#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/44/2214440.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214440_Fobs loop_ _publ_author_name 'Zhou, Hao-Fei' 'Bian, Zu-Qiang' 'Liu, Zhi-Wei' 'Huang, Chun-Hui' 'Zhao, Yong-Liang' _publ_section_title ; Chlorido(\h^6^-p-cymene)[6-(2-hydroxyphenyl)-2,2'-bipyridine]ruthenium(II) chloride chloroform solvate ; _journal_coeditor_code XU2245 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1851 _journal_page_last m1852 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 105.406 _cell_angle_beta 109.022 _cell_angle_gamma 102.663 _cell_length_a 9.2135 _cell_length_b 12.8915 _cell_length_c 13.5267 _exptl_crystal_F_000 680.00 _reflns_d_resolution_high 0.7600 _[local]_cod_data_source_file xu2245Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' _R60705e' _shelx_refln_list_code 4 _shelx_f_calc_maximum 167.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 139.89 194.05 9.55 o 3 0 0 2673.33 2603.13 66.47 o 4 0 0 140.31 186.04 22.71 o 5 0 0 495.13 482.50 47.12 o 6 0 0 1015.84 944.70 63.79 o 7 0 0 1407.10 1401.22 83.27 o 8 0 0 124.48 171.52 66.33 o 9 0 0 306.47 296.24 39.53 o 10 0 0 536.30 451.51 47.17 o -11 1 0 486.80 460.40 58.54 o -10 1 0 3198.32 3218.19 152.98 o -9 1 0 1464.79 1509.85 125.10 o -8 1 0 22.05 33.97 27.93 o -7 1 0 0.45 14.19 32.59 o -6 1 0 115.72 85.58 73.69 o -5 1 0 23.70 19.72 20.14 o -4 1 0 4026.21 4022.05 167.24 o -3 1 0 16272.47 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