47.01 2.51 o -4 -5 3 125.38 140.09 6.62 o -3 -5 3 57.68 69.51 3.71 o -2 -5 3 65.51 77.97 4.02 o 0 -5 3 5.06 5.70 0.41 o 1 -5 3 178.06 189.03 5.86 o 3 -5 3 13.93 12.95 0.70 o 4 -5 3 112.27 106.38 4.97 o 5 -5 3 102.34 106.90 5.02 o -3 -4 3 127.88 161.75 5.19 o -2 -4 3 222.12 261.66 7.80 o 0 -4 3 10.53 5.99 0.30 o 1 -4 3 9.86 18.13 1.20 o 3 -4 3 5.42 4.51 0.58 o 4 -4 3 153.09 179.05 12.76 o 5 -4 3 143.36 147.96 4.77 o 6 -4 3 8.18 10.14 0.94 o -6 -3 3 175.28 169.86 7.67 o -5 -3 3 5.79 6.76 0.49 o -4 -3 3 252.35 273.90 11.57 o -2 -3 3 2.46 2.06 0.17 o 1 -3 3 108.65 123.20 3.98 o 2 -3 3 325.92 156.08 6.93 o 4 -3 3 16.62 18.53 0.92 o 5 -3 3 288.29 380.28 15.50 o 6 -3 3 29.42 26.05 1.33 o -7 -2 3 19.97 19.06 0.99 o -6 -2 3 58.87 65.53 3.44 o -4 -2 3 109.95 92.33 3.15 o -1 -2 3 9.70 15.79 0.58 o 2 -2 3 209.25 94.60 4.47 o 4 -2 3 3.49 4.61 0.37 o 5 -2 3 0.56 0.31 0.18 o 6 -2 3 406.62 376.59 15.47 o -7 -1 3 91.08 93.50 3.29 o -6 -1 3 4.11 2.71 0.75 o -3 -1 3 50.44 59.06 1.72 o 3 -1 3 112.07 97.30 3.22 o 4 -1 3 101.89 107.58 4.94 o 5 -1 3 6.95 7.17 0.46 o 6 -1 3 83.22 92.55 4.57 o -7 0 3 35.69 38.05 1.60 o 3 0 3 54.81 48.34 2.66 o 4 0 3 257.25 222.11 9.67 o 5 0 3 183.95 213.41 12.34 o 6 0 3 24.08 26.35 2.80 o -7 1 3 5.86 6.70 0.52 o -5 1 3 22.30 12.46 0.95 o -4 1 3 11.27 15.38 1.85 o 0 1 3 15.91 10.16 0.51 o 1 1 3 16.50 22.28 0.76 o 4 1 3 4.60 3.66 0.55 o 6 1 3 86.09 91.33 4.57 o -4 2 3 10.85 10.03 0.55 o -1 2 3 33.86 47.06 1.41 o 1 2 3 75.54 77.98 2.17 o 4 2 3 26.55 22.97 1.46 o 5 2 3 19.98 8.85 0.76 o -7 3 3 143.33 124.11 4.47 o -6 3 3 2.76 5.26 0.39 o -3 3 3 22.08 23.90 0.84 o -1 3 3 0.68 0.84 0.15 o 2 3 3 1.77 3.42 0.42 o 3 3 3 0.32 0.28 0.15 o 4 3 3 185.03 178.98 7.93 o 5 3 3 1.91 1.75 0.35 o -7 4 3 8.69 10.82 0.94 o -6 4 3 190.76 186.38 5.81 o -5 4 3 23.79 24.83 1.34 o -2 4 3 6.11 7.23 0.47 o 0 4 3 59.49 58.26 2.17 o 1 4 3 19.27 24.27 1.08 o 3 4 3 8.84 8.95 0.59 o 4 4 3 25.14 34.00 2.09 o -6 5 3 135.45 151.24 7.01 o -5 5 3 20.24 16.79 1.18 o -4 5 3 20.75 14.46 1.04 o -3 5 3 309.68 255.44 10.80 o -2 5 3 86.58 102.51 3.52 o -1 5 3 175.22 180.74 5.68 o 0 5 3 318.69 297.22 12.53 o 1 5 3 0.57 0.37 0.33 o 2 5 3 135.28 118.47 10.52 o 3 5 3 181.13 178.78 5.70 o -5 6 3 198.48 76.01 3.85 o -4 6 3 3.29 2.43 0.41 o -3 6 3 3.80 5.69 0.83 o -2 6 3 179.35 191.45 6.02 o -1 6 3 34.18 35.31 1.48 o 1 6 3 261.68 255.56 11.07 o 2 6 3 65.88 68.89 3.70 o 3 6 3 275.10 230.57 10.19 o -4 7 3 44.31 34.89 2.24 o -3 7 3 14.10 16.67 1.24 o -1 7 3 10.88 13.31 0.91 o 0 7 3 25.37 25.27 1.19 o -2 -7 4 398.12 453.03 18.19 o -1 -7 4 90.07 92.53 4.71 o 0 -7 4 157.01 170.62 7.72 o 1 -7 4 43.32 83.17 4.33 o -4 -6 4 98.72 91.64 4.63 o -3 -6 4 0.68 0.85 0.38 o -1 -6 4 201.70 202.70 9.03 o 0 -6 4 80.97 75.48 3.85 o 1 -6 4 133.45 134.72 6.35 o 2 -6 4 4.40 7.02 1.01 o 3 -6 4 73.90 73.83 3.76 o 4 -6 4 101.37 95.66 4.56 o -4 -5 4 126.60 159.45 7.33 o -3 -5 4 223.95 280.74 11.99 o -2 -5 4 20.24 13.65 1.10 o 3 -5 4 9.65 2.96 0.46 o 4 -5 4 140.79 141.62 6.37 o 5 -5 4 90.29 19.50 1.27 o -3 -4 4 303.27 198.91 8.76 o -2 -4 4 2.64 2.78 0.71 o -1 -4 4 97.39 81.33 3.89 o 0 -4 4 130.24 120.03 5.55 o 1 -4 4 23.13 24.36 1.06 o 5 -4 4 205.17 174.68 7.61 o -4 -3 4 13.20 13.19 0.70 o -3 -3 4 190.78 168.89 5.29 o -1 -3 4 197.37 184.85 6.70 o 1 -3 4 122.31 123.95 5.70 o 5 -3 4 12.79 16.23 1.11 o -6 -2 4 0.27 0.45 0.27 o -4 -2 4 58.02 72.11 2.09 o -3 -2 4 27.53 31.41 1.28 o -1 -2 4 0.59 0.78 0.16 o 0 -2 4 8.52 16.94 0.77 o 2 -2 4 123.69 125.78 7.12 o 3 -2 4 0.57 0.51 0.32 o 5 -2 4 14.23 16.19 0.85 o 6 -2 4 129.59 155.35 7.31 o -7 -1 4 57.70 71.02 2.68 o -6 -1 4 396.33 213.07 9.21 o -5 -1 4 34.48 27.64 1.21 o -2 -1 4 0.58 0.75 0.11 o 0 -1 4 171.13 149.18 6.71 o 1 -1 4 122.85 104.85 3.44 o 3 -1 4 9.34 4.45 0.47 o 4 -1 4 27.37 24.07 1.79 o 5 -1 4 58.68 79.43 2.84 o 6 -1 4 0.28 0.27 0.20 o -7 0 4 108.73 104.13 3.59 o -6 0 4 149.18 159.95 5.13 o -5 0 4 94.71 64.40 3.40 o -4 0 4 125.09 117.65 3.87 o 1 0 4 88.90 99.71 4.74 o 3 0 4 126.75 131.70 4.26 o 4 0 4 34.82 36.35 1.47 o 5 0 4 116.10 105.26 5.63 o 6 0 4 20.48 28.03 1.87 o -7 1 4 81.74 54.34 3.06 o -6 1 4 21.09 27.98 2.53 o -5 1 4 124.32 185.45 14.05 o -4 1 4 0.27 1.06 0.26 o -3 1 4 162.43 178.02 7.82 o -1 1 4 10.74 11.68 0.46 o 2 1 4 60.87 82.13 3.60 o 4 1 4 194.65 169.64 7.56 o 5 1 4 2.62 3.06 0.57 o -7 2 4 231.30 230.58 7.03 o -6 2 4 1.78 1.80 0.27 o -4 2 4 6.17 6.82 0.44 o -1 2 4 6.52 4.06 0.48 o 0 2 4 13.92 10.65 0.65 o 2 2 4 1.26 0.91 0.27 o 3 2 4 10.19 7.86 0.75 o 5 2 4 1.88 1.03 0.29 o -7 3 4 141.42 139.53 7.04 o -5 3 4 31.57 32.19 1.35 o -3 3 4 6.51 6.15 0.33 o -2 3 4 110.98 123.02 3.98 o 0 3 4 0.37 0.70 0.26 o 1 3 4 3.15 3.84 0.71 o 3 3 4 0.54 0.28 0.20 o 4 3 4 67.28 66.34 3.43 o -7 4 4 0.15 0.56 0.35 o -5 4 4 3.21 2.28 0.59 o -4 4 4 57.32 68.68 3.62 o -2 4 4 16.27 15.95 0.79 o -1 4 4 63.21 78.40 2.76 o 0 4 4 140.99 90.97 3.15 o 1 4 4 1.52 3.00 0.31 o 2 4 4 205.33 260.73 8.42 o 3 4 4 5.49 6.18 0.48 o 4 4 4 22.61 32.44 2.00 o -6 5 4 3.46 3.44 0.51 o -5 5 4 253.89 260.05 11.09 o -4 5 4 6.90 6.96 0.66 o -1 5 4 145.88 148.25 4.80 o 0 5 4 98.19 84.26 4.10 o 1 5 4 81.76 86.25 3.08 o 2 5 4 3.69 4.51 0.49 o 3 5 4 109.88 101.88 3.56 o -5 6 4 149.34 147.89 6.84 o -3 6 4 73.50 84.19 3.15 o -1 6 4 87.44 85.45 3.10 o 0 6 4 31.79 29.82 1.35 o 1 6 4 591.62 603.02 23.45 o 2 6 4 2.18 1.96 0.55 o -3 7 4 11.51 12.13 1.00 o -2 7 4 6.86 6.69 0.79 o -1 7 4 220.85 241.10 7.41 o 0 7 4 1.73 1.91 0.39 o -1 -7 5 1.51 1.34 0.34 o 0 -7 5 26.59 21.72 1.51 o 1 -7 5 362.45 481.85 19.18 o -3 -6 5 6.77 6.24 0.68 o -2 -6 5 15.52 15.89 1.18 o 0 -6 5 0.51 0.42 0.31 o 1 -6 5 14.48 17.00 0.88 o 2 -6 5 118.64 125.95 5.89 o 3 -6 5 11.74 17.39 1.25 o -4 -5 5 129.43 191.42 8.56 o -3 -5 5 237.09 289.46 12.12 o -2 -5 5 5.43 5.70 0.49 o 0 -5 5 181.10 178.03 5.57 o 1 -5 5 5.37 5.97 0.44 o 2 -5 5 296.95 411.50 16.65 o 3 -5 5 0.63 0.33 0.33 o 4 -5 5 0.55 0.66 0.33 o -4 -4 5 41.09 46.22 1.86 o -1 -4 5 2.46 3.59 0.42 o 0 -4 5 247.95 244.87 10.42 o 2 -4 5 8.33 6.24 1.30 o -6 -3 5 88.14 81.92 4.18 o -5 -3 5 242.56 275.25 11.56 o -4 -3 5 20.94 31.66 1.35 o -3 -3 5 188.76 201.87 6.21 o 0 -3 5 32.45 29.93 1.23 o 2 -3 5 10.72 9.08 0.54 o 3 -3 5 69.40 119.32 5.62 o 5 -3 5 0.25 0.49 0.28 o -6 -2 5 40.94 40.92 2.38 o -5 -2 5 2.78 3.59 0.55 o -3 -2 5 27.53 22.39 1.15 o -2 -2 5 100.94 120.32 3.94 o 1 -2 5 49.75 48.03 1.80 o 3 -2 5 0.43 0.84 0.34 o 4 -2 5 170.91 168.13 7.45 o 5 -2 5 191.55 302.18 12.36 o -7 -1 5 0.94 0.70 0.29 o -5 -1 5 12.16 12.52 0.97 o -4 -1 5 93.97 102.64 3.46 o -2 -1 5 98.12 97.48 3.28 o -1 -1 5 43.93 57.26 2.09 o 0 -1 5 118.76 119.11 5.53 o 3 -1 5 0.55 0.54 0.27 o 4 -1 5 2.83 1.85 0.39 o -7 0 5 26.34 31.88 1.99 o -6 0 5 19.26 21.11 1.46 o 0 0 5 17.31 17.98 0.65 o 1 0 5 0.96 0.76 0.12 o 2 0 5 119.33 134.91 3.56 o 4 0 5 0.63 0.69 0.19 o 5 0 5 19.20 17.44 1.24 o -7 1 5 338.87 216.39 9.59 o -6 1 5 21.33 23.10 1.08 o -3 1 5 15.23 20.57 0.76 o 0 1 5 100.54 118.23 3.88 o 2 1 5 82.09 79.10 2.26 o 3 1 5 39.21 42.28 1.71 o 5 1 5 30.75 43.30 2.59 o -7 2 5 212.17 235.57 7.17 o -6 2 5 45.39 47.16 1.86 o -5 2 5 4.06 4.98 0.39 o -3 2 5 6.81 12.48 0.54 o -2 2 5 1.18 2.59 0.26 o 0 2 5 122.84 123.34 4.03 o 1 2 5 248.33 199.62 8.78 o 3 2 5 19.76 16.96 0.86 o 4 2 5 32.37 32.61 1.95 o -5 3 5 5.80 4.48 0.39 o -4 3 5 4.60 4.60 0.37 o -2 3 5 97.77 113.43 5.42 o -1 3 5 92.81 137.45 8.11 o 1 3 5 37.79 43.26 1.71 o 3 3 5 194.16 174.87 5.57 o 4 3 5 8.57 8.48 0.76 o -6 4 5 8.86 9.36 0.64 o -5 4 5 134.44 127.92 6.06 o -4 4 5 7.03 5.08 0.52 o -3 4 5 111.09 133.24 6.27 o -2 4 5 68.32 92.90 7.93 o -1 4 5 45.19 41.17 4.68 o 0 4 5 161.60 188.97 8.47 o 1 4 5 7.94 11.56 0.67 o 2 4 5 21.75 24.53 1.15 o 3 4 5 330.03 287.39 12.26 o -6 5 5 27.44 29.47 1.93 o -5 5 5 58.81 40.92 2.32 o -4 5 5 125.93 92.52 4.54 o -3 5 5 3.04 3.16 0.54 o -2 5 5 249.42 306.76 12.96 o -1 5 5 8.99 9.29 0.60 o 0 5 5 30.26 30.49 1.33 o 2 5 5 69.25 81.93 2.99 o -5 6 5 54.04 43.29 2.47 o -3 6 5 5.86 6.33 0.52 o -2 6 5 40.64 40.93 1.69 o -1 6 5 306.50 326.39 13.73 o 0 6 5 3.54 3.37 0.37 o 1 6 5 60.76 73.66 2.78 o -2 7 5 32.60 44.65 2.67 o 1 -7 6 17.01 22.06 1.56 o -3 -6 6 192.33 174.82 7.88 o -2 -6 6 52.03 51.41 2.81 o -1 -6 6 112.44 119.71 5.68 o 0 -6 6 144.98 152.69 4.94 o 1 -6 6 0.63 0.40 0.20 o -4 -5 6 39.39 39.94 2.35 o -3 -5 6 115.22 114.18 3.86 o -2 -5 6 3.38 2.27 0.26 o -1 -5 6 9.23 8.06 0.51 o 0 -5 6 140.22 111.82 3.73 o 1 -5 6 4.50 4.71 0.45 o 2 -5 6 113.62 118.24 3.98 o -5 -4 6 147.41 171.98 7.80 o -4 -4 6 272.82 214.55 8.52 o -3 -4 6 16.61 18.22 0.92 o -1 -4 6 12.13 7.64 0.64 o 0 -4 6 0.98 0.89 0.20 o 3 -4 6 76.02 85.59 4.31 o 4 -4 6 294.81 309.21 12.73 o -6 -3 6 53.68 58.52 3.22 o -5 -3 6 14.76 15.16 1.16 o -3 -3 6 43.56 59.11 2.88 o -2 -3 6 105.26 108.61 3.66 o 0 -3 6 27.57 26.19 1.12 o 1 -3 6 68.34 75.65 2.68 o 3 -3 6 10.34 14.56 1.12 o 4 -3 6 43.50 38.62 2.24 o -5 -2 6 3.10 3.20 0.55 o -4 -2 6 0.50 0.62 0.19 o -2 -2 6 82.35 77.61 2.72 o 1 -2 6 7.74 9.72 0.55 o 3 -2 6 115.82 146.70 6.71 o 4 -2 6 32.38 31.86 1.89 o -6 -1 6 10.23 11.23 0.98 o -5 -1 6 137.82 182.27 8.11 o -4 -1 6 18.83 20.05 0.95 o -2 -1 6 1.00 1.37 0.46 o -1 -1 6 5.68 6.43 0.42 o 1 -1 6 3.29 5.13 0.38 o 2 -1 6 192.34 173.51 5.44 o 5 -1 6 62.22 75.24 3.90 o -6 0 6 3.38 4.26 0.58 o -5 0 6 34.96 13.85 1.07 o -4 0 6 43.13 29.51 1.28 o -3 0 6 59.86 69.30 2.50 o -1 0 6 12.52 11.02 0.59 o 0 0 6 8.87 8.69 0.92 o 2 0 6 76.82 73.62 2.67 o 3 0 6 157.13 153.96 6.91 o -6 1 6 138.21 113.89 5.32 o -5 1 6 92.38 88.17 4.35 o -3 1 6 31.89 33.30 1.38 o -2 1 6 189.43 345.64 13.95 o 0 1 6 5.97 5.44 0.40 o 1 1 6 87.34 89.02 4.19 o 2 1 6 140.67 134.80 6.27 o -5 2 6 30.31 32.67 1.92 o -4 2 6 100.53 106.59 5.09 o -2 2 6 132.61 145.55 4.68 o -1 2 6 78.47 85.30 3.95 o 1 2 6 34.46 37.58 1.53 o 2 2 6 146.96 139.32 4.55 o 3 2 6 145.05 97.59 4.73 o -6 3 6 36.77 46.76 1.89 o -5 3 6 210.85 172.63 5.40 o -4 3 6 28.17 30.99 1.32 o -1 3 6 19.20 18.27 0.88 o 1 3 6 78.81 82.05 2.91 o 2 3 6 59.33 63.83 2.39 o 3 3 6 226.50 158.46 7.30 o -6 4 6 6.24 5.73 0.73 o -5 4 6 61.14 25.61 1.61 o -4 4 6 13.41 12.26 0.97 o -3 4 6 6.99 6.55 0.46 o -1 4 6 77.68 78.51 2.81 o 0 4 6 32.03 37.53 1.80 o 1 4 6 312.17 241.99 10.52 o 2 4 6 6.41 6.11 0.54 o 3 4 6 166.35 191.13 6.08 o -5 5 6 27.81 24.32 1.58 o -4 5 6 167.30 308.92 12.93 o -3 5 6 61.25 68.19 3.62 o -2 5 6 27.98 31.49 1.35 o -1 5 6 179.25 194.62 6.10 o 0 5 6 0.24 0.74 0.21 o 1 5 6 277.88 296.41 12.01 o -4 6 6 36.71 42.90 2.49 o -2 6 6 31.24 32.43 1.44 o -1 6 6 2.33 1.94 0.33 o 0 6 6 140.63 169.29 7.67 o -1 -6 7 5.80 5.14 0.51 o 0 -6 7 609.86 638.46 24.13 o 1 -6 7 13.83 15.13 0.85 o -3 -5 7 24.16 19.60 0.98 o -2 -5 7 341.38 380.98 15.35 o -1 -5 7 58.14 52.97 2.05 o 0 -5 7 13.77 17.28 1.48 o 2 -5 7 0.36 -0.09 0.29 o -5 -4 7 16.64 12.82 1.02 o -4 -4 7 200.72 287.46 23.04 o -3 -4 7 35.89 37.33 1.86 o -2 -4 7 180.68 198.62 9.62 o -1 -4 7 334.90 340.90 9.86 o 0 -4 7 60.61 52.74 2.00 o 1 -4 7 63.09 44.54 2.53 o 2 -4 7 91.81 63.13 8.84 o 3 -4 7 20.67 23.68 1.62 o -5 -3 7 8.33 8.36 0.84 o -4 -3 7 13.18 13.06 1.05 o -2 -3 7 32.59 29.39 1.25 o -1 -3 7 61.50 58.78 2.19 o 1 -3 7 14.23 14.14 0.73 o 2 -3 7 15.68 15.21 0.94 o 3 -3 7 49.19 53.73 2.93 o -6 -2 7 173.98 159.84 7.29 o -4 -2 7 14.09 13.98 0.77 o -2 -2 7 211.43 224.53 6.84 o -1 -2 7 26.92 21.23 0.94 o 1 -2 7 90.43 89.22 3.10 o 2 -2 7 69.24 64.11 2.37 o 3 -2 7 112.26 120.47 5.71 o 4 -2 7 33.20 56.00 3.01 o -6 -1 7 37.68 31.04 1.96 o -5 -1 7 217.52 205.58 9.00 o -4 -1 7 127.85 124.03 4.10 o -3 -1 7 30.13 26.50 1.17 o -1 -1 7 34.18 38.37 1.56 o 0 -1 7 30.79 34.89 2.30 o 2 -1 7 0.56 0.85 0.36 o 3 -1 7 253.89 271.12 11.39 o -6 0 7 13.87 12.79 1.10 o -5 0 7 0.69 0.29 0.31 o -3 0 7 73.85 78.41 2.80 o 2 0 7 54.35 61.13 2.30 o -5 1 7 0.69 1.22 0.43 o -4 1 7 10.94 11.12 0.67 o -2 1 7 26.52 22.86 1.29 o -1 1 7 78.88 82.26 2.90 o 0 1 7 334.72 130.93 5.98 o 1 1 7 12.67 12.23 0.97 o 2 1 7 228.71 216.01 9.46 o -6 2 7 111.95 145.19 6.69 o -4 2 7 22.96 30.29 1.92 o -3 2 7 229.49 239.72 10.16 o -2 2 7 165.88 211.44 13.08 o -1 2 7 59.87 75.43 3.95 o 0 2 7 161.59 113.59 5.46 o 1 2 7 14.32 15.75 1.20 o 2 2 7 54.45 61.80 3.40 o -6 3 7 45.76 49.00 2.76 o -5 3 7 161.14 201.92 8.90 o -3 3 7 17.70 17.09 1.26 o -1 3 7 57.23 76.04 3.93 o 0 3 7 5.17 6.90 0.84 o 1 3 7 142.58 103.14 5.05 o 2 3 7 15.01 15.90 1.26 o -3 4 7 2.62 3.37 0.34 o -2 4 7 343.05 231.51 7.08 o 0 4 7 39.93 39.50 2.38 o 1 4 7 434.99 481.10 19.21 o -5 5 7 9.36 6.06 0.73 o -4 5 7 107.06 124.93 5.92 o -3 5 7 30.59 34.62 1.48 o -2 5 7 7.76 8.01 0.56 o -1 5 7 340.02 344.23 14.34 o 0 5 7 107.64 121.27 4.12 o 1 5 7 0.40 0.44 0.28 o -3 6 7 200.57 180.99 5.79 o -2 6 7 20.60 21.83 1.51 o -2 -5 8 233.24 237.11 7.25 o -1 -5 8 253.76 266.29 7.96 o 0 -5 8 56.13 53.19 2.07 o 1 -5 8 378.36 372.35 15.02 o -4 -4 8 9.13 12.14 1.59 o -3 -4 8 130.73 116.79 3.93 o -2 -4 8 9.96 10.79 0.61 o -1 -4 8 247.79 225.69 6.88 o 0 -4 8 102.05 99.48 3.43 o 1 -4 8 8.99 8.19 0.78 o 2 -4 8 212.48 198.19 8.71 o -4 -3 8 60.98 70.97 3.79 o -3 -3 8 36.35 54.68 2.18 o -2 -3 8 41.74 42.40 1.73 o -1 -3 8 2.86 3.60 0.36 o 1 -3 8 9.85 9.27 0.59 o 2 -3 8 82.85 87.29 7.01 o -5 -2 8 207.17 223.04 9.65 o -4 -2 8 287.35 260.53 7.81 o -3 -2 8 14.58 12.23 0.71 o -2 -2 8 85.17 73.29 2.64 o -1 -2 8 0.62 0.61 0.20 o 0 -2 8 26.33 22.23 1.03 o 1 -2 8 194.01 197.59 6.14 o 2 -2 8 0.19 0.29 0.17 o 3 -2 8 87.00 100.21 4.95 o -5 -1 8 1.99 1.67 0.40 o -3 -1 8 0.44 0.98 0.25 o 2 -1 8 115.85 110.64 3.78 o 3 -1 8 96.09 98.28 4.86 o -5 0 8 2.87 2.61 0.53 o -4 0 8 248.17 273.11 11.48 o -3 0 8 70.67 74.64 2.68 o -2 0 8 0.29 0.28 0.17 o 0 0 8 151.77 138.16 4.50 o 1 0 8 23.00 25.96 1.19 o 2 0 8 296.21 284.39 12.07 o -6 1 8 90.90 161.71 7.40 o -5 1 8 176.65 212.76 9.30 o -4 1 8 15.72 15.66 0.84 o -3 1 8 371.36 266.40 11.37 o -2 1 8 16.17 19.57 0.97 o -1 1 8 6.05 4.68 0.41 o 1 1 8 64.75 80.14 4.19 o 2 1 8 38.26 37.64 2.31 o -6 2 8 21.39 38.01 2.32 o -5 2 8 101.98 118.13 5.69 o -4 2 8 63.29 66.65 3.49 o -3 2 8 11.86 15.26 1.14 o -2 2 8 196.08 171.11 7.74 o -1 2 8 3.77 5.12 0.67 o 0 2 8 6.68 6.73 0.71 o 1 2 8 158.52 163.07 7.49 o 2 2 8 96.46 92.00 4.67 o -3 3 8 7.46 7.00 0.74 o -2 3 8 54.92 55.62 3.08 o 0 3 8 64.12 87.26 4.57 o -3 4 8 70.70 69.75 3.70 o -2 4 8 53.63 51.82 2.91 o -1 4 8 351.04 455.97 18.29 o 0 4 8 66.37 72.97 3.85 o -2 -4 9 48.45 46.08 1.87 o -1 -4 9 8.87 7.88 0.55 o -4 -3 9 11.06 8.71 0.76 o -3 -3 9 18.81 13.15 1.32 o -2 -3 9 119.31 116.46 4.84 o -1 -3 9 9.73 9.90 0.62 o 0 -3 9 171.30 165.69 5.29 o 1 -3 9 152.57 161.34 5.21 o -4 -2 9 297.20 249.16 7.56 o -3 -2 9 0.20 0.17 0.18 o -2 -2 9 34.97 31.99 1.39 o -1 -2 9 194.83 178.23 5.64 o 0 -2 9 21.60 16.12 0.85 o 1 -2 9 163.35 114.92 5.44 o 2 -2 9 145.76 153.36 7.00 o -4 -1 9 216.47 209.20 14.78 o -3 -1 9 137.54 155.18 5.06 o -2 -1 9 38.34 37.09 2.49 o -1 -1 9 370.81 345.07 14.01 o 0 -1 9 26.93 26.10 1.18 o 1 -1 9 19.94 21.47 1.23 o 2 -1 9 178.40 175.05 5.61 o -5 0 9 168.30 175.91 7.92 o -4 0 9 86.73 76.94 2.78 o -2 0 9 49.89 58.36 3.59 o -1 0 9 24.26 23.34 1.10 o 0 0 9 522.35 664.75 24.89 o 1 0 9 0.32 0.28 0.35 o 2 0 9 0.38 0.66 0.39 o -4 1 9 51.87 58.50 6.36 o -3 1 9 28.16 31.07 1.40 o -2 1 9 254.21 280.32 11.95 o -1 1 9 1.30 2.77 0.58 o 0 1 9 153.59 151.39 7.05 o 1 1 9 74.02 72.22 3.84 o -5 2 9 18.97 17.56 1.34 o -3 2 9 114.57 121.55 5.86 o -2 2 9 79.22 79.35 4.19 o -1 2 9 128.01 135.08 6.41 o 0 2 9 12.59 9.51 0.91 o -3 3 9 46.97 45.06 2.65 o -2 3 9 11.22 13.10 1.10 o -1 3 9 347.17 315.88 13.25 o -2 -2 10 44.83 47.35 1.92 o -1 -2 10 366.69 448.26 17.64 o -4 -1 10 49.22 43.46 2.57 o -3 -1 10 168.55 187.82 5.94 o -2 -1 10 30.13 20.16 1.20 o -1 -1 10 14.32 11.77 0.69 o -4 0 10 10.11 9.98 0.90 o -3 0 10 1.00 0.90 0.26 o -2 0 10 249.90 270.62 8.06 o -1 0 10 85.78 70.99 2.62 o -4 1 10 226.26 241.56 7.45 o