#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2216736.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216736_Fobs loop_ _publ_author_name 'Wang, Lin' 'Zhou, Li-Na' 'Bao, Ying' 'Wang, Jing-Kang' _publ_section_title ; 2-n-Butyl-3-[2'-(1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1-azonia-3-azaspiro[4.4]non-1-en-4-one bromide sesquihydrate ; _journal_coeditor_code RN2028 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4933 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.778 _cell_angle_gamma 90.000 _cell_length_a 12.4817 _cell_length_b 25.2852 _cell_length_c 8.6938 _exptl_crystal_F_000 1116.00 _reflns_d_resolution_high 0.8255 _[local]_cod_data_source_file rn2028Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 251.80 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3095.45 3681.78 74.66 o 3 0 0 63403.74 52586.05 2595.38 o 4 0 0 2840.63 2637.89 47.89 o 5 0 0 8665.80 8833.01 221.04 o 6 0 0 11676.13 12987.85 342.51 o 7 0 0 355.88 313.86 58.07 o 8 0 0 3693.51 3756.32 101.59 o 9 0 0 2.32 0.00 20.95 o 10 0 0 636.53 619.70 35.59 o 11 0 0 2092.05 2144.38 79.35 o 12 0 0 720.34 741.72 57.14 o 13 0 0 195.47 162.75 30.76 o 14 0 0 53.64 38.97 27.10 o 2 1 0 1649.48 2127.79 16.90 o 3 1 0 4461.80 3628.71 55.94 o 4 1 0 73.72 220.40 8.23 o 5 1 0 2034.98 1941.62 49.22 o 6 1 0 54.47 67.83 17.94 o 7 1 0 1973.12 2235.10 40.36 o 8 1 0 199.40 172.53 14.44 o 9 1 0 391.43 403.04 37.47 o 10 1 0 223.83 238.06 19.41 o 11 1 0 452.30 445.48 27.97 o 12 1 0 705.04 682.01 31.50 o 13 1 0 86.79 67.32 18.10 o 14 1 0 44.64 29.39 18.42 o 2 2 0 2585.33 3093.32 26.86 o 3 2 0 12595.41 13093.61 206.80 o 4 2 0 89.81 52.10 6.57 o 5 2 0 6826.35 6893.92 90.60 o 6 2 0 7.65 2.49 7.67 o 7 2 0 24.99 63.58 12.10 o 8 2 0 1212.87 1181.70 32.81 o 9 2 0 59.69 53.83 14.29 o 10 2 0 32.70 37.13 12.88 o 11 2 0 354.63 357.48 23.58 o 12 2 0 222.74 203.37 21.11 o 13 2 0 86.17 63.18 17.38 o 14 2 0 24.97 9.44 20.19 o 2 3 0 9285.17 9101.96 109.20 o 3 3 0 2457.47 2243.60 23.49 o 4 3 0 14391.42 14079.87 238.65 o 5 3 0 102.49 109.71 8.03 o 6 3 0 5178.50 4784.37 91.59 o 7 3 0 6552.80 6261.45 99.00 o 8 3 0 95.58 100.74 14.32 o 9 3 0 3788.69 3799.41 84.91 o 10 3 0 203.78 231.85 17.65 o 11 3 0 617.10 677.22 28.11 o 12 3 0 1354.36 1382.40 42.93 o 13 3 0 36.88 46.91 16.97 o 14 3 0 389.90 437.29 29.43 o 0 4 0 12733.18 12653.40 294.99 o 1 4 0 292.25 481.18 14.41 o 2 4 0 166.60 260.06 7.98 o 3 4 0 1072.66 1168.00 14.52 o 4 4 0 4795.29 4923.50 54.70 o 5 4 0 1870.70 1834.59 23.23 o 6 4 0 2714.65 2925.37 39.10 o 7 4 0 2351.54 2401.77 34.85 o 8 4 0 949.84 901.12 21.75 o 9 4 0 13.62 18.25 12.62 o 10 4 0 897.37 852.79 33.07 o 11 4 0 535.72 573.51 28.15 o 12 4 0 88.48 67.89 18.20 o 13 4 0 142.14 148.46 25.52 o 14 4 0 24.78 0.00 18.52 o 1 5 0 401.06 438.85 9.79 o 2 5 0 3170.03 2966.41 46.55 o 3 5 0 273.55 367.02 12.05 o 4 5 0 2178.72 2611.47 28.51 o 5 5 0 158.89 111.80 11.14 o 6 5 0 1828.40 1666.23 23.72 o 7 5 0 22.05 14.95 9.26 o 8 5 0 48.41 54.49 10.21 o 9 5 0 1319.02 1251.00 29.23 o 10 5 0 45.09 35.77 15.00 o 11 5 0 26.06 31.66 16.76 o 12 5 0 239.05 293.24 21.77 o 13 5 0 7.54 0.48 16.59 o 14 5 0 190.35 211.57 26.30 o 0 6 0 6715.49 7624.45 152.42 o 1 6 0 6259.25 5079.32 74.44 o 2 6 0 13301.24 14427.82 403.39 o 3 6 0 12901.13 13498.89 260.68 o 4 6 0 443.74 343.00 10.59 o 5 6 0 9463.32 9389.04 140.63 o 6 6 0 547.47 471.25 13.88 o 7 6 0 96.82 93.12 10.01 o 8 6 0 1788.54 1733.60 29.51 o 9 6 0 0.36 0.78 13.61 o 10 6 0 719.46 743.79 26.62 o 11 6 0 162.92 158.15 19.53 o 12 6 0 117.53 112.89 22.68 o 13 6 0 580.63 622.33 30.81 o 14 6 0 68.48 45.40 24.18 o 1 7 0 4023.94 3556.05 45.63 o 2 7 0 15007.69 13515.15 314.50 o 3 7 0 1194.66 1339.96 26.94 o 4 7 0 2317.69 2292.77 34.89 o 5 7 0 1563.69 1582.25 24.31 o 6 7 0 2627.64 2639.99 40.39 o 7 7 0 279.62 253.85 11.97 o 8 7 0 89.30 81.26 10.89 o 9 7 0 7.03 28.02 10.63 o 10 7 0 278.27 269.82 18.11 o 11 7 0 409.03 418.27 29.23 o 12 7 0 3.31 10.74 17.01 o 13 7 0 35.84 38.34 21.10 o 14 7 0 115.66 152.06 25.72 o 0 8 0 4609.20 5282.49 110.89 o 1 8 0 3536.33 4010.62 54.77 o 2 8 0 10692.66 10202.26 213.54 o 3 8 0 336.27 264.93 34.46 o 4 8 0 426.23 388.63 12.32 o 5 8 0 915.59 818.26 19.44 o 6 8 0 1005.45 1026.04 20.05 o 7 8 0 1298.00 1331.51 31.90 o 8 8 0 888.97 903.88 19.87 o 9 8 0 45.29 47.74 11.58 o 10 8 0 209.49 257.25 25.54 o 11 8 0 417.91 453.96 26.93 o 12 8 0 2.78 9.57 17.44 o 13 8 0 68.46 91.31 20.94 o 14 8 0 41.64 77.30 27.23 o 1 9 0 10838.95 10032.73 173.55 o 2 9 0 3893.25 3529.73 59.96 o 3 9 0 1908.43 2001.55 49.71 o 4 9 0 2545.47 2315.38 33.29 o 5 9 0 2347.42 2410.36 37.62 o 6 9 0 4668.96 4863.60 91.18 o 7 9 0 450.07 370.50 16.69 o 8 9 0 5.03 19.35 11.64 o 9 9 0 699.06 810.68 31.68 o 10 9 0 64.26 77.07 15.03 o 11 9 0 746.24 810.88 39.07 o 12 9 0 174.61 218.21 27.83 o 13 9 0 5.81 0.00 26.30 o 0 10 0 102.61 28.57 9.45 o 1 10 0 722.96 522.43 14.48 o 2 10 0 218.59 226.24 12.58 o 3 10 0 388.71 407.14 18.91 o 4 10 0 129.23 167.60 9.99 o 5 10 0 178.28 132.49 9.61 o 6 10 0 27.20 50.98 9.81 o 7 10 0 20.43 10.81 12.60 o 8 10 0 131.55 130.20 12.72 o 9 10 0 164.75 179.80 15.85 o 10 10 0 290.46 305.44 20.41 o 11 10 0 9.88 0.00 22.80 o 12 10 0 17.33 20.78 24.64 o 13 10 0 190.63 179.26 29.50 o 1 11 0 4772.12 5037.30 81.83 o 2 11 0 62.89 63.06 11.23 o 3 11 0 304.12 263.47 14.86 o 4 11 0 3543.24 3401.71 64.53 o 5 11 0 332.24 357.30 12.81 o 6 11 0 1329.53 1314.50 30.98 o 7 11 0 858.94 887.33 31.33 o 8 11 0 13.94 0.00 11.78 o 9 11 0 850.50 995.93 37.34 o 10 11 0 621.33 687.39 28.40 o 11 11 0 43.26 27.23 21.31 o 12 11 0 88.73 121.30 25.99 o 13 11 0 9.80 17.31 25.14 o 0 12 0 3127.58 3228.66 67.29 o 1 12 0 2539.56 2800.87 58.17 o 2 12 0 1587.56 1305.33 29.89 o 3 12 0 926.68 789.43 29.25 o 4 12 0 671.98 717.33 19.05 o 5 12 0 1464.22 1278.77 28.50 o 6 12 0 1087.70 1113.28 26.31 o 7 12 0 1308.69 1394.27 44.13 o 8 12 0 1366.24 1446.61 36.07 o 9 12 0 24.90 29.91 13.54 o 10 12 0 1032.99 1105.85 43.45 o 11 12 0 316.18 395.70 33.97 o 12 12 0 80.73 90.64 27.61 o 13 12 0 476.46 625.68 54.41 o 1 13 0 915.79 833.81 32.72 o 2 13 0 263.91 244.16 15.96 o 3 13 0 348.82 462.17 20.06 o 4 13 0 276.44 226.64 20.60 o 5 13 0 425.80 448.61 21.58 o 6 13 0 13.93 4.13 13.47 o 7 13 0 128.65 111.80 16.41 o 8 13 0 27.14 26.74 12.97 o 9 13 0 67.39 74.82 20.25 o 10 13 0 59.89 58.17 16.85 o 11 13 0 120.99 130.82 20.66 o 12 13 0 40.72 65.17 31.07 o 13 13 0 0.38 0.00 28.60 o 0 14 0 925.09 815.12 39.52 o 1 14 0 251.24 259.05 22.89 o 2 14 0 129.60 99.45 12.69 o 3 14 0 4061.57 4228.26 91.71 o 4 14 0 1051.57 938.62 39.63 o 5 14 0 392.74 380.03 16.12 o 6 14 0 269.87 301.86 15.12 o 7 14 0 114.79 89.27 14.08 o 8 14 0 1333.65 1339.63 37.69 o 9 14 0 65.44 65.09 14.75 o 10 14 0 142.37 146.29 20.52 o 11 14 0 127.50 107.80 20.48 o 12 14 0 16.01 20.14 28.79 o 1 15 0 4923.15 4697.62 85.66 o 2 15 0 1863.81 1771.41 42.34 o 3 15 0 651.24 627.23 23.02 o 4 15 0 3248.75 3088.67 62.75 o 5 15 0 806.73 778.00 22.88 o 6 15 0 1611.55 1620.67 36.58 o 7 15 0 347.62 349.23 25.73 o 8 15 0 5.91 8.12 16.02 o 9 15 0 1071.07 1157.48 49.75 o 10 15 0 213.46 235.08 25.10 o 11 15 0 77.91 107.17 19.32 o 12 15 0 298.85 355.78 39.46 o 0 16 0 2030.78 1798.41 66.23 o 1 16 0 2157.03 2154.17 40.78 o 2 16 0 608.17 588.80 23.18 o 3 16 0 423.88 394.80 23.20 o 4 16 0 7.42 2.74 11.78 o 5 16 0 1091.38 967.48 23.88 o 6 16 0 696.30 717.25 30.13 o 7 16 0 4.46 0.00 11.66 o 8 16 0 3.44 0.00 14.83 o 9 16 0 72.77 62.56 20.03 o 10 16 0 68.60 86.97 25.39 o 11 16 0 12.47 36.96 23.99 o 12 16 0 18.04 40.96 34.76 o 1 17 0 752.09 671.63 23.52 o 2 17 0 22.34 32.62 14.16 o 3 17 0 598.12 628.16 25.99 o 4 17 0 571.35 589.54 26.54 o 5 17 0 358.35 359.04 20.74 o 6 17 0 502.18 544.40 22.03 o 7 17 0 94.67 88.87 13.67 o 8 17 0 0.08 0.00 16.57 o 9 17 0 544.07 595.91 36.10 o 10 17 0 91.23 77.60 17.15 o 11 17 0 1.34 0.00 17.22 o 12 17 0 28.14 10.26 19.57 o 0 18 0 215.58 207.31 22.17 o 1 18 0 727.03 708.83 25.27 o 2 18 0 4752.38 4733.55 119.35 o 3 18 0 620.27 583.29 29.71 o 4 18 0 96.68 89.91 20.04 o 5 18 0 1119.06 1081.89 36.74 o 6 18 0 329.84 334.38 16.57 o 7 18 0 1168.39 1136.53 32.23 o 8 18 0 720.59 789.86 27.45 o 9 18 0 129.36 98.60 24.92 o 10 18 0 705.46 739.89 69.80 o 11 18 0 107.69 117.43 26.51 o 1 19 0 755.69 801.36 29.01 o 2 19 0 184.00 193.78 20.00 o 3 19 0 77.87 74.84 17.93 o 4 19 0 1234.26 1190.86 46.85 o 5 19 0 17.26 19.66 14.99 o 6 19 0 60.03 51.25 12.82 o 7 19 0 609.91 540.13 21.34 o 8 19 0 139.94 110.67 16.43 o 9 19 0 85.31 59.50 20.64 o 10 19 0 53.52 41.89 19.75 o 11 19 0 52.24 45.28 24.56 o 0 20 0 642.40 626.85 43.37 o 1 20 0 69.74 43.16 17.08 o 2 20 0 109.77 99.55 18.73 o 3 20 0 908.03 879.54 35.58 o 4 20 0 173.33 135.24 20.93 o 5 20 0 126.97 138.64 22.30 o 6 20 0 26.50 38.57 12.31 o 7 20 0 22.86 30.14 13.51 o 8 20 0 5.10 4.38 14.87 o 9 20 0 18.45 23.16 19.83 o 10 20 0 51.18 53.75 16.10 o 11 20 0 4.97 3.81 23.57 o 1 21 0 266.18 273.32 22.57 o 2 21 0 1246.65 1255.12 56.22 o 3 21 0 615.77 661.63 43.80 o 4 21 0 653.92 660.07 38.88 o 5 21 0 29.65 30.02 21.00 o 6 21 0 25.88 10.46 14.64 o 7 21 0 502.50 577.16 27.02 o 8 21 0 256.44 223.91 23.72 o 9 21 0 422.88 441.20 34.80 o 10 21 0 26.51 15.01 19.64 o 0 22 0 522.91 617.09 78.10 o 1 22 0 0.41 0.00 14.94 o 2 22 0 467.32 440.00 28.67 o 3 22 0 512.91 523.87 30.87 o 4 22 0 126.65 142.40 29.14 o 5 22 0 35.27 50.39 19.90 o 6 22 0 3.09 2.35 14.87 o 7 22 0 31.44 22.21 14.27 o 8 22 0 100.33 95.72 16.00 o 9 22 0 1.72 2.95 21.96 o 10 22 0 81.94 68.55 30.27 o 1 23 0 162.70 154.57 19.99 o 2 23 0 49.45 70.27 20.83 o 3 23 0 341.95 385.98 29.62 o 4 23 0 16.32 14.96 20.41 o 5 23 0 101.13 69.90 31.70 o 6 23 0 106.09 87.20 16.81 o 7 23 0 78.22 66.28 15.64 o 8 23 0 23.34 33.23 15.61 o 9 23 0 28.33 32.93 15.54 o 0 24 0 823.65 956.22 99.44 o 1 24 0 528.27 506.43 32.86 o 2 24 0 15.02 0.00 19.34 o 3 24 0 1000.83 1060.16 54.29 o 4 24 0 282.33 224.21 32.09 o 5 24 0 536.79 563.20 31.68 o 6 24 0 54.70 66.55 16.35 o 7 24 0 159.39 145.73 18.03 o 8 24 0 224.26 179.77 19.72 o 9 24 0 30.98 26.24 24.24 o 1 25 0 43.82 26.09 27.87 o 2 25 0 177.38 169.60 29.96 o 3 25 0 7.00 0.00 20.65 o 4 25 0 425.59 403.69 38.92 o 5 25 0 97.12 61.83 21.01 o 6 25 0 3.55 10.98 15.44 o 7 25 0 15.46 23.85 15.99 o 8 25 0 7.69 3.82 16.35 o 0 26 0 239.18 242.37 35.95 o 1 26 0 11.97 5.23 24.19 o 2 26 0 39.08 70.68 27.59 o 3 26 0 42.58 5.96 21.67 o 4 26 0 12.35 22.61 23.19 o 5 26 0 152.94 169.17 28.13 o 6 26 0 14.14 8.75 16.10 o 7 26 0 0.30 0.00 17.14 o 1 27 0 512.43 566.18 53.34 o 2 27 0 20.68 59.63 27.84 o 3 27 0 1.30 0.00 25.88 o 4 27 0 593.38 691.34 63.43 o 5 27 0 5.47 11.61 24.96 o 6 27 0 89.88 78.07 22.39 o 0 28 0 10.39 41.90 46.57 o 1 28 0 0.15 0.00 26.30 o 2 28 0 11.06 0.00 26.43 o 3 28 0 19.69 0.00 32.90 o 4 28 0 40.09 40.88 30.86 o 5 28 0 32.25 32.88 24.30 o 1 29 0 126.18 103.71 37.34 o 2 29 0 28.56 0.00 24.26 o 3 29 0 11.96 77.98 28.46 o 4 29 0 12.31 0.00 29.13 o 0 30 0 130.68 306.85 103.52 o 1 30 0 71.67 123.41 56.62 o 2 30 0 321.10 301.60 36.46 o -14 1 1 83.95 64.70 23.61 o -13 1 1 30.95 30.55 20.96 o -12 1 1 583.11 597.48 47.12 o -11 1 1 7.57 0.00 18.65 o -10 1 1 858.46 934.17 53.67 o -9 1 1 1115.23 1135.14 41.86 o -8 1 1 96.91 179.47 18.69 o -7 1 1 691.57 591.64 18.21 o -6 1 1 782.04 858.12 20.44 o -5 1 1 4575.76 3789.34 50.36 o -4 1 1 4570.91 4133.16 66.02 o -3 1 1 267.20 194.09 9.54 o -2 1 1 1678.29 1168.51 13.91 o 1 1 1 301.24 254.73 5.55 o 2 1 1 2024.00 2002.57 20.55 o 3 1 1 4448.70 4684.57 47.13 o 4 1 1 9975.33 10328.97 137.54 o 5 1 1 1323.44 1340.66 22.65 o 6 1 1 2481.45 2397.83 44.11 o 7 1 1 2915.82 3046.75 60.03 o 8 1 1 696.53 826.80 31.24 o 9 1 1 717.30 750.16 25.89 o 10 1 1 135.01 150.48 18.54 o 11 1 1 520.43 543.16 26.65 o 12 1 1 137.94 138.28 21.53 o 13 1 1 0.90 12.38 18.85 o 14 1 1 113.79 105.14 21.89 o -14 2 1 210.92 181.02 46.87 o -13 2 1 159.60 172.35 36.36 o -12 2 1 45.43 21.54 18.28 o -11 2 1 1399.58 1312.87 40.62 o -10 2 1 1289.74 1505.71 39.66 o -9 2 1 930.84 911.63 45.22 o -8 2 1 2195.94 2029.76 42.31 o -7 2 1 3793.94 4233.25 71.72 o -6 2 1 949.70 689.09 27.35 o -5 2 1 365.09 238.32 11.66 o -4 2 1 3574.10 3436.32 41.59 o -3 2 1 51816.68 51796.70 1950.13 o -2 2 1 8916.21 7611.07 106.85 o -1 2 1 2948.79 2530.90 40.63 o 1 2 1 16.18 1.93 2.41 o 2 2 1 12371.66 10564.97 125.14 o 3 2 1 2431.31 1722.52 23.10 o 4 2 1 4964.23 5901.97 66.46 o 5 2 1 6307.94 6933.13 91.05 o 6 2 1 141.82 154.92 9.83 o 7 2 1 1411.79 1320.87 34.76 o 8 2 1 3570.87 3848.03 68.40 o 9 2 1 184.96 210.25 15.45 o 10 2 1 19.34 24.77 15.04 o 11 2 1 68.20 77.38 20.20 o 12 2 1 208.08 182.92 20.77 o 13 2 1 513.62 564.91 28.55 o 14 2 1 79.84 53.67 22.45 o -14 3 1 9.03 25.86 26.15 o -13 3 1 6.14 11.51 16.90 o -12 3 1 37.64 41.51 23.08 o -11 3 1 55.82 17.66 17.85 o -10 3 1 353.90 347.94 26.07 o -9 3 1 16.22 12.86 13.07 o -8 3 1 62.77 66.48 11.92 o -7 3 1 3563.45 4057.82 86.61 o -6 3 1 1014.08 905.12 29.97 o -5 3 1 193.44 239.36 16.96 o -4 3 1 30.34 16.65 4.96 o -3 3 1 7436.98 8344.23 118.08 o -2 3 1 3642.87 2743.06 34.70 o -1 3 1 17625.72 13450.92 222.15 o 0 3 1 6956.23 4435.42 47.20 o 1 3 1 9563.14 6706.10 127.43 o 2 3 1 2250.32 3182.84 29.15 o 3 3 1 233.59 421.96 15.02 o 4 3 1 5.29 19.97 6.29 o 5 3 1 0.02 20.53 7.03 o 6 3 1 674.37 730.51 20.03 o 7 3 1 1197.68 1233.42 32.09 o 8 3 1 34.43 44.82 13.04 o 9 3 1 2.27 0.00 12.73 o 10 3 1 641.41 597.35 23.16 o 11 3 1 13.84 0.41 16.84 o 12 3 1 162.16 117.49 20.47 o 13 3 1 41.84 66.54 21.25 o 14 3 1 0.12 10.44 20.61 o -14 4 1 114.69 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21.61 o 1 22 2 8.94 31.05 19.40 o 2 22 2 60.04 16.58 19.50 o 3 22 2 164.76 171.30 22.06 o 4 22 2 575.66 582.08 36.98 o 5 22 2 1.61 20.41 13.88 o 6 22 2 122.22 108.36 17.97 o 7 22 2 331.78 297.61 33.99 o 8 22 2 13.79 0.00 17.03 o -9 23 2 0.77 0.00 24.66 o -8 23 2 51.00 34.74 35.94 o -7 23 2 443.47 437.63 30.74 o -6 23 2 78.34 65.66 11.47 o -5 23 2 10.68 78.56 22.45 o -4 23 2 115.57 163.31 28.61 o -3 23 2 108.73 136.80 21.67 o -2 23 2 5.13 4.98 18.14 o -1 23 2 400.20 420.01 24.57 o 0 23 2 855.74 840.94 31.65 o 1 23 2 31.75 37.87 19.14 o 2 23 2 37.09 29.52 19.19 o 3 23 2 111.66 83.92 20.88 o 4 23 2 206.80 140.17 21.53 o 5 23 2 1.40 21.09 14.57 o 6 23 2 6.02 4.68 15.59 o 7 23 2 7.14 11.24 18.79 o 8 23 2 19.12 0.00 15.61 o -9 24 2 1.77 2.19 28.63 o -8 24 2 129.21 134.74 35.27 o -7 24 2 17.32 10.25 11.74 o -6 24 2 256.36 269.99 30.56 o -5 24 2 110.83 131.77 25.22 o -4 24 2 206.59 244.86 27.27 o -3 24 2 211.89 224.44 28.98 o -2 24 2 31.85 13.81 18.39 o -1 24 2 595.76 667.93 31.38 o 0 24 2 546.29 560.34 33.10 o 1 24 2 281.85 306.03 37.19 o 2 24 2 398.71 403.18 30.12 o 3 24 2 317.01 365.03 50.88 o 4 24 2 163.60 171.87 41.79 o 5 24 2 236.83 209.41 22.17 o 6 24 2 2.17 0.00 15.61 o 7 24 2 190.00 165.93 25.40 o -8 25 2 10.84 11.17 30.04 o -7 25 2 24.05 15.02 24.77 o -6 25 2 27.86 0.00 25.95 o -5 25 2 0.81 0.00 31.55 o -4 25 2 225.18 203.51 26.42 o -3 25 2 32.82 24.70 22.72 o -2 25 2 117.46 104.44 26.12 o -1 25 2 49.25 23.96 24.90 o 0 25 2 70.37 94.76 23.93 o 1 25 2 501.75 520.73 41.94 o 2 25 2 0.01 41.93 26.82 o 3 25 2 183.48 170.63 25.59 o 4 25 2 9.57 6.33 17.43 o 5 25 2 4.96 13.00 15.29 o 6 25 2 120.98 83.18 17.53 o 7 25 2 12.79 9.68 18.98 o -7 26 2 0.59 0.00 28.44 o -6 26 2 6.93 44.93 30.44 o -5 26 2 0.76 0.00 39.06 o -4 26 2 15.53 19.50 31.00 o -3 26 2 267.13 253.07 33.49 o -2 26 2 76.36 122.90 32.47 o -1 26 2 10.48 0.00 39.79 o 0 26 2 63.98 76.12 28.87 o 1 26 2 57.79 67.90 23.57 o 2 26 2 113.12 85.77 23.74 o 3 26 2 110.05 118.80 25.16 o 4 26 2 99.63 66.96 19.51 o 5 26 2 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28.08 22.57 o -13 1 3 143.13 110.41 44.53 o -12 1 3 1111.25 1122.57 42.79 o -11 1 3 154.33 174.55 17.00 o -10 1 3 2064.62 1943.84 120.77 o -9 1 3 21.34 2.30 13.31 o -8 1 3 289.21 231.71 28.30 o -7 1 3 4831.69 5097.36 128.83 o -6 1 3 10.64 22.72 12.84 o -5 1 3 706.62 618.90 21.64 o -4 1 3 4946.49 5139.21 80.65 o -3 1 3 3742.90 3692.39 49.99 o -2 1 3 198.89 166.45 22.62 o -1 1 3 5390.45 4765.78 58.56 o 0 1 3 22782.36 24104.50 516.27 o 1 1 3 4292.04 4984.13 46.23 o 2 1 3 803.02 799.10 9.53 o 3 1 3 1544.86 1455.20 18.49 o 4 1 3 2840.22 3091.17 45.67 o 5 1 3 4809.21 4973.97 62.47 o 6 1 3 1055.74 1097.46 22.17 o 7 1 3 783.40 926.75 24.71 o 8 1 3 3737.44 3867.42 68.87 o 9 1 3 203.62 238.74 19.27 o 10 1 3 0.94 0.00 14.80 o 11 1 3 601.51 749.76 31.38 o 12 1 3 17.11 39.10 19.82 o -15 2 3 1.19 8.95 21.73 o -14 2 3 329.78 291.61 39.15 o -13 2 3 62.90 61.89 22.55 o -12 2 3 141.63 97.38 21.93 o -11 2 3 1872.90 1979.65 52.11 o -10 2 3 979.02 1121.29 119.48 o -9 2 3 1033.94 1020.17 38.87 o -8 2 3 732.42 790.40 41.92 o -7 2 3 4885.54 4999.67 115.10 o -6 2 3 660.98 595.83 33.34 o -5 2 3 6819.33 7526.07 134.69 o -4 2 3 4618.34 4429.14 69.10 o -3 2 3 4835.33 4386.94 71.13 o -2 2 3 235.75 305.94 8.68 o -1 2 3 14895.23 15350.15 345.83 o 0 2 3 5149.44 5368.21 51.42 o 1 2 3 498.36 568.67 9.30 o 2 2 3 4703.87 5354.59 53.80 o 3 2 3 972.04 985.04 12.34 o 4 2 3 1368.26 1184.58 17.08 o 5 2 3 1470.88 1525.84 22.89 o 6 2 3 24.45 51.09 8.69 o 7 2 3 1760.15 1803.16 36.67 o 8 2 3 669.17 738.86 24.13 o 9 2 3 1365.13 1487.92 35.79 o 10 2 3 21.23 25.97 14.72 o 11 2 3 0.56 0.00 16.02 o 12 2 3 271.81 219.63 25.18 o -15 3 3 0.24 0.00 31.72 o -14 3 3 22.81 20.19 24.05 o -13 3 3 15.26 5.06 21.04 o -12 3 3 0.05 0.00 19.33 o -11 3 3 278.82 331.16 38.96 o -10 3 3 462.90 453.42 23.00 o -9 3 3 1676.94 1717.38 55.75 o -8 3 3 142.64 204.50 19.13 o -7 3 3 2030.98 2000.28 62.52 o -6 3 3 1157.96 1207.24 32.53 o -5 3 3 128.20 209.38 18.64 o -4 3 3 86.20 95.34 9.48 o -3 3 3 11.80 42.69 6.18 o -2 3 3 5704.43 4860.27 77.23 o -1 3 3 2420.17 2972.25 47.99 o 0 3 3 250.91 364.11 11.48 o 1 3 3 6978.71 8416.16 106.04 o 2 3 3 57.82 32.89 4.64 o 3 3 3 375.18 541.73 12.71 o 4 3 3 111.30 91.15 7.14 o 5 3 3 179.67 197.22 10.70 o 6 3 3 114.83 116.37 11.99 o 7 3 3 1.33 15.55 11.11 o 8 3 3 214.36 234.22 15.51 o 9 3 3 260.20 215.79 17.30 o 10 3 3 279.46 287.80 19.65 o 11 3 3 163.38 123.25 19.22 o 12 3 3 0.70 0.00 17.83 o -14 4 3 93.30 64.27 21.75 o -13 4 3 762.39 955.69 41.36 o -12 4 3 784.20 1019.02 75.73 o -11 4 3 132.48 107.36 22.19 o -10 4 3 28.82 26.66 12.11 o -9 4 3 1476.46 1495.56 61.74 o -8 4 3 1718.83 1828.44 34.22 o -7 4 3 104.30 193.15 15.68 o -6 4 3 8081.94 7788.02 160.18 o -5 4 3 1010.63 904.12 36.20 o -4 4 3 2544.62 2746.86 36.79 o -3 4 3 405.44 463.64 8.35 o -2 4 3 231.63 270.12 12.48 o -1 4 3 6264.33 5924.34 65.75 o 0 4 3 159.27 141.11 7.06 o 1 4 3 2212.10 2006.03 28.39 o 2 4 3 2801.36 2494.60 23.73 o 3 4 3 3643.51 4035.62 45.26 o 4 4 3 4317.91 4558.21 55.14 o 5 4 3 1314.66 1390.05 24.10 o 6 4 3 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