#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:43:47 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181087 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/67/2216702.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216702_Fobs loop_ _publ_author_name 'Martins, Roberto S.' 'Filgueiras, Carlos A. L.' 'do Visentin, Lorenzo' 'Bordinh\~ao, Jairo' 'Ferreira, Leonardo C.' _publ_section_title ; 2,3-Bis(2-ethylphenylimino)butane ; _journal_coeditor_code OM2165 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4544 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.757 _cell_angle_gamma 90.000 _cell_length_a 7.1898 _cell_length_b 8.3807 _cell_length_c 14.7836 _exptl_crystal_F_000 316.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file om2165Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sad in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 68.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 186.43 166.49 2.08 o 4 0 0 138.97 145.46 2.07 o 6 0 0 0.12 0.33 0.19 o 8 0 0 7.23 8.07 0.50 o 2 1 0 397.21 382.89 3.84 o 3 1 0 57.80 60.68 0.62 o 4 1 0 536.72 531.96 4.98 o 5 1 0 178.16 188.82 1.89 o 6 1 0 93.97 89.10 0.99 o 7 1 0 1.57 1.06 0.19 o 8 1 0 2.54 2.17 0.27 o 0 2 0 426.80 400.07 8.20 o 2 2 0 226.37 219.07 2.57 o 3 2 0 348.13 373.84 4.24 o 4 2 0 287.34 304.43 3.29 o 5 2 0 22.55 23.08 0.36 o 6 2 0 23.20 24.56 0.40 o 7 2 0 18.22 14.78 0.32 o 8 2 0 1.88 1.12 0.36 o 1 3 0 158.05 175.17 2.46 o 2 3 0 27.55 29.99 0.44 o 3 3 0 344.36 334.75 3.79 o 4 3 0 1.19 1.21 0.12 o 5 3 0 84.93 79.82 1.05 o 6 3 0 0.86 0.00 0.18 o 7 3 0 0.30 0.40 0.19 o 8 3 0 5.88 5.90 0.44 o 0 4 0 165.48 168.40 3.20 o 1 4 0 2.18 1.99 0.16 o 2 4 0 223.45 238.24 3.19 o 3 4 0 0.28 0.00 0.10 o 4 4 0 161.46 165.54 1.96 o 5 4 0 18.56 20.04 0.36 o 6 4 0 30.92 27.75 0.47 o 7 4 0 0.06 0.00 0.19 o 1 5 0 12.70 17.37 0.45 o 2 5 0 0.00 0.00 0.15 o 3 5 0 44.94 45.07 0.69 o 4 5 0 1.27 1.09 0.16 o 5 5 0 14.27 11.28 0.32 o 6 5 0 1.99 2.40 0.18 o 7 5 0 0.60 0.00 0.41 o 0 6 0 162.16 188.30 3.64 o 1 6 0 1.14 2.46 0.21 o 2 6 0 2.60 3.98 0.23 o 3 6 0 0.55 0.43 0.21 o 4 6 0 4.25 5.15 0.24 o 5 6 0 0.20 0.31 0.16 o 6 6 0 0.05 1.28 0.34 o 1 7 0 1.48 1.12 0.27 o 2 7 0 4.54 4.87 0.37 o 3 7 0 13.45 12.46 0.42 o 4 7 0 8.58 8.48 0.34 o 5 7 0 2.01 1.48 0.32 o 0 8 0 0.01 0.00 0.25 o 1 8 0 0.74 0.24 0.25 o 2 8 0 0.28 0.00 0.28 o 3 8 0 1.15 0.79 0.43 o 4 8 0 0.00 0.03 0.36 o 5 8 0 9.92 8.76 0.69 o 1 9 0 0.85 0.00 0.38 o 2 9 0 0.25 0.45 0.50 o 3 9 0 0.51 0.00 0.33 o -7 0 1 21.02 21.37 0.54 o -5 0 1 0.42 0.19 0.17 o -3 0 1 0.45 0.91 0.08 o -1 0 1 391.45 271.03 9.06 o 1 0 1 1146.61 944.90 26.21 o 3 0 1 1151.42 1296.69 15.89 o 5 0 1 192.80 194.07 2.75 o 7 0 1 3.71 3.74 0.28 o -8 1 1 1.60 2.18 0.31 o -7 1 1 6.05 5.67 0.25 o -6 1 1 13.63 14.76 0.29 o -5 1 1 29.88 28.61 0.40 o -4 1 1 49.73 42.97 0.46 o -3 1 1 2.32 4.43 0.11 o -2 1 1 2720.08 2560.87 32.55 o 1 1 1 1883.16 1746.56 32.28 o 2 1 1 777.24 774.48 7.75 o 3 1 1 0.04 0.06 0.07 o 4 1 1 230.49 254.40 2.55 o 5 1 1 28.11 27.60 0.38 o 6 1 1 0.39 0.03 0.13 o 7 1 1 19.70 18.00 0.37 o 8 1 1 9.30 8.49 0.42 o -8 2 1 0.57 0.00 0.26 o -7 2 1 8.17 8.42 0.25 o -6 2 1 31.24 33.19 0.52 o -5 2 1 21.35 18.85 0.30 o -4 2 1 48.73 44.85 0.54 o -3 2 1 202.50 218.90 2.28 o -2 2 1 19.99 25.32 0.36 o -1 2 1 3755.10 3760.92 108.25 o 0 2 1 1407.70 1397.84 18.06 o 1 2 1 357.89 369.29 4.84 o 2 2 1 33.27 33.65 0.45 o 3 2 1 88.49 87.08 0.96 o 4 2 1 8.68 8.14 0.18 o 5 2 1 18.93 20.47 0.32 o 6 2 1 58.60 57.89 0.74 o 7 2 1 11.85 12.57 0.31 o 8 2 1 5.13 6.51 0.50 o -8 3 1 0.35 0.28 0.33 o -7 3 1 0.18 0.00 0.16 o -6 3 1 43.21 36.28 0.53 o -5 3 1 334.99 346.80 3.64 o -4 3 1 1.28 1.57 0.10 o -3 3 1 54.87 41.72 0.57 o -2 3 1 72.12 89.01 1.19 o -1 3 1 75.13 68.26 0.95 o 0 3 1 9.50 10.01 0.22 o 1 3 1 0.00 0.04 0.10 o 2 3 1 211.87 240.85 3.21 o 3 3 1 80.02 77.33 0.95 o 4 3 1 97.61 87.67 1.10 o 5 3 1 226.61 230.74 2.73 o 6 3 1 4.83 5.55 0.18 o 7 3 1 1.30 1.63 0.36 o -7 4 1 3.52 2.27 0.25 o -6 4 1 0.87 1.32 0.21 o -5 4 1 4.65 4.70 0.19 o -4 4 1 2.37 1.55 0.15 o -3 4 1 3.87 4.65 0.17 o -2 4 1 135.77 139.52 2.02 o -1 4 1 237.83 266.21 3.52 o 0 4 1 389.77 390.77 5.11 o 1 4 1 215.07 241.74 3.41 o 2 4 1 77.61 83.44 1.29 o 3 4 1 10.63 12.56 0.26 o 4 4 1 42.85 40.71 0.60 o 5 4 1 8.31 8.49 0.22 o 6 4 1 10.62 10.08 0.27 o 7 4 1 1.71 0.87 0.38 o -7 5 1 0.55 0.68 0.29 o -6 5 1 4.75 5.50 0.22 o -5 5 1 54.80 45.59 0.66 o -4 5 1 10.15 10.80 0.28 o -3 5 1 0.85 0.98 0.14 o -2 5 1 52.56 54.78 0.91 o -1 5 1 495.56 539.56 7.06 o 0 5 1 120.84 119.93 1.78 o 1 5 1 17.24 16.50 0.36 o 2 5 1 17.57 20.64 0.44 o 3 5 1 2.43 0.94 0.18 o 4 5 1 12.40 12.64 0.32 o 5 5 1 29.60 31.66 0.55 o 6 5 1 0.03 0.00 0.18 o 7 5 1 3.05 2.96 0.49 o -6 6 1 0.25 0.00 0.26 o -5 6 1 0.39 0.21 0.25 o -4 6 1 33.42 34.17 0.74 o -3 6 1 76.32 73.82 1.11 o -2 6 1 9.16 10.48 0.33 o -1 6 1 14.40 13.84 0.38 o 0 6 1 11.90 10.75 0.30 o 1 6 1 3.49 3.51 0.22 o 2 6 1 0.05 0.10 0.18 o 3 6 1 1.00 0.70 0.18 o 4 6 1 93.73 97.21 1.48 o 5 6 1 0.35 0.03 0.18 o 6 6 1 0.47 1.63 0.56 o -6 7 1 1.43 1.30 0.36 o -5 7 1 0.62 0.67 0.26 o -4 7 1 1.78 0.60 0.18 o -3 7 1 0.51 0.05 0.25 o -2 7 1 31.59 32.81 0.91 o -1 7 1 34.28 35.31 0.81 o 0 7 1 0.00 0.04 0.15 o 1 7 1 5.56 6.36 0.31 o 2 7 1 19.68 19.29 0.54 o 3 7 1 1.15 1.37 0.94 o 4 7 1 13.86 11.29 0.53 o 5 7 1 0.00 0.11 0.32 o -5 8 1 4.61 5.37 0.58 o -4 8 1 23.80 21.90 0.73 o -3 8 1 0.42 0.94 0.30 o -2 8 1 4.87 4.66 0.45 o -1 8 1 5.46 6.45 0.37 o 0 8 1 7.49 8.47 0.35 o 1 8 1 16.74 16.52 0.84 o 2 8 1 1.98 0.70 0.30 o 3 8 1 0.96 0.91 0.44 o 4 8 1 0.39 0.39 0.28 o -3 9 1 12.95 14.97 0.77 o -2 9 1 4.94 4.61 0.49 o -1 9 1 5.40 4.33 0.31 o 0 9 1 9.86 9.59 0.43 o 1 9 1 1.36 0.63 0.33 o 2 9 1 6.27 6.50 0.59 o 3 9 1 6.37 6.57 0.65 o -8 0 2 4.90 5.24 0.76 o -6 0 2 9.23 6.55 0.29 o -4 0 2 5.70 3.63 0.16 o -2 0 2 157.34 155.92 2.38 o 2 0 2 40.84 41.11 0.65 o 4 0 2 286.60 298.95 3.93 o 6 0 2 21.37 17.47 0.41 o 8 0 2 9.81 10.92 0.83 o -8 1 2 1.28 1.12 0.31 o -7 1 2 20.29 20.23 0.41 o -6 1 2 50.05 55.51 0.78 o -5 1 2 24.64 23.57 0.35 o -4 1 2 9.56 7.07 0.15 o -3 1 2 12.28 10.70 0.18 o -2 1 2 1242.54 1204.09 13.46 o -1 1 2 96.54 79.65 1.02 o 0 1 2 162.98 152.29 1.69 o 1 1 2 32.60 26.42 0.36 o 2 1 2 24.40 32.05 0.41 o 3 1 2 641.39 677.40 7.02 o 4 1 2 290.12 311.96 3.31 o 5 1 2 1.41 1.71 0.12 o 6 1 2 5.40 6.16 0.18 o 7 1 2 3.56 2.97 0.23 o 8 1 2 0.07 0.15 0.39 o -8 2 2 0.83 0.96 0.36 o -7 2 2 0.40 0.00 0.20 o -6 2 2 216.10 212.26 2.23 o -5 2 2 2.21 1.29 0.13 o -4 2 2 1.54 1.26 0.10 o -3 2 2 144.31 164.43 1.68 o -2 2 2 228.40 220.31 2.49 o -1 2 2 877.53 864.25 11.20 o 0 2 2 806.55 786.96 10.30 o 1 2 2 877.86 845.18 10.97 o 2 2 2 565.23 581.67 6.51 o 3 2 2 57.05 66.62 0.91 o 4 2 2 6.75 5.94 0.17 o 5 2 2 15.51 15.68 0.29 o 6 2 2 7.43 6.70 0.23 o 7 2 2 0.06 0.00 0.21 o 8 2 2 0.21 0.00 0.33 o -8 3 2 0.01 0.17 0.28 o -7 3 2 0.01 0.00 0.18 o -6 3 2 44.87 44.92 0.60 o -5 3 2 5.81 4.22 0.20 o -4 3 2 1.41 2.44 0.12 o -3 3 2 72.48 67.54 0.88 o -2 3 2 1953.89 2062.95 25.48 o -1 3 2 114.03 120.68 1.64 o 0 3 2 986.28 993.88 12.94 o 1 3 2 49.07 54.76 0.80 o 2 3 2 31.48 29.25 0.48 o 3 3 2 102.99 93.36 1.10 o 4 3 2 52.36 53.64 0.67 o 5 3 2 2.55 3.03 0.21 o 6 3 2 0.33 0.02 0.24 o 7 3 2 9.92 12.59 0.47 o -7 4 2 2.20 3.17 0.31 o -6 4 2 37.92 38.45 0.58 o -5 4 2 83.23 77.72 0.97 o -4 4 2 0.03 0.00 0.13 o -3 4 2 48.49 47.79 0.66 o -2 4 2 0.28 0.01 0.16 o -1 4 2 161.73 179.80 2.42 o 0 4 2 16.26 17.03 0.39 o 1 4 2 0.26 0.13 0.12 o 2 4 2 315.74 333.38 4.94 o 3 4 2 128.36 124.51 1.61 o 4 4 2 192.40 198.35 2.25 o 5 4 2 68.37 65.95 1.16 o 6 4 2 2.25 1.53 0.29 o 7 4 2 1.29 1.08 0.52 o -7 5 2 0.03 0.03 0.36 o -6 5 2 0.25 0.00 0.18 o -5 5 2 2.39 3.16 0.17 o -4 5 2 9.43 6.83 0.21 o -3 5 2 26.73 28.57 0.51 o -2 5 2 3.20 3.50 0.19 o -1 5 2 60.34 65.42 1.04 o 0 5 2 119.41 114.61 2.05 o 1 5 2 80.50 88.09 1.35 o 2 5 2 6.32 5.00 0.23 o 3 5 2 110.47 121.32 1.84 o 4 5 2 185.49 188.32 2.34 o 5 5 2 70.20 63.13 1.05 o 6 5 2 2.45 3.74 0.30 o 7 5 2 0.10 0.00 0.43 o -6 6 2 0.00 0.08 0.25 o -5 6 2 0.74 0.54 0.20 o -4 6 2 4.87 3.58 0.23 o -3 6 2 0.53 0.00 0.23 o -2 6 2 0.47 0.33 0.16 o -1 6 2 98.51 99.29 1.38 o 0 6 2 82.76 90.80 1.32 o 1 6 2 79.15 77.69 1.24 o 2 6 2 20.32 21.74 0.55 o 3 6 2 8.24 7.96 0.39 o 4 6 2 4.85 3.99 0.23 o 5 6 2 0.01 0.00 0.31 o 6 6 2 28.13 29.03 1.02 o -6 7 2 28.99 33.67 1.30 o -5 7 2 4.37 3.50 0.29 o -4 7 2 1.46 0.85 0.24 o -3 7 2 7.43 6.76 0.31 o -2 7 2 2.57 1.85 0.27 o -1 7 2 18.02 15.80 0.40 o 0 7 2 46.40 40.27 0.68 o 1 7 2 8.68 7.62 0.32 o 2 7 2 14.67 13.93 0.45 o 3 7 2 141.56 156.09 3.17 o 4 7 2 0.92 0.69 0.21 o 5 7 2 6.53 6.81 0.88 o -5 8 2 8.08 8.26 0.59 o -4 8 2 20.42 18.02 0.87 o -3 8 2 7.73 7.71 0.48 o -2 8 2 41.88 38.69 1.32 o -1 8 2 0.56 0.11 0.23 o 0 8 2 14.95 13.29 0.40 o 1 8 2 3.68 3.82 0.38 o 2 8 2 0.13 0.55 0.50 o 3 8 2 0.73 0.00 0.27 o 4 8 2 0.32 0.20 0.34 o -3 9 2 9.24 7.71 0.79 o -2 9 2 14.88 16.83 0.63 o -1 9 2 31.13 30.21 1.13 o 0 9 2 0.09 0.00 0.29 o 1 9 2 8.55 8.83 0.76 o 2 9 2 15.06 16.18 1.00 o 3 9 2 0.04 0.43 0.43 o -7 0 3 190.12 197.28 3.51 o -5 0 3 15.41 13.33 0.36 o -3 0 3 72.40 68.59 1.06 o -1 0 3 394.90 358.73 6.07 o 1 0 3 734.06 728.27 10.86 o 3 0 3 1368.07 1465.56 21.02 o 5 0 3 68.24 63.43 0.99 o 7 0 3 25.64 25.14 1.00 o -8 1 3 6.38 6.81 0.38 o -7 1 3 6.09 6.84 0.27 o -6 1 3 4.06 3.94 0.21 o -5 1 3 7.96 7.60 0.19 o -4 1 3 4.39 5.29 0.14 o -3 1 3 228.02 221.33 2.46 o -2 1 3 1959.96 1960.33 20.94 o -1 1 3 3675.78 3514.44 51.15 o 0 1 3 227.59 191.90 2.09 o 1 1 3 1993.75 1869.56 20.45 o 2 1 3 225.10 206.98 2.34 o 3 1 3 78.51 73.65 0.85 o 4 1 3 20.12 17.56 0.29 o 5 1 3 0.73 0.91 0.12 o 6 1 3 0.00 0.00 0.14 o 7 1 3 7.48 6.85 0.39 o 8 1 3 0.01 0.00 0.59 o -8 2 3 1.12 0.37 0.30 o -7 2 3 51.50 55.11 0.78 o -6 2 3 107.52 107.07 1.20 o -5 2 3 12.05 11.73 0.24 o -4 2 3 23.95 27.84 0.39 o -3 2 3 33.14 39.09 0.55 o -2 2 3 187.39 178.19 2.11 o -1 2 3 4658.07 4631.41 85.05 o 0 2 3 40.33 44.87 0.59 o 1 2 3 252.09 272.84 3.17 o 2 2 3 823.70 821.16 9.95 o 3 2 3 364.04 404.89 4.64 o 4 2 3 14.23 14.93 0.26 o 5 2 3 4.14 3.63 0.17 o 6 2 3 18.71 19.33 0.45 o 7 2 3 12.27 12.17 0.46 o -8 3 3 4.96 5.50 0.38 o -7 3 3 31.04 28.57 0.49 o -6 3 3 1.56 1.32 0.22 o -5 3 3 158.52 155.48 1.81 o -4 3 3 2.62 1.62 0.11 o -3 3 3 111.63 113.86 1.46 o -2 3 3 164.16 176.62 2.33 o -1 3 3 53.85 57.45 0.84 o 0 3 3 82.72 69.62 0.92 o 1 3 3 15.47 12.79 0.22 o 2 3 3 1053.18 1139.64 13.18 o 3 3 3 41.94 37.25 0.54 o 4 3 3 13.97 16.59 0.32 o 5 3 3 9.57 10.84 0.28 o 6 3 3 1.10 0.76 0.20 o 7 3 3 0.12 0.00 0.32 o -7 4 3 0.42 0.00 0.19 o -6 4 3 6.45 4.21 0.21 o -5 4 3 3.12 2.24 0.21 o -4 4 3 36.62 38.06 0.60 o -3 4 3 212.27 254.32 3.28 o -2 4 3 745.74 720.15 8.96 o -1 4 3 220.21 253.12 3.37 o 0 4 3 30.74 29.10 0.46 o 1 4 3 29.60 28.60 0.49 o 2 4 3 78.59 81.44 1.53 o 3 4 3 7.62 7.52 0.22 o 4 4 3 29.39 29.66 0.44 o 5 4 3 4.06 4.17 0.18 o 6 4 3 6.74 7.12 0.37 o 7 4 3 16.50 17.23 0.60 o -7 5 3 5.45 7.56 0.48 o -6 5 3 6.25 7.40 0.26 o -5 5 3 3.60 3.31 0.18 o -4 5 3 5.96 3.52 0.20 o -3 5 3 6.20 5.58 0.23 o -2 5 3 10.49 9.70 0.28 o -1 5 3 45.85 46.99 0.80 o 0 5 3 6.19 5.46 0.19 o 1 5 3 84.70 82.76 1.28 o 2 5 3 27.92 26.71 0.57 o 3 5 3 442.99 462.97 6.62 o 4 5 3 67.48 64.69 1.06 o 5 5 3 1.73 1.23 0.16 o 6 5 3 31.39 33.50 1.01 o -6 6 3 5.49 5.82 0.47 o -5 6 3 1.99 3.18 0.21 o -4 6 3 1.25 1.49 0.22 o -3 6 3 89.38 82.92 1.34 o -2 6 3 17.99 20.12 0.46 o -1 6 3 6.41 5.36 0.21 o 0 6 3 28.92 29.76 0.52 o 1 6 3 25.77 26.87 0.59 o 2 6 3 331.76 347.37 4.91 o 3 6 3 38.75 40.06 1.10 o 4 6 3 129.15 125.45 2.33 o 5 6 3 9.14 7.02 0.26 o 6 6 3 4.05 6.66 0.56 o -6 7 3 0.00 0.00 0.59 o -5 7 3 1.25 1.15 0.29 o -4 7 3 30.01 26.22 0.66 o -3 7 3 7.88 8.06 0.39 o -2 7 3 0.65 0.50 0.20 o -1 7 3 70.91 74.36 1.23 o 0 7 3 3.78 4.65 0.20 o 1 7 3 37.33 32.44 0.71 o 2 7 3 1.24 0.65 0.60 o 3 7 3 10.37 11.49 0.49 o 4 7 3 3.24 2.43 0.32 o 5 7 3 25.52 25.39 0.80 o -5 8 3 8.89 7.47 0.52 o -4 8 3 2.58 2.60 0.41 o -3 8 3 22.40 23.98 0.76 o -2 8 3 4.69 4.05 0.30 o -1 8 3 0.00 0.35 0.18 o 0 8 3 90.57 96.55 1.92 o 1 8 3 47.82 51.40 1.47 o 2 8 3 0.16 0.66 0.38 o 3 8 3 7.15 7.56 0.41 o 4 8 3 3.97 3.56 0.37 o -3 9 3 5.53 5.94 0.57 o -2 9 3 9.19 8.85 0.59 o -1 9 3 2.04 1.94 0.34 o 0 9 3 29.80 27.59 0.88 o 1 9 3 44.30 46.39 1.11 o 2 9 3 25.17 27.83 0.89 o 3 9 3 6.55 8.19 0.58 o -8 0 4 6.06 7.02 0.65 o -6 0 4 69.57 72.19 1.13 o -4 0 4 334.46 353.17 4.78 o -2 0 4 31.68 31.96 0.66 o 0 0 4 554.59 526.72 7.76 o 2 0 4 12.30 9.91 0.23 o 4 0 4 2.05 1.52 0.20 o 6 0 4 61.29 62.70 2.42 o -8 1 4 73.86 73.76 1.34 o -7 1 4 32.46 28.81 0.51 o -6 1 4 62.49 62.42 0.80 o -5 1 4 38.44 42.64 0.55 o -4 1 4 23.44 22.26 0.31 o -3 1 4 254.94 255.17 2.81 o -2 1 4 121.09 117.17 1.43 o -1 1 4 818.62 763.96 7.90 o 0 1 4 314.84 294.21 3.10 o 1 1 4 490.95 460.58 4.84 o 2 1 4 417.52 446.63 5.10 o 3 1 4 28.30 37.68 0.47 o 4 1 4 1.37 0.78 0.11 o 5 1 4 0.02 0.00 0.11 o 6 1 4 0.27 0.30 0.24 o 7 1 4 3.96 3.90 0.34 o -8 2 4 0.21 0.00 0.30 o -7 2 4 93.33 91.05 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