#------------------------------------------------------------------------------
#$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $
#$Revision: 26025 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2214419.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2214419_Fobs
loop_
_publ_author_name
'Abdelhedi, Mohamed'
'Ktari, Lilia'
'Dammak, Mohamed'
'Cousson, Alain'
'Kolsi, Abdelwaheb'
_publ_section_title
;
 K~2~(SO~4~)~0.63~(SeO~4~)~0.37~·Te(OH)~6~
;
_journal_coeditor_code           WM2119
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i153
_journal_page_last               i154
_journal_volume                  63
_journal_year                    2007
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_audit_creation_date             07-04-01
_audit_creation_method           CRYSTALS
_cell_angle_alpha                102.138(2)
_cell_angle_beta                 90.073(2)
_cell_angle_gamma                116.9430(10)
_cell_length_a                   6.2463(2)
_cell_length_b                   6.6470(2)
_cell_length_c                   13.1326(4)
_[local]_cod_data_source_file    wm2119Isup2.hkl
_[local]_cod_data_source_block   I
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_meas
_refln_F_squared_calc
_refln_F_squared_sigma
_refln_observed_status
1 0 0 88.07 90.55 3.48 x
2 0 0 680.72 460.24 24.38 o
3 0 0 61.75 70.62 3.39 x
4 0 0 1502.98 1680.07 53.54 o
5 0 0 134.19 127.19 7.06 o
6 0 0 125.78 154.08 7.65 o
7 0 0 -0.47 0.44 5.16 <
-8 1 0 48.92 62.29 7.09 x
-7 1 0 55.55 59.53 6.00 x
-6 1 0 1745.01 1700.86 63.02 o
-5 1 0 27.76 31.61 3.20 x
-4 1 0 2751.23 2529.38 96.91 o
-3 1 0 720.15 737.86 26.21 o
-2 1 0 6732.46 6130.65 235.08 o
-1 1 0 8.28 25.33 0.95 x
0 1 0 1912.98 1236.09 67.66 x
1 1 0 -0.41 0.09 0.64 <
2 1 0 784.18 1137.92 28.02 o
3 1 0 435.91 376.43 16.27 o
4 1 0 677.93 660.53 25.06 o
5 1 0 86.28 88.65 5.61 x
6 1 0 569.71 519.21 22.75 o
7 1 0 17.02 19.03 5.25 <
-8 2 0 985.53 864.85 38.50 o
-7 2 0 189.79 171.35 10.66 o
-6 2 0 433.19 481.50 17.89 o
-5 2 0 214.53 257.57 9.77 o
-4 2 0 2918.59 3165.95 102.84 o
-3 2 0 112.86 117.43 5.30 o
-2 2 0 2882.93 2309.52 101.45 o
-1 2 0 660.62 797.04 23.82 o
0 2 0 1256.07 1574.71 44.29 o
1 2 0 1691.68 1516.16 58.94 o
2 2 0 984.86 876.12 34.92 o
3 2 0 118.02 136.75 5.74 o
4 2 0 1487.33 1552.55 53.44 o
5 2 0 267.51 261.08 12.03 o
6 2 0 172.73 209.49 10.06 o
-8 3 0 451.18 515.35 20.49 o
-7 3 0 58.74 78.49 6.17 x
-6 3 0 1034.14 1005.80 38.68 o
-5 3 0 74.65 68.77 5.08 x
-4 3 0 1084.63 1061.07 39.63 o
-3 3 0 2976.51 2888.86 105.20 o
-2 3 0 823.71 1042.29 30.09 o
-1 3 0 379.79 484.33 14.19 o
0 3 0 1352.13 1227.84 47.56 o
1 3 0 93.35 129.55 4.39 x
2 3 0 2731.62 2796.07 95.57 o
3 3 0 388.26 409.85 15.26 o
4 3 0 681.90 707.55 25.86 o
5 3 0 -0.41 0.07 4.53 <
6 3 0 485.99 375.11 20.99 o
-8 4 0 269.38 225.32 14.72 o
-7 4 0 -0.01 0.06 5.08 <
-6 4 0 151.90 167.98 8.79 o
-5 4 0 557.04 569.81 21.98 o
-4 4 0 1466.64 1428.80 53.20 o
-3 4 0 690.78 739.86 25.97 o
-2 4 0 1755.47 1676.51 62.48 o
-1 4 0 265.65 286.14 10.52 o
0 4 0 5013.29 4926.25 174.39 o
1 4 0 206.33 206.84 8.70 o
2 4 0 508.41 550.69 19.32 o
3 4 0 11.75 13.73 3.08 <
4 4 0 832.13 777.36 31.61 o
5 4 0 -0.67 0.07 5.32 <
-8 5 0 201.38 199.99 12.69 o
-7 5 0 176.41 154.61 10.96 o
-6 5 0 1148.14 1185.53 43.28 o
-5 5 0 26.48 38.96 3.90 x
-4 5 0 1037.48 1122.49 38.64 o
-3 5 0 78.96 76.93 5.25 x
-2 5 0 3742.51 3837.60 131.45 o
-1 5 0 12.42 23.53 2.28 x
0 5 0 892.89 957.76 32.80 o
1 5 0 9.08 8.21 2.69 <
2 5 0 521.67 479.20 20.42 o
3 5 0 0.87 0.41 3.89 <
4 5 0 205.76 227.04 11.32 o
-8 6 0 583.98 622.84 25.58 o
-7 6 0 116.25 70.03 8.95 o
-6 6 0 732.57 728.22 29.46 o
-5 6 0 14.45 18.30 3.96 <
-4 6 0 1654.51 1723.73 60.27 o
-3 6 0 31.96 23.44 4.02 x
-2 6 0 798.54 859.88 30.13 o
-1 6 0 123.17 84.00 7.11 o
0 6 0 386.95 351.00 16.04 o
1 6 0 0.63 0.96 3.72 <
2 6 0 321.98 343.41 14.44 o
3 6 0 43.08 16.99 5.68 x
-8 7 0 396.57 399.65 20.20 o
-7 7 0 1.29 2.28 6.87 <
-6 7 0 303.85 363.45 15.42 o
-5 7 0 0.55 0.69 5.82 <
-4 7 0 1144.95 1178.38 43.05 o
-3 7 0 143.21 110.20 8.72 o
-2 7 0 128.20 100.25 8.35 o
-1 7 0 33.63 23.18 4.75 x
0 7 0 482.87 498.69 20.21 o
1 7 0 115.20 71.15 8.29 o
-7 8 0 27.94 36.10 7.51 <
-6 8 0 366.99 303.28 18.31 o
-5 8 0 217.52 171.78 13.12 o
-4 8 0 318.16 371.78 15.60 o
-3 8 0 24.27 17.35 5.65 x
-2 8 0 197.21 162.78 11.69 o
-1 8 0 68.77 39.46 7.05 x
0 8 0 501.78 539.83 22.02 o
-5 9 0 40.15 17.72 7.96 x
-4 9 0 304.78 228.82 16.87 o
-3 9 0 4.08 3.86 6.53 <
3 -9 1 62.08 58.02 8.09 x
4 -9 1 50.01 38.30 7.68 x
5 -9 1 476.38 403.89 22.15 o
0 -8 1 19.33 26.62 5.54 <
1 -8 1 72.58 71.99 7.09 x
2 -8 1 11.44 14.97 4.83 <
3 -8 1 661.21 648.95 26.95 o
4 -8 1 19.25 21.22 5.35 <
5 -8 1 567.13 727.10 24.44 o
6 -8 1 6.02 7.05 6.34 <
7 -8 1 433.19 415.99 21.38 o
-2 -7 1 6.94 6.87 4.34 <
-1 -7 1 232.86 220.27 11.94 o
0 -7 1 5.34 6.79 4.11 <
1 -7 1 519.14 550.10 20.89 o
2 -7 1 77.84 59.41 6.14 x
3 -7 1 1766.88 1957.09 64.07 o
4 -7 1 8.73 10.28 4.08 <
5 -7 1 482.27 448.54 20.79 o
6 -7 1 12.99 18.56 5.22 <
7 -7 1 374.17 427.93 18.54 o
8 -7 1 98.96 76.59 10.05 x
-3 -6 1 385.36 343.85 16.80 o
-2 -6 1 5.40 6.50 3.52 <
-1 -6 1 624.26 669.11 24.15 o
0 -6 1 237.84 189.07 10.92 o
1 -6 1 1708.30 1741.23 61.38 o
2 -6 1 100.24 56.41 6.02 o
3 -6 1 370.54 383.01 15.48 o
4 -6 1 132.84 116.58 7.96 o
5 -6 1 659.61 655.58 26.27 o
6 -6 1 585.22 566.04 24.27 o
7 -6 1 464.04 430.10 20.89 o
8 -6 1 64.72 32.39 7.93 x
-4 -5 1 16.22 18.33 4.35 <
-3 -5 1 356.13 398.69 15.01 o
-2 -5 1 174.95 138.65 8.61 o
-1 -5 1 1049.54 989.86 38.13 o
0 -5 1 266.38 248.92 10.91 o
1 -5 1 1085.40 1127.97 39.25 o
2 -5 1 96.68 157.31 5.32 x
3 -5 1 686.64 641.81 25.95 o
4 -5 1 318.95 316.63 13.75 o
5 -5 1 939.16 987.97 35.54 o
6 -5 1 3.57 3.23 3.74 <
7 -5 1 614.56 597.04 25.73 o
8 -5 1 1.53 1.86 6.93 <
-5 -4 1 161.60 183.16 9.79 o
-4 -4 1 190.24 149.26 9.65 o
-3 -4 1 1295.39 1278.26 46.83 o
-2 -4 1 206.40 196.84 8.89 o
-1 -4 1 318.74 325.66 12.26 o
0 -4 1 9.48 29.77 1.61 x
1 -4 1 1186.42 1309.77 42.31 o
2 -4 1 244.52 256.98 10.02 o
3 -4 1 2490.17 2480.61 88.36 o
4 -4 1 4.13 3.78 2.11 <
5 -4 1 1584.48 1608.39 57.43 o
6 -4 1 45.28 61.54 4.82 x
7 -4 1 664.21 731.37 26.91 o
8 -4 1 22.32 26.02 6.09 <
-6 -3 1 59.89 56.29 6.68 x
-5 -3 1 340.92 305.68 14.92 o
-4 -3 1 78.19 83.90 5.27 x
-3 -3 1 658.33 663.92 24.46 o
-2 -3 1 69.06 63.99 3.74 x
-1 -3 1 1455.48 1602.29 51.06 o
0 -3 1 634.63 581.12 22.69 o
1 -3 1 2510.76 2190.13 87.90 o
2 -3 1 24.11 2.65 2.05 x
3 -3 1 5076.66 4980.43 177.84 o
4 -3 1 9.85 9.85 2.13 x
5 -3 1 369.16 386.39 15.20 o
6 -3 1 41.97 45.87 4.49 x
7 -3 1 1573.78 1485.51 58.00 o
8 -3 1 65.37 46.25 7.45 x
-6 -2 1 8.04 9.69 4.18 <
-5 -2 1 371.88 418.18 15.37 o
-4 -2 1 12.73 19.46 2.53 x
-3 -2 1 1645.97 1809.76 58.23 o
-2 -2 1 0.78 0.18 1.25 <
-1 -2 1 717.97 550.03 25.45 o
0 -2 1 591.98 710.84 21.03 o
1 -2 1 7748.68 7255.13 270.58 o
2 -2 1 927.42 953.39 33.15 o
3 -2 1 1543.42 1301.26 54.96 o
4 -2 1 145.58 156.21 6.91 o
5 -2 1 2525.09 2599.09 89.72 o
6 -2 1 220.67 212.13 10.70 o
7 -2 1 97.83 121.56 7.42 x
8 -2 1 4.46 6.29 5.30 <
-7 -1 1 127.94 171.84 8.94 o
-6 -1 1 37.45 39.31 4.64 x
-5 -1 1 1359.16 1313.24 49.03 o
-4 -1 1 130.01 118.81 6.28 o
-3 -1 1 656.96 550.55 23.86 o
-2 -1 1 12.50 6.15 1.17 x
-1 -1 1 7439.21 7128.79 265.04 o
0 -1 1 43.41 64.73 1.88 x
1 -1 1 1718.48 1039.10 60.39 x
2 -1 1 215.99 270.81 8.44 o
3 -1 1 751.80 1066.34 27.35 o
4 -1 1 368.50 394.96 14.49 o
5 -1 1 1045.47 1022.86 38.38 o
6 -1 1 13.59 15.89 3.56 <
7 -1 1 480.12 411.00 20.38 o
8 -1 1 -0.08 0.08 6.20 <
-7 0 1 1227.05 1094.18 45.68 o
-6 0 1 6.31 6.55 3.38 <
-5 0 1 311.36 322.84 12.94 o
-4 0 1 296.85 329.27 11.81 o
-3 0 1 1995.70 2387.15 70.21 o
-2 0 1 45.32 41.23 2.34 x
-1 0 1 2244.73 1474.45 79.18 x
0 0 1 -1.40 0.24 0.21 <
1 0 1 4698.73 4668.48 164.00 x
2 0 1 915.57 928.32 32.67 o
3 0 1 2320.83 2004.89 81.64 o
4 0 1 190.95 212.72 8.40 o
5 0 1 1340.87 1393.33 48.62 o
6 0 1 20.62 28.57 3.98 x
7 0 1 244.16 288.21 12.72 o
-8 1 1 0.93 2.12 6.15 <
-7 1 1 248.79 298.73 12.44 o
-6 1 1 132.58 150.77 7.83 o
-5 1 1 1386.43 1476.45 49.99 o
-4 1 1 81.53 70.12 4.60 x
-3 1 1 2990.27 2526.89 105.06 o
-2 1 1 293.23 339.97 11.10 o
-1 1 1 4192.50 4657.26 147.24 x
0 1 1 -0.27 0.01 0.58 <
1 1 1 749.50 524.33 26.68 o
2 1 1 1237.25 1341.56 43.79 o
3 1 1 3157.78 3378.90 110.53 o
4 1 1 996.71 1079.87 36.20 o
5 1 1 541.55 572.68 21.13 o
6 1 1 0.54 1.77 4.22 <
7 1 1 868.24 722.31 34.02 o
-8 2 1 3.78 3.27 5.25 <
-7 2 1 679.84 610.75 27.17 o
-6 2 1 16.52 17.98 3.45 x
-5 2 1 533.90 552.76 20.72 o
-4 2 1 467.87 525.62 18.03 o
-3 2 1 1705.87 1995.30 60.75 o
-2 2 1 520.38 598.06 19.40 o
-1 2 1 294.61 171.63 11.24 o
0 2 1 5.56 3.36 0.95 x
1 2 1 8716.92 8086.39 302.61 o
2 2 1 14.56 5.18 1.74 x
3 2 1 1128.70 1098.37 40.59 o
4 2 1 33.36 33.94 3.57 x
5 2 1 1124.96 1029.88 41.44 o
6 2 1 26.65 29.18 5.14 x
-8 3 1 69.08 60.96 7.64 x
-7 3 1 214.67 246.94 11.69 o
-6 3 1 188.49 193.02 9.74 o
-5 3 1 994.05 1008.67 36.91 o
-4 3 1 159.30 159.40 7.73 o
-3 3 1 2759.68 2477.42 97.99 o
-2 3 1 318.85 336.02 12.61 o
-1 3 1 5872.19 5733.31 204.82 o
0 3 1 1.16 2.82 1.30 <
1 3 1 1223.56 1220.69 43.43 o
2 3 1 98.56 88.18 5.30 x
3 3 1 1168.97 1163.97 42.24 o
4 3 1 20.59 31.64 3.64 x
5 3 1 92.69 114.48 6.90 x
-8 4 1 122.60 88.37 9.66 o
-7 4 1 1291.72 1288.96 48.55 o
-6 4 1 6.27 6.72 3.39 <
-5 4 1 224.34 249.21 10.73 o
-4 4 1 168.40 243.82 8.38 o
-3 4 1 4016.51 4033.34 141.57 o
-2 4 1 152.46 164.73 7.22 o
-1 4 1 1733.94 1691.93 61.51 o
0 4 1 53.56 88.41 3.48 x
1 4 1 466.81 437.90 17.83 o
2 4 1 84.86 105.11 5.23 x
3 4 1 633.06 667.95 24.18 o
4 4 1 129.03 92.63 8.02 o
5 4 1 286.70 247.67 14.20 o
-8 5 1 49.20 25.43 7.28 x
-7 5 1 517.69 558.11 22.45 o
-6 5 1 56.94 110.69 5.77 x
-5 5 1 1278.64 1247.24 47.51 o
-4 5 1 70.49 80.22 5.20 x
-3 5 1 1414.48 1545.98 51.40 o
-2 5 1 1017.29 1042.91 37.32 o
-1 5 1 589.38 588.03 22.34 o
0 5 1 19.80 22.66 3.01 x
1 5 1 715.93 806.88 27.07 o
2 5 1 105.20 77.81 6.60 o
3 5 1 571.11 554.39 22.72 o
4 5 1 162.83 106.25 10.04 o
-8 6 1 2.98 2.74 6.07 <
-7 6 1 337.93 346.92 16.67 o
-6 6 1 0.97 0.04 4.67 <
-5 6 1 789.21 813.64 30.85 o
-4 6 1 191.78 168.29 10.01 o
-3 6 1 502.25 481.91 20.34 o
-2 6 1 67.84 69.10 5.25 x
-1 6 1 345.84 352.38 14.84 o
0 6 1 89.56 87.16 6.32 x
1 6 1 1543.59 1539.33 56.07 o
2 6 1 134.55 89.67 8.67 o
3 6 1 224.71 240.61 12.26 o
-8 7 1 73.05 35.50 8.53 x
-7 7 1 235.89 193.55 13.86 o
-6 7 1 240.71 192.82 13.37 o
-5 7 1 367.84 393.48 17.13 o
-4 7 1 36.99 33.02 5.37 x
-3 7 1 643.38 636.28 25.66 o
-2 7 1 12.44 11.91 4.48 <
-1 7 1 1220.36 1272.32 45.61 o
0 7 1 88.90 63.55 7.28 x
1 7 1 441.03 451.74 19.40 o
-7 8 1 322.57 373.60 17.93 o
-6 8 1 86.10 48.00 8.83 x
-5 8 1 536.30 463.74 23.76 o
-4 8 1 2.47 1.92 5.66 <
-3 8 1 696.66 802.44 28.52 o
-2 8 1 3.48 4.24 4.81 <
-1 8 1 386.28 375.98 18.23 o
0 8 1 0.06 0.93 2.81 <
-4 9 1 5.32 6.72 6.51 <
2 -9 2 244.20 208.60 14.08 o
3 -9 2 0.21 0.63 6.13 <
4 -9 2 428.95 575.27 20.46 o
5 -9 2 0.92 0.05 7.33 <
6 -9 2 294.68 228.50 17.46 o
0 -8 2 280.71 243.65 14.05 o
1 -8 2 32.81 19.44 5.77 x
2 -8 2 623.51 686.64 25.44 o
3 -8 2 5.47 5.73 4.57 <
4 -8 2 683.55 642.52 27.82 o
5 -8 2 209.44 167.88 12.33 o
6 -8 2 178.35 218.55 11.97 o
7 -8 2 131.21 88.83 11.32 o
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-1 -7 2 129.52 76.62 8.15 o
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1 -7 2 -0.01 0.00 4.59 <
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3 -7 2 184.75 134.97 9.79 o
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5 -7 2 321.46 282.04 15.34 o
6 -7 2 497.18 474.85 21.72 o
7 -7 2 2.80 4.81 5.70 <
8 -7 2 102.18 92.70 10.15 o
-3 -6 2 293.92 209.68 13.12 o
-2 -6 2 813.75 805.52 30.47 o
-1 -6 2 146.14 104.50 8.00 o
0 -6 2 1026.96 1083.85 37.70 o
1 -6 2 177.95 141.73 8.47 o
2 -6 2 353.89 328.19 14.57 o
3 -6 2 138.30 98.93 7.48 o
4 -6 2 371.33 388.54 15.90 o
5 -6 2 51.55 67.06 5.19 x
6 -6 2 551.06 561.56 23.04 o
7 -6 2 18.91 20.79 5.40 <
8 -6 2 517.87 527.59 23.37 o
-4 -5 2 555.30 525.45 22.19 o
-3 -5 2 8.56 8.26 3.23 <
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-1 -5 2 2.46 1.95 2.24 <
0 -5 2 181.41 144.42 7.88 o
1 -5 2 165.38 156.74 7.40 o
2 -5 2 592.27 583.26 22.18 o
3 -5 2 7.11 6.79 2.25 <
4 -5 2 2451.23 2489.98 87.37 o
5 -5 2 5.38 7.28 3.09 <
6 -5 2 687.92 731.52 27.38 o
7 -5 2 68.16 65.93 6.96 x
8 -5 2 862.62 874.14 35.05 o
-5 -4 2 6.76 8.80 4.09 <
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-2 -4 2 339.21 320.48 13.08 o
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0 -4 2 1130.01 1131.00 39.93 o
1 -4 2 155.71 166.48 6.55 o
2 -4 2 4305.50 4440.60 150.78 o
3 -4 2 29.83 58.52 2.80 x
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5 -4 2 584.53 606.66 22.94 o
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8 -4 2 271.21 288.17 14.79 o
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-2 -3 2 142.81 117.15 5.98 o
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0 -3 2 6240.68 5998.97 216.94 o
1 -3 2 663.93 619.62 23.77 o
2 -3 2 2305.52 2039.26 81.16 o
3 -3 2 90.68 171.13 4.74 x
4 -3 2 1710.71 1846.61 61.21 o
5 -3 2 343.74 347.39 14.35 o
6 -3 2 419.80 464.50 17.60 o
7 -3 2 0.53 0.38 5.30 <
8 -3 2 298.17 238.27 15.56 o
-6 -2 2 808.87 684.30 30.87 o
-5 -2 2 -0.03 0.00 3.00 <
-4 -2 2 394.35 406.70 15.48 o
-3 -2 2 941.65 1024.96 33.63 o
-2 -2 2 5671.48 5595.91 197.10 o
-1 -2 2 18.26 40.64 1.20 x
0 -2 2 1913.57 1584.58 67.08 o
1 -2 2 356.57 458.99 13.03 o
2 -2 2 293.98 501.74 11.31 o
3 -2 2 855.93 933.39 31.03 o
4 -2 2 2267.30 2134.04 80.50 o
5 -2 2 50.65 41.36 4.09 x
6 -2 2 933.11 930.57 35.14 o
7 -2 2 10.74 13.58 4.39 <
8 -2 2 283.77 331.39 15.17 o
-7 -1 2 2.45 2.38 4.70 <
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-5 -1 2 315.82 334.01 13.12 o
-4 -1 2 1363.93 1487.39 48.56 o
-3 -1 2 48.61 59.05 2.91 x
-2 -1 2 1231.99 987.34 43.19 o
-1 -1 2 29.06 27.43 1.35 x
0 -1 2 4005.39 4390.82 148.48 x
1 -1 2 28.94 45.37 1.58 x
2 -1 2 202.37 97.37 8.04 o
3 -1 2 360.02 365.75 13.80 o
4 -1 2 3987.86 4117.07 139.96 o
5 -1 2 64.19 72.56 4.71 x
6 -1 2 193.15 217.74 9.96 o
7 -1 2 9.13 9.43 4.61 <
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-6 0 2 761.15 742.29 28.86 o
-5 0 2 14.24 18.53 2.68 x
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