#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/68/2216817.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216817_Fobs loop_ _publ_author_name 'Srinivasan, Krishnan' 'Govindarajan, Subbaiah' 'Harrison, William T. A.' _publ_section_title ; Redetermination of tris(ethyl carbazate-\k^2^N,O)cobalt(II) dinitrate ; _journal_coeditor_code TK2213 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m3028 _journal_page_last m3029 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.244 _cell_angle_gamma 90.000 _cell_length_a 28.0291 _cell_length_b 8.6245 _cell_length_c 35.6763 _exptl_crystal_F_000 4112.00 _reflns_d_resolution_high 0.7688 _[local]_cod_data_source_file tk2213Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' KS20 SRINI SOTON DATA' _shelx_refln_list_code 4 _shelx_f_calc_maximum 518.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 122056.52 120810.88 2517.27 o 8 0 0 55041.73 52880.95 1149.51 o 10 0 0 1764.25 1515.39 52.55 o 12 0 0 21016.90 21016.92 405.49 o 14 0 0 7.03 51.30 27.62 o 16 0 0 7580.66 7135.94 185.06 o 18 0 0 6451.85 7109.21 230.63 o 20 0 0 21824.64 22278.54 454.53 o 22 0 0 3467.80 3860.42 145.96 o 24 0 0 19077.16 18946.49 620.54 o 26 0 0 146.78 69.66 59.01 o 28 0 0 475.68 571.62 175.89 o 30 0 0 195.72 201.53 107.29 o 32 0 0 79.77 -138.09 383.79 o 34 0 0 87.41 36.68 141.99 o 3 1 0 13.87 -9.77 9.77 o 4 1 0 138197.50 120806.55 2216.68 o 5 1 0 3835.45 3347.75 52.26 o 6 1 0 115222.54 114225.34 1675.11 o 7 1 0 1321.48 1013.34 30.23 o 8 1 0 20400.42 20631.96 305.89 o 9 1 0 404.54 427.74 21.47 o 10 1 0 676.17 767.00 38.46 o 11 1 0 184.88 209.82 16.32 o 12 1 0 21694.59 21532.14 309.90 o 13 1 0 1783.18 1647.07 76.59 o 14 1 0 4759.75 4857.58 93.13 o 15 1 0 274.07 366.83 35.39 o 16 1 0 33.86 156.18 26.21 o 17 1 0 5566.95 5589.34 107.49 o 18 1 0 10.99 22.01 20.70 o 19 1 0 5916.70 6038.07 135.95 o 20 1 0 12458.82 12005.46 219.98 o 21 1 0 240.46 222.29 45.82 o 22 1 0 12401.24 12805.42 359.41 o 23 1 0 1412.12 1342.32 63.86 o 24 1 0 1264.30 1123.68 72.50 o 25 1 0 1.64 -6.57 40.34 o 26 1 0 5371.38 5746.29 184.88 o 27 1 0 0.82 25.82 76.77 o 28 1 0 9292.31 10025.08 356.01 o 29 1 0 3.22 -43.15 73.05 o 30 1 0 1250.40 750.21 212.00 o 31 1 0 4.87 -107.71 159.19 o 32 1 0 110.52 125.68 83.56 o 33 1 0 117.65 133.51 89.03 o 34 1 0 942.07 749.73 288.65 o 1 2 0 661.04 625.20 14.93 o 3 2 0 523.56 492.04 14.70 o 4 2 0 21036.79 20449.44 300.52 o 5 2 0 8157.61 7556.96 107.52 o 6 2 0 136088.88 132492.17 1898.41 o 7 2 0 91.32 78.76 9.22 o 8 2 0 22876.74 24515.81 274.62 o 9 2 0 2286.50 2266.03 48.55 o 10 2 0 8299.62 7911.81 112.41 o 11 2 0 1.21 37.32 14.89 o 12 2 0 54.27 111.07 18.97 o 13 2 0 14684.38 14398.45 196.50 o 14 2 0 4321.83 4094.12 79.09 o 15 2 0 277.49 256.95 21.89 o 16 2 0 53.16 86.93 26.22 o 17 2 0 2695.47 2833.13 65.38 o 18 2 0 8271.67 7910.86 149.33 o 19 2 0 996.17 902.90 72.62 o 20 2 0 3287.12 3278.70 127.39 o 21 2 0 4052.12 3942.74 121.43 o 22 2 0 515.23 480.57 43.70 o 23 2 0 1516.30 1297.36 75.03 o 24 2 0 6568.10 6888.48 192.38 o 25 2 0 743.94 799.95 90.04 o 26 2 0 1981.31 1908.64 88.29 o 27 2 0 3449.05 3717.14 166.85 o 28 2 0 3141.30 3217.39 231.26 o 29 2 0 187.04 183.78 74.87 o 30 2 0 2939.51 2589.22 239.64 o 31 2 0 708.15 693.31 94.37 o 32 2 0 325.19 306.73 92.70 o 33 2 0 845.44 888.84 90.61 o 1 3 0 50.49 21.75 9.41 o 2 3 0 12092.44 10820.65 135.70 o 3 3 0 731.40 607.47 27.08 o 4 3 0 1981.86 2436.13 64.08 o 5 3 0 7.37 35.45 5.67 o 6 3 0 29877.99 27634.06 338.85 o 7 3 0 6625.50 5867.28 86.06 o 8 3 0 36895.38 37102.54 429.85 o 9 3 0 460.72 371.61 16.41 o 10 3 0 11277.90 11945.05 175.03 o 11 3 0 203.88 203.31 17.42 o 12 3 0 1208.46 1032.47 41.50 o 13 3 0 5709.50 5550.19 106.92 o 14 3 0 425.70 339.12 28.98 o 15 3 0 5376.31 5335.59 146.96 o 16 3 0 8610.86 9279.61 199.10 o 17 3 0 1381.60 1385.07 77.17 o 18 3 0 2016.03 1807.02 67.77 o 19 3 0 518.20 485.34 41.69 o 20 3 0 65.11 95.90 40.92 o 21 3 0 2477.75 2448.28 83.76 o 22 3 0 5947.44 5940.50 186.83 o 23 3 0 135.58 143.83 56.70 o 24 3 0 1109.95 1215.28 75.15 o 25 3 0 879.14 952.31 84.29 o 26 3 0 7052.53 6615.57 253.19 o 27 3 0 502.74 576.92 66.01 o 28 3 0 2334.13 2127.19 124.32 o 29 3 0 157.14 89.05 67.20 o 30 3 0 6.27 39.26 76.24 o 31 3 0 15.98 121.72 87.80 o 32 3 0 415.16 455.85 79.52 o 0 4 0 9695.98 7958.98 178.12 o 1 4 0 48.29 44.75 11.75 o 2 4 0 11943.28 11413.44 167.41 o 3 4 0 31.61 34.75 17.42 o 4 4 0 41987.22 41558.82 595.27 o 5 4 0 1125.09 1094.74 37.04 o 6 4 0 55457.30 55109.92 803.85 o 7 4 0 25.13 19.77 23.10 o 8 4 0 2767.64 2711.08 67.25 o 9 4 0 42.73 63.99 17.16 o 10 4 0 636.60 784.84 26.93 o 11 4 0 223.43 205.78 19.30 o 12 4 0 14558.14 15132.00 239.56 o 13 4 0 2190.43 2348.82 60.48 o 14 4 0 462.52 483.45 40.05 o 15 4 0 2699.51 2708.56 94.78 o 16 4 0 133.13 74.26 35.99 o 17 4 0 1516.42 1533.15 66.95 o 18 4 0 1102.35 1137.30 67.26 o 19 4 0 1396.71 1375.72 87.67 o 20 4 0 2371.50 2415.42 97.18 o 21 4 0 240.79 194.78 42.63 o 22 4 0 13.91 12.04 47.08 o 23 4 0 1315.99 1396.88 74.00 o 24 4 0 1551.84 1816.31 103.10 o 25 4 0 24.37 70.15 50.83 o 26 4 0 1148.34 1220.52 99.09 o 27 4 0 2450.93 2266.96 99.50 o 28 4 0 1428.61 1642.69 95.66 o 29 4 0 361.13 307.42 61.52 o 30 4 0 1154.29 991.39 92.89 o 31 4 0 290.64 258.11 66.26 o 1 5 0 12.97 19.04 13.22 o 2 5 0 42602.38 40515.48 495.39 o 3 5 0 1925.05 1909.61 55.81 o 4 5 0 20972.50 19823.60 283.47 o 5 5 0 135.12 139.53 34.20 o 6 5 0 183.37 356.21 29.72 o 7 5 0 17.80 41.40 23.66 o 8 5 0 5180.67 5131.25 102.91 o 9 5 0 559.36 504.93 39.81 o 10 5 0 5976.85 6200.29 130.48 o 11 5 0 99.32 74.14 23.28 o 12 5 0 625.00 578.07 37.06 o 13 5 0 1467.77 1509.10 73.60 o 14 5 0 12397.82 12701.94 285.48 o 15 5 0 24.49 55.83 27.72 o 16 5 0 3266.31 3104.27 86.38 o 17 5 0 618.97 616.26 55.30 o 18 5 0 64.21 98.73 58.67 o 19 5 0 169.94 72.90 37.08 o 20 5 0 5672.12 5673.73 193.78 o 21 5 0 1990.58 1861.60 91.69 o 22 5 0 4583.14 4299.28 154.99 o 23 5 0 757.87 589.59 76.01 o 24 5 0 36.16 35.71 62.43 o 25 5 0 4623.68 4900.90 223.48 o 26 5 0 2137.87 2307.68 122.88 o 27 5 0 8.38 -32.22 69.70 o 28 5 0 1951.03 1820.33 177.57 o 29 5 0 199.38 162.46 93.81 o 30 5 0 72.05 221.98 82.96 o 0 6 0 7779.51 6851.59 190.39 o 1 6 0 3.40 7.19 14.30 o 2 6 0 2298.02 2266.77 66.20 o 3 6 0 154.80 154.67 31.84 o 4 6 0 16995.55 16938.00 251.89 o 5 6 0 135.52 180.77 50.47 o 6 6 0 12532.09 12303.80 235.70 o 7 6 0 40.04 -11.95 36.11 o 8 6 0 3534.52 3715.65 102.98 o 9 6 0 46.21 81.56 28.89 o 10 6 0 2875.71 3058.00 109.90 o 11 6 0 17.92 79.29 39.14 o 12 6 0 1584.22 1861.48 87.59 o 13 6 0 457.23 466.80 42.88 o 14 6 0 3324.64 3536.08 115.49 o 15 6 0 1172.40 1249.19 106.01 o 16 6 0 78.06 138.10 87.46 o 17 6 0 238.25 323.31 51.88 o 18 6 0 2106.72 2219.65 169.89 o 19 6 0 1857.15 1856.27 200.48 o 20 6 0 996.32 1073.70 113.55 o 21 6 0 349.04 349.36 145.14 o 22 6 0 243.77 355.64 99.83 o 23 6 0 1175.31 1367.99 139.41 o 24 6 0 2789.19 2826.41 158.60 o 25 6 0 86.05 -16.20 75.48 o 26 6 0 1112.26 918.03 119.81 o 27 6 0 1229.32 1313.80 151.59 o 28 6 0 384.00 213.36 123.62 o 1 7 0 2243.07 2261.41 76.43 o 2 7 0 52161.34 52966.99 924.56 o 3 7 0 871.75 841.73 55.24 o 4 7 0 1162.28 1275.82 75.54 o 5 7 0 594.36 499.21 66.04 o 6 7 0 15123.99 15451.09 332.83 o 7 7 0 621.46 782.05 54.88 o 8 7 0 13347.20 13874.71 289.39 o 9 7 0 2639.31 2720.73 157.63 o 10 7 0 2367.05 2405.60 149.70 o 11 7 0 2360.40 2466.35 95.50 o 12 7 0 47.11 129.19 56.05 o 13 7 0 1229.26 1154.74 69.98 o 14 7 0 324.68 290.51 62.54 o 15 7 0 1636.31 1570.12 112.17 o 16 7 0 1767.56 1728.61 153.03 o 17 7 0 1909.42 2028.60 177.07 o 18 7 0 1304.99 1513.06 91.34 o 19 7 0 295.91 312.55 66.34 o 20 7 0 880.70 876.03 168.43 o 21 7 0 485.21 695.52 92.16 o 22 7 0 1518.79 1154.24 237.18 o 23 7 0 140.70 111.20 83.58 o 24 7 0 30.31 -35.12 90.03 o 25 7 0 4094.75 4023.19 259.26 o 26 7 0 435.10 471.13 113.34 o 0 8 0 9734.58 9990.19 523.81 o 1 8 0 2.49 46.41 56.82 o 2 8 0 448.99 628.99 82.96 o 3 8 0 2464.52 2641.91 155.64 o 4 8 0 9736.27 10163.68 297.78 o 5 8 0 1692.56 1615.18 96.61 o 6 8 0 2613.61 2773.39 139.87 o 7 8 0 13.90 18.50 52.29 o 8 8 0 461.62 456.27 74.48 o 9 8 0 2587.70 2585.25 112.63 o 10 8 0 10202.50 10280.19 333.61 o 11 8 0 1103.71 1149.87 105.67 o 12 8 0 4635.35 4486.58 150.51 o 13 8 0 74.30 98.48 82.85 o 14 8 0 1233.76 1268.64 89.27 o 15 8 0 526.10 431.59 105.59 o 16 8 0 56.53 0.25 123.52 o 17 8 0 261.99 372.71 69.78 o 18 8 0 65.23 83.41 59.75 o 19 8 0 564.46 627.96 74.16 o 20 8 0 496.83 637.46 84.81 o 21 8 0 150.22 84.16 124.21 o 22 8 0 63.74 75.82 95.25 o 23 8 0 565.64 616.71 113.87 o 1 9 0 50.77 41.70 99.28 o 2 9 0 2836.13 3104.10 172.82 o 3 9 0 5.04 125.75 120.09 o 4 9 0 1691.19 1721.86 270.78 o 5 9 0 662.89 728.18 86.46 o 6 9 0 7063.76 7150.41 323.78 o 7 9 0 0.14 -45.06 82.09 o 8 9 0 21157.07 20765.74 531.51 o 9 9 0 664.55 604.74 147.60 o 10 9 0 1244.03 1380.30 152.40 o 11 9 0 0.44 -12.44 79.99 o 12 9 0 3435.00 3152.69 128.96 o 13 9 0 139.66 169.96 61.69 o 14 9 0 1772.03 1722.92 115.62 o 15 9 0 525.57 443.78 93.31 o 16 9 0 1659.92 1466.88 208.52 o 17 9 0 826.19 734.33 111.79 o 18 9 0 14.71 -2.17 142.58 o 19 9 0 1334.79 1372.78 123.01 o 20 9 0 1164.61 1173.09 146.03 o 0 10 0 2241.10 2739.14 246.60 o 1 10 0 133.86 25.26 85.41 o 2 10 0 124.37 70.42 201.48 o 3 10 0 5.51 -86.86 133.08 o 4 10 0 1460.93 1074.67 147.36 o 5 10 0 327.26 295.88 180.72 o 7 10 0 0.94 52.15 130.91 o 8 10 0 22.13 -2.18 128.96 o 9 10 0 87.38 82.25 88.09 o 10 10 0 1792.30 2026.96 186.71 o 11 10 0 1267.43 1558.59 183.35 o 12 10 0 89.00 215.75 100.79 o 13 10 0 578.50 618.72 132.62 o 14 10 0 3.85 207.08 132.70 o 15 10 0 882.61 978.04 119.02 o 1 11 0 26.62 86.50 119.58 o 2 11 0 377.21 396.73 187.72 o 3 11 0 284.55 388.81 291.35 o 4 11 0 1049.10 1259.96 331.59 o 5 11 0 146.07 245.58 179.75 o -33 0 1 2646.16 2542.42 256.12 o -31 0 1 5812.88 6516.90 411.65 o -29 0 1 4344.34 4595.52 483.70 o -27 0 1 559.18 736.86 111.44 o -25 0 1 12330.89 12929.08 529.26 o -23 0 1 1538.96 1250.03 93.75 o -21 0 1 2137.33 2121.55 100.84 o -19 0 1 262.67 160.80 46.90 o -17 0 1 1055.20 901.12 76.74 o -15 0 1 11004.87 11018.96 240.01 o -13 0 1 25255.27 24200.60 482.18 o -11 0 1 1517.53 1534.02 50.99 o -9 0 1 3169.37 3114.58 82.64 o -7 0 1 2618.21 2473.94 107.53 o -5 0 1 3865.04 3643.98 98.57 o 5 0 1 959.70 950.10 32.57 o 7 0 1 1556.75 1354.08 75.75 o 9 0 1 2380.18 2563.73 70.60 o 11 0 1 6345.89 6295.43 155.56 o 13 0 1 2336.53 2335.86 75.61 o 15 0 1 6907.22 6460.15 159.15 o 17 0 1 3142.74 3058.21 114.00 o 19 0 1 13070.46 13189.89 382.41 o 21 0 1 10984.52 10110.23 280.14 o 23 0 1 22032.63 21236.31 567.84 o 25 0 1 7560.81 7918.09 341.74 o 27 0 1 8105.73 8478.95 407.97 o 29 0 1 5004.93 4862.61 378.39 o 31 0 1 51.04 31.95 112.96 o 33 0 1 1684.98 1800.28 189.87 o -34 1 1 117.65 -25.38 106.71 o -33 1 1 1668.61 1499.67 125.30 o -32 1 1 0.66 5.83 93.31 o -31 1 1 2232.23 2606.73 157.27 o -30 1 1 236.97 326.32 75.80 o -29 1 1 3303.21 3536.56 147.19 o -28 1 1 178.50 293.11 66.96 o -27 1 1 10152.79 10677.77 334.39 o -26 1 1 15.03 12.12 75.47 o -25 1 1 1077.81 1144.46 79.79 o -24 1 1 1069.89 1142.03 66.95 o -23 1 1 228.63 353.25 42.10 o -22 1 1 1655.31 1693.49 89.79 o -21 1 1 257.88 286.95 36.46 o -20 1 1 231.84 236.00 41.71 o -19 1 1 53.71 10.93 36.26 o -18 1 1 1724.52 1878.36 90.30 o -17 1 1 15490.70 15387.08 214.37 o -16 1 1 2105.17 1929.66 65.42 o -15 1 1 3136.45 3174.59 67.76 o -14 1 1 5457.00 5895.53 96.69 o -13 1 1 7660.60 7120.75 120.54 o -12 1 1 5114.12 5285.45 89.68 o -11 1 1 619.29 493.83 26.09 o -10 1 1 5656.64 5306.58 89.29 o -9 1 1 427.95 429.45 19.73 o -8 1 1 6275.55 6002.04 93.40 o -7 1 1 27286.14 26408.65 349.54 o -6 1 1 449.14 455.55 17.56 o -5 1 1 1488.13 1482.17 27.26 o -4 1 1 134.75 130.91 10.31 o -3 1 1 2030.99 1736.34 58.09 o 2 1 1 186.84 153.39 15.31 o 3 1 1 1282.52 1109.89 36.35 o 4 1 1 5527.61 5280.18 77.93 o 5 1 1 703.41 551.66 21.02 o 6 1 1 3137.25 3076.36 54.46 o 7 1 1 145.49 213.17 13.18 o 8 1 1 1415.04 1595.59 36.25 o 9 1 1 1179.41 1090.05 30.47 o 10 1 1 17717.24 18367.91 246.17 o 11 1 1 10.69 29.81 13.64 o 12 1 1 38081.19 37750.98 492.59 o 13 1 1 12066.25 11817.70 194.43 o 14 1 1 10586.76 10798.59 178.53 o 15 1 1 6139.60 6258.02 137.62 o 16 1 1 372.16 454.83 29.44 o 17 1 1 16868.79 16571.27 235.80 o 18 1 1 7420.99 7325.55 130.19 o 19 1 1 3470.49 3395.67 95.79 o 20 1 1 64.12 105.59 30.55 o 21 1 1 17419.77 17621.71 278.14 o 22 1 1 8205.52 8283.85 175.83 o 23 1 1 6745.35 6792.36 182.53 o 24 1 1 696.40 636.16 81.84 o 25 1 1 1724.97 1862.08 119.50 o 26 1 1 2583.38 2321.29 165.86 o 27 1 1 12669.62 12978.14 341.25 o 28 1 1 318.52 376.76 72.20 o 29 1 1 278.76 355.92 71.54 o 30 1 1 224.55 346.99 78.21 o 31 1 1 1811.13 1623.01 224.97 o 32 1 1 649.63 723.73 105.55 o 33 1 1 2.16 85.84 99.84 o -33 2 1 6265.51 5799.51 338.28 o -32 2 1 26.09 -33.66 67.40 o -31 2 1 113.75 116.10 80.50 o -30 2 1 173.89 173.40 78.92 o -29 2 1 5709.36 6193.80 197.50 o -28 2 1 49.40 69.35 51.76 o -27 2 1 411.51 327.16 181.08 o -26 2 1 3.55 14.06 69.48 o -25 2 1 287.10 362.31 71.89 o -24 2 1 158.94 213.87 50.35 o -23 2 1 25.08 16.70 43.66 o -22 2 1 1395.21 1511.40 90.43 o -21 2 1 896.55 904.84 53.23 o -20 2 1 1639.92 1673.48 96.31 o -19 2 1 3762.77 4129.87 110.62 o -18 2 1 1412.17 1581.41 56.60 o -17 2 1 5360.07 5340.54 120.69 o -16 2 1 127.11 190.74 25.55 o -15 2 1 3430.62 3476.78 76.69 o -14 2 1 2.73 14.44 22.64 o -13 2 1 40321.85 38931.58 494.42 o -12 2 1 5547.78 5823.08 90.96 o -11 2 1 259.76 413.11 26.89 o -10 2 1 151.89 211.33 28.08 o -9 2 1 5103.46 4672.90 65.25 o -8 2 1 1444.06 1281.56 32.14 o -7 2 1 7208.13 7066.05 82.97 o -6 2 1 23147.18 21418.09 253.84 o -5 2 1 33.13 17.47 9.75 o -4 2 1 41653.76 40803.48 561.71 o -3 2 1 608.58 627.72 21.46 o -2 2 1 4656.59 4909.47 87.45 o -1 2 1 288.28 275.24 10.00 o 0 2 1 38427.71 39179.79 635.33 o 1 2 1 26.81 39.72 6.53 o 2 2 1 21689.25 22178.65 351.42 o 3 2 1 74.74 -7.79 7.79 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608.04 450.87 105.06 o -14 0 44 10793.15 11601.50 476.39 o -12 0 44 562.33 496.93 116.14 o -10 0 44 8473.30 8711.36 371.98 o -8 0 44 177.33 151.21 286.72 o -6 0 44 13177.60 13461.20 649.29 o -4 0 44 13511.07 13713.65 655.06 o -2 0 44 6606.70 6820.60 342.96 o -22 1 44 905.08 945.79 295.98 o -21 1 44 95.42 51.41 110.35 o -20 1 44 1251.24 1026.95 145.78 o -19 1 44 31.28 46.51 81.65 o -18 1 44 1262.44 1063.88 93.07 o -17 1 44 261.94 328.58 112.16 o -16 1 44 7605.57 7294.96 304.06 o -15 1 44 1052.99 1152.58 127.36 o -14 1 44 272.50 214.99 94.36 o -13 1 44 13.80 141.04 93.16 o -12 1 44 9201.88 9053.29 225.90 o -11 1 44 65.91 72.72 82.75 o -10 1 44 1734.01 1567.98 150.69 o -9 1 44 355.95 261.07 97.10 o -8 1 44 2478.17 2421.44 155.65 o -7 1 44 273.68 128.81 102.12 o -6 1 44 3913.88 3666.20 161.04 o -5 1 44 274.61 206.36 86.42 o -4 1 44 5.31 52.89 94.42 o -3 1 44 13.02 26.27 105.77 o -2 1 44 1113.41 1136.26 109.40 o -20 2 44 1366.85 1410.70 218.35 o -19 2 44 78.55 125.65 109.93 o -18 2 44 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317.06 o -7 0 45 3981.65 4412.79 524.84 o -5 0 45 1359.24 1119.89 148.79 o -19 1 45 510.61 607.73 96.79 o -18 1 45 153.64 201.41 106.26 o -17 1 45 620.54 715.47 100.10 o -16 1 45 272.62 279.16 75.60 o -15 1 45 770.45 579.99 147.79 o -14 1 45 1536.70 1508.92 126.75 o -13 1 45 321.07 293.23 105.88 o -12 1 45 395.63 589.37 114.12 o -11 1 45 374.17 336.34 86.04 o -10 1 45 14.06 86.75 85.31 o -9 1 45 3261.26 3018.29 203.70 o -8 1 45 851.01 736.82 120.85 o -7 1 45 375.67 182.09 155.43 o -6 1 45 129.04 81.59 132.36 o -5 1 45 808.65 617.10 138.27 o -17 2 45 249.00 462.42 168.84 o -16 2 45 18.73 -58.06 139.85 o -15 2 45 635.26 611.86 116.72 o -14 2 45 389.21 288.57 83.57 o -13 2 45 505.37 453.98 83.16 o -12 2 45 390.52 160.28 83.93 o -11 2 45 390.26 408.30 122.37 o -10 2 45 3.88 104.48 104.56 o -9 2 45 7.69 19.36 103.63 o -8 2 45 142.61 243.69 96.08 o -7 2 45 1684.76 1610.00 248.66 o -16 0 46 195.57 543.04 211.06 o -14 0 46 2593.59 2740.62 240.30 o -12 0 46 371.77 148.56 215.76 o -10 0 46 276.10 67.86 203.35 o -15 1 46 454.06 547.06 187.89 o -14 1 46 848.32 940.97 97.47 o -13 1 46 182.24 106.16 86.19 o -12 1 46 546.22 449.30 97.51 o -11 1 46 546.13 456.46 133.42 o