#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:43:21 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181086 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/66/2216658.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216658_Fobs loop_ _publ_author_name 'Weil, Matthias' _publ_section_title ; The high-temperature \b modification of iron(II) sulfate ; _journal_coeditor_code MG2037 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i192 _journal_volume 63 _journal_year 2007 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.7042 _cell_length_b 6.8013 _cell_length_c 4.7868 _exptl_crystal_F_000 296.00 _reflns_d_resolution_high 0.5533 _cod_data_source_file mg2037Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' beta-FeSO4 in Pnma; Habituskorrigiert' _shelx_refln_list_code 4 _shelx_f_calc_maximum 125.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 9619.18 9383.07 31.60 o 8 0 0 2232.98 2169.81 29.98 o 10 0 0 982.24 956.64 8.06 o 12 0 0 732.42 719.52 11.51 o 14 0 0 82.77 90.42 3.34 o 2 1 0 4199.84 4097.74 35.71 o 4 1 0 670.59 585.40 10.70 o 6 1 0 2.41 14.55 3.54 o 8 1 0 6.57 12.03 0.49 o 10 1 0 122.98 126.86 2.55 o 12 1 0 414.90 411.62 4.13 o 14 1 0 66.75 72.55 2.05 o 0 2 0 342.54 360.04 2.25 o 2 2 0 13375.21 12738.43 349.77 o 4 2 0 7477.83 7358.72 111.51 o 6 2 0 333.31 300.25 2.74 o 8 2 0 4170.94 4036.92 22.13 o 10 2 0 1077.92 1054.43 7.46 o 12 2 0 112.45 113.88 2.40 o 14 2 0 1018.72 1042.35 7.23 o 4 3 0 539.46 533.40 2.82 o 6 3 0 748.98 710.19 4.39 o 8 3 0 2.32 6.51 1.35 o 10 3 0 681.39 676.43 8.60 o 12 3 0 354.55 355.16 4.10 o 14 3 0 0.01 -0.95 1.12 o 0 4 0 15723.58 15092.27 253.31 o 2 4 0 1366.10 1355.86 11.56 o 4 4 0 967.52 995.05 9.55 o 6 4 0 5921.25 5903.50 38.54 o 8 4 0 430.42 412.18 3.91 o 10 4 0 723.27 712.39 9.07 o 12 4 0 1093.35 1087.06 15.42 o 14 4 0 73.54 75.26 1.69 o 2 5 0 1741.33 1728.81 10.31 o 4 5 0 429.15 424.69 5.34 o 6 5 0 9.67 9.36 0.44 o 8 5 0 20.51 20.28 0.76 o 10 5 0 31.40 31.90 0.94 o 12 5 0 282.66 291.78 5.83 o 14 5 0 69.28 75.04 1.48 o 0 6 0 255.94 266.69 7.44 o 2 6 0 4086.96 4193.97 59.41 o 4 6 0 5466.73 5485.65 57.47 o 6 6 0 90.06 87.70 1.53 o 8 6 0 980.72 955.59 18.74 o 10 6 0 640.41 630.00 10.19 o 12 6 0 342.90 351.00 4.68 o 2 7 0 316.68 313.67 3.67 o 4 7 0 301.44 302.36 3.47 o 6 7 0 38.51 42.66 0.77 o 8 7 0 0.35 2.76 1.83 o 10 7 0 154.79 156.32 4.63 o 12 7 0 196.39 201.34 5.09 o 0 8 0 3049.87 3117.52 19.24 o 2 8 0 316.51 322.89 6.94 o 4 8 0 646.44 657.59 8.27 o 6 8 0 2144.51 2128.52 26.50 o 8 8 0 51.20 50.60 1.26 o 10 8 0 393.01 389.15 7.45 o 2 9 0 46.29 50.40 2.12 o 4 9 0 171.43 172.58 3.89 o 6 9 0 155.42 155.85 2.37 o 8 9 0 9.75 9.99 0.88 o 10 9 0 153.39 151.03 3.30 o 0 10 0 11.29 9.51 1.44 o 2 10 0 1217.32 1245.47 26.38 o 4 10 0 1230.75 1226.47 28.88 o 6 10 0 23.20 24.97 0.95 o 8 10 0 558.85 553.52 10.94 o 2 11 0 285.57 280.44 5.83 o 4 11 0 111.61 111.01 2.31 o 6 11 0 8.57 10.86 1.29 o 0 12 0 1558.65 1543.77 25.99 o 2 12 0 105.01 119.14 5.65 o 1 0 1 4420.42 4509.75 84.79 o 2 0 1 332.31 344.00 3.73 o 3 0 1 13303.58 11595.38 259.20 o 4 0 1 39.76 40.74 0.62 o 5 0 1 2172.72 1995.17 56.92 o 6 0 1 33.93 34.56 0.70 o 7 0 1 2690.29 2472.81 15.90 o 8 0 1 1.16 2.01 0.54 o 9 0 1 2279.16 2253.21 22.28 o 10 0 1 0.01 -0.59 0.74 o 11 0 1 86.14 86.18 1.47 o 12 0 1 0.59 0.13 0.77 o 13 0 1 1312.15 1323.30 10.16 o 14 0 1 12.33 10.82 0.82 o 15 0 1 482.86 490.92 5.11 o 0 1 1 34.46 35.03 0.47 o 1 1 1 5290.76 5194.90 83.19 o 2 1 1 48.54 50.23 0.47 o 3 1 1 3.68 8.67 0.52 o 4 1 1 0.12 1.58 0.32 o 5 1 1 1559.93 1518.62 8.47 o 6 1 1 55.82 54.65 0.59 o 7 1 1 859.27 804.25 6.90 o 8 1 1 26.59 25.34 0.41 o 9 1 1 54.03 49.59 0.53 o 10 1 1 3.35 4.29 0.41 o 11 1 1 80.27 83.77 1.25 o 12 1 1 9.66 10.12 0.49 o 13 1 1 153.79 153.16 1.85 o 14 1 1 0.27 0.00 0.84 o 15 1 1 61.73 63.74 0.88 o 1 2 1 5664.02 5498.27 71.12 o 2 2 1 1712.35 1861.38 13.17 o 3 2 1 3798.97 3834.00 70.32 o 4 2 1 8.23 6.22 0.28 o 5 2 1 8208.88 7993.87 79.83 o 6 2 1 681.23 657.27 2.93 o 7 2 1 1054.41 1034.95 7.05 o 8 2 1 1.51 1.70 0.39 o 9 2 1 327.11 312.84 2.33 o 10 2 1 178.27 179.09 1.90 o 11 2 1 2767.23 2793.12 14.09 o 12 2 1 12.20 11.17 0.52 o 13 2 1 166.58 166.95 1.78 o 14 2 1 42.38 42.95 0.77 o 15 2 1 106.83 118.00 2.76 o 0 3 1 1576.09 1760.41 7.84 o 1 3 1 1205.78 1228.14 10.28 o 2 3 1 18.78 20.02 0.21 o 3 3 1 213.64 228.33 2.04 o 4 3 1 1034.39 1054.27 9.85 o 5 3 1 456.10 442.87 4.87 o 6 3 1 38.01 36.21 0.42 o 7 3 1 1316.00 1286.39 4.50 o 8 3 1 436.87 425.75 2.70 o 9 3 1 152.35 141.28 1.58 o 10 3 1 0.64 0.98 0.61 o 11 3 1 151.31 148.80 1.59 o 12 3 1 153.65 155.04 1.65 o 13 3 1 250.39 256.28 3.20 o 14 3 1 0.79 1.85 0.74 o 15 3 1 15.56 17.44 0.93 o 1 4 1 3469.41 3537.35 25.58 o 2 4 1 298.35 340.92 1.49 o 3 4 1 5299.94 5241.67 23.08 o 4 4 1 21.80 21.47 0.27 o 5 4 1 589.21 573.14 3.87 o 6 4 1 176.14 166.84 1.51 o 7 4 1 2254.55 2212.07 14.50 o 8 4 1 0.60 1.15 0.83 o 9 4 1 2107.00 2060.55 11.86 o 10 4 1 99.55 97.58 1.09 o 11 4 1 22.36 21.87 0.79 o 12 4 1 0.70 1.57 0.72 o 13 4 1 863.11 873.82 5.42 o 14 4 1 7.54 9.03 0.63 o 0 5 1 105.13 100.56 1.32 o 1 5 1 1698.20 1730.03 10.21 o 2 5 1 21.39 20.44 0.47 o 3 5 1 2.26 4.47 0.73 o 4 5 1 36.78 34.38 0.39 o 5 5 1 885.46 874.89 8.51 o 6 5 1 32.84 30.31 0.50 o 7 5 1 450.73 434.74 3.13 o 8 5 1 0.59 0.56 0.56 o 9 5 1 28.95 34.16 1.70 o 10 5 1 5.45 5.91 0.91 o 11 5 1 51.27 58.77 2.05 o 12 5 1 0.09 -0.06 1.04 o 13 5 1 72.33 73.50 0.95 o 14 5 1 0.02 0.23 1.03 o 1 6 1 3147.44 3205.61 16.46 o 2 6 1 39.89 39.10 0.43 o 3 6 1 414.26 422.72 2.70 o 4 6 1 7.95 6.05 0.28 o 5 6 1 2590.45 2604.52 17.06 o 6 6 1 0.57 0.77 0.53 o 7 6 1 846.47 804.21 5.43 o 8 6 1 2.51 3.11 0.47 o 9 6 1 317.93 303.13 4.54 o 10 6 1 0.29 0.54 1.02 o 11 6 1 1364.54 1354.42 7.95 o 12 6 1 4.67 5.87 0.72 o 13 6 1 57.17 55.75 0.94 o 0 7 1 2.63 4.41 0.70 o 1 7 1 681.44 700.12 7.40 o 2 7 1 4.09 4.42 0.47 o 3 7 1 8.86 11.38 0.34 o 4 7 1 23.24 25.49 0.55 o 5 7 1 310.27 303.01 3.43 o 6 7 1 14.93 15.36 0.43 o 7 7 1 468.47 466.74 4.41 o 8 7 1 37.11 37.54 0.75 o 9 7 1 35.10 36.14 1.12 o 10 7 1 0.00 0.50 0.85 o 11 7 1 35.63 34.46 0.85 o 12 7 1 20.34 21.76 0.80 o 1 8 1 960.06 965.44 8.73 o 2 8 1 174.83 179.84 2.48 o 3 8 1 1617.69 1633.05 14.76 o 4 8 1 5.40 6.25 0.45 o 5 8 1 102.03 101.20 2.23 o 6 8 1 166.28 163.80 1.98 o 7 8 1 1043.42 1023.80 6.14 o 8 8 1 0.22 1.61 0.66 o 9 8 1 1079.11 1044.05 10.24 o 10 8 1 113.40 113.92 2.34 o 11 8 1 5.80 8.47 0.87 o 0 9 1 63.96 63.61 1.12 o 1 9 1 291.61 297.24 3.36 o 2 9 1 7.07 7.65 0.42 o 3 9 1 32.51 33.97 0.55 o 4 9 1 71.36 71.76 0.78 o 5 9 1 169.46 172.26 1.73 o 6 9 1 8.94 8.99 0.60 o 7 9 1 307.46 310.80 2.89 o 8 9 1 97.74 96.30 1.06 o 9 9 1 54.39 55.29 1.26 o 10 9 1 1.88 0.39 1.15 o 1 10 1 805.42 835.02 5.78 o 2 10 1 1.14 1.35 0.55 o 3 10 1 134.47 142.00 1.54 o 4 10 1 4.55 5.43 0.75 o 5 10 1 997.24 993.84 7.42 o 6 10 1 11.66 12.65 0.61 o 7 10 1 283.65 280.05 3.04 o 8 10 1 2.71 4.60 0.78 o 0 11 1 35.14 36.32 1.00 o 1 11 1 303.18 313.99 3.69 o 2 11 1 1.58 2.28 0.64 o 3 11 1 1.28 1.38 0.77 o 4 11 1 10.06 10.07 0.60 o 5 11 1 158.38 157.98 1.65 o 6 11 1 9.63 11.84 0.72 o 1 12 1 194.80 208.64 3.75 o 2 12 1 0.93 1.87 0.82 o 0 0 2 9683.55 9343.69 352.04 o 1 0 2 2212.70 2403.37 10.82 o 2 0 2 1923.62 1989.34 21.78 o 3 0 2 589.80 636.38 6.20 o 4 0 2 5069.05 5177.33 76.08 o 5 0 2 715.08 692.65 4.60 o 6 0 2 7128.21 7064.77 189.87 o 7 0 2 1.29 2.04 0.58 o 8 0 2 44.04 51.65 0.80 o 9 0 2 72.38 71.98 1.10 o 10 0 2 820.62 812.38 5.63 o 11 0 2 22.79 21.31 0.74 o 12 0 2 1951.17 1983.38 9.79 o 13 0 2 0.06 -1.13 1.77 o 14 0 2 88.97 91.14 1.75 o 15 0 2 15.92 19.92 0.97 o 1 1 2 219.94 235.35 1.43 o 3 1 2 238.09 245.26 1.69 o 4 1 2 591.56 571.41 2.85 o 5 1 2 1.15 4.18 0.88 o 6 1 2 981.42 952.70 4.59 o 7 1 2 7.67 9.73 0.48 o 8 1 2 24.12 29.81 1.57 o 9 1 2 0.64 0.22 0.54 o 10 1 2 718.30 701.60 3.73 o 11 1 2 12.29 13.23 0.50 o 12 1 2 277.24 285.56 2.61 o 13 1 2 37.33 38.36 0.71 o 14 1 2 5.75 7.59 0.79 o 15 1 2 0.26 2.28 0.84 o 0 2 2 639.90 663.97 8.61 o 1 2 2 13.73 12.53 0.40 o 2 2 2 8912.66 8816.77 105.85 o 3 2 2 113.58 125.15 0.95 o 4 2 2 4821.57 4808.15 62.42 o 5 2 2 15.91 17.65 0.30 o 6 2 2 183.83 184.72 1.57 o 7 2 2 144.91 137.01 1.34 o 8 2 2 3520.51 3493.73 21.89 o 9 2 2 56.80 54.01 0.62 o 10 2 2 1080.94 1056.40 8.29 o 11 2 2 49.58 46.79 0.67 o 12 2 2 95.18 102.59 2.63 o 13 2 2 19.85 22.00 0.65 o 14 2 2 748.48 754.79 4.47 o 15 2 2 2.25 0.70 0.96 o 1 3 2 233.14 252.07 2.95 o 2 3 2 130.50 129.94 1.34 o 3 3 2 69.96 83.55 1.41 o 4 3 2 570.05 556.12 2.45 o 5 3 2 261.62 250.29 1.70 o 6 3 2 253.93 241.34 1.83 o 7 3 2 122.91 120.48 1.22 o 8 3 2 25.45 26.87 0.95 o 9 3 2 90.52 90.67 0.98 o 10 3 2 380.50 377.85 2.89 o 11 3 2 109.33 107.50 1.16 o 12 3 2 199.46 198.88 2.01 o 13 3 2 0.09 0.10 0.87 o 14 3 2 4.29 4.44 0.69 o 0 4 2 7738.29 7658.26 63.42 o 1 4 2 125.64 115.61 0.99 o 2 4 2 1019.44 1004.39 6.24 o 3 4 2 1.14 2.73 0.66 o 4 4 2 1690.54 1706.40 13.11 o 5 4 2 46.35 37.20 0.43 o 6 4 2 4744.54 4846.30 30.51 o 7 4 2 102.21 100.74 1.08 o 8 4 2 132.46 129.71 1.35 o 9 4 2 0.28 2.40 0.76 o 10 4 2 590.95 579.15 3.69 o 11 4 2 4.44 4.24 0.57 o 12 4 2 1237.76 1260.19 5.83 o 13 4 2 19.19 18.59 0.69 o 14 4 2 87.19 89.82 1.03 o 1 5 2 182.05 167.09 1.82 o 2 5 2 6.24 8.70 0.75 o 3 5 2 194.45 176.99 1.38 o 4 5 2 363.17 367.70 3.01 o 5 5 2 3.62 3.78 0.29 o 6 5 2 606.29 604.05 3.78 o 7 5 2 31.42 30.45 0.55 o 8 5 2 19.98 19.79 0.51 o 9 5 2 6.73 7.48 0.49 o 10 5 2 499.03 491.27 4.40 o 11 5 2 1.08 0.86 0.63 o 12 5 2 224.81 236.28 2.40 o 13 5 2 35.38 36.41 0.80 o 0 6 2 570.99 567.47 9.22 o 1 6 2 353.61 335.52 3.04 o 2 6 2 3268.35 3350.94 21.29 o 3 6 2 62.82 54.72 0.76 o 4 6 2 1219.41 1194.91 8.09 o 5 6 2 235.41 232.96 2.03 o 6 6 2 74.66 70.31 0.75 o 7 6 2 1.50 1.56 0.74 o 8 6 2 2518.71 2503.90 14.16 o 9 6 2 6.81 7.84 0.54 o 10 6 2 599.23 585.06 4.35 o 11 6 2 1.06 0.19 1.03 o 12 6 2 17.89 17.04 0.73 o 13 6 2 3.42 2.76 0.89 o 1 7 2 1.21 0.51 0.62 o 2 7 2 19.30 22.36 0.63 o 3 7 2 25.09 23.54 0.65 o 4 7 2 306.11 311.00 2.21 o 5 7 2 7.82 8.45 0.52 o 6 7 2 221.80 221.03 2.50 o 7 7 2 6.74 8.22 0.48 o 8 7 2 10.11 11.51 0.55 o 9 7 2 4.45 4.26 0.70 o 10 7 2 321.81 320.74 4.66 o 11 7 2 18.71 20.39 0.76 o 12 7 2 102.03 102.65 1.20 o 0 8 2 2893.28 2977.66 37.51 o 1 8 2 2.25 3.00 0.57 o 2 8 2 256.45 257.18 2.78 o 3 8 2 28.07 28.26 0.49 o 4 8 2 416.81 421.51 4.91 o 5 8 2 0.23 -0.67 0.71 o 6 8 2 1965.88 1949.08 14.73 o 7 8 2 98.94 99.88 1.36 o 8 8 2 97.24 95.57 1.62 o 9 8 2 17.31 17.25 0.70 o 10 8 2 274.46 269.18 4.11 o 11 8 2 13.14 12.79 0.78 o 1 9 2 2.97 2.64 0.52 o 2 9 2 65.95 68.52 1.22 o 3 9 2 1.43 1.71 0.53 o 4 9 2 152.95 156.72 2.03 o 5 9 2 59.67 60.32 0.89 o 6 9 2 92.57 90.42 1.13 o 7 9 2 11.03 10.68 0.61 o 8 9 2 13.79 16.22 1.08 o 9 9 2 16.61 15.52 0.72 o 10 9 2 100.83 99.14 1.71 o 0 10 2 77.22 82.54 2.20 o 1 10 2 53.01 53.17 0.70 o 2 10 2 1031.89 1047.49 6.56 o 3 10 2 0.93 1.88 0.68 o 4 10 2 545.29 561.64 5.76 o 5 10 2 45.14 46.71 0.89 o 6 10 2 33.19 35.29 1.00 o 7 10 2 4.89 5.83 0.82 o 8 10 2 865.84 831.86 9.27 o 1 11 2 22.91 23.52 0.72 o 2 11 2 0.07 2.57 0.85 o 3 11 2 59.66 60.61 0.85 o 4 11 2 91.95 92.78 1.02 o 5 11 2 6.00 4.54 0.75 o 6 11 2 114.85 111.41 1.84 o 1 0 3 5007.34 5299.91 62.12 o 2 0 3 333.19 345.81 2.76 o 3 0 3 3588.21 3709.58 20.64 o 4 0 3 80.13 91.11 1.27 o 5 0 3 293.40 302.67 2.49 o 6 0 3 13.48 14.62 0.46 o 7 0 3 2800.56 2831.87 21.57 o 8 0 3 10.76 9.81 0.60 o 9 0 3 2441.49 2404.36 17.98 o 10 0 3 23.40 20.74 0.77 o 11 0 3 6.27 6.88 0.72 o 12 0 3 54.83 58.86 1.40 o 13 0 3 648.08 671.32 5.96 o 14 0 3 44.29 43.87 1.15 o 0 1 3 1289.21 1353.46 18.03 o 1 1 3 972.88 989.15 5.86 o 2 1 3 111.14 118.82 1.19 o 3 1 3 55.35 62.77 0.77 o 4 1 3 349.55 352.56 1.77 o 5 1 3 439.55 418.91 2.63 o 6 1 3 158.71 154.12 1.44 o 7 1 3 725.29 697.16 5.51 o 8 1 3 3.25 4.08 0.62 o 9 1 3 93.45 88.92 2.03 o 10 1 3 0.02 0.79 0.54 o 11 1 3 85.02 87.73 0.97 o 12 1 3 1.97 1.78 0.59 o 13 1 3 142.69 142.57 1.66 o 14 1 3 24.54 25.50 0.73 o 1 2 3 5990.11 6186.30 73.02 o 2 2 3 225.75 240.73 1.64 o 3 2 3 461.97 484.29 2.87 o 4 2 3 45.85 42.19 0.67 o 5 2 3 2972.22 3029.41 27.74 o 6 2 3 8.10 10.03 0.32 o 7 2 3 1584.80 1574.40 11.84 o 8 2 3 5.20 5.84 0.39 o 9 2 3 536.79 536.62 3.32 o 10 2 3 3.93 5.36 0.65 o 11 2 3 1343.29 1348.09 8.32 o 12 2 3 102.23 100.70 1.09 o 13 2 3 65.62 65.86 1.34 o 14 2 3 3.08 3.71 0.89 o 0 3 3 846.66 862.75 7.24 o 1 3 3 2460.61 2551.67 31.15 o 2 3 3 76.22 77.80 0.79 o 3 3 3 160.78 153.65 1.95 o 4 3 3 172.21 160.24 1.66 o 5 3 3 1203.46 1163.91 4.82 o 6 3 3 181.74 174.43 1.73 o 7 3 3 182.38 180.73 3.80 o 8 3 3 5.43 5.73 0.42 o 9 3 3 2.82 9.80 1.61 o 10 3 3 0.38 0.19 0.62 o 11 3 3 0.52 1.64 0.77 o 12 3 3 6.15 6.16 0.63 o 13 3 3 29.99 31.07 0.81 o 14 3 3 11.78 12.56 1.20 o 1 4 3 1235.01 1227.19 14.98 o 2 4 3 162.21 148.54 2.42 o 3 4 3 4192.26 4311.07 41.30 o 4 4 3 78.49 80.18 0.87 o 5 4 3 637.23 609.47 6.94 o 6 4 3 2.62 3.17 0.35 o 7 4 3 1155.50 1127.22 5.19 o 8 4 3 2.94 3.68 0.49 o 9 4 3 1223.97 1202.81 6.96 o 10 4 3 23.29 24.37 1.22 o 11 4 3 64.17 65.47 0.82 o 12 4 3 32.86 34.26 0.77 o 13 4 3 780.83 793.73 4.84 o 0 5 3 545.39 520.36 4.48 o 1 5 3 360.17 366.53 2.94 o 2 5 3 76.54 75.24 0.92 o 3 5 3 87.04 97.73 2.24 o 4 5 3 201.59 190.25 2.06 o 5 5 3 172.15 168.18 2.39 o 6 5 3 83.35 77.90 1.09 o 7 5 3 545.08 534.30 3.82 o 8 5 3 3.19 2.32 0.84 o 9 5 3 125.36 129.27 2.10 o 10 5 3 0.19 -0.04 0.99 o 11 5 3 90.52 93.80 1.31 o 12 5 3 0.10 -0.99 0.99 o 13 5 3 127.84 130.73 1.72 o 1 6 3 1233.39 1232.21 6.78 o 2 6 3 132.67 127.15 1.62 o 3 6 3 661.54 655.52 4.36 o 4 6 3 26.21 20.98 0.52 o 5 6 3 2583.84 2595.32 16.71 o 6 6 3 1.88 3.79 0.42 o 7 6 3 338.92 329.82 2.70 o 8 6 3 0.83 1.81 0.57 o 9 6 3 94.47 92.97 1.22 o 10 6 3 0.58 2.14 0.88 o 11 6 3 1327.13 1339.95 6.88 o 12 6 3 80.27 81.88 1.06 o 0 7 3 326.81 317.19 4.23 o 1 7 3 511.47 510.72 3.38 o 2 7 3 24.80 24.94 0.66 o 3 7 3 0.93 3.85 1.20 o 4 7 3 51.86 49.91 0.60 o 5 7 3 261.82 260.62 2.22 o 6 7 3 90.31 86.44 0.97 o 7 7 3 273.47 265.75 3.88 o 8 7 3 1.97 2.26 0.65 o 9 7 3 7.56 8.05 0.98 o 10 7 3 0.24 0.04 1.10 o 11 7 3 19.45 20.35 0.77 o 1 8 3 229.29 233.51 2.82 o 2 8 3 42.44 41.55 0.59 o 3 8 3 2063.70 2091.80 17.23 o 4 8 3 39.31 42.04 1.13 o 5 8 3 357.37 346.03 3.46 o 6 8 3 0.15 0.05 0.67 o 7 8 3 343.85 337.01 3.61 o 8 8 3 0.79 2.73 0.80 o 9 8 3 490.39 480.52 4.91 o 10 8 3 17.56 18.24 0.77 o 0 9 3 143.16 145.41 2.19 o 1 9 3 459.83 469.39 5.24 o 2 9 3 38.27 37.97 0.70 o 3 9 3 10.13 13.18 1.06 o 4 9 3 64.13 66.36 1.06 o 5 9 3 291.64 291.11 3.61 o 6 9 3 36.28 36.54 0.74 o 7 9 3 55.34 54.93 1.09 o 8 9 3 4.97 5.96 1.42 o 9 9 3 1.26 0.12 0.98 o 1 10 3 581.26 588.49 7.08 o 2 10 3 48.80 50.96 0.96 o 3 10 3 150.02 154.37 2.34 o 4 10 3 10.89 10.43 0.61 o 5 10 3 767.93 765.39 8.45 o 6 10 3 0.29 0.60 0.80 o 7 10 3 199.19 195.53 2.61 o 0 11 3 136.17 139.99 3.15 o 1 11 3 66.56 69.65 0.90 o 2 11 3 5.28 5.42 0.78 o 3 11 3 20.69 22.23 0.71 o 4 11 3 22.29 23.60 0.73 o 0 0 4 5835.54 6071.17 17.34 o 1 0 4 34.18 42.77 0.84 o 2 0 4 901.16 928.27 7.93 o 3 0 4 156.39 156.26 1.90 o 4 0 4 1144.54 1201.39 5.21 o 5 0 4 0.45 0.85 0.54 o 6 0 4 3281.27 3349.37 10.71 o 7 0 4 585.72 572.41 11.48 o 8 0 4 205.43 207.00 2.84 o 9 0 4 77.43 77.92 1.51 o 10 0 4 590.31 594.50 8.42 o 11 0 4 48.86 54.92 1.36 o 12 0 4 897.92 900.42 11.07 o 13 0 4 177.55 173.96 2.56 o 1 1 4 19.04 18.47 0.28 o 2 1 4 273.74 260.81 1.56 o 3 1 4 2.13 4.29 0.27 o 4 1 4 300.50 293.56 1.93 o 5 1 4 279.52 282.85 1.89 o 6 1 4 65.20 67.27 0.83 o 7 1 4 78.70 77.86 1.07 o 8 1 4 13.49 12.43 0.46 o 9 1 4 90.06 91.10 1.03 o 10 1 4 152.20 148.27 1.72 o 11 1 4 193.57 189.04 3.71 o 12 1 4 159.07 159.06 1.71 o 13 1 4 11.55 13.47 0.68 o 0 2 4 6.39 8.13 0.46 o 1 2 4 470.59 485.68 2.14 o 2 2 4 3479.41 3655.13 24.65 o 3 2 4 0.04 1.65 0.37 o 4 2 4 3801.74 3919.33 23.80 o 5 2 4 331.67 333.01 2.48 o 6 2 4 197.18 203.35 2.25 o 7 2 4 92.78 90.24 0.97 o 8 2 4 1144.01 1154.31 5.43 o 9 2 4 15.49 14.52 0.66 o 10 2 4 548.24 530.00 7.73 o 11 2 4 39.16 39.60 0.73 o 12 2 4 274.48 277.98 4.71 o 13 2 4 3.62 5.27 0.66 o 1 3 4 70.40 70.45 0.85 o 2 3 4 780.45 772.94 2.95 o 3 3 4 247.53 250.38 2.10 o 4 3 4 258.65 257.17 2.69 o 5 3 4 21.16 21.49 0.41 o 6 3 4 5.49 4.69 0.36 o 7 3 4 0.06 0.57 0.62 o 8 3 4 4.76 8.30 1.29 o 9 3 4 11.40 12.31 0.79 o 10 3 4 33.31 34.49 0.68 o 11 3 4 38.09 36.43 0.79 o 12 3 4 147.61 146.12 1.98 o 13 3 4 55.66 57.63 0.93 o 0 4 4 5213.60 5546.11 92.14 o 1 4 4 268.46 270.60 1.88 o 2 4 4 570.58 558.28 4.11 o 3 4 4 0.36 1.47 0.47 o 4 4 4 374.16 378.30 2.58 o 5 4 4 94.74 86.63 1.03 o 6 4 4 2314.43 2302.80 12.09 o 7 4 4 201.60 193.27 1.99 o 8 4 4 334.53 313.47 4.92 o 9 4 4 2.25 3.89 1.04 o 10 4 4 503.92 509.71 3.74 o 11 4 4 3.70 4.68 0.82 o 12 4 4 529.80 530.70 4.06 o 1 5 4 10.74 12.49 0.42 o 2 5 4 107.46 106.60 1.90 o 3 5 4 0.86 2.45 0.48 o 4 5 4 196.66 200.52 2.24 o 5 5 4 245.44 242.41 2.09 o 6 5 4 93.02 92.07 1.06 o 7 5 4 70.13 69.66 0.86 o 8 5 4 11.27 10.96 0.52 o 9 5 4 64.64 63.22 0.85 o 10 5 4 134.68 133.06 1.56 o 11 5 4 190.63 195.78 2.05 o 12 5 4 126.30 132.32 1.96 o 0 6 4 103.63 90.49 2.87 o 1 6 4 30.70 31.49 1.47 o 2 6 4 1752.00 1716.02 27.29 o 3 6 4 86.84 92.28 1.06 o 4 6 4 1189.59 1181.43 11.53 o 5 6 4 20.47 21.87 0.55 o 6 6 4 89.14 85.27 0.93 o 7 6 4 197.83 193.25 2.39 o 8 6 4 1101.35 1084.23 5.36 o 9 6 4 96.36 98.96 1.05 o 10 6 4 387.85 385.40 3.99 o 11 6 4 88.07 86.14 1.11 o 1 7 4 0.70 0.67 0.57 o 2 7 4 192.76 201.46 2.21 o 3 7 4 41.67 39.88 0.63 o 4 7 4 156.11 157.17 2.18 o 5 7 4 60.35 61.12 0.92 o 6 7 4 5.22 5.57 0.51 o 7 7 4 23.61 26.07 0.65 o 8 7 4 3.96 5.59 0.61 o 9 7 4 44.81 46.55 0.87 o 10 7 4 54.07 54.82 1.10 o 0 8 4 2511.53 2510.68 36.53 o 1 8 4 199.91 201.30 3.80 o 2 8 4 218.19 216.60 2.60 o 3 8 4 5.17 5.43 0.73 o 4 8 4 82.38 83.20 1.03 o 5 8 4 99.76 97.51 1.17 o 6 8 4 1095.82 1081.49 9.45 o 7 8 4 61.96 62.00 0.89 o 8 8 4 274.99 263.31 2.64 o 9 8 4 4.05 4.39 1.04 o 1 9 4 33.11 35.23 0.99 o 2 9 4 177.17 171.14 2.65 o 3 9 4 34.39 34.78 0.81 o 4 9 4 69.83 68.17 0.90 o 5 9 4 22.92 24.89 1.02 o 6 9 4 0.79 2.15 0.92 o 7 9 4 0.76 -0.81 1.10 o 0 10 4 26.55 29.25 1.01 o 1 10 4 38.93 38.67 0.88 o 2 10 4 655.46 663.21 5.55 o 3 10 4 7.29 6.80 0.70 o 4 10 4 542.55 543.47 5.35 o 5 10 4 26.52 28.14 0.91 o 1 0 5 918.03 945.24 4.74 o 2 0 5 144.46 143.16 1.92 o 3 0 5 2462.76 2539.71 23.97 o 4 0 5 201.13 208.88 2.47 o 5 0 5 357.95 354.56 3.31 o 6 0 5 426.11 419.16 3.83 o 7 0 5 791.08 818.34 8.28 o 8 0 5 0.03 -0.52 1.23 o 9 0 5 1032.18 1031.55 7.29 o 10 0 5 514.63 502.84 14.22 o 11 0 5 85.81 90.50 2.23 o 12 0 5 34.90 36.25 1.17 o 0 1 5 93.19 100.73 1.40 o 1 1 5 321.75 312.60 2.16 o 2 1 5 152.19 158.26 1.44 o 3 1 5 14.77 18.24 0.52 o 4 1 5 6.76 7.34 0.35 o 5 1 5 160.02 151.29 1.50 o 6 1 5 274.77 271.55 2.89 o 7 1 5 260.31 254.06 3.74 o 8 1 5 302.17 296.84 3.31 o 9 1 5 35.51 36.00 0.68 o 10 1 5 5.48 6.70 0.63 o 11 1 5 30.17 29.14 0.78 o 12 1 5 125.32 126.20 2.71 o 1 2 5 1305.97 1314.64 6.07 o 2 2 5 99.38 105.12 1.44 o 3 2 5 603.23 625.31 3.97 o 4 2 5 111.29 114.29 1.55 o 5 2 5 2064.44 2124.17 7.74 o 6 2 5 80.98 82.29 1.19 o 7 2 5 412.98 418.78 10.04 o 8 2 5 25.60 25.20 0.59 o 9 2 5 143.14 149.73 1.87 o 10 2 5 36.69 37.49 0.99 o 11 2 5 1083.47 1070.95 17.62 o 12 2 5 119.65 113.52 1.69 o 0 3 5 703.53 719.38 6.63 o 1 3 5 139.19 140.47 1.53 o 2 3 5 102.31 104.67 1.16 o 3 3 5 54.26 58.40 0.73 o 4 3 5 114.39 112.80 1.46 o 5 3 5 45.71 41.81 0.55 o 6 3 5 265.48 258.72 2.31 o 7 3 5 324.19 318.56 2.63 o 8 3 5 24.28 23.74 0.59 o 9 3 5 81.35 82.78 0.91 o 10 3 5 1.69 2.34 0.99 o 11 3 5 37.78 36.54 0.85 o 12 3 5 16.26 17.04 0.77 o 1 4 5 847.46 866.27 7.63 o 2 4 5 8.19 8.98 0.40 o 3 4 5 1468.91 1473.31 5.04 o 4 4 5 146.33 145.83 2.19 o 5 4 5 175.55 168.66 1.70 o 6 4 5 64.15 64.86 0.93 o 7 4 5 804.89 802.30 4.86 o 8 4 5 0.40 3.11 0.62 o 9 4 5 926.77 906.74 8.45 o 10 4 5 171.59 168.09 2.15 o 11 4 5 34.55 34.15 0.84 o 0 5 5 12.67 13.44 0.87 o 1 5 5 230.87 234.34 2.09 o 2 5 5 118.72 119.91 1.28 o 3 5 5 8.32 9.04 0.44 o 4 5 5 17.63 18.16 0.50 o 5 5 5 130.28 127.90 1.37 o 6 5 5 152.63 152.20 1.79 o 7 5 5 165.63 162.03 1.78 o 8 5 5 314.81 308.77 3.28 o 9 5 5 20.64 21.10 0.97 o 10 5 5 5.13 4.74 0.82 o 11 5 5 26.53 26.85 0.84 o 1 6 5 942.76 919.47 11.12 o 2 6 5 25.49 24.57 0.77 o 3 6 5 187.53 176.71 3.33 o 4 6 5 68.48 67.64 0.84 o 5 6 5 1026.25 1003.02 4.82 o 6 6 5 312.51 310.17 2.76 o 7 6 5 397.25 381.80 3.24 o 8 6 5 16.22 14.76 0.69 o 9 6 5 137.72 135.39 1.45 o 10 6 5 158.88 164.02 1.76 o 0 7 5 163.41 149.16 9.20 o 1 7 5 134.08 123.97 3.31 o 2 7 5 43.84 44.04 0.93 o 3 7 5 6.29 7.34 0.88 o 4 7 5 0.29 -0.31 1.01 o 5 7 5 56.25 56.28 0.94 o 6 7 5 177.01 175.22 1.81 o 7 7 5 133.98 132.92 1.39 o 8 7 5 61.41 61.23 0.94 o 9 7 5 16.41 17.53 0.97 o 1 8 5 419.64 410.94 5.85 o 2 8 5 53.15 52.92 1.38 o 3 8 5 641.10 618.48 6.86 o 4 8 5 73.10 76.19 1.43 o 5 8 5 88.95 87.96 1.40 o 6 8 5 1.02 0.88 0.85 o 7 8 5 479.03 472.32 3.97 o 0 9 5 127.15 127.85 1.99 o 1 9 5 45.27 45.05 1.12 o 2 9 5 59.31 59.05 0.93 o 3 9 5 19.85 20.75 0.78 o 4 9 5 48.39 48.65 0.96 o 5 9 5 21.00 23.12 0.75 o 1 10 5 330.31 318.40 4.56 o 0 0 6 2437.80 2429.34 23.44 o 1 0 6 393.98 401.92 5.28 o 2 0 6 371.96 372.21 6.19 o 3 0 6 0.06 0.14 0.62 o 4 0 6 284.87 287.31 3.22 o 5 0 6 161.24 166.10 3.20 o 6 0 6 1317.28 1331.45 13.33 o 7 0 6 252.76 245.86 5.18 o 8 0 6 284.90 292.30 3.95 o 9 0 6 0.04 -1.53 1.53 o 10 0 6 291.89 298.29 5.90 o 11 0 6 2.97 4.02 1.21 o 1 1 6 44.89 47.22 0.57 o 2 1 6 67.31 66.96 0.83 o 3 1 6 158.68 160.70 1.68 o 4 1 6 125.48 123.24 1.28 o 5 1 6 89.26 87.59 0.94 o 6 1 6 30.74 32.18 0.91 o 7 1 6 1.26 1.55 0.57 o 8 1 6 17.55 17.53 0.64 o 9 1 6 27.42 27.92 0.83 o 10 1 6 67.08 67.12 1.33 o 11 1 6 86.14 85.55 1.43 o 0 2 6 576.60 577.51 6.14 o 1 2 6 408.53 416.59 2.61 o 2 2 6 1251.44 1268.56 4.69 o 3 2 6 0.10 0.97 0.53 o 4 2 6 402.77 407.65 2.77 o 5 2 6 292.50 293.73 2.81 o 6 2 6 141.98 142.71 1.55 o 7 2 6 65.77 64.62 0.79 o 8 2 6 1279.93 1271.95 10.86 o 9 2 6 22.75 20.23 1.11 o 10 2 6 323.98 324.94 3.31 o 11 2 6 24.61 22.63 0.80 o 1 3 6 42.59 43.98 0.58 o 2 3 6 29.69 30.99 0.53 o 3 3 6 189.77 195.48 1.94 o 4 3 6 107.79 108.44 1.15 o 5 3 6 35.24 36.27 0.75 o 6 3 6 251.43 245.77 2.38 o 7 3 6 3.31 4.34 1.03 o 8 3 6 10.06 10.54 0.61 o 9 3 6 14.86 16.16 0.70 o 10 3 6 258.11 262.38 2.95 o 0 4 6 1035.78 1047.53 6.35 o 1 4 6 323.16 325.73 3.34 o 2 4 6 283.96 280.23 2.59 o 3 4 6 1.68 1.55 0.86 o 4 4 6 613.28 611.85 4.04 o 5 4 6 127.14 124.42 1.29 o 6 4 6 1033.03 1022.42 5.66 o 7 4 6 162.30 156.51 1.98 o 8 4 6 58.64 60.53 1.27 o 9 4 6 0.02 0.17 1.00 o 10 4 6 245.94 248.72 4.30 o 1 5 6 32.68 33.95 0.60 o 2 5 6 95.89 96.75 1.02 o 3 5 6 73.96 73.74 0.81 o 4 5 6 88.50 88.95 0.94 o 5 5 6 92.61 92.25 1.03 o 6 5 6 5.45 5.93 0.91 o 7 5 6 0.46 1.24 0.83 o 8 5 6 18.29 16.90 0.84 o 9 5 6 18.76 17.73 0.76 o 0 6 6 49.51 50.97 1.04 o 1 6 6 210.37 210.21 2.76 o 2 6 6 770.27 756.59 7.51 o 3 6 6 2.02 3.83 0.57 o 4 6 6 718.09 699.32 9.12 o 5 6 6 167.30 163.98 1.79 o 6 6 6 90.92 90.05 1.00 o 7 6 6 65.66 64.14 0.93 o 8 6 6 414.85 406.62 3.63 o 1 7 6 12.96 13.41 0.65 o 2 7 6 6.34 8.51 1.15 o 3 7 6 122.40 116.32 2.07 o 4 7 6 56.15 53.46 1.05 o 5 7 6 15.47 15.39 0.94 o 6 7 6 35.67 35.04 0.81 o 0 8 6 348.27 320.64 12.92 o 1 8 6 183.68 171.94 5.23 o 2 8 6 162.88 150.51 4.09 o 3 8 6 4.78 4.98 0.70 o 4 8 6 494.30 476.45 8.32 o 1 0 7 168.63 171.96 2.75 o 2 0 7 264.81 270.23 3.38 o 3 0 7 1229.14 1239.73 8.12 o 4 0 7 158.90 160.50 2.30 o 5 0 7 410.04 413.84 5.35 o 6 0 7 8.82 10.71 1.05 o 7 0 7 202.57 217.28 8.08 o 8 0 7 0.22 0.03 1.58 o 9 0 7 274.38 270.85 4.79 o 0 1 7 561.62 570.90 4.79 o 1 1 7 147.51 146.36 1.50 o 2 1 7 99.85 100.41 1.06 o 3 1 7 5.92 7.95 0.77 o 4 1 7 135.95 136.97 1.75 o 5 1 7 81.87 80.76 0.89 o 6 1 7 169.97 171.57 1.83 o 7 1 7 13.57 15.69 0.66 o 8 1 7 21.81 21.04 0.73 o 9 1 7 0.32 0.78 0.92 o 1 2 7 629.55 636.27 4.01 o 2 2 7 62.58 61.39 0.72 o 3 2 7 194.64 195.07 1.87 o 4 2 7 69.55 69.84 0.83 o 5 2 7 664.48 659.32 5.73 o 6 2 7 85.09 86.03 0.96 o 7 2 7 322.36 318.67 3.03 o 8 2 7 9.28 8.48 0.69 o 0 3 7 228.54 229.41 3.80 o 1 3 7 45.32 47.38 0.67 o 2 3 7 62.96 63.27 0.74 o 3 3 7 6.39 7.60 1.02 o 4 3 7 5.13 5.17 0.86 o 5 3 7 20.52 22.64 0.68 o 6 3 7 154.03 157.74 2.00 o 7 3 7 65.11 63.87 0.92 o 8 3 7 93.32 91.71 1.07 o 1 4 7 240.96 237.52 2.36 o 2 4 7 55.07 53.08 0.78 o 3 4 7 785.85 787.34 4.43 o 4 4 7 114.97 112.28 1.20 o 5 4 7 213.23 211.67 2.34 o 6 4 7 10.69 10.88 0.64 o 7 4 7 237.82 233.00 2.32 o 0 5 7 409.71 410.23 4.66 o 1 5 7 133.48 130.98 1.38 o 2 5 7 90.64 89.00 1.06 o 3 5 7 11.39 11.74 0.63 o 4 5 7 148.68 146.89 2.46 o 5 5 7 82.75 80.99 0.98 o 6 5 7 111.08 108.81 1.17 o 1 6 7 611.63 594.37 6.64 o 2 6 7 178.09 174.85 2.73 o 3 6 7 61.42 62.57 1.18 o 4 6 7 49.28 47.61 0.87 o 5 6 7 281.12 278.63 6.32 o 0 7 7 286.56 282.16 5.28 o 1 7 7 47.17 48.39 0.99 o 2 7 7 25.32 24.97 0.78 o 0 0 8 566.94 559.99 7.47 o 1 0 8 252.51 249.54 3.58 o 2 0 8 233.91 235.60 6.30 o 3 0 8 1.76 1.89 1.11 o 4 0 8 235.03 235.58 3.29 o 5 0 8 96.81 99.28 1.50 o 1 1 8 12.83 13.64 0.61 o 2 1 8 30.40 31.11 0.70 o 3 1 8 68.70 66.74 0.88 o 4 1 8 16.17 15.97 0.67 o 5 1 8 84.73 83.23 1.00 o 0 2 8 87.32 85.76 1.35 o 1 2 8 60.18 59.99 0.85 o 2 2 8 415.99 417.81 3.33 o 3 2 8 56.44 58.50 1.33 o 4 2 8 443.33 450.40 3.56 o 5 2 8 43.86 42.37 0.93 o 1 3 8 11.77 14.03 0.63 o 2 3 8 62.71 65.92 0.88 o 3 3 8 11.39 12.35 0.66 o 4 3 8 21.28 21.12 0.72 o 0 4 8 585.94 577.30 5.71 o 1 4 8 93.00 95.41 1.06 o 2 4 8 188.23 189.76 2.47 o 3 4 8 11.03 12.10 1.00 o