#------------------------------------------------------------------------------
#$Date: 2016-04-03 01:47:52 +0300 (Sun, 03 Apr 2016) $
#$Revision: 181097 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/77/2217763.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2217763_Fobs
loop_
_publ_author_name
'Lee, Chi-Shen'
'Weng, Sheng-Feng'
_publ_section_title
;
 A quaternary germanium(II) phosphate, Na[Ge~4~(PO~4~)~3~]
;
_journal_coeditor_code           FI2055
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i17
_journal_volume                  64
_journal_year                    2008
_space_group_IT_number           161
_symmetry_space_group_name_Hall  'R 3 -2"c'
_symmetry_space_group_name_H-M   'R 3 c :H'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                120.000
_cell_length_a                   9.3766
_cell_length_b                   9.3766
_cell_length_c                   23.4805
_exptl_crystal_F_000             1680.00
_reflns_d_resolution_high        0.7500
_cod_data_source_file            fi2055Isup2.hkl
_cod_data_source_block           I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' dd161final06 in R3c'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            702.56
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'-y, -x, z+1/2'
'-x+y, y, z+1/2'
'x, x-y, z+1/2'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'-y+2/3, -x+1/3, z+5/6'
'-x+y+2/3, y+1/3, z+5/6'
'x+2/3, x-y+1/3, z+5/6'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'-y+1/3, -x+2/3, z+7/6'
'-x+y+1/3, y+2/3, z+7/6'
'x+1/3, x-y+2/3, z+7/6'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
-4 10 -14 3751.46 3214.73 1412.87 o
-6 11 -14 507.14 782.09 786.69 o
-9 10 -13 1547.55 974.29 1165.46 o
-6 10 -13 8233.08 5353.97 1538.61 o
-5 11 -13 1497.85 2295.14 1258.49 o
-3 9 -12 6392.07 3887.43 1094.92 o
-8 10 -12 10882.80 6818.47 1773.75 o
-5 10 -12 7076.87 6931.43 1540.66 o
-7 11 -12 5210.11 2635.58 1225.27 o
-7 10 -11 14711.20 12885.00 2136.17 o
-4 10 -11 7698.27 7516.72 1553.44 o
-6 11 -11 1622.97 142.10 1117.92 o
-7 9 -10 3181.15 3143.17 1344.88 o
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-9 10 -10 1259.88 232.21 789.45 o
-6 10 -10 3991.97 3032.76 1096.45 o
-8 11 -10 4474.28 3740.66 1461.70 o
-5 11 -10 2880.08 2799.67 1447.12 o
-6 9 -9 645.17 543.88 855.18 o
-3 9 -9 5479.07 4737.50 1207.89 o
-8 10 -9 2357.70 1425.50 840.14 o
-5 10 -9 11406.10 8623.91 1664.87 o
-7 11 -9 1785.09 2070.28 948.64 o
-1 7 -8 25643.83 29481.08 1883.14 o
-3 8 -8 11720.04 8904.03 1398.04 o
-8 9 -8 9324.86 7359.47 1255.51 o
-5 9 -8 10934.52 7763.10 1467.05 o
-10 10 -8 8015.94 6623.20 1953.17 o
-7 10 -8 5184.10 4921.75 2290.80 o
-4 10 -8 675.25 1494.71 782.50 o
-9 11 -8 706.65 199.70 1075.20 o
-6 11 -8 7233.12 7745.72 2259.36 o
-1 6 -7 32646.99 45561.91 1914.32 o
-5 8 -7 10070.29 7828.02 1494.65 o
-2 8 -7 3786.66 5994.96 1954.71 o
-7 9 -7 176.51 641.91 641.85 o
-4 9 -7 3047.50 2486.32 1256.45 o
-9 10 -7 541.53 108.22 874.79 o
-6 10 -7 4036.22 2647.76 919.59 o
-3 10 -7 3727.34 8055.49 1389.35 o
-8 11 -7 1975.08 2530.05 1078.00 o
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-7 12 -7 2669.48 3411.16 1010.34 o
-1 5 -6 100754.17 109815.69 3471.34 o
0 6 -6 17244.45 24825.37 1422.58 o
-2 7 -6 5252.44 4288.70 979.91 o
-7 8 -6 12418.47 11404.76 1370.98 o
-4 8 -6 17152.18 12664.18 1583.60 o
-1 8 -6 13586.30 16658.44 1267.18 o
-9 9 -6 18992.21 19299.13 2442.87 o
-6 9 -6 18962.42 17394.73 1585.81 o
-3 9 -6 31081.60 35569.09 2235.34 o
-8 10 -6 19593.71 20727.87 1997.05 o
-5 10 -6 10888.63 10525.96 1920.97 o
-10 11 -6 8991.89 7582.15 2133.61 o
-7 11 -6 385.77 -1015.18 1546.28 o
-4 11 -6 2184.06 4976.73 1575.42 o
-6 12 -6 3372.29 6478.54 1891.83 o
-1 4 -5 15035.95 12463.29 700.30 o
-2 6 -5 12085.04 12806.38 1051.84 o
-4 7 -5 33754.64 35432.61 2543.57 o
-1 7 -5 3638.37 4548.37 842.92 o
-6 8 -5 8216.86 6000.19 2316.61 o
-3 8 -5 19314.37 18733.78 2099.37 o
-8 9 -5 2604.08 2757.44 1046.03 o
-5 9 -5 2724.55 3749.34 1221.18 o
-2 9 -5 4602.27 5681.12 992.69 o
-7 10 -5 15455.07 12333.20 1685.32 o
-4 10 -5 10269.89 14737.11 4992.06 o
-9 11 -5 742.02 531.61 1353.57 o
-6 11 -5 738.88 1059.77 614.42 o
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-5 12 -5 15052.68 32213.28 3014.87 o
0 4 -4 4437.51 6749.69 2170.16 o
-2 5 -4 10457.54 15829.84 634.87 o
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-1 6 -4 23442.59 30582.93 4076.31 o
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0 7 -4 13542.48 15787.41 1039.72 o
-8 8 -4 35004.74 29622.68 2639.67 o
-5 8 -4 2791.49 1991.59 738.08 o
-2 8 -4 5529.63 5682.14 966.11 o
-7 9 -4 5818.41 9347.19 1560.80 o
-4 9 -4 4474.45 5045.54 2081.99 o
-9 10 -4 5934.97 5914.21 2077.39 o
-6 10 -4 3032.19 2361.59 1626.54 o
-3 10 -4 494.84 1063.74 810.71 o
-8 11 -4 7420.63 7444.13 2506.25 o
-5 11 -4 6503.69 6844.97 1100.70 o
-7 12 -4 351.42 631.80 990.64 o
-1 5 -3 109920.67 118886.60 6191.22 o
-3 6 -3 4420.51 4823.64 548.74 o
-5 7 -3 20215.31 19611.90 2020.90 o
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-1 8 -3 15744.75 19232.68 1377.09 o
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-3 9 -3 3884.37 4462.42 1522.77 o
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-4 11 -3 2301.98 4651.63 1610.18 o
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0 2 -2 471205.16 511158.47 13627.73 o
-2 3 -2 40699.74 54134.19 1550.37 o
-1 4 -2 187.26 381.65 126.55 o
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-2 9 -2 22953.23 27698.13 1857.07 o
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-3 11 -2 12364.97 11515.07 1367.88 o
-8 12 -2 3972.61 6585.37 1682.76 o
-5 12 -2 1408.78 1408.78 894.54 o
-1 3 -1 79972.33 86515.98 5206.89 o
-3 4 -1 13858.31 18271.73 2454.63 o
-2 5 -1 44464.60 57970.11 5186.31 o
-4 6 -1 8681.26 8995.99 538.38 o
-1 6 -1 47472.45 42961.98 1596.76 o
-6 7 -1 15006.23 13344.15 1383.06 o
-3 7 -1 48963.03 47053.53 1005.67 o
-5 8 -1 612.21 864.38 1064.25 o
-2 8 -1 5743.07 7377.83 967.64 o
-4 9 -1 5759.21 6086.92 911.74 o
-1 9 -1 690.99 1335.68 705.92 o
-6 10 -1 2339.64 3422.78 979.91 o
-3 10 -1 6704.33 7068.94 1140.42 o
-8 11 -1 1508.42 2383.06 920.61 o
-5 11 -1 1074.01 2155.59 964.06 o
-7 12 -1 6001.79 7606.17 1447.12 o
-4 12 -1 4467.08 6054.78 1394.47 o
-1 2 0 7678.34 7191.23 261.32 o
-3 3 0 56927.98 57608.77 1574.43 o
0 3 0 54971.04 56644.29 1323.96 o
-2 4 0 204073.89 244999.98 3611.00 o
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-3 5 1 45363.46 51498.45 1491.99 o
-5 6 1 48119.31 41814.29 1433.48 o
-2 6 1 10177.95 8961.62 369.92 o
-4 7 1 48748.27 51580.70 1769.71 o
-1 7 1 14213.11 14087.70 572.13 o
-3 8 1 1509.75 3600.40 714.87 o
-5 9 1 5918.55 6547.04 1081.12 o
-2 9 1 2699.28 1855.03 815.82 o
-7 10 1 7854.13 9346.70 1501.30 o
-4 10 1 3227.81 2741.39 707.97 o
-9 11 1 362.37 763.17 855.69 o
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-3 11 1 1862.13 2150.99 872.56 o
-8 12 1 5352.35 7176.28 1470.12 o
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0 1 2 5011.70 5087.55 173.34 o
-2 2 2 442982.19 503144.88 13505.56 o
-1 3 2 41849.04 49836.54 1335.38 o
-3 4 2 559.53 641.88 269.46 o
0 4 2 66799.66 62980.95 1556.65 o
-5 5 2 24917.50 30059.72 1545.26 o
-2 5 2 25638.80 27302.43 1664.73 o
-4 6 2 2643.07 3280.36 456.50 o
-1 6 2 29212.40 26139.97 689.99 o
-6 7 2 43963.99 41734.29 1850.94 o
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-1 5 3 71294.35 57349.55 1968.13 o
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-1 8 3 6426.54 7047.51 500.16 o
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-10 11 3 5334.00 6274.68 1098.97 o
-7 11 3 2027.08 2587.02 881.25 o
-4 11 3 1835.05 1431.27 760.62 o
-6 12 3 3237.16 2602.87 921.12 o
-1 1 4 2724.29 2710.94 190.13 o
0 2 4 49159.64 50787.74 852.32 o
-2 3 4 60728.77 65540.88 2136.12 o
-4 4 4 2984.76 4656.11 994.73 o
-1 4 4 2676.00 2689.06 234.88 o
-3 5 4 12875.01 15487.48 541.25 o
0 5 4 14850.62 16844.17 763.87 o
-5 6 4 26236.36 29280.23 3644.03 o
-2 6 4 43426.25 38931.33 870.31 o
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-4 7 4 28103.97 32973.65 1278.18 o
-1 7 4 36351.17 34676.77 1130.22 o
-6 8 4 6801.73 7533.06 2400.19 o
-3 8 4 3137.15 3049.81 466.07 o
0 8 4 33792.67 32611.95 2321.72 o
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-5 9 4 3115.83 6528.12 1416.45 o
-2 9 4 7666.21 9008.64 633.93 o
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-4 10 4 2923.89 3459.58 968.66 o
-1 10 4 6374.93 5950.50 1137.86 o
-9 11 4 17114.67 19380.14 2009.66 o
-6 11 4 6435.04 6742.81 1374.53 o
-3 11 4 7565.77 7309.19 1240.60 o
-8 12 4 4350.63 6037.00 1262.84 o
-5 12 4 510.75 748.86 656.85 o
-1 3 5 43914.09 38522.52 627.56 o
-3 4 5 12648.30 13875.13 457.07 o
-2 5 5 22392.72 22169.20 612.64 o
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-1 6 5 43693.92 38423.66 1878.23 o
-6 7 5 2821.78 3185.08 471.96 o
-3 7 5 36070.12 34743.04 915.88 o
-5 8 5 15411.38 16040.76 1592.29 o
-2 8 5 7999.33 8226.91 643.37 o
-7 9 5 4142.19 4493.11 886.59 o
-4 9 5 2358.69 2922.57 523.09 o
-1 9 5 2706.23 4151.26 721.11 o
-9 10 5 5561.68 7353.78 1225.83 o
-6 10 5 9094.41 9964.19 1292.23 o
-3 10 5 13269.89 12550.16 1034.85 o
-8 11 5 3118.81 3925.08 908.99 o
-5 11 5 463.56 120.12 757.04 o
-2 11 5 509.84 295.97 837.80 o
-7 12 5 12974.16 12983.15 1635.74 o
-4 12 5 5461.70 6272.03 1156.26 o
0 0 6 493585.25 425264.88 12794.79 o
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-1 8 6 11723.46 11385.44 586.16 o
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-3 9 6 18150.01 17683.77 1126.41 o
0 9 6 18777.04 14830.51 1547.82 o
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-2 10 6 18867.66 20436.99 1784.49 o
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-7 11 6 2011.76 2894.64 755.78 o
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-2 3 7 100671.94 109407.25 3069.35 o
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-3 11 7 2674.23 2620.25 1016.71 o
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