#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/45/2214529.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214529_Fobs loop_ _publ_author_name 'Cao, Yuan' 'Zhang, Jin-Fang' 'Qian, Jun' 'Zhang, Chi' _publ_section_title ; catena-Poly[[tetrakis(hexamethylphosphoramide-\kO)bis(nitrato- \k^2^O,O')ytterbium(III)] [silver(I)-di-\m-sulfido-tungstate(VI)(Ag---W)-di-\m-sulfido]] ; _journal_coeditor_code BR2049 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2076 _journal_page_last m2077 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.798 _cell_angle_gamma 90.000 _cell_length_a 15.7241 _cell_length_b 29.5280 _cell_length_c 11.3464 _exptl_crystal_F_000 2835.24 _reflns_d_resolution_high 0.8300 _[local]_cod_data_source_file br2049Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' _Z673-5 P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 951.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 29871.96 28498.46 632.03 o 4 0 0 904842.31 648526.94 16924.35 o 5 0 0 35666.57 30401.24 609.94 o 6 0 0 202629.03 195770.13 3095.82 o 7 0 0 95731.21 93955.58 1553.19 o 8 0 0 37628.93 38619.25 889.92 o 9 0 0 53826.12 56264.13 829.66 o 10 0 0 259.79 259.78 156.63 o 11 0 0 16278.83 17480.18 447.66 o 12 0 0 36435.99 36922.17 939.80 o 13 0 0 7219.34 6783.45 474.64 o 14 0 0 4323.07 4788.51 665.89 o 15 0 0 20106.91 23036.72 1525.00 o 16 0 0 34824.33 35272.48 2458.57 o 17 0 0 30542.35 32379.94 1954.42 o 18 0 0 9331.07 8814.52 1099.58 o 3 1 0 29765.34 29358.67 434.71 o 4 1 0 138278.78 130475.66 1231.56 o 5 1 0 3888.66 3783.94 148.21 o 6 1 0 120964.44 116997.38 1144.54 o 7 1 0 3425.96 4588.13 117.92 o 8 1 0 216707.00 211948.31 2400.65 o 9 1 0 50049.61 51763.07 8102.79 o 10 1 0 162377.28 158485.36 2339.29 o 11 1 0 40935.76 40876.98 624.55 o 12 1 0 27218.72 26987.84 507.93 o 13 1 0 60739.57 65595.80 1404.38 o 14 1 0 32901.99 35031.87 1016.47 o 15 1 0 41966.93 45101.07 1637.61 o 16 1 0 35.35 913.35 271.94 o 17 1 0 38051.38 38693.17 1599.28 o 18 1 0 11.60 778.73 990.02 o 3 2 0 191642.06 178869.17 2010.45 o 4 2 0 21395.25 21401.72 307.77 o 5 2 0 233829.38 216091.25 2346.88 o 6 2 0 306.07 418.92 89.32 o 7 2 0 313805.69 290577.78 3539.32 o 8 2 0 9109.44 8227.36 199.92 o 9 2 0 212979.63 205885.94 3280.43 o 10 2 0 46131.94 47233.57 690.13 o 11 2 0 73287.52 72422.21 825.92 o 12 2 0 31351.52 31694.28 583.16 o 13 2 0 23031.83 23374.93 1402.11 o 14 2 0 48485.57 50631.50 1424.02 o 15 2 0 3374.08 4969.62 1358.59 o 16 2 0 42016.51 43974.11 2716.26 o 17 2 0 3.48 809.23 248.21 o 18 2 0 23654.86 22890.39 1784.15 o 2 3 0 56146.08 56687.11 767.83 o 3 3 0 301858.78 281362.84 4510.27 o 4 3 0 12474.35 11899.74 243.80 o 5 3 0 180775.13 170358.59 1719.05 o 6 3 0 75329.03 73209.97 720.41 o 7 3 0 42990.53 45406.36 623.27 o 8 3 0 88493.90 83729.21 979.67 o 9 3 0 6646.57 6001.93 239.96 o 10 3 0 10333.55 9996.84 214.81 o 11 3 0 4221.89 4206.15 215.73 o 12 3 0 552.62 691.29 92.73 o 13 3 0 2499.86 2586.46 271.87 o 14 3 0 24120.05 24513.60 720.57 o 15 3 0 9372.88 9455.58 518.04 o 16 3 0 17245.95 19402.74 1103.38 o 17 3 0 17667.77 19793.85 1132.03 o 18 3 0 49736.14 52825.48 2082.91 o 1 4 0 4236.67 4588.59 140.40 o 2 4 0 184523.89 182565.58 2051.12 o 3 4 0 28449.99 29182.98 447.90 o 4 4 0 1034.46 1179.35 104.71 o 5 4 0 56771.06 54673.10 753.31 o 6 4 0 367.57 369.28 77.89 o 7 4 0 65124.82 67787.39 933.82 o 8 4 0 35674.55 38312.14 604.18 o 9 4 0 116789.76 110485.59 1095.73 o 10 4 0 59690.48 60277.51 602.02 o 11 4 0 35527.84 35668.75 550.45 o 12 4 0 27438.40 27513.98 536.33 o 13 4 0 28569.72 28900.00 988.63 o 14 4 0 38262.02 39162.43 1440.04 o 15 4 0 5886.10 5603.47 311.65 o 16 4 0 20346.17 21568.50 1229.96 o 17 4 0 11.19 84.99 201.57 o 18 4 0 12025.42 14220.58 1121.60 o 1 5 0 198286.20 193711.81 4506.99 o 2 5 0 14541.54 15189.32 277.20 o 3 5 0 26443.07 26829.35 400.70 o 4 5 0 72175.88 73096.41 708.84 o 5 5 0 39108.52 39431.58 558.51 o 6 5 0 64931.79 62098.98 1352.96 o 7 5 0 4096.50 3925.46 169.77 o 8 5 0 102100.95 95766.86 1115.81 o 9 5 0 3655.09 3357.57 139.63 o 10 5 0 47571.57 47613.90 684.32 o 11 5 0 65294.06 64645.85 859.54 o 12 5 0 42637.92 41255.34 719.35 o 13 5 0 21851.05 21540.63 584.39 o 14 5 0 10190.96 9532.97 409.52 o 15 5 0 35686.59 36880.65 927.22 o 16 5 0 4147.97 3758.44 380.33 o 17 5 0 12531.68 12356.03 898.24 o 18 5 0 0.51 391.45 229.39 o 1 6 0 19991.36 20484.37 389.60 o 2 6 0 190656.55 193985.48 2434.18 o 3 6 0 5561.98 5769.48 167.38 o 4 6 0 38526.26 37503.59 527.72 o 5 6 0 30173.83 29119.62 419.05 o 6 6 0 108857.12 106424.38 1238.06 o 7 6 0 7097.78 6928.26 167.81 o 8 6 0 23721.35 22721.14 332.46 o 9 6 0 3079.20 3707.80 150.98 o 10 6 0 21024.40 21085.98 372.23 o 11 6 0 2288.36 1884.77 145.80 o 12 6 0 537.65 742.57 152.04 o 13 6 0 10414.67 10001.28 372.94 o 14 6 0 76.25 29.69 124.73 o 15 6 0 8680.13 8792.55 412.80 o 16 6 0 2310.06 1883.59 310.08 o 17 6 0 20902.06 22783.85 1519.93 o 18 6 0 4049.51 3944.02 548.43 o 1 7 0 512.17 770.12 380.30 o 2 7 0 13179.97 15982.56 530.69 o 3 7 0 4830.76 6339.85 158.10 o 4 7 0 28230.17 28307.45 406.54 o 5 7 0 3968.47 3897.48 141.87 o 6 7 0 40635.06 37666.70 523.72 o 7 7 0 1813.60 1896.95 141.06 o 8 7 0 58103.09 60235.59 827.10 o 9 7 0 14931.54 14323.26 271.00 o 10 7 0 30387.80 30588.20 518.91 o 11 7 0 3433.43 3509.12 151.20 o 12 7 0 5448.93 5237.28 212.06 o 13 7 0 11988.04 12641.55 515.77 o 14 7 0 5350.34 5398.21 327.28 o 15 7 0 12819.69 12554.66 551.75 o 16 7 0 441.91 451.07 334.21 o 17 7 0 2374.03 2914.68 407.89 o 18 7 0 118.43 389.47 219.09 o 0 8 0 103.71 707.02 118.92 o 1 8 0 5875.45 6159.87 169.32 o 2 8 0 9667.47 10225.10 219.08 o 3 8 0 10049.42 9806.79 200.50 o 4 8 0 4524.31 4828.54 161.91 o 5 8 0 21820.56 21620.07 355.43 o 6 8 0 5798.65 5782.02 137.86 o 7 8 0 36440.74 36961.74 510.51 o 8 8 0 4702.18 4987.60 187.71 o 9 8 0 10430.08 10682.73 230.61 o 10 8 0 20481.94 18745.51 373.06 o 11 8 0 8556.08 8712.96 224.22 o 12 8 0 12076.07 11281.29 357.90 o 13 8 0 9892.47 9934.21 400.27 o 14 8 0 13196.26 12973.94 383.08 o 15 8 0 3544.63 3530.73 344.75 o 16 8 0 6788.62 5993.02 494.11 o 17 8 0 3151.46 2467.79 434.63 o 18 8 0 400.52 86.97 215.70 o 1 9 0 15563.67 15990.78 283.06 o 2 9 0 10.55 130.84 50.06 o 3 9 0 50661.16 52068.18 724.95 o 4 9 0 19859.49 20778.68 319.56 o 5 9 0 45264.92 45872.64 629.63 o 6 9 0 843.03 1204.39 82.09 o 7 9 0 33917.31 36165.24 542.49 o 8 9 0 39879.31 41500.35 599.89 o 9 9 0 7998.89 8259.13 192.17 o 10 9 0 5310.66 5346.04 201.81 o 11 9 0 9629.64 8871.93 300.90 o 12 9 0 2058.19 2337.18 221.93 o 13 9 0 321.78 227.86 175.24 o 14 9 0 6476.57 6237.76 266.90 o 15 9 0 2689.76 2213.63 236.22 o 16 9 0 6082.15 6227.68 483.15 o 17 9 0 0.06 -147.71 488.14 o 18 9 0 7809.75 6711.62 649.56 o 0 10 0 41548.11 43442.20 889.43 o 1 10 0 316.68 444.61 91.30 o 2 10 0 232.96 398.99 55.59 o 3 10 0 24575.41 25714.08 405.36 o 4 10 0 200.31 237.15 50.62 o 5 10 0 7328.46 7428.99 177.42 o 6 10 0 15686.23 17676.81 327.84 o 7 10 0 11316.68 11416.53 244.97 o 8 10 0 709.10 753.03 116.74 o 9 10 0 8465.23 8536.02 197.88 o 10 10 0 18226.66 19388.38 387.24 o 11 10 0 2945.25 3107.09 171.11 o 12 10 0 1801.29 1698.55 214.56 o 13 10 0 10330.58 9893.57 349.36 o 14 10 0 7521.29 7179.47 294.02 o 15 10 0 1806.86 2224.13 346.04 o 16 10 0 707.36 587.89 155.51 o 17 10 0 969.53 1417.51 339.24 o 18 10 0 117.04 195.20 530.71 o 1 11 0 9665.18 9714.36 340.60 o 2 11 0 779.22 1041.71 132.23 o 3 11 0 2812.14 2830.03 153.89 o 4 11 0 13332.54 13165.15 334.15 o 5 11 0 2360.57 2498.36 130.73 o 6 11 0 21386.46 22771.46 344.15 o 7 11 0 3464.31 3459.78 140.11 o 8 11 0 74.79 193.17 69.60 o 9 11 0 3307.75 3323.63 158.13 o 10 11 0 2480.96 2056.47 180.45 o 11 11 0 1623.71 1674.30 135.82 o 12 11 0 10009.33 9936.86 346.04 o 13 11 0 5065.38 4998.94 297.02 o 14 11 0 2700.61 2697.41 172.20 o 15 11 0 1053.19 771.62 138.87 o 16 11 0 3273.64 3497.51 392.28 o 17 11 0 691.03 969.08 309.74 o 18 11 0 3109.21 3490.14 615.39 o 0 12 0 29898.69 28026.08 692.82 o 1 12 0 10482.69 6476.84 409.67 o 2 12 0 20673.01 21181.84 391.58 o 3 12 0 3750.34 3176.88 181.19 o 4 12 0 87654.45 94338.80 1188.87 o 5 12 0 1592.09 1843.73 118.08 o 6 12 0 48146.52 49918.58 697.57 o 7 12 0 31253.54 32591.26 486.49 o 8 12 0 27737.93 27442.13 499.65 o 9 12 0 39534.18 39114.42 653.38 o 10 12 0 46389.03 47684.84 713.02 o 11 12 0 11116.65 10895.23 343.54 o 12 12 0 3671.72 3540.99 234.95 o 13 12 0 22528.26 23645.17 587.12 o 14 12 0 3336.89 3797.76 258.93 o 15 12 0 10916.22 11250.39 472.98 o 16 12 0 10255.33 9993.83 600.45 o 17 12 0 12988.07 13455.65 1059.96 o 1 13 0 32936.59 37080.32 737.62 o 2 13 0 2500.41 2642.08 275.34 o 3 13 0 7180.85 7345.72 214.70 o 4 13 0 19982.60 22135.19 358.32 o 5 13 0 10567.82 10448.45 218.48 o 6 13 0 813.68 1058.04 95.63 o 7 13 0 7599.16 7128.67 186.31 o 8 13 0 4816.26 5125.83 171.66 o 9 13 0 3713.90 3576.17 246.43 o 10 13 0 125.77 387.47 97.50 o 11 13 0 4437.57 4485.57 256.05 o 12 13 0 1777.79 1953.87 227.81 o 13 13 0 135.24 343.83 111.96 o 14 13 0 6695.80 6607.65 281.11 o 15 13 0 3254.81 3301.45 276.25 o 16 13 0 2520.16 2202.27 327.55 o 17 13 0 4801.53 5933.90 648.42 o 0 14 0 46247.92 46292.16 909.04 o 1 14 0 1790.34 2288.20 198.54 o 2 14 0 38371.52 41079.59 1456.48 o 3 14 0 14250.37 14534.79 397.84 o 4 14 0 16959.39 17606.34 344.78 o 5 14 0 656.65 757.34 77.34 o 6 14 0 13916.78 14623.12 304.14 o 7 14 0 1656.43 1635.33 113.54 o 8 14 0 21704.97 22799.36 443.12 o 9 14 0 7697.46 7129.46 260.69 o 10 14 0 1587.94 1662.24 135.79 o 11 14 0 738.92 969.40 84.56 o 12 14 0 3948.59 3690.98 265.53 o 13 14 0 3997.79 3755.14 230.29 o 14 14 0 1072.53 1146.16 159.62 o 15 14 0 4974.79 5789.99 536.94 o 16 14 0 256.51 397.58 187.79 o 17 14 0 6315.83 6523.67 569.44 o 1 15 0 20574.10 22609.88 490.95 o 2 15 0 410.84 556.38 252.30 o 3 15 0 35930.19 35330.02 631.06 o 4 15 0 1055.19 1587.97 134.45 o 5 15 0 34125.30 36388.32 575.94 o 6 15 0 7549.25 7674.23 281.05 o 7 15 0 24309.27 24802.60 438.20 o 8 15 0 47857.24 47938.99 632.18 o 9 15 0 21991.93 22265.33 536.20 o 10 15 0 30081.98 31874.73 804.64 o 11 15 0 11317.05 11737.69 408.20 o 12 15 0 24108.51 25197.42 550.97 o 13 15 0 4431.22 4614.99 264.83 o 14 15 0 20336.33 20917.83 621.34 o 15 15 0 10149.35 10043.86 584.34 o 16 15 0 14000.89 13938.96 963.43 o 17 15 0 9373.12 10474.32 843.65 o 0 16 0 134220.06 132942.61 4340.40 o 1 16 0 6003.49 5922.28 368.74 o 2 16 0 43106.49 43226.54 661.82 o 3 16 0 4838.56 5117.18 313.72 o 4 16 0 24106.45 24724.72 438.73 o 5 16 0 1194.58 1334.60 216.73 o 6 16 0 11050.40 11281.04 289.10 o 7 16 0 431.85 357.29 103.84 o 8 16 0 31.62 253.62 62.28 o 9 16 0 659.95 604.36 140.44 o 10 16 0 567.91 639.13 142.38 o 11 16 0 775.09 472.57 97.91 o 12 16 0 737.95 790.61 126.94 o 13 16 0 6144.46 6252.16 480.79 o 14 16 0 468.65 510.20 109.92 o 15 16 0 574.33 540.08 128.73 o 16 16 0 1284.11 1342.84 508.50 o 1 17 0 61725.71 65222.11 1122.63 o 2 17 0 257.64 317.62 156.53 o 3 17 0 38108.35 38731.90 666.44 o 4 17 0 4132.23 4667.27 294.14 o 5 17 0 14876.75 15052.98 359.37 o 6 17 0 253.34 228.91 58.43 o 7 17 0 15721.98 15758.30 324.74 o 8 17 0 9456.76 9305.53 268.20 o 9 17 0 1180.79 948.73 92.97 o 10 17 0 77.81 487.15 113.95 o 11 17 0 503.53 467.75 92.91 o 12 17 0 317.54 342.33 89.91 o 13 17 0 138.44 320.41 117.02 o 14 17 0 2024.30 2060.67 253.81 o 15 17 0 4785.95 4476.92 383.43 o 16 17 0 2748.03 2402.13 335.99 o 0 18 0 11617.86 13018.61 366.79 o 1 18 0 260.12 1169.89 327.27 o 2 18 0 4174.00 4462.97 236.55 o 3 18 0 8272.78 9181.99 360.99 o 4 18 0 16017.14 16960.62 564.08 o 5 18 0 44117.63 44257.67 699.75 o 6 18 0 7838.46 7643.47 221.68 o 7 18 0 54807.42 55081.97 802.44 o 8 18 0 11087.28 11411.49 397.65 o 9 18 0 44223.70 44499.68 872.70 o 10 18 0 17646.70 18071.23 502.51 o 11 18 0 30595.89 31513.09 577.55 o 12 18 0 10145.28 10692.32 377.41 o 13 18 0 24436.15 25079.34 815.55 o 14 18 0 17323.93 17586.40 703.64 o 15 18 0 12808.87 13943.33 718.71 o 16 18 0 15299.95 15550.09 873.94 o 1 19 0 66807.02 72846.88 827.43 o 2 19 0 18542.94 19715.65 924.51 o 3 19 0 27635.59 28540.12 602.17 o 4 19 0 8689.77 8231.74 308.24 o 5 19 0 24421.71 25990.05 514.88 o 6 19 0 39412.83 40156.25 614.33 o 7 19 0 1659.47 1545.86 174.02 o 8 19 0 18788.42 19113.23 427.27 o 9 19 0 695.57 773.32 91.99 o 10 19 0 14989.29 13962.62 538.58 o 11 19 0 1741.56 1503.15 206.61 o 12 19 0 834.06 867.49 130.68 o 13 19 0 4131.39 3639.83 324.89 o 14 19 0 687.28 817.91 185.60 o 15 19 0 4189.63 4647.53 467.49 o 16 19 0 4190.57 4813.90 467.11 o 0 20 0 92176.23 96747.97 1844.42 o 1 20 0 247.05 949.71 229.63 o 2 20 0 99279.45 103868.27 2360.34 o 3 20 0 14372.82 14320.01 419.91 o 4 20 0 71312.13 73718.53 979.34 o 5 20 0 3280.14 3262.67 278.84 o 6 20 0 13033.35 12146.68 922.74 o 7 20 0 9238.65 9336.95 254.95 o 8 20 0 5543.11 5510.33 263.44 o 9 20 0 8340.79 8985.56 368.00 o 10 20 0 235.03 407.94 189.07 o 11 20 0 685.03 611.72 120.68 o 12 20 0 3526.58 3158.91 309.31 o 13 20 0 477.76 879.02 195.27 o 14 20 0 7473.69 8477.54 1326.97 o 15 20 0 2342.87 2198.89 359.37 o 1 21 0 3080.13 3522.89 166.24 o 2 21 0 7434.15 8026.95 416.50 o 3 21 0 5591.92 5835.95 660.01 o 4 21 0 31970.08 31460.60 1307.34 o 5 21 0 750.40 700.93 103.30 o 6 21 0 68923.05 69331.00 1135.85 o 7 21 0 4840.36 4222.48 257.16 o 8 21 0 31139.44 30655.68 556.48 o 9 21 0 42472.07 42514.77 821.08 o 10 21 0 55977.87 56541.20 1355.75 o 11 21 0 34841.49 35953.33 919.88 o 12 21 0 26750.35 25955.57 874.86 o 13 21 0 43772.86 47175.94 1291.57 o 14 21 0 25880.58 27563.47 867.78 o 15 21 0 27975.37 28705.55 1129.40 o 0 22 0 90472.29 88428.24 1913.65 o 1 22 0 2804.19 3623.47 241.15 o 2 22 0 46084.90 43647.84 1740.14 o 3 22 0 16804.01 17916.46 687.45 o 4 22 0 46744.35 46410.64 878.70 o 5 22 0 25092.15 23612.32 523.83 o 6 22 0 17466.65 16640.99 523.35 o 7 22 0 34030.10 32427.63 711.90 o 8 22 0 54.53 228.76 94.22 o 9 22 0 10020.89 9938.71 636.03 o 10 22 0 296.96 704.67 145.51 o 11 22 0 5938.57 6212.61 445.76 o 12 22 0 10687.88 11296.21 637.70 o 13 22 0 27.87 -9.35 505.22 o 14 22 0 9169.34 8850.55 634.39 o 1 23 0 69096.18 69936.61 1641.61 o 2 23 0 2177.08 2615.25 230.65 o 3 23 0 78820.59 78366.14 1683.30 o 4 23 0 53999.24 51558.67 1027.06 o 5 23 0 30569.42 29444.09 941.88 o 6 23 0 25143.29 24348.11 566.15 o 7 23 0 20620.36 22808.67 769.57 o 8 23 0 28752.21 26243.51 625.64 o 9 23 0 1454.02 1345.87 270.37 o 10 23 0 8354.27 8240.23 609.03 o 11 23 0 67.57 93.88 263.37 o 12 23 0 2251.19 1690.68 396.95 o 13 23 0 6389.35 5428.60 526.48 o 14 23 0 170.18 269.96 152.70 o 0 24 0 4945.58 4882.73 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