#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/67/2216761.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2216761_Fobs
loop_
_publ_author_name
'Boag, Neil M.'
'Ravetz, Megan S.'
_publ_section_title
;
 Di-\m-chlorido-bis[chlorido(\h^2^-ethene)platinum(II)]
;
_journal_coeditor_code           SI2052
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m3103
_journal_page_last               m3104
_journal_volume                  63
_journal_year                    2007
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                87.230
_cell_angle_beta                 75.462
_cell_angle_gamma                73.142
_cell_length_a                   6.6413
_cell_length_b                   10.1222
_cell_length_c                   12.2397
_exptl_crystal_F_000             768.00
_reflns_d_resolution_high        0.7681
_[local]_cod_data_source_file    si2052Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' MEGUNKC in P-1'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            425.82
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 3316.81 3561.47 63.96 o
2 0 0 1441.26 1219.79 45.48 o
3 0 0 52681.30 49978.34 462.46 o
4 0 0 32182.13 30368.10 439.27 o
5 0 0 1238.55 1161.77 86.53 o
6 0 0 2821.90 2720.40 117.42 o
7 0 0 2878.59 2977.64 139.34 o
8 0 0 814.51 827.80 148.73 o
-7 1 0 148.88 343.04 121.77 o
-6 1 0 285.02 340.78 105.65 o
-5 1 0 4082.86 3949.76 139.19 o
-4 1 0 6367.87 6080.46 152.04 o
-3 1 0 3310.98 3278.34 90.31 o
-2 1 0 5050.67 5034.86 109.44 o
-1 1 0 428.41 525.86 60.39 o
0 1 0 33913.28 27406.80 1011.79 o
1 1 0 25247.07 27500.30 438.95 o
2 1 0 7749.78 7733.87 143.61 o
3 1 0 4269.16 4109.54 89.35 o
4 1 0 57268.73 54423.47 562.63 o
5 1 0 3107.99 2776.82 109.04 o
6 1 0 673.75 505.38 91.08 o
7 1 0 7067.54 7000.92 186.88 o
8 1 0 82.88 220.49 129.83 o
-7 2 0 361.81 348.85 152.53 o
-6 2 0 17724.23 17119.32 347.68 o
-5 2 0 1090.64 1275.70 117.27 o
-4 2 0 7826.87 7788.79 183.96 o
-3 2 0 18643.09 19227.97 307.33 o
-2 2 0 35321.71 36654.26 552.87 o
-1 2 0 16041.23 16543.64 274.50 o
0 2 0 3621.13 3517.95 129.98 o
1 2 0 36788.41 46623.89 675.56 o
2 2 0 3700.67 3556.34 154.56 o
3 2 0 1762.53 1781.57 91.68 o
4 2 0 1620.15 1626.49 84.29 o
5 2 0 1040.50 1110.07 83.82 o
6 2 0 5931.50 6132.02 167.93 o
7 2 0 124.33 -46.87 103.72 o
8 2 0 466.68 497.57 129.48 o
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-6 3 0 5878.68 5135.90 225.30 o
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-4 3 0 3.53 -95.64 121.38 o
-3 3 0 1245.82 1080.56 115.79 o
-2 3 0 164928.69 174844.25 1510.93 o
-1 3 0 2904.87 2809.08 135.20 o
0 3 0 374.69 297.65 92.40 o
1 3 0 60094.76 58209.72 823.47 o
2 3 0 55582.49 67925.80 950.54 o
3 3 0 12808.42 11597.23 283.94 o
4 3 0 14094.76 14422.41 296.91 o
5 3 0 11876.48 12721.57 258.47 o
6 3 0 44.78 -111.01 111.01 o
7 3 0 851.38 802.14 128.37 o
8 3 0 1652.24 1670.41 151.12 o
-6 4 0 2022.95 2338.34 207.33 o
-5 4 0 109.05 301.93 149.81 o
-4 4 0 3131.68 2769.65 176.04 o
-3 4 0 1906.69 1752.43 152.80 o
-2 4 0 2960.79 2321.58 148.45 o
-1 4 0 5893.44 5650.25 188.79 o
0 4 0 60.12 119.95 141.17 o
1 4 0 2885.17 3002.51 178.82 o
2 4 0 52317.73 58864.45 975.35 o
3 4 0 6479.71 6619.24 276.00 o
4 4 0 444.39 561.08 186.39 o
5 4 0 14559.84 14124.52 350.63 o
6 4 0 61.54 71.45 147.89 o
7 4 0 5781.31 5465.95 214.87 o
8 4 0 2244.19 2682.04 181.96 o
-6 5 0 1632.00 1658.87 220.72 o
-5 5 0 4591.70 3808.90 229.72 o
-4 5 0 9280.25 7917.33 261.70 o
-3 5 0 11269.14 9383.01 274.93 o
-2 5 0 1190.55 1133.49 160.39 o
-1 5 0 34440.04 37370.19 614.68 o
0 5 0 14.63 232.45 169.39 o
1 5 0 5.41 254.66 161.71 o
2 5 0 20907.78 20315.96 437.64 o
3 5 0 3229.88 4313.69 267.29 o
4 5 0 3200.69 3752.50 272.91 o
5 5 0 282.10 -232.83 232.83 o
6 5 0 7.82 96.03 202.81 o
7 5 0 3877.13 3276.98 240.76 o
8 5 0 554.38 345.82 204.04 o
-6 6 0 389.06 -104.50 253.96 o
-5 6 0 440.39 381.15 214.01 o
-4 6 0 18188.85 14225.69 371.31 o
-3 6 0 1141.89 1170.79 198.40 o
-2 6 0 234.39 439.90 179.80 o
-1 6 0 25239.04 26766.72 542.33 o
0 6 0 16925.90 20372.56 1157.24 o
1 6 0 14257.86 18675.42 403.69 o
2 6 0 31794.37 34662.81 668.79 o
3 6 0 20695.38 21725.82 527.73 o
4 6 0 2349.72 2677.55 301.48 o
5 6 0 2066.40 1939.93 287.85 o
6 6 0 16367.65 15691.55 459.63 o
7 6 0 16.93 -250.05 250.05 o
8 6 0 35.45 225.86 248.52 o
-5 7 0 1778.62 1247.16 264.20 o
-4 7 0 150.51 26.89 220.88 o
-3 7 0 175.50 536.29 200.53 o
-2 7 0 2725.02 1999.59 238.73 o
-1 7 0 359.92 343.90 194.81 o
0 7 0 5569.09 6877.57 197.04 o
1 7 0 1685.48 1996.89 227.82 o
2 7 0 256.45 280.86 225.92 o
3 7 0 8209.46 10147.98 363.77 o
4 7 0 817.02 1175.90 307.91 o
5 7 0 10669.34 10474.04 415.57 o
6 7 0 7558.14 7148.44 380.59 o
7 7 0 566.92 717.80 307.79 o
8 7 0 3530.07 3366.79 364.98 o
-4 8 0 772.85 342.04 259.03 o
-3 8 0 10711.88 11248.95 370.58 o
-2 8 0 705.90 556.51 229.83 o
-1 8 0 5.71 64.15 224.32 o
0 8 0 25568.75 31346.44 814.32 o
1 8 0 2018.10 2268.82 250.94 o
2 8 0 56.93 181.31 240.85 o
3 8 0 5689.05 6681.72 341.38 o
4 8 0 2268.25 2251.94 312.52 o
5 8 0 1576.57 1963.40 324.22 o
6 8 0 1261.22 1998.48 319.88 o
7 8 0 18.35 202.04 333.02 o
-4 9 0 842.00 1032.28 289.01 o
-3 9 0 4445.80 3925.62 310.95 o
-2 9 0 2466.22 2762.29 284.39 o
-1 9 0 2478.47 2736.12 277.11 o
0 9 0 20826.72 24514.88 626.09 o
1 9 0 14365.75 16901.70 451.22 o
2 9 0 3596.52 4739.25 299.79 o
3 9 0 2966.32 4835.27 320.01 o
4 9 0 36626.29 42434.98 843.07 o
5 9 0 15.72 24.20 310.36 o
6 9 0 62.11 -256.59 329.96 o
7 9 0 5247.49 5528.75 470.27 o
-3 10 0 6.34 271.18 268.49 o
-2 10 0 0.71 -43.40 253.12 o
-1 10 0 28.63 -265.42 265.42 o
0 10 0 922.99 988.48 182.96 o
1 10 0 1102.21 1250.99 261.42 o
2 10 0 306.87 55.32 272.01 o
3 10 0 5003.80 6206.97 350.55 o
4 10 0 8163.39 10208.24 437.16 o
5 10 0 599.04 856.55 322.79 o
6 10 0 4733.92 4262.57 420.05 o
7 10 0 997.20 1382.14 397.42 o
-2 11 0 10063.58 10248.48 431.53 o
-1 11 0 521.20 621.71 282.42 o
0 11 0 325.18 472.53 189.76 o
1 11 0 8270.97 8922.78 393.81 o
2 11 0 4092.61 4444.28 329.81 o
3 11 0 47.46 -283.86 283.86 o
4 11 0 1444.92 970.88 329.91 o
5 11 0 1609.61 925.19 357.62 o
6 11 0 1396.07 1297.56 373.70 o
-1 12 0 4463.23 4745.64 339.77 o
0 12 0 625.52 751.46 203.37 o
1 12 0 2107.51 2316.85 315.04 o
2 12 0 23484.78 24507.38 630.87 o
3 12 0 4.62 337.63 301.14 o
4 12 0 57.17 376.44 313.06 o
5 12 0 8780.86 10187.54 473.27 o
2 13 0 2049.32 2491.21 316.93 o
3 13 0 303.83 -134.46 326.94 o
-3 -13 1 57.77 14.60 308.83 o
-2 -13 1 124.72 327.28 295.40 o
-5 -12 1 753.39 1159.03 366.23 o
-4 -12 1 8295.31 8877.63 433.01 o
-3 -12 1 86.75 912.69 286.17 o
-2 -12 1 231.43 870.90 307.72 o
-1 -12 1 15965.87 15588.16 469.50 o
0 -12 1 1547.60 1526.77 397.39 o
1 -12 1 24.93 587.69 289.62 o
-6 -11 1 522.58 851.85 370.79 o
-5 -11 1 626.58 934.93 320.48 o
-4 -11 1 3122.89 4094.91 339.54 o
-3 -11 1 2680.36 3340.25 330.22 o
-2 -11 1 763.51 1099.17 288.24 o
-1 -11 1 4270.76 5211.49 322.90 o
0 -11 1 9272.63 10316.78 279.42 o
1 -11 1 946.51 420.49 299.80 o
2 -11 1 48.33 73.75 301.53 o
-6 -10 1 935.78 566.53 362.44 o
-5 -10 1 1595.49 1819.69 309.56 o
-4 -10 1 977.44 895.63 320.97 o
-3 -10 1 8704.78 9319.29 404.93 o
-2 -10 1 1149.78 1510.17 271.43 o
-1 -10 1 172.00 109.10 261.23 o
0 -10 1 740.01 765.95 183.61 o
1 -10 1 170.97 -123.31 265.83 o
2 -10 1 738.63 310.14 282.08 o
3 -10 1 31.13 446.72 277.71 o
-7 -9 1 1577.42 1649.16 386.82 o
-6 -9 1 6848.05 7024.17 410.30 o
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-1 -9 1 1123.85 1655.98 264.91 o
0 -9 1 20649.46 26464.53 1481.98 o
1 -9 1 25743.82 33037.82 690.51 o
2 -9 1 1051.62 1093.66 262.55 o
3 -9 1 1277.26 672.41 307.18 o
4 -9 1 5583.49 5671.19 350.84 o
-7 -8 1 2104.68 1695.20 361.96 o
-6 -8 1 574.33 515.30 316.64 o
-5 -8 1 2141.33 2076.60 303.20 o
-4 -8 1 203.19 -284.29 284.29 o
-3 -8 1 6644.01 6936.77 344.75 o
-2 -8 1 12613.55 14502.39 403.59 o
-1 -8 1 1069.69 1650.31 244.55 o
0 -8 1 227.21 458.06 171.27 o
1 -8 1 32477.04 42188.43 809.32 o
2 -8 1 362.32 391.90 246.28 o
3 -8 1 876.80 1038.93 273.28 o
4 -8 1 9219.74 9768.93 369.20 o
-7 -7 1 2870.79 2800.01 312.52 o
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-1 -7 1 256.73 686.59 219.77 o
0 -7 1 665.91 984.60 157.00 o
1 -7 1 268.00 162.90 231.29 o
2 -7 1 408.83 771.57 235.54 o
3 -7 1 3446.11 4460.60 272.72 o
4 -7 1 4.10 480.90 236.61 o
5 -7 1 941.11 725.66 291.72 o
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0 -6 1 13760.38 16852.93 1293.16 o
1 -6 1 3296.11 4935.77 245.98 o
2 -6 1 27295.48 33779.01 614.06 o
3 -6 1 1112.27 893.17 235.69 o
4 -6 1 168.61 240.48 217.05 o
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-3 -5 1 474.62 405.47 199.08 o
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0 -5 1 483.05 821.57 128.82 o
1 -5 1 1399.97 1750.53 199.72 o
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3 -5 1 7227.94 7192.60 297.10 o
4 -5 1 6918.35 6157.55 268.54 o
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-5 -4 1 944.40 643.19 140.33 o
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-3 -4 1 113.21 126.39 140.60 o
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0 -4 1 4169.70 4515.61 341.34 o
1 -4 1 840.97 501.15 178.46 o
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3 -4 1 74.42 -15.75 165.95 o
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-8 -3 1 15.57 104.09 129.44 o
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-6 -3 1 1343.81 1396.25 119.98 o
-5 -3 1 722.59 880.60 96.48 o
-4 -3 1 20567.39 21038.74 352.01 o
-3 -3 1 66974.61 58737.08 830.93 o
-2 -3 1 23971.95 22734.33 405.16 o
-1 -3 1 8602.45 9152.92 254.64 o
0 -3 1 46557.87 57840.34 3598.33 o
1 -3 1 91.18 41.11 156.36 o
2 -3 1 3.00 741.32 156.33 o
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4 -3 1 2716.04 2563.96 180.25 o
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6 -3 1 6443.38 5555.18 257.05 o
7 -3 1 858.78 1039.60 202.16 o
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-5 -2 1 4708.09 4751.66 136.60 o
-4 -2 1 616.70 606.95 66.50 o
-3 -2 1 9008.83 8785.56 155.76 o
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-1 -2 1 40.35 137.14 104.10 o
0 -2 1 53449.52 67964.07 656.53 o
1 -2 1 9690.30 10043.20 272.72 o
2 -2 1 23131.77 19713.09 378.64 o
3 -2 1 17822.00 16940.26 341.76 o
4 -2 1 12586.29 12705.86 270.18 o
5 -2 1 8002.57 7785.57 225.55 o
6 -2 1 190.52 -156.35 156.35 o
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-6 -1 1 8501.52 8331.17 183.34 o
-5 -1 1 551.57 463.48 79.17 o
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0 -1 1 12525.33 11254.58 139.68 o
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-2 1 1 10477.02 10425.18 168.08 o
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1 1 1 39149.35 45553.52 344.05 o
2 1 1 19527.37 21440.56 427.54 o
3 1 1 20146.13 18847.92 294.13 o
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6 1 1 680.30 682.95 87.63 o
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8 1 1 7037.46 7283.83 217.27 o
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6 4 1 25917.43 22317.24 493.52 o
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8 4 1 1822.09 2036.37 188.45 o
-6 5 1 510.00 429.19 204.03 o
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-4 5 1 9752.43 9247.55 264.09 o
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