#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/44/2214447.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214447_Fobs loop_ _publ_author_name 'Liu, Yen-Hsiang' 'Ding, Miao-Tzu' _publ_section_title ; Poly[[tetraaqua(\m~6~-benzene-1,2,4,5-tetracarboxylato)dicobalt(II)] dihydrate] ; _journal_coeditor_code XU2263 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1828 _journal_page_last m1829 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 90.342 _cell_angle_beta 109.848 _cell_angle_gamma 93.161 _cell_length_a 6.9362 _cell_length_b 7.4559 _cell_length_c 8.2797 _exptl_crystal_F_000 240.00 _reflns_d_resolution_high 0.7575 _[local]_cod_data_source_file xu2263Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' EN007A in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 95.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1168.11 1061.83 28.71 o 2 0 0 5538.39 5174.97 94.41 o 3 0 0 1065.02 1181.37 52.71 o 4 0 0 1345.10 1372.99 50.00 o 5 0 0 20.09 15.55 3.51 o 6 0 0 478.54 503.49 18.90 o 7 0 0 41.12 47.29 5.42 o 8 0 0 45.55 41.86 6.38 o -8 1 0 3.13 7.34 4.62 o -7 1 0 935.55 924.04 19.30 o -6 1 0 71.57 72.64 4.86 o -5 1 0 687.92 679.08 28.63 o -4 1 0 37.48 37.32 3.51 o -3 1 0 5522.27 4935.11 105.10 o -2 1 0 20.59 13.56 2.15 o -1 1 0 2481.74 2118.74 31.18 o 1 1 0 544.26 676.67 49.64 o 2 1 0 796.86 860.41 42.02 o 3 1 0 1447.86 1384.15 57.97 o 4 1 0 439.63 454.84 17.54 o 5 1 0 698.98 681.71 29.50 o 6 1 0 99.65 100.47 5.50 o 7 1 0 129.23 127.43 8.13 o 8 1 0 0.11 1.52 4.31 o -8 2 0 254.62 261.55 12.36 o -7 2 0 5.63 1.52 4.55 o -6 2 0 832.76 837.36 22.73 o -5 2 0 12.71 14.51 3.19 o -4 2 0 1300.11 1193.81 44.50 o -3 2 0 146.89 151.75 7.42 o -2 2 0 2043.31 1869.53 59.49 o 1 2 0 663.58 693.91 17.61 o 2 2 0 415.26 420.00 16.67 o 3 2 0 55.55 51.83 4.07 o 4 2 0 1032.68 1018.30 41.94 o 5 2 0 43.14 42.50 4.62 o 6 2 0 191.95 181.89 6.94 o 7 2 0 11.35 12.12 4.78 o 8 2 0 95.05 90.59 8.61 o -8 3 0 54.65 62.52 6.94 o -7 3 0 23.05 13.16 4.94 o -6 3 0 105.24 109.96 5.26 o -5 3 0 290.95 284.76 10.69 o -4 3 0 370.93 348.55 14.35 o -3 3 0 1575.45 1632.70 55.18 o -2 3 0 443.96 460.67 18.74 o -1 3 0 70.58 60.11 2.99 o 0 3 0 995.27 1162.63 51.11 o 1 3 0 2804.86 3283.44 61.79 o 2 3 0 47.54 58.61 3.83 o 3 3 0 1009.73 1022.52 45.05 o 4 3 0 59.40 67.54 4.78 o 5 3 0 102.07 100.47 5.74 o 6 3 0 4.21 4.70 2.79 o 7 3 0 174.10 178.78 10.05 o 8 3 0 2.75 0.00 5.82 o -8 4 0 135.56 157.65 9.89 o -7 4 0 21.66 25.60 5.58 o -6 4 0 838.37 853.95 17.78 o -5 4 0 56.00 58.61 4.39 o -4 4 0 167.22 181.25 8.53 o -3 4 0 14.72 14.59 3.43 o -2 4 0 576.38 576.85 22.49 o -1 4 0 200.31 242.77 19.46 o 0 4 0 1298.06 1280.00 39.95 o 1 4 0 33.08 42.02 6.58 o 2 4 0 260.83 245.12 11.24 o 3 4 0 138.33 133.17 6.46 o 4 4 0 77.74 91.46 5.42 o 5 4 0 8.80 7.10 3.11 o 6 4 0 398.39 384.35 13.40 o 7 4 0 1.55 6.38 4.62 o -7 5 0 65.08 65.15 6.46 o -6 5 0 25.56 28.31 4.94 o -5 5 0 199.54 209.24 7.42 o -4 5 0 14.71 11.32 3.19 o -3 5 0 521.96 547.66 19.70 o -2 5 0 42.27 45.85 4.62 o 0 5 0 122.23 134.07 8.29 o 1 5 0 397.07 468.39 21.13 o 2 5 0 16.94 11.64 3.91 o 3 5 0 525.64 531.79 24.80 o 4 5 0 17.03 24.80 3.99 o 5 5 0 238.06 234.60 10.13 o 6 5 0 0.66 1.04 4.78 o 7 5 0 138.83 124.95 10.05 o -7 6 0 0.75 3.11 4.94 o -6 6 0 192.38 216.18 10.53 o -5 6 0 9.70 4.78 4.78 o -4 6 0 472.09 486.98 16.83 o -3 6 0 141.71 141.14 7.10 o -2 6 0 617.14 635.46 27.59 o -1 6 0 24.88 21.16 3.18 o 0 6 0 334.63 371.33 10.26 o 1 6 0 101.74 107.55 4.45 o 2 6 0 298.23 313.54 11.72 o 3 6 0 2.24 -3.51 3.59 o 4 6 0 513.02 513.69 14.91 o 5 6 0 5.90 3.99 5.02 o 6 6 0 151.32 158.76 9.57 o -6 7 0 102.29 117.06 9.33 o -5 7 0 298.45 338.82 13.08 o -4 7 0 39.44 30.22 6.22 o -3 7 0 308.93 297.04 14.43 o -2 7 0 0.20 0.80 3.11 o -1 7 0 125.47 122.71 4.88 o 0 7 0 53.47 58.38 3.41 o 1 7 0 668.76 731.97 33.93 o 2 7 0 25.63 25.36 3.83 o 3 7 0 906.17 886.24 19.14 o 4 7 0 54.70 43.70 6.94 o 5 7 0 206.91 194.89 11.48 o -5 8 0 9.74 0.00 5.74 o -4 8 0 139.72 129.26 10.21 o -3 8 0 6.04 10.84 4.31 o -2 8 0 203.33 220.01 11.40 o -1 8 0 14.37 19.06 3.81 o 0 8 0 711.16 742.90 13.36 o 1 8 0 0.38 4.25 3.21 o 2 8 0 113.57 120.57 8.45 o 3 8 0 1.29 2.87 4.70 o 4 8 0 122.44 131.73 9.89 o -3 9 0 352.46 319.44 17.38 o -2 9 0 57.36 54.30 7.89 o -1 9 0 360.78 323.43 11.36 o 0 9 0 3.05 3.53 3.43 o 1 9 0 353.72 383.18 10.31 o 2 9 0 7.09 5.42 4.78 o 3 9 0 193.55 167.06 11.00 o -3 -9 1 65.83 59.57 8.05 o -2 -9 1 0.14 12.12 5.26 o -1 -9 1 288.19 278.36 12.08 o 0 -9 1 21.60 24.22 8.45 o 1 -9 1 105.23 80.71 11.00 o 2 -9 1 2.90 -2.31 5.18 o 3 -9 1 157.37 118.58 13.40 o -4 -8 1 334.93 327.42 13.95 o -3 -8 1 0.27 2.07 4.62 o -2 -8 1 190.57 219.77 10.13 o -1 -8 1 36.65 31.75 4.65 o 0 -8 1 297.98 271.31 19.38 o 1 -8 1 0.49 0.31 3.67 o 2 -8 1 231.50 210.92 13.56 o 3 -8 1 0.64 4.55 4.86 o 4 -8 1 242.08 264.58 14.75 o 5 -8 1 0.02 1.20 5.18 o -5 -7 1 121.93 118.26 9.09 o -4 -7 1 10.64 3.99 5.18 o -3 -7 1 486.68 493.12 14.51 o -2 -7 1 29.56 29.82 4.15 o -1 -7 1 556.57 590.40 18.86 o 0 -7 1 11.11 11.69 2.73 o 1 -7 1 324.13 295.28 11.80 o 2 -7 1 0.68 2.87 3.03 o 3 -7 1 303.34 233.64 14.03 o 4 -7 1 83.97 52.71 8.45 o 5 -7 1 120.31 114.59 9.01 o 6 -7 1 38.17 46.01 7.10 o -6 -6 1 191.50 177.90 11.16 o -5 -6 1 18.27 17.46 5.50 o -4 -6 1 579.18 613.05 16.51 o -3 -6 1 7.41 0.64 3.67 o -2 -6 1 499.78 522.70 21.05 o -1 -6 1 150.45 159.58 11.76 o 0 -6 1 974.72 975.71 39.15 o 1 -6 1 143.44 116.58 7.50 o 3 -6 1 37.28 32.61 4.31 o 4 -6 1 265.13 255.41 8.93 o 5 -6 1 42.30 41.70 5.42 o 6 -6 1 204.99 197.92 10.61 o -7 -5 1 254.92 271.36 12.52 o -6 -5 1 67.83 64.59 6.86 o -5 -5 1 378.99 372.23 13.64 o -4 -5 1 27.17 20.65 3.91 o -3 -5 1 645.04 697.58 27.99 o -2 -5 1 15.12 5.42 3.91 o -1 -5 1 870.77 965.78 29.10 o 0 -5 1 42.74 40.32 3.18 o 4 -5 1 271.44 292.25 10.29 o 5 -5 1 955.83 986.40 20.17 o 6 -5 1 38.68 35.56 5.66 o 7 -5 1 100.30 105.98 8.53 o -7 -4 1 0.05 -0.40 4.07 o -6 -4 1 779.61 794.78 17.62 o -5 -4 1 64.52 69.06 4.86 o -4 -4 1 1232.94 1291.41 36.92 o -3 -4 1 321.19 365.93 14.67 o -2 -4 1 2244.01 2534.50 66.66 o -1 -4 1 179.49 201.60 11.96 o 1 -4 1 71.18 52.85 3.26 o 3 -4 1 1.07 9.49 3.27 o 4 -4 1 5.22 6.94 3.11 o 5 -4 1 454.11 445.28 16.67 o 6 -4 1 92.23 84.84 7.02 o 7 -4 1 23.64 31.58 5.42 o -8 -3 1 0.02 6.78 4.94 o -7 -3 1 426.32 388.90 13.95 o -6 -3 1 35.05 35.48 3.99 o -5 -3 1 325.51 317.85 11.56 o -4 -3 1 13.46 13.56 3.51 o -3 -3 1 499.51 514.89 20.02 o -2 -3 1 804.78 927.23 31.66 o -1 -3 1 859.59 859.21 31.02 o 1 -3 1 12.50 16.77 2.03 o 3 -3 1 651.33 641.04 22.41 o 4 -3 1 23.69 23.28 3.59 o 5 -3 1 351.17 336.43 16.51 o 6 -3 1 15.92 16.51 3.27 o 7 -3 1 190.24 195.76 10.37 o 8 -3 1 1.07 -4.47 5.26 o -8 -2 1 136.85 139.87 9.17 o -7 -2 1 17.72 27.03 4.86 o -6 -2 1 16.19 12.44 3.51 o -5 -2 1 433.70 436.90 15.31 o -4 -2 1 115.12 99.52 5.18 o -3 -2 1 203.22 235.72 11.24 o -2 -2 1 28.58 32.30 3.03 o -1 -2 1 186.03 295.70 8.64 o 0 -2 1 51.32 35.39 2.42 o 2 -2 1 1597.88 1629.19 56.30 o 3 -2 1 0.67 5.66 2.15 o 4 -2 1 533.65 486.42 18.98 o 5 -2 1 213.43 233.40 9.73 o 6 -2 1 753.32 751.96 19.38 o 7 -2 1 19.13 24.00 4.47 o 8 -2 1 151.49 190.50 10.45 o -8 -1 1 74.17 81.97 7.50 o -7 -1 1 70.00 64.43 6.86 o -6 -1 1 0.18 3.59 2.71 o -5 -1 1 629.96 621.34 30.06 o -4 -1 1 332.15 380.76 15.15 o -3 -1 1 1348.24 1268.92 52.71 o -2 -1 1 2633.18 2865.26 69.30 o -1 -1 1 4896.67 5156.53 150.31 o 0 -1 1 57.46 23.12 6.38 o 2 -1 1 2.39 6.86 2.07 o 3 -1 1 2194.85 2057.80 71.13 o 4 -1 1 49.75 48.24 4.23 o 5 -1 1 154.03 162.03 6.70 o 6 -1 1 93.02 95.13 5.26 o 7 -1 1 208.62 183.80 10.05 o 8 -1 1 31.81 26.16 6.46 o -8 0 1 110.71 106.93 8.77 o -7 0 1 0.22 -0.88 2.79 o -6 0 1 435.74 414.26 18.66 o -5 0 1 5.57 6.06 2.71 o -4 0 1 852.80 752.04 26.71 o -3 0 1 41.43 35.96 2.79 o -2 0 1 83.30 111.24 3.91 o -1 0 1 329.84 243.56 6.86 o 0 0 1 5882.77 4973.79 39.15 o 1 0 1 19.13 19.31 5.38 o 2 0 1 1647.77 1561.41 62.60 o 3 0 1 21.97 27.75 3.03 o 4 0 1 1808.92 1811.16 58.29 o 5 0 1 81.75 82.85 5.18 o 6 0 1 709.07 758.74 20.49 o 7 0 1 11.59 17.78 5.18 o 8 0 1 180.68 173.92 10.53 o -8 1 1 2.11 3.83 4.15 o -7 1 1 732.00 693.27 16.75 o -6 1 1 209.19 201.67 8.53 o -5 1 1 312.64 301.74 11.88 o -4 1 1 43.91 49.76 3.59 o -3 1 1 4271.79 3998.47 92.66 o -2 1 1 119.64 131.73 7.26 o -1 1 1 5544.98 5423.00 50.59 o 0 1 1 186.17 174.52 11.24 o 1 1 1 1589.32 1681.05 38.05 o 2 1 1 62.45 74.32 4.55 o 3 1 1 1882.07 1810.05 65.39 o 4 1 1 451.62 444.00 16.98 o 5 1 1 1000.80 937.84 31.82 o 6 1 1 54.37 46.65 4.47 o 7 1 1 346.46 344.16 12.92 o 8 1 1 2.09 2.87 5.50 o -8 2 1 95.44 84.69 7.89 o -7 2 1 9.74 14.03 4.39 o -6 2 1 401.55 338.34 15.63 o -5 2 1 9.05 9.17 3.03 o -4 2 1 2074.42 2028.86 57.97 o -3 2 1 16.17 13.95 2.47 o -2 2 1 3790.48 3491.47 81.10 o -1 2 1 582.69 713.10 24.59 o 0 2 1 4722.31 4800.62 191.86 o 1 2 1 992.30 1209.48 36.84 o 2 2 1 2677.00 3044.04 85.00 o 3 2 1 47.26 38.20 3.75 o 4 2 1 1457.28 1422.27 48.16 o 5 2 1 46.78 40.43 4.39 o 6 2 1 559.31 540.89 15.87 o 7 2 1 14.80 3.19 5.18 o -8 3 1 10.04 16.83 4.94 o -7 3 1 239.04 215.94 10.45 o -6 3 1 39.47 34.21 3.99 o -5 3 1 279.83 267.53 10.45 o -4 3 1 12.16 14.27 3.27 o -3 3 1 1492.55 1372.27 51.99 o -2 3 1 521.90 575.09 20.89 o -1 3 1 1032.23 946.08 26.14 o 0 3 1 34.86 27.74 2.27 o 1 3 1 4363.70 4622.73 74.16 o 2 3 1 11.71 9.97 2.79 o 3 3 1 1598.09 1687.88 54.54 o 4 3 1 49.06 58.53 4.70 o 5 3 1 334.09 330.69 15.71 o 6 3 1 17.03 4.94 5.02 o 7 3 1 39.36 47.29 6.46 o -8 4 1 9.52 18.74 5.10 o -7 4 1 16.99 14.11 4.55 o -6 4 1 872.38 888.00 19.54 o -5 4 1 31.92 32.22 3.67 o -4 4 1 740.30 683.46 29.27 o -3 4 1 168.59 215.14 9.81 o -2 4 1 1402.23 1624.41 54.38 o -1 4 1 3.22 -1.78 2.99 o 0 4 1 2433.27 2724.57 143.14 o 1 4 1 53.56 46.47 2.96 o 2 4 1 1150.20 1224.11 46.01 o 3 4 1 18.88 24.32 4.15 o 4 4 1 164.19 163.39 7.26 o 5 4 1 68.65 66.90 4.70 o 6 4 1 338.79 324.31 12.68 o 7 4 1 12.30 16.11 5.42 o -7 5 1 315.90 343.21 12.76 o -6 5 1 5.45 2.95 4.15 o -5 5 1 412.35 410.19 15.87 o -4 5 1 1.41 -1.52 3.27 o -3 5 1 763.62 743.75 30.78 o -2 5 1 343.29 343.53 14.11 o -1 5 1 1190.15 1322.00 32.56 o 0 5 1 27.12 32.71 2.70 o 1 5 1 10.06 4.27 2.59 o 2 5 1 155.14 173.76 6.78 o 3 5 1 171.32 169.77 7.42 o 4 5 1 112.27 101.51 5.90 o 5 5 1 116.41 123.68 8.13 o 6 5 1 1.24 2.95 5.10 o -7 6 1 3.55 2.23 4.94 o -6 6 1 100.55 125.91 8.05 o -5 6 1 117.77 131.33 7.50 o -4 6 1 288.05 323.35 13.95 o -3 6 1 6.55 12.84 3.27 o -2 6 1 372.27 409.39 20.17 o -1 6 1 42.76 44.73 6.06 o 0 6 1 318.08 320.21 8.71 o 1 6 1 1.16 -5.33 6.58 o 2 6 1 378.71 355.01 17.62 o 3 6 1 1.29 1.20 3.27 o 4 6 1 265.08 277.26 11.48 o 5 6 1 22.78 16.91 5.74 o 6 6 1 102.57 96.73 8.37 o -6 7 1 0.37 1.12 4.94 o -5 7 1 173.41 174.71 9.57 o -4 7 1 36.84 26.71 5.82 o -3 7 1 277.49 303.26 12.76 o -2 7 1 3.17 1.36 3.43 o -1 7 1 110.69 126.26 4.42 o 0 7 1 9.60 9.94 2.59 o 1 7 1 259.04 301.80 9.65 o 2 7 1 1.42 3.35 3.27 o 3 7 1 591.08 574.14 15.63 o 4 7 1 85.24 71.21 7.73 o 5 7 1 181.06 146.80 10.13 o -5 8 1 4.77 -4.94 5.34 o -4 8 1 341.91 401.66 14.11 o -3 8 1 123.21 109.17 8.45 o -2 8 1 270.89 298.63 11.96 o -1 8 1 88.79 85.89 5.59 o 0 8 1 1259.42 1238.41 94.25 o 1 8 1 101.96 101.27 5.58 o 2 8 1 357.45 359.31 13.72 o 3 8 1 54.13 46.89 7.26 o 4 8 1 108.87 96.33 9.25 o -4 9 1 0.71 3.67 5.74 o -3 9 1 252.86 282.04 12.92 o -2 9 1 5.23 7.02 5.34 o -1 9 1 264.33 275.28 9.08 o 0 9 1 16.27 15.25 4.31 o 1 9 1 137.19 130.43 8.77 o 2 9 1 0.55 0.00 5.02 o -3 -9 2 93.26 81.89 9.17 o -2 -9 2 14.64 5.34 5.82 o -1 -9 2 536.02 563.27 13.65 o 0 -9 2 2.10 1.95 3.97 o 1 -9 2 158.40 122.78 16.39 o 2 -9 2 35.98 32.85 7.18 o 3 -9 2 150.14 135.40 14.35 o -4 -8 2 290.63 286.35 13.16 o -3 -8 2 1.72 0.00 4.78 o -2 -8 2 239.45 249.83 11.48 o -1 -8 2 14.83 15.53 5.10 o 0 -8 2 51.17 41.74 9.93 o 1 -8 2 43.08 47.73 7.97 o 2 -8 2 82.70 75.12 9.73 o 3 -8 2 89.78 76.07 9.65 o 4 -8 2 123.76 124.80 11.16 o -6 -7 2 0.94 7.73 4.78 o -5 -7 2 105.59 96.97 8.21 o -4 -7 2 17.44 23.44 5.42 o -3 -7 2 111.19 119.05 8.13 o -2 -7 2 89.99 109.41 5.10 o -1 -7 2 79.18 85.59 4.02 o 0 -7 2 93.18 72.76 4.54 o 1 -7 2 229.07 173.60 9.41 o 2 -7 2 3.14 1.12 3.43 o 4 -7 2 42.86 46.65 7.26 o 5 -7 2 134.27 125.19 11.16 o -6 -6 2 64.24 80.86 8.05 o -5 -6 2 114.07 97.92 7.73 o -4 -6 2 297.70 312.19 12.20 o -3 -6 2 95.34 97.92 5.74 o -2 -6 2 288.66 281.49 10.37 o -1 -6 2 282.85 289.82 19.26 o 0 -6 2 1698.31 1632.86 48.72 o 1 -6 2 13.43 7.81 2.76 o 3 -6 2 110.80 102.87 6.78 o 4 -6 2 473.31 410.43 16.91 o 5 -6 2 23.94 31.66 4.86 o 6 -6 2 214.95 230.45 11.88 o -7 -5 2 401.75 384.59 14.35 o -6 -5 2 1.53 -2.31 5.10 o -5 -5 2 570.65 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