#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/44/2214424.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214424_Fobs loop_ _publ_author_name 'Li, Wei' 'Ye, Ning' _publ_section_title ; Na~2~[BeB~2~O~5~] ; _journal_coeditor_code WM2126 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i160 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.665 _cell_angle_gamma 90.000 _cell_length_a 5.8117 _cell_length_b 8.1666 _cell_length_c 8.9830 _exptl_crystal_F_000 304.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file wm2126Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' kbbf in C 2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 113.46 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2005.70 1865.85 20.11 o 4 0 0 502.54 498.75 11.19 o 6 0 0 4684.70 4699.09 31.18 o 1 1 0 11.43 12.79 0.72 o 3 1 0 65.19 57.64 1.69 o 5 1 0 24.84 24.99 2.26 o 7 1 0 14.44 14.15 2.53 o 0 2 0 704.23 762.32 11.10 o 2 2 0 2601.92 2500.57 9.72 o 4 2 0 879.69 874.85 8.95 o 6 2 0 31.31 31.83 3.17 o 1 3 0 2808.51 2619.20 10.81 o 3 3 0 3220.84 3203.82 15.18 o 5 3 0 963.99 960.89 16.50 o 7 3 0 113.85 114.84 5.39 o 0 4 0 187.35 221.96 3.90 o 2 4 0 204.57 209.50 3.14 o 4 4 0 93.16 88.56 3.80 o 6 4 0 0.30 0.99 1.86 o 1 5 0 1028.88 982.34 7.41 o 3 5 0 8290.75 7950.62 20.88 o 5 5 0 244.93 247.30 5.00 o 0 6 0 513.75 518.87 6.79 o 2 6 0 28.67 29.88 1.61 o 4 6 0 14.70 11.83 1.97 o 6 6 0 83.36 81.17 6.10 o 1 7 0 954.25 938.13 9.47 o 3 7 0 175.21 179.76 4.41 o 5 7 0 261.26 257.04 6.86 o 0 8 0 1601.11 1621.50 25.69 o 2 8 0 927.84 937.57 9.38 o 4 8 0 377.60 383.84 6.73 o 1 9 0 120.49 120.95 5.24 o 3 9 0 3.56 2.90 2.21 o 0 10 0 1043.19 1110.25 25.01 o 2 10 0 93.44 87.20 5.14 o -7 1 1 176.49 176.84 6.27 o -5 1 1 100.41 95.59 2.68 o -3 1 1 2996.44 3156.49 15.67 o -1 1 1 3.16 7.78 0.80 o 1 1 1 0.05 2.57 0.49 o 3 1 1 4207.75 4252.27 20.88 o 5 1 1 308.69 298.58 5.76 o 7 1 1 25.82 28.70 2.93 o -6 2 1 40.82 35.23 3.34 o -4 2 1 40.02 36.55 2.08 o -2 2 1 2196.76 2424.83 16.07 o 0 2 1 0.08 1.10 0.20 o 2 2 1 2003.84 2069.59 11.67 o 4 2 1 300.32 309.77 3.92 o 6 2 1 12.83 14.84 3.04 o -7 3 1 1.37 3.12 2.06 o -5 3 1 199.80 190.12 4.20 o -3 3 1 1210.10 1311.23 7.89 o -1 3 1 628.73 675.23 4.30 o 1 3 1 458.35 541.41 4.92 o 3 3 1 462.55 487.15 4.65 o 5 3 1 225.80 230.61 5.87 o 7 3 1 12.07 18.30 4.87 o -6 4 1 338.65 329.63 7.66 o -4 4 1 91.94 90.36 2.58 o -2 4 1 59.87 55.79 1.84 o 0 4 1 6958.46 6944.72 23.49 o 2 4 1 402.12 395.50 3.86 o 4 4 1 261.80 271.48 3.72 o 6 4 1 791.29 809.33 11.27 o -5 5 1 132.34 119.27 3.67 o -3 5 1 13.52 12.23 1.45 o -1 5 1 12.78 13.17 2.03 o 1 5 1 527.45 573.63 3.54 o 3 5 1 9.54 9.77 1.16 o 5 5 1 72.07 70.13 4.82 o -6 6 1 0.00 1.73 1.47 o -4 6 1 69.98 65.02 2.40 o -2 6 1 30.67 28.81 1.79 o 0 6 1 228.66 202.52 3.03 o 2 6 1 19.10 23.47 1.91 o 4 6 1 24.39 22.72 2.80 o -5 7 1 134.83 140.24 5.36 o -3 7 1 110.44 113.10 4.41 o -1 7 1 375.77 389.10 5.83 o 1 7 1 128.91 105.41 5.17 o 3 7 1 301.53 309.70 6.35 o 5 7 1 434.68 450.30 15.96 o -4 8 1 53.63 49.13 2.76 o -2 8 1 8.31 11.50 2.55 o 0 8 1 877.43 822.36 13.43 o 2 8 1 54.29 54.09 3.01 o 4 8 1 20.29 11.40 4.12 o -3 9 1 206.62 208.04 6.67 o -1 9 1 0.43 -0.48 1.80 o 1 9 1 277.23 263.09 8.35 o 3 9 1 431.54 472.74 7.73 o -2 10 1 105.03 107.56 5.04 o 0 10 1 0.73 -0.15 2.99 o 2 10 1 77.47 78.83 4.67 o -6 0 2 62.25 62.43 4.77 o -4 0 2 787.44 760.35 11.91 o -2 0 2 2188.52 1946.92 13.44 o 0 0 2 1471.64 1595.30 9.61 o 2 0 2 1.19 0.77 0.96 o 4 0 2 71.65 74.18 4.30 o 6 0 2 157.30 163.07 14.08 o -7 1 2 6.03 4.18 2.13 o -5 1 2 2548.84 2550.96 22.17 o -3 1 2 130.41 131.15 3.52 o -1 1 2 631.95 713.53 4.45 o 3 1 2 32.35 31.02 0.95 o 5 1 2 228.93 222.11 4.93 o 7 1 2 508.89 497.64 8.47 o -6 2 2 340.02 328.42 7.42 o -4 2 2 366.12 369.42 4.28 o -2 2 2 3274.26 3378.90 13.24 o 0 2 2 1835.32 1783.94 5.64 o 2 2 2 9.82 5.35 0.87 o 4 2 2 206.00 192.61 3.91 o 6 2 2 54.58 51.22 4.27 o -7 3 2 115.69 114.18 7.15 o -5 3 2 631.13 636.69 7.39 o -3 3 2 349.45 338.84 4.16 o -1 3 2 68.29 40.77 1.29 o 1 3 2 1715.56 1817.53 6.42 o 3 3 2 91.47 96.06 1.96 o 5 3 2 69.26 60.67 4.02 o -6 4 2 3.74 5.93 1.84 o -4 4 2 73.91 64.09 2.27 o -2 4 2 541.82 514.04 4.98 o 0 4 2 9.95 9.56 1.43 o 2 4 2 71.62 80.38 1.80 o 4 4 2 245.38 247.30 4.43 o 6 4 2 33.37 29.65 5.18 o -5 5 2 367.38 353.17 6.08 o -3 5 2 2.14 0.82 0.87 o -1 5 2 558.04 564.10 4.74 o 1 5 2 264.16 282.64 5.07 o 3 5 2 71.84 75.04 3.70 o 5 5 2 10.83 10.74 6.69 o -6 6 2 2.47 1.58 2.00 o -4 6 2 8.89 7.10 1.28 o -2 6 2 5183.20 4978.97 32.64 o 0 6 2 59.97 56.51 3.02 o 2 6 2 295.19 294.59 7.03 o 4 6 2 1811.98 1884.96 15.88 o -5 7 2 51.97 41.87 4.67 o -3 7 2 649.37 659.36 7.49 o -1 7 2 160.78 157.17 3.84 o 1 7 2 68.11 64.19 3.63 o 3 7 2 237.76 240.08 5.43 o 5 7 2 9.23 8.05 2.99 o -4 8 2 96.91 83.41 3.61 o -2 8 2 43.33 39.42 3.42 o 0 8 2 49.23 40.68 6.58 o 2 8 2 3.07 4.38 1.49 o 4 8 2 18.08 16.67 3.22 o -3 9 2 15.29 8.02 3.50 o -1 9 2 55.06 54.62 4.38 o 1 9 2 54.00 48.59 4.19 o 3 9 2 71.96 70.87 3.64 o -2 10 2 32.82 50.21 4.01 o 0 10 2 7.95 4.22 2.94 o -7 1 3 82.98 81.68 5.30 o -5 1 3 1039.62 1013.68 8.97 o -3 1 3 2722.29 2586.04 15.47 o -1 1 3 865.78 739.26 4.97 o 1 1 3 3804.80 3912.76 14.10 o 3 1 3 3304.74 3328.34 12.76 o 5 1 3 188.75 179.39 4.69 o -6 2 3 84.69 78.50 3.33 o -4 2 3 109.05 102.46 3.10 o -2 2 3 12873.65 12408.80 42.17 o 0 2 3 1674.64 1609.62 15.42 o 2 2 3 173.52 155.67 1.97 o 4 2 3 2997.86 3028.94 19.66 o 6 2 3 188.00 185.63 6.44 o -7 3 3 94.82 105.53 5.55 o -5 3 3 1628.95 1570.40 11.68 o -3 3 3 471.42 479.77 4.94 o -1 3 3 1276.07 1306.54 9.51 o 1 3 3 6206.96 6334.85 21.03 o 3 3 3 334.12 345.33 3.67 o 5 3 3 245.16 263.26 11.59 o -6 4 3 269.96 279.12 6.17 o -4 4 3 265.24 279.72 4.39 o -2 4 3 1121.01 1075.65 8.36 o 0 4 3 3589.74 3435.33 36.62 o 2 4 3 455.31 442.92 4.32 o 4 4 3 305.89 299.50 4.72 o 6 4 3 546.10 570.39 13.41 o -5 5 3 448.76 429.92 5.83 o -3 5 3 53.61 52.13 2.02 o -1 5 3 9.23 10.84 1.09 o 1 5 3 1124.78 1157.06 9.86 o 3 5 3 142.59 134.20 3.40 o 5 5 3 7.83 8.72 4.27 o -6 6 3 271.66 270.50 6.12 o -4 6 3 578.69 567.80 6.49 o -2 6 3 1376.67 1344.96 8.24 o 0 6 3 1799.92 1776.19 15.66 o 2 6 3 852.83 857.02 8.47 o 4 6 3 601.79 634.99 9.56 o -5 7 3 1174.80 1266.96 12.06 o -3 7 3 149.11 150.52 3.74 o -1 7 3 6.42 7.92 1.89 o 1 7 3 2486.43 2411.72 20.02 o 3 7 3 244.93 238.33 7.09 o -4 8 3 268.86 276.28 7.57 o -2 8 3 247.27 246.07 5.04 o 0 8 3 24.16 20.92 4.13 o 2 8 3 461.72 446.14 7.22 o 4 8 3 176.63 175.30 6.17 o -3 9 3 408.22 437.65 9.88 o -1 9 3 388.51 361.54 9.89 o 1 9 3 16.99 21.37 2.50 o 3 9 3 419.69 427.54 12.34 o 0 10 3 59.31 63.74 5.58 o -6 0 4 8.96 10.22 6.93 o -4 0 4 4025.64 3921.86 33.72 o -2 0 4 145.03 173.92 6.53 o 0 0 4 3713.56 4097.58 32.36 o 2 0 4 2556.93 2807.45 18.34 o 4 0 4 21.66 28.06 3.01 o 6 0 4 694.60 701.72 12.79 o -7 1 4 63.97 67.89 5.31 o -5 1 4 799.29 762.37 10.42 o -3 1 4 4.46 4.80 1.96 o -1 1 4 13.39 15.76 1.48 o 1 1 4 2746.60 3031.79 12.16 o 3 1 4 49.86 55.64 1.60 o 5 1 4 0.45 0.60 1.39 o -6 2 4 84.59 81.08 3.90 o -4 2 4 9.18 8.95 1.50 o -2 2 4 177.86 187.31 5.95 o 0 2 4 86.61 79.93 3.28 o 2 2 4 465.96 504.79 3.64 o 4 2 4 89.35 89.33 3.15 o 6 2 4 32.79 31.80 3.30 o -7 3 4 125.78 118.56 7.13 o -5 3 4 20.88 18.34 2.20 o -3 3 4 2.07 1.87 1.03 o -1 3 4 182.26 196.07 2.65 o 1 3 4 48.25 38.95 2.10 o 3 3 4 390.17 403.89 6.34 o 5 3 4 80.25 73.03 4.32 o -6 4 4 65.26 60.59 3.36 o -4 4 4 0.03 2.04 1.19 o -2 4 4 233.11 233.18 3.35 o 0 4 4 342.39 347.04 3.37 o 2 4 4 14.75 8.53 0.92 o 4 4 4 158.87 149.23 15.65 o -5 5 4 75.88 75.71 2.87 o -3 5 4 233.78 219.77 3.81 o -1 5 4 1559.49 1557.69 11.57 o 1 5 4 1.24 3.37 1.98 o 3 5 4 848.77 876.75 13.23 o 5 5 4 205.43 197.47 12.38 o -6 6 4 3.81 3.46 2.08 o -4 6 4 145.65 140.50 3.58 o -2 6 4 1405.29 1385.99 15.72 o 0 6 4 125.53 123.44 3.04 o 2 6 4 15.15 16.96 2.26 o 4 6 4 596.62 603.46 12.82 o -5 7 4 7.80 11.05 1.82 o -3 7 4 124.20 118.48 3.75 o -1 7 4 661.22 669.49 10.85 o 1 7 4 42.26 41.44 2.98 o 3 7 4 43.74 42.75 3.66 o -4 8 4 102.67 102.35 4.82 o -2 8 4 82.91 74.06 3.29 o 0 8 4 32.95 30.79 2.99 o 2 8 4 2.18 3.36 1.33 o -3 9 4 180.12 178.56 7.91 o -1 9 4 0.80 4.05 2.10 o 1 9 4 3.48 2.51 1.57 o -7 1 5 982.35 1059.22 20.40 o -5 1 5 568.71 554.98 8.84 o -3 1 5 25.21 26.12 2.83 o -1 1 5 5851.29 5879.63 34.73 o 1 1 5 1199.54 1203.94 7.03 o 3 1 5 71.98 66.90 2.24 o 5 1 5 246.85 233.16 6.02 o -6 2 5 56.17 55.17 3.88 o -4 2 5 107.16 107.93 3.97 o -2 2 5 279.86 249.77 3.88 o 0 2 5 36.50 31.95 1.92 o 2 2 5 6.27 5.91 0.72 o 4 2 5 65.77 63.02 3.49 o 6 2 5 7.98 7.38 2.13 o -5 3 5 6.67 7.71 2.12 o -3 3 5 357.46 374.48 4.72 o -1 3 5 559.15 610.53 6.80 o 1 3 5 9.36 8.41 1.65 o 3 3 5 100.26 95.23 2.76 o 5 3 5 212.01 210.09 10.70 o -6 4 5 36.88 38.39 2.82 o -4 4 5 3069.51 2973.10 14.07 o -2 4 5 1519.48 1536.77 8.41 o 0 4 5 1.63 1.50 0.78 o 2 4 5 1897.26 1946.64 11.49 o 4 4 5 236.63 236.55 8.09 o -5 5 5 0.83 1.63 1.43 o -3 5 5 36.87 34.97 2.11 o -1 5 5 11.31 8.20 1.82 o 1 5 5 24.06 22.25 2.89 o 3 5 5 35.03 32.48 2.84 o 5 5 5 8.00 10.74 3.48 o -4 6 5 324.89 347.54 5.47 o -2 6 5 151.04 150.29 3.95 o 0 6 5 9.94 7.02 1.98 o 2 6 5 171.39 168.22 4.24 o 4 6 5 0.44 2.75 2.67 o -5 7 5 92.84 87.24 3.77 o -3 7 5 69.09 67.09 3.16 o -1 7 5 326.35 319.37 6.92 o 1 7 5 239.75 246.10 5.98 o 3 7 5 0.23 1.75 1.92 o -4 8 5 464.73 495.60 9.44 o -2 8 5 0.92 1.15 1.92 o 0 8 5 358.88 340.01 7.55 o 2 8 5 415.29 403.35 7.06 o -1 9 5 625.64 650.92 11.45 o 1 9 5 171.90 166.83 8.41 o -6 0 6 0.09 2.65 3.12 o -4 0 6 5878.34 5853.35 45.14 o -2 0 6 2934.91 2888.23 27.55 o 0 0 6 336.73 298.39 8.89 o 2 0 6 5857.02 5976.30 23.92 o 4 0 6 1045.82 1066.68 15.39 o -5 1 6 218.25 238.85 7.79 o -3 1 6 223.29 222.02 6.57 o -1 1 6 2.88 1.71 1.69 o 1 1 6 938.65 940.32 5.83 o 3 1 6 90.12 91.48 3.45 o 5 1 6 1.82 0.47 1.92 o -6 2 6 139.93 145.66 5.45 o -4 2 6 36.25 33.88 6.47 o -2 2 6 1585.46 1516.12 11.74 o 0 2 6 862.44 895.22 8.26 o 2 2 6 61.18 60.10 1.89 o 4 2 6 612.76 634.96 12.63 o -5 3 6 708.58 699.40 8.68 o -3 3 6 460.30 474.33 5.48 o -1 3 6 953.21 944.92 8.99 o 1 3 6 2515.23 2497.59 11.62 o 3 3 6 545.31 538.81 7.60 o 5 3 6 53.81 54.60 5.64 o -6 4 6 2.36 2.53 1.08 o -4 4 6 0.63 2.74 1.24 o -2 4 6 94.26 85.35 2.35 o 0 4 6 13.55 13.05 1.58 o 2 4 6 13.28 16.23 1.98 o 4 4 6 48.60 51.38 5.84 o -5 5 6 339.70 339.25 5.88 o -3 5 6 95.69 100.39 3.18 o -1 5 6 4243.21 4193.66 37.94 o 1 5 6 1037.67 1049.61 10.95 o 3 5 6 114.25 124.74 4.62 o -4 6 6 13.50 15.15 2.15 o -2 6 6 703.38 689.49 17.45 o 0 6 6 211.44 211.90 5.63 o 2 6 6 5.18 4.11 1.32 o 4 6 6 420.03 424.10 11.77 o -3 7 6 449.42 456.45 11.56 o -1 7 6 56.02 52.61 3.75 o 1 7 6 164.83 168.97 5.34 o 3 7 6 393.15 398.60 8.68 o -2 8 6 593.18 607.35 12.74 o 0 8 6 480.32 468.72 8.81 o 2 8 6 271.50 285.84 9.74 o -1 9 6 17.98 16.15 2.77 o -5 1 7 21.22 19.15 4.68 o -3 1 7 201.09 198.27 6.50 o -1 1 7 0.06 2.72 2.27 o 1 1 7 109.46 108.73 4.55 o 3 1 7 25.24 23.96 2.34 o 5 1 7 6.97 7.83 2.96 o -6 2 7 745.43 783.61 11.87 o -4 2 7 431.26 417.28 15.09 o -2 2 7 518.92 506.26 7.40 o 0 2 7 768.82 769.17 19.55 o 2 2 7 175.50 167.40 3.13 o 4 2 7 357.19 341.52 12.13 o -5 3 7 0.05 3.04 1.87 o -3 3 7 517.88 490.82 10.05 o -1 3 7 463.00 467.89 8.88 o 1 3 7 83.52 77.10 2.58 o 3 3 7 118.05 125.21 5.66 o -6 4 7 61.88 59.64 5.42 o -4 4 7 0.40 0.32 1.19 o -2 4 7 4.68 1.67 1.43 o 0 4 7 32.67 33.54 2.95 o 2 4 7 44.74 48.66 3.22 o 4 4 7 46.78 43.17 10.80 o -5 5 7 46.55 45.67 2.67 o -3 5 7 194.18 189.84 4.77 o -1 5 7 96.48 93.31 4.11 o 1 5 7 150.30 156.79 4.84 o 3 5 7 14.00 10.88 5.57 o -4 6 7 59.22 52.18 3.93 o -2 6 7 54.77 50.02 4.20 o 0 6 7 43.12 35.65 3.12 o 2 6 7 0.51 4.56 3.18 o -3 7 7 359.75 393.22 10.71 o -1 7 7 47.45 47.30 3.77 o 1 7 7 474.79 475.11 8.87 o -2 8 7 32.45 32.55 3.50 o 0 8 7 15.76 15.02 3.41 o -6 0 8 134.83 141.02 10.59 o -4 0 8 705.72 715.80 18.11 o -2 0 8 6.09 5.89 5.48 o 0 0 8 72.79 76.89 6.08 o 2 0 8 549.71 560.05 14.38 o 4 0 8 25.90 15.14 3.79 o -5 1 8 89.00 95.35 5.83 o -3 1 8 1619.33 1634.17 17.57 o -1 1 8 283.89 286.65 11.17 o 1 1 8 152.98 155.01 4.07 o 3 1 8 611.85 586.39 11.36 o -6 2 8 214.54 216.53 6.86 o -4 2 8 507.69 489.76 10.93 o -2 2 8 274.67 285.54 7.35 o 0 2 8 287.75 284.91 5.82 o 2 2 8 264.34 252.56 5.47 o 4 2 8 50.49 43.26 6.51 o -5 3 8 52.61 60.23 4.21 o -3 3 8 225.28 231.05 5.40 o -1 3 8 833.57 836.71 12.65 o 1 3 8 78.45 83.02 3.61 o 3 3 8 0.19 2.04 2.01 o -4 4 8 6.51 8.13 2.05 o -2 4 8 33.89 32.17 2.36 o 0 4 8 382.56 382.47 7.42 o 2 4 8 23.91 22.97 2.67 o -3 5 8 117.21 120.30 5.04 o -1 5 8 463.22 450.56 8.42 o 1 5 8 4.26 4.58 1.96 o 3 5 8 3.32 2.43 2.73 o -4 6 8 324.23 328.37 11.15 o -2 6 8 145.90 142.99 5.72 o 0 6 8 1114.87 1138.92 13.54 o 2 6 8 209.65 209.68 6.49 o -3 7 8 120.62 121.92 5.63 o -1 7 8 40.35 40.28 3.82 o 1 7 8 166.73 163.99 5.88 o -5 1 9 7.90 5.82 2.70 o -3 1 9 64.42 64.24 4.90 o -1 1 9 1665.67 1599.29 17.17 o 1 1 9 211.88 202.54 6.96 o 3 1 9 45.87 39.20 3.46 o -4 2 9 279.81 283.23 8.71 o -2 2 9 115.57 110.23 5.35 o 0 2 9 670.94 661.25 11.38 o 2 2 9 256.64 252.12 11.50 o -5 3 9 161.25 185.48 6.50 o -3 3 9 718.51 718.28 11.60 o -1 3 9 41.31 42.22 3.76 o 1 3 9 286.95 289.58 6.55 o 3 3 9 371.96 370.78 15.25 o -4 4 9 738.58 766.27 11.53 o -2 4 9 67.48 69.92 4.35 o 0 4 9 4.82 7.34 2.78 o 2 4 9 840.95 860.31 14.46 o -3 5 9 31.73 26.71 3.40 o -1 5 9 112.60 107.54 5.01 o 1 5 9 8.78 9.49 2.50 o -2 6 9 168.65 167.64 6.37 o 0 6 9 228.56 235.15 7.45 o -4 0 10 157.01 137.63 9.17 o -2 0 10 1137.15 1169.89 22.65 o 0 0 10 449.37 435.71 14.05 o 2 0 10 347.95 339.54 13.34 o -3 1 10 3.83 3.68 1.96 o -1 1 10 19.14 15.85 3.45 o 1 1 10 2.04 4.26 2.47 o -4 2 10 117.39 124.97 6.43 o -2 2 10 47.14 43.99 3.98 o 0 2 10 47.18 44.18 3.84 o 2 2 10 44.88 39.45 6.38 o -3 3 10 333.57 336.25 7.75 o -1 3 10 14.85 9.07 3.32 o 1 3 10 48.03 45.97 7.17 o -2 4 10 16.24 12.89 3.19 o 0 4 10 26.74 23.16 2.77 o -1 5 10 161.37 151.13 8.86 o -3 1 11 482.90 509.21 12.05 o -1 1 11 36.62 38.22 3.72 o 1 1 11 136.02 141.76 6.83 o -2 2 11 46.82 43.86 4.49 o 0 2 11 305.58 321.60 13.44 o -1 3 11 57.41 59.75 5.46 o