#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/60/2216093.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216093_Fobs loop_ _publ_author_name 'Sun, Yi-Feng' 'Wang, Xin-Li' 'Li, Ji-Kun' 'Cheng, Xue-Li' 'Wu, Ren-Tao' _publ_section_title ; 4-Hydroxy-3,5-dimethoxybenzaldehyde isonicotinoylhydrazone monohydrate ; _journal_coeditor_code PV2036 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4467 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.653 _cell_angle_gamma 90.000 _cell_length_a 9.0139 _cell_length_b 21.6630 _cell_length_c 7.8198 _exptl_crystal_F_000 672.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file pv2036Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 243.70 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 17.60 20.24 0.65 o 2 0 0 1189.77 1056.60 21.12 o 3 0 0 2011.21 1992.47 39.53 o 4 0 0 1212.49 1220.04 17.71 o 5 0 0 635.48 679.49 9.28 o 6 0 0 445.71 430.85 6.38 o 7 0 0 446.16 496.09 7.39 o 8 0 0 0.75 -0.31 0.72 o 9 0 0 7.70 7.49 1.25 o 1 1 0 961.50 980.68 11.33 o 2 1 0 1835.14 1708.91 45.88 o 3 1 0 2419.88 2296.74 28.84 o 4 1 0 470.64 461.03 5.84 o 5 1 0 60.87 46.36 0.96 o 6 1 0 165.44 145.27 2.06 o 7 1 0 362.82 347.59 4.14 o 8 1 0 12.74 11.04 0.83 o 9 1 0 0.00 -0.74 0.50 o 10 1 0 6.08 6.63 1.96 o 0 2 0 16.57 19.43 0.88 o 1 2 0 1854.50 1983.70 22.94 o 2 2 0 16.81 23.27 0.86 o 3 2 0 3659.99 3473.17 63.15 o 4 2 0 270.90 237.14 2.85 o 5 2 0 21.92 18.67 0.91 o 6 2 0 6.79 5.03 0.42 o 7 2 0 71.40 83.86 1.46 o 8 2 0 50.97 41.61 1.23 o 9 2 0 40.03 35.56 2.11 o 10 2 0 0.02 -0.06 1.25 o 1 3 0 11160.46 14318.37 442.49 o 2 3 0 59.30 74.96 1.30 o 3 3 0 69.25 72.72 1.25 o 4 3 0 0.13 -0.09 0.20 o 5 3 0 133.30 148.53 1.98 o 6 3 0 55.41 52.13 1.03 o 7 3 0 0.66 1.10 0.40 o 8 3 0 13.71 16.83 0.87 o 9 3 0 0.60 1.45 0.94 o 10 3 0 0.03 -0.55 1.07 o 0 4 0 1710.31 1303.82 85.83 o 1 4 0 37.18 26.66 0.57 o 2 4 0 13527.10 16560.65 326.26 o 3 4 0 213.82 210.27 2.66 o 4 4 0 607.21 631.19 6.76 o 5 4 0 156.30 157.67 2.08 o 6 4 0 2.14 1.07 0.32 o 7 4 0 82.12 76.40 1.57 o 8 4 0 41.89 45.67 1.39 o 9 4 0 1.71 0.22 0.80 o 10 4 0 4.39 4.89 1.41 o 1 5 0 42.47 39.42 0.82 o 2 5 0 363.85 408.51 5.05 o 3 5 0 468.57 521.74 5.97 o 4 5 0 3.39 2.70 0.32 o 5 5 0 314.30 313.04 3.57 o 6 5 0 57.57 65.26 1.26 o 7 5 0 55.24 66.37 1.46 o 8 5 0 3.24 2.64 0.75 o 9 5 0 145.17 141.19 3.32 o 10 5 0 10.39 12.93 1.79 o 0 6 0 2500.56 2484.03 41.09 o 1 6 0 1527.35 1419.23 16.49 o 2 6 0 689.04 699.20 7.76 o 3 6 0 8.28 8.01 0.39 o 4 6 0 1009.26 1039.91 10.82 o 5 6 0 313.82 316.43 3.62 o 6 6 0 57.02 53.62 1.14 o 7 6 0 36.14 35.28 1.09 o 8 6 0 19.86 21.64 1.30 o 9 6 0 2.24 5.34 1.02 o 10 6 0 57.67 58.30 4.01 o 1 7 0 88.60 86.00 1.40 o 2 7 0 247.35 221.16 2.62 o 3 7 0 795.05 822.33 8.60 o 4 7 0 386.26 346.40 4.03 o 5 7 0 661.90 694.24 7.16 o 6 7 0 16.54 25.24 0.88 o 7 7 0 75.36 66.28 1.78 o 8 7 0 24.75 22.44 1.51 o 9 7 0 26.15 27.95 1.58 o 10 7 0 2.80 3.12 1.64 o 0 8 0 767.61 703.19 12.00 o 1 8 0 959.59 978.29 10.76 o 2 8 0 1196.02 1163.48 11.93 o 3 8 0 90.78 92.10 1.41 o 4 8 0 82.13 93.93 1.55 o 5 8 0 34.68 30.84 0.99 o 6 8 0 101.12 104.08 2.02 o 7 8 0 33.87 34.83 1.71 o 8 8 0 81.86 83.28 2.42 o 9 8 0 21.97 26.22 1.58 o 10 8 0 58.72 57.39 2.61 o 1 9 0 56.64 44.61 0.91 o 2 9 0 230.10 243.26 2.92 o 3 9 0 144.73 134.77 1.90 o 4 9 0 6.44 6.80 0.44 o 5 9 0 212.65 201.22 2.59 o 6 9 0 14.23 8.38 0.77 o 7 9 0 315.29 298.10 5.18 o 8 9 0 39.24 37.21 1.70 o 9 9 0 9.55 9.36 1.21 o 10 9 0 1.41 -0.69 0.95 o 0 10 0 19.47 19.45 0.81 o 1 10 0 1091.30 1253.61 14.91 o 2 10 0 161.66 165.63 2.08 o 3 10 0 241.25 258.66 3.01 o 4 10 0 16.35 15.04 0.60 o 5 10 0 165.74 182.25 2.84 o 6 10 0 60.08 60.05 1.71 o 7 10 0 270.05 285.19 5.07 o 8 10 0 7.93 7.75 1.08 o 9 10 0 9.00 8.51 1.21 o 1 11 0 204.17 198.33 2.95 o 2 11 0 269.89 278.17 3.72 o 3 11 0 6.46 9.90 0.49 o 4 11 0 340.60 333.67 3.82 o 5 11 0 81.03 84.20 1.77 o 6 11 0 440.99 443.21 6.93 o 7 11 0 66.06 67.66 2.15 o 8 11 0 6.47 4.96 0.99 o 9 11 0 1.52 2.19 0.99 o 0 12 0 39.39 38.79 1.21 o 1 12 0 119.97 132.67 2.25 o 2 12 0 17.25 15.02 0.59 o 3 12 0 95.33 85.64 1.33 o 4 12 0 295.08 270.89 3.28 o 5 12 0 14.92 15.41 0.93 o 6 12 0 413.82 420.31 6.71 o 7 12 0 0.71 1.49 0.77 o 8 12 0 7.40 7.40 1.10 o 9 12 0 1.86 -0.73 0.88 o 1 13 0 1021.21 1029.53 12.58 o 2 13 0 15.61 17.76 0.62 o 3 13 0 211.50 230.25 2.70 o 4 13 0 320.63 303.36 3.86 o 5 13 0 299.18 304.08 4.65 o 6 13 0 640.78 652.92 9.72 o 7 13 0 90.22 94.76 3.12 o 8 13 0 11.00 11.04 1.26 o 9 13 0 0.47 -0.60 0.90 o 0 14 0 225.80 226.13 3.74 o 1 14 0 616.46 672.30 8.58 o 2 14 0 40.03 44.86 0.96 o 3 14 0 370.03 381.75 4.11 o 4 14 0 446.05 430.52 5.59 o 5 14 0 416.84 410.54 8.71 o 6 14 0 253.40 277.87 5.03 o 7 14 0 39.16 38.80 1.78 o 8 14 0 27.98 23.00 1.75 o 1 15 0 151.38 159.83 2.73 o 2 15 0 561.70 589.17 5.95 o 3 15 0 96.27 98.03 1.76 o 4 15 0 72.16 68.80 1.79 o 5 15 0 102.82 111.02 2.73 o 6 15 0 13.90 12.38 1.17 o 7 15 0 78.42 78.09 2.81 o 8 15 0 4.45 4.41 1.08 o 0 16 0 127.86 146.48 3.39 o 1 16 0 1.31 0.11 0.32 o 2 16 0 0.31 0.46 0.39 o 3 16 0 0.82 -0.49 0.44 o 4 16 0 303.24 291.58 7.44 o 5 16 0 9.49 10.63 1.06 o 6 16 0 5.74 2.37 1.04 o 7 16 0 0.05 -1.01 0.82 o 8 16 0 17.71 13.50 1.48 o 1 17 0 14.06 11.78 0.60 o 2 17 0 14.82 14.76 0.73 o 3 17 0 33.58 34.46 1.24 o 4 17 0 264.48 262.59 4.73 o 5 17 0 0.98 0.25 0.76 o 6 17 0 3.92 4.29 0.98 o 7 17 0 1.59 2.39 1.00 o 8 17 0 3.34 5.00 1.23 o 0 18 0 0.11 -0.41 0.54 o 1 18 0 14.72 13.25 0.67 o 2 18 0 13.17 14.87 0.77 o 3 18 0 131.97 131.69 2.69 o 4 18 0 143.74 139.23 3.14 o 5 18 0 78.77 80.52 2.38 o 6 18 0 17.03 14.36 1.31 o 7 18 0 0.39 -0.02 0.87 o 1 19 0 36.03 34.27 1.53 o 2 19 0 19.74 19.13 0.85 o 3 19 0 13.71 15.25 1.19 o 4 19 0 96.79 95.08 2.59 o 5 19 0 1.69 0.63 0.75 o 6 19 0 7.02 5.58 1.04 o 7 19 0 24.84 18.45 1.58 o 0 20 0 131.29 143.42 3.06 o 1 20 0 4.78 4.73 0.60 o 2 20 0 0.83 0.99 0.51 o 3 20 0 17.12 15.47 1.23 o 4 20 0 11.59 8.09 1.73 o 5 20 0 4.75 2.67 0.99 o 6 20 0 0.23 -0.62 0.82 o 1 21 0 45.85 47.75 1.29 o 2 21 0 8.48 7.78 1.02 o 3 21 0 2.55 1.72 0.81 o 4 21 0 11.25 9.32 1.11 o 5 21 0 10.27 6.38 1.09 o 6 21 0 0.04 -0.33 0.86 o 0 22 0 15.16 12.20 1.86 o 1 22 0 36.46 39.98 1.40 o 2 22 0 0.01 0.88 0.75 o 3 22 0 4.62 2.81 0.88 o 4 22 0 0.14 0.37 0.80 o 5 22 0 2.75 1.44 0.87 o 1 23 0 0.53 0.72 0.60 o 2 23 0 0.05 1.02 1.20 o 3 23 0 1.04 2.22 0.92 o 4 23 0 4.44 6.70 1.12 o 0 24 0 136.03 150.12 3.76 o 1 24 0 6.69 6.44 1.13 o 2 24 0 6.49 6.02 1.13 o 3 24 0 0.28 0.44 0.86 o 1 25 0 33.24 33.71 2.37 o 2 25 0 0.26 -0.36 0.90 o -10 1 1 2.03 1.01 1.20 o -9 1 1 6.27 4.26 1.18 o -8 1 1 13.90 15.36 1.39 o -7 1 1 44.17 38.43 1.19 o -6 1 1 209.29 195.97 2.52 o -5 1 1 327.67 328.30 3.90 o -4 1 1 482.05 495.32 5.80 o -3 1 1 953.75 1005.05 12.89 o -2 1 1 1488.48 1581.28 19.91 o -1 1 1 179.11 159.32 2.29 o 0 1 1 7959.04 6521.48 243.86 o 1 1 1 876.55 872.19 10.23 o 2 1 1 505.50 475.82 6.34 o 3 1 1 52.89 34.65 0.81 o 4 1 1 2.67 3.92 0.34 o 5 1 1 202.57 217.38 2.53 o 6 1 1 284.25 298.45 3.37 o 7 1 1 69.10 68.73 1.32 o 8 1 1 0.89 1.72 0.52 o 9 1 1 2.31 0.10 0.81 o 10 1 1 8.44 8.89 1.98 o -10 2 1 4.48 1.69 1.47 o -9 2 1 13.86 8.73 1.11 o -8 2 1 4.30 6.76 0.85 o -7 2 1 4.39 4.39 0.53 o -6 2 1 26.65 30.93 0.95 o -5 2 1 3.89 5.22 0.43 o -4 2 1 1763.16 1670.23 24.06 o -3 2 1 410.37 334.20 3.94 o -2 2 1 8148.96 7545.62 198.88 o -1 2 1 1.48 6.43 0.66 o 0 2 1 24.75 11.90 0.32 o 1 2 1 743.39 635.62 8.33 o 2 2 1 166.18 173.81 2.36 o 3 2 1 1340.77 1364.68 15.99 o 4 2 1 41.46 45.51 0.88 o 5 2 1 2169.60 2219.29 20.13 o 6 2 1 5.35 5.22 0.43 o 7 2 1 60.99 56.66 1.19 o 8 2 1 9.49 12.76 0.80 o 9 2 1 54.17 63.44 2.26 o 10 2 1 35.09 35.42 3.50 o -10 3 1 4.35 3.35 1.28 o -9 3 1 10.42 13.35 1.34 o -8 3 1 7.98 4.51 0.79 o -7 3 1 303.89 316.97 4.11 o -6 3 1 107.31 114.00 1.73 o -5 3 1 28.43 29.39 0.79 o -4 3 1 122.55 120.90 1.59 o -3 3 1 77.29 74.03 1.15 o -2 3 1 59388.34 44097.36 2169.15 o -1 3 1 24.85 19.23 0.75 o 0 3 1 1580.85 1463.91 37.39 o 1 3 1 3421.81 3206.55 143.59 o 2 3 1 7906.58 8599.13 119.37 o 3 3 1 133.63 171.70 2.47 o 4 3 1 1474.19 1498.94 14.44 o 5 3 1 890.82 958.53 9.58 o 6 3 1 8.67 8.10 0.50 o 7 3 1 23.13 18.69 1.02 o 8 3 1 56.40 65.94 1.80 o 9 3 1 97.55 111.26 2.54 o 10 3 1 23.00 21.16 2.79 o -10 4 1 0.08 -0.81 1.15 o -9 4 1 55.57 52.16 3.17 o -8 4 1 80.69 74.79 1.87 o -7 4 1 124.86 134.46 2.84 o -6 4 1 40.87 43.99 1.08 o -5 4 1 323.56 305.85 3.48 o -4 4 1 33.83 26.43 0.62 o -3 4 1 755.28 764.75 8.50 o -2 4 1 14210.97 13792.51 221.26 o -1 4 1 935.93 851.87 13.93 o 0 4 1 2.41 1.15 0.16 o 1 4 1 439.84 418.07 5.11 o 2 4 1 336.24 355.57 4.48 o 3 4 1 2319.69 2275.21 22.81 o 4 4 1 223.57 196.87 2.54 o 5 4 1 32.21 29.31 0.85 o 6 4 1 170.16 179.35 2.43 o 7 4 1 27.29 28.79 1.08 o 8 4 1 7.16 8.66 0.95 o 9 4 1 24.04 24.15 1.44 o 10 4 1 3.74 7.18 2.17 o -10 5 1 0.00 1.79 1.30 o -9 5 1 3.34 3.26 1.11 o -8 5 1 6.58 9.61 0.88 o -7 5 1 30.98 31.86 1.16 o -6 5 1 13.43 16.47 0.71 o -5 5 1 1006.16 1006.39 10.01 o -4 5 1 432.07 393.61 4.19 o -3 5 1 750.09 768.52 8.00 o -2 5 1 37.42 45.07 1.08 o -1 5 1 3535.54 3630.79 45.58 o 0 5 1 91.01 70.34 1.12 o 1 5 1 2.38 4.32 0.27 o 2 5 1 310.48 284.74 3.71 o 3 5 1 200.07 211.93 2.59 o 4 5 1 268.96 291.55 3.49 o 5 5 1 155.25 154.28 2.39 o 6 5 1 1.63 0.39 0.33 o 7 5 1 97.76 84.87 1.70 o 8 5 1 73.03 66.43 1.88 o 9 5 1 78.08 74.99 2.36 o 10 5 1 69.08 79.29 4.04 o -10 6 1 39.59 34.57 2.53 o -9 6 1 87.37 95.13 4.59 o -8 6 1 47.91 55.24 1.64 o -7 6 1 29.45 21.73 1.21 o -6 6 1 0.62 0.16 0.40 o -5 6 1 7.08 6.46 0.44 o -4 6 1 90.60 82.34 1.25 o -3 6 1 1237.50 1189.89 11.51 o -2 6 1 91.52 74.62 1.19 o -1 6 1 2570.63 2452.20 40.22 o 0 6 1 795.63 755.35 9.87 o 1 6 1 0.70 0.53 0.18 o 2 6 1 56.81 59.52 0.97 o 3 6 1 1289.59 1417.35 14.46 o 4 6 1 28.81 22.32 0.67 o 5 6 1 145.13 162.78 2.20 o 6 6 1 242.97 242.28 3.07 o 7 6 1 18.58 17.02 0.88 o 8 6 1 87.49 89.84 2.18 o 9 6 1 18.25 17.80 1.36 o 10 6 1 7.51 8.64 1.39 o -10 7 1 15.84 12.20 1.88 o -9 7 1 212.73 217.53 4.44 o -8 7 1 26.85 29.83 1.30 o -7 7 1 4.69 3.63 0.70 o -6 7 1 153.35 162.12 2.69 o -5 7 1 8.56 10.38 0.56 o -4 7 1 1526.90 1553.11 15.00 o -3 7 1 1465.30 1559.65 14.96 o -2 7 1 804.86 859.53 8.89 o -1 7 1 4.05 5.14 0.30 o 0 7 1 31.13 28.17 1.15 o 1 7 1 719.53 668.54 7.52 o 2 7 1 13.85 12.53 0.46 o 3 7 1 1.21 3.31 0.31 o 4 7 1 161.88 166.06 2.16 o 5 7 1 55.29 57.35 1.15 o 6 7 1 12.83 12.90 0.70 o 7 7 1 15.78 17.34 0.98 o 8 7 1 44.58 46.99 3.39 o 9 7 1 48.59 52.72 2.37 o 10 7 1 0.23 -0.10 0.92 o -10 8 1 4.79 3.10 1.44 o -9 8 1 0.19 0.19 0.96 o -8 8 1 36.95 39.85 1.60 o -7 8 1 42.26 50.92 1.52 o -6 8 1 30.22 27.25 1.27 o -5 8 1 215.33 222.49 3.26 o -4 8 1 411.38 389.80 4.24 o -3 8 1 3.43 2.78 0.33 o -2 8 1 307.59 326.38 3.50 o -1 8 1 758.15 766.55 8.03 o 0 8 1 3736.11 3846.48 44.09 o 1 8 1 233.16 235.63 2.64 o 2 8 1 322.80 334.66 3.61 o 3 8 1 210.89 210.64 2.52 o 4 8 1 900.94 963.61 9.62 o 5 8 1 3.78 1.88 0.38 o 6 8 1 48.40 59.96 1.45 o 7 8 1 62.26 63.32 1.74 o 8 8 1 7.57 7.13 0.97 o 9 8 1 4.31 3.38 0.94 o 10 8 1 18.78 17.38 1.77 o -10 9 1 9.66 8.75 1.77 o -9 9 1 4.60 3.72 1.01 o -8 9 1 154.93 157.49 3.52 o -7 9 1 112.24 115.93 2.39 o -6 9 1 14.08 11.66 0.81 o -5 9 1 10.24 11.09 0.78 o -4 9 1 150.61 166.43 2.14 o -3 9 1 4.08 1.24 0.28 o -2 9 1 2.90 3.76 0.31 o -1 9 1 174.91 153.15 1.90 o 0 9 1 241.32 234.24 3.06 o 1 9 1 513.84 516.53 5.30 o 2 9 1 31.78 25.25 0.80 o 3 9 1 15.91 12.97 0.55 o 4 9 1 705.58 707.61 7.28 o 5 9 1 33.62 25.27 0.94 o 6 9 1 177.78 190.76 3.02 o 7 9 1 18.94 15.43 1.13 o 8 9 1 18.07 15.94 1.28 o 9 9 1 0.04 -0.77 0.83 o -9 10 1 22.99 25.84 1.65 o -8 10 1 365.51 378.82 6.50 o -7 10 1 211.04 233.95 3.98 o -6 10 1 641.98 621.83 7.78 o -5 10 1 466.68 466.05 5.96 o -4 10 1 1.39 2.41 0.47 o -3 10 1 640.76 624.83 6.42 o -2 10 1 22.54 15.28 0.80 o -1 10 1 680.96 769.18 7.70 o 0 10 1 115.09 113.67 1.79 o 1 10 1 952.56 974.12 9.59 o 2 10 1 27.55 23.70 0.68 o 3 10 1 207.33 191.70 2.41 o 4 10 1 0.36 0.47 0.34 o 5 10 1 88.70 82.56 1.59 o 6 10 1 91.57 91.65 2.09 o 7 10 1 29.22 31.34 1.75 o 8 10 1 24.83 30.84 1.99 o 9 10 1 31.30 33.16 2.13 o -9 11 1 5.59 4.66 1.11 o -8 11 1 13.29 15.85 1.32 o -7 11 1 129.14 130.99 2.84 o -6 11 1 219.72 211.89 3.42 o -5 11 1 87.05 79.58 1.75 o -4 11 1 44.44 50.86 1.31 o -3 11 1 1.56 0.78 0.29 o -2 11 1 123.89 106.07 1.56 o -1 11 1 4808.86 5212.20 71.28 o 0 11 1 20.98 23.37 0.73 o 1 11 1 268.80 251.02 2.93 o 2 11 1 11.60 12.87 0.59 o 3 11 1 255.58 230.95 2.82 o 4 11 1 0.09 0.07 0.33 o 5 11 1 30.33 29.20 0.98 o 6 11 1 389.69 376.07 6.12 o 7 11 1 90.70 93.36 2.52 o 8 11 1 1.90 2.19 0.87 o 9 11 1 0.41 0.71 0.93 o -9 12 1 0.36 -1.34 0.89 o -8 12 1 6.98 5.51 1.07 o -7 12 1 19.50 21.02 1.36 o -6 12 1 0.08 0.04 0.62 o -5 12 1 77.55 74.57 1.72 o -4 12 1 6.83 7.17 0.64 o -3 12 1 151.35 140.01 2.09 o -2 12 1 37.87 34.71 0.78 o -1 12 1 599.83 667.03 6.79 o 0 12 1 762.68 750.32 17.94 o 1 12 1 225.74 229.14 2.62 o 2 12 1 263.28 272.46 3.28 o 3 12 1 0.21 0.11 0.39 o 4 12 1 60.02 53.03 1.24 o 5 12 1 21.10 22.57 0.99 o 6 12 1 6.95 5.23 0.91 o 7 12 1 55.99 51.34 2.13 o 8 12 1 2.81 2.36 0.90 o 9 12 1 19.91 22.65 1.66 o -9 13 1 3.94 1.92 1.05 o -8 13 1 2.44 0.82 0.92 o -7 13 1 2.43 1.40 0.81 o -6 13 1 152.05 148.04 2.78 o -5 13 1 5.24 5.05 1.00 o -4 13 1 25.26 18.73 1.02 o -3 13 1 125.02 147.95 2.36 o -2 13 1 115.35 150.32 1.93 o -1 13 1 459.01 517.18 5.20 o 0 13 1 17.61 24.56 0.99 o 1 13 1 117.00 135.87 1.91 o 2 13 1 273.97 245.59 2.98 o 3 13 1 121.45 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