#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:53:41 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181114 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/94/2219404.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219404_Fobs loop_ _publ_author_name 'Wang, Xiao-Feng' 'Wang, Jin-Feng' 'Liu, Xiao-Yang' _publ_section_title ; catena-Poly[[[diaquacopper(II)]-bis[\m-1,1'-(butane-1,4-diyl)diimidazole-\k^2^N^3^:N^3'^]] dinitrate] ; _journal_coeditor_code NG2477 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1220 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 126.375 _cell_angle_gamma 90.000 _cell_length_a 22.1608 _cell_length_b 10.3341 _cell_length_c 14.3663 _exptl_crystal_F_000 1260.00 _reflns_d_resolution_high 0.7702 _cod_data_source_file ng2477Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' G38 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 324.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 279.26 248.06 4.22 o 6 0 0 25153.37 26731.74 445.82 o 8 0 0 12707.92 11509.79 122.50 o 10 0 0 27370.75 26934.81 363.98 o 12 0 0 4108.14 3714.63 44.67 o 14 0 0 944.06 1084.84 15.48 o 16 0 0 1979.79 2169.97 29.90 o 18 0 0 2253.31 2548.35 32.37 o 20 0 0 3443.89 3297.25 108.84 o 22 0 0 521.50 423.28 14.52 o 3 1 0 3143.72 2911.25 26.76 o 5 1 0 11152.15 10678.24 71.19 o 7 1 0 1278.35 1319.85 16.71 o 9 1 0 47.28 60.24 7.55 o 11 1 0 643.85 694.30 7.15 o 13 1 0 1987.79 2033.42 18.18 o 15 1 0 410.91 355.98 8.86 o 17 1 0 250.77 216.01 6.71 o 19 1 0 836.47 836.67 12.70 o 21 1 0 87.87 137.31 20.28 o 23 1 0 336.41 331.32 14.84 o 0 2 0 57921.78 55292.44 1436.33 o 2 2 0 1207.62 1466.53 17.76 o 4 2 0 5.17 33.18 1.01 o 6 2 0 3314.04 4556.93 50.67 o 8 2 0 1314.77 1230.61 11.02 o 10 2 0 3010.02 3277.03 31.61 o 12 2 0 38.83 38.71 4.81 o 14 2 0 10.29 17.01 4.19 o 16 2 0 1051.77 952.04 11.32 o 18 2 0 10.50 -2.36 5.37 o 20 2 0 1014.37 1029.94 16.58 o 22 2 0 163.67 159.00 11.79 o 1 3 0 12614.52 12190.93 101.86 o 3 3 0 7826.82 7411.46 57.22 o 5 3 0 9840.14 10144.74 109.62 o 7 3 0 7752.83 7630.84 62.87 o 9 3 0 6134.34 6974.71 62.04 o 11 3 0 1850.29 1916.22 21.74 o 13 3 0 851.93 689.28 10.60 o 15 3 0 1371.34 1341.08 18.31 o 17 3 0 589.90 684.54 14.57 o 19 3 0 1025.25 1042.09 18.11 o 21 3 0 1147.02 1077.64 23.89 o 0 4 0 20563.42 22564.92 322.31 o 2 4 0 3481.25 3422.47 27.29 o 4 4 0 4761.43 4935.76 33.06 o 6 4 0 1785.39 1876.65 16.25 o 8 4 0 2344.36 1963.11 21.50 o 10 4 0 5362.76 5229.18 49.66 o 12 4 0 981.74 1009.61 13.99 o 14 4 0 39.88 90.79 9.30 o 16 4 0 3.11 5.40 4.48 o 18 4 0 1105.46 1097.05 19.00 o 20 4 0 556.25 584.20 15.08 o 22 4 0 192.11 216.79 12.49 o 1 5 0 3485.95 3376.38 28.23 o 3 5 0 498.11 492.99 9.03 o 5 5 0 181.03 208.45 8.83 o 7 5 0 1145.99 1320.84 13.43 o 9 5 0 1887.11 1907.14 19.67 o 11 5 0 250.25 189.22 8.10 o 13 5 0 19.54 7.26 4.85 o 15 5 0 421.41 490.53 14.22 o 17 5 0 64.42 70.92 6.12 o 19 5 0 5.63 7.30 6.13 o 21 5 0 461.84 429.95 13.27 o 0 6 0 178.36 222.56 12.98 o 2 6 0 1728.86 1574.55 14.79 o 4 6 0 2909.91 3425.66 28.82 o 6 6 0 6213.41 6180.71 48.48 o 8 6 0 978.65 1022.79 12.03 o 10 6 0 3130.57 3256.95 34.77 o 12 6 0 70.85 59.12 6.98 o 14 6 0 60.92 62.44 6.40 o 16 6 0 829.02 755.20 14.00 o 18 6 0 348.11 358.08 15.64 o 20 6 0 1447.60 1460.09 30.15 o 1 7 0 180.93 231.59 9.11 o 3 7 0 3101.05 2986.90 24.82 o 5 7 0 585.64 543.34 9.56 o 7 7 0 561.16 634.68 10.75 o 9 7 0 247.42 258.14 8.43 o 11 7 0 269.60 229.97 17.54 o 13 7 0 76.05 64.66 5.91 o 15 7 0 157.64 208.94 10.03 o 17 7 0 226.09 251.13 8.83 o 19 7 0 362.31 327.48 20.34 o 0 8 0 295.20 338.22 14.98 o 2 8 0 173.43 159.55 6.77 o 4 8 0 307.73 280.52 14.14 o 6 8 0 2399.37 2448.99 20.51 o 8 8 0 1.43 3.52 4.00 o 10 8 0 63.35 55.79 5.62 o 12 8 0 362.36 412.47 10.43 o 14 8 0 358.28 341.02 9.67 o 16 8 0 262.87 298.88 11.45 o 18 8 0 201.33 187.24 18.57 o 1 9 0 1438.05 1288.89 19.78 o 3 9 0 3284.06 3329.58 37.01 o 5 9 0 2648.39 2698.49 27.31 o 7 9 0 262.65 238.70 12.02 o 9 9 0 8.03 19.06 5.89 o 11 9 0 164.19 236.85 18.53 o 13 9 0 480.88 638.09 16.36 o 15 9 0 568.35 589.37 12.32 o 17 9 0 537.00 474.01 33.30 o 0 10 0 615.58 572.74 15.76 o 2 10 0 649.52 671.37 17.17 o 4 10 0 41.15 34.59 6.66 o 6 10 0 46.38 34.22 3.35 o 8 10 0 48.47 69.88 6.83 o 10 10 0 315.92 342.11 13.67 o 12 10 0 221.52 197.59 11.06 o 14 10 0 2.44 4.37 5.40 o 1 11 0 114.08 122.07 9.68 o 3 11 0 96.27 81.98 5.98 o 5 11 0 499.28 479.48 11.58 o 7 11 0 9.48 4.77 7.20 o 9 11 0 28.74 17.92 5.46 o 11 11 0 0.67 -7.57 7.57 o 13 11 0 8.09 21.12 15.41 o 0 12 0 1200.38 1178.86 27.29 o 2 12 0 612.25 631.95 24.31 o 4 12 0 204.97 191.18 15.06 o 6 12 0 236.92 248.80 32.14 o 8 12 0 58.28 57.83 12.56 o 10 12 0 467.11 452.88 16.03 o 1 13 0 130.60 132.36 9.19 o 3 13 0 58.90 60.51 10.42 o 5 13 0 52.25 52.48 15.56 o -23 1 1 405.97 388.12 9.84 o -21 1 1 983.17 980.07 16.20 o -19 1 1 1976.79 2112.71 26.47 o -17 1 1 2332.64 2332.95 21.81 o -15 1 1 2533.10 2355.12 21.48 o -13 1 1 2413.37 2360.11 21.34 o -11 1 1 2002.26 2271.87 22.03 o -9 1 1 1178.64 1361.22 13.98 o -7 1 1 2081.56 2077.57 14.18 o -5 1 1 5778.26 5538.41 42.85 o -3 1 1 1729.35 1552.75 11.70 o 1 1 1 7557.49 6166.85 94.13 o 3 1 1 54340.66 51441.88 1164.55 o 5 1 1 34764.88 35681.94 479.31 o 7 1 1 3861.56 4126.54 30.67 o 9 1 1 169.14 141.14 5.75 o 11 1 1 336.96 315.70 4.78 o 13 1 1 2350.68 2568.61 19.81 o 15 1 1 1121.56 1044.52 11.70 o 17 1 1 1180.70 1136.85 24.12 o 19 1 1 726.25 669.76 20.53 o 21 1 1 636.03 657.92 15.27 o -22 2 1 1129.55 1079.66 22.31 o -20 2 1 2263.97 2231.26 23.60 o -18 2 1 2214.48 2188.44 26.39 o -16 2 1 18.17 34.20 4.96 o -14 2 1 32.68 50.09 4.21 o -12 2 1 4616.82 4560.73 35.72 o -10 2 1 14943.42 13901.72 128.52 o -8 2 1 23.42 65.92 7.70 o -6 2 1 297.57 336.64 6.38 o -4 2 1 70431.58 66639.75 1862.33 o -2 2 1 83104.19 74930.68 1699.84 o 0 2 1 20361.44 22240.83 276.39 o 2 2 1 10544.66 11774.40 135.45 o 4 2 1 798.69 937.45 12.63 o 6 2 1 77.08 48.16 1.97 o 8 2 1 4355.10 4097.77 27.57 o 10 2 1 654.17 385.70 5.75 o 12 2 1 1116.76 993.59 12.79 o 14 2 1 1050.82 1108.65 17.00 o 16 2 1 339.89 435.88 10.40 o 18 2 1 1509.21 1563.88 25.08 o 20 2 1 155.61 148.41 9.26 o -23 3 1 32.03 48.19 8.15 o -21 3 1 0.15 -4.01 6.55 o -19 3 1 24.85 38.94 6.16 o -17 3 1 256.81 315.30 9.51 o -15 3 1 140.68 122.58 7.69 o -13 3 1 469.51 463.58 12.77 o -11 3 1 537.74 455.78 9.85 o -9 3 1 320.88 274.92 7.30 o -7 3 1 799.85 681.75 17.20 o -5 3 1 3143.27 2734.51 44.39 o -3 3 1 323.45 490.85 7.83 o -1 3 1 53.34 92.84 2.83 o 1 3 1 906.47 742.45 5.68 o 3 3 1 105.10 134.48 7.52 o 5 3 1 147.43 143.67 6.25 o 7 3 1 155.42 212.35 4.07 o 9 3 1 207.31 260.31 5.61 o 11 3 1 205.45 273.05 6.83 o 13 3 1 21.83 20.36 4.05 o 15 3 1 595.06 704.82 11.04 o 17 3 1 883.57 867.26 24.31 o 19 3 1 125.42 118.76 10.84 o 21 3 1 23.04 30.95 8.04 o -22 4 1 2359.77 2329.93 31.64 o -20 4 1 852.56 971.56 17.43 o -18 4 1 1967.56 1820.02 24.65 o -16 4 1 919.29 825.57 20.47 o -14 4 1 25.18 25.59 5.92 o -12 4 1 4009.29 4027.63 42.07 o -10 4 1 4531.08 4843.34 45.85 o -8 4 1 1095.87 849.86 11.40 o -6 4 1 7189.93 6614.63 70.91 o -4 4 1 21171.30 21301.97 225.60 o -2 4 1 36292.75 40168.87 498.41 o 0 4 1 1503.98 1848.97 20.38 o 2 4 1 2036.99 2449.03 19.19 o 4 4 1 9265.86 9530.18 84.00 o 6 4 1 7899.92 7866.30 55.22 o 8 4 1 11619.41 11554.05 111.42 o 10 4 1 2453.53 2355.50 27.19 o 12 4 1 435.67 554.69 10.23 o 14 4 1 3400.88 3336.17 39.58 o 16 4 1 14.51 25.77 4.80 o 18 4 1 515.07 552.24 18.04 o 20 4 1 218.34 231.74 9.56 o -21 5 1 1028.13 974.94 18.14 o -19 5 1 535.87 574.48 17.97 o -17 5 1 1466.30 1643.96 21.52 o -15 5 1 1029.94 1090.49 16.39 o -13 5 1 527.66 452.71 13.92 o -11 5 1 951.77 905.20 12.86 o -9 5 1 2110.91 2286.75 22.94 o -7 5 1 3494.53 3586.50 45.64 o -5 5 1 4814.81 4987.47 43.75 o -3 5 1 9241.75 9065.79 82.76 o -1 5 1 6408.68 6374.33 48.30 o 1 5 1 7253.57 6840.79 50.83 o 3 5 1 410.72 272.91 5.70 o 5 5 1 1120.07 979.79 7.34 o 7 5 1 7395.13 8074.88 68.11 o 9 5 1 9748.59 10849.26 97.90 o 11 5 1 892.61 856.57 14.56 o 13 5 1 246.80 256.31 24.89 o 15 5 1 147.60 160.76 11.38 o 17 5 1 958.07 1083.92 14.93 o 19 5 1 382.85 364.41 13.68 o -20 6 1 130.45 125.58 17.52 o -18 6 1 0.18 -3.79 7.91 o -16 6 1 181.64 174.24 8.41 o -14 6 1 98.20 108.70 8.36 o -12 6 1 66.46 91.31 6.34 o -10 6 1 305.56 242.47 8.74 o -8 6 1 141.69 171.58 13.36 o -6 6 1 219.15 227.32 9.35 o -4 6 1 480.66 422.98 7.52 o -2 6 1 260.55 279.55 6.76 o 0 6 1 527.27 627.28 7.46 o 2 6 1 1188.76 1251.46 11.39 o 4 6 1 246.85 248.03 7.06 o 6 6 1 801.08 917.62 11.76 o 8 6 1 0.57 4.01 3.77 o 10 6 1 263.97 242.73 7.83 o 12 6 1 3.26 19.91 4.15 o 14 6 1 266.04 262.57 20.80 o 16 6 1 116.90 87.48 7.79 o 18 6 1 7.34 -1.34 4.84 o -19 7 1 67.50 44.71 7.18 o -17 7 1 796.83 707.38 20.86 o -15 7 1 843.58 879.04 13.76 o -13 7 1 627.72 720.53 13.55 o -11 7 1 585.12 532.15 12.30 o -9 7 1 41.57 34.04 7.94 o -7 7 1 753.77 765.17 12.61 o -5 7 1 610.94 734.45 14.40 o -3 7 1 3567.16 4019.43 38.61 o -1 7 1 3649.31 3728.20 34.36 o 1 7 1 2508.44 2588.69 27.03 o 3 7 1 1147.99 959.52 9.57 o 5 7 1 739.34 792.26 10.90 o 7 7 1 1969.94 1975.21 19.43 o 9 7 1 2380.69 2300.17 27.58 o 11 7 1 286.82 284.86 11.39 o 13 7 1 35.13 48.22 6.47 o 15 7 1 116.90 118.40 6.14 o 17 7 1 213.31 200.23 16.52 o -18 8 1 243.40 249.77 10.23 o -16 8 1 693.26 704.48 17.21 o -14 8 1 397.12 373.04 12.24 o -12 8 1 3472.29 3375.84 39.86 o -10 8 1 523.46 582.87 12.22 o -8 8 1 1050.59 971.28 22.36 o -6 8 1 153.13 165.29 5.06 o -4 8 1 3588.74 3785.07 35.08 o -2 8 1 4078.29 4269.54 41.82 o 0 8 1 6785.81 6377.03 65.01 o 2 8 1 2770.11 2661.31 28.34 o 4 8 1 1735.99 1656.79 16.75 o 6 8 1 994.72 916.91 14.54 o 8 8 1 4270.17 4437.54 44.54 o 10 8 1 1110.21 1219.92 21.39 o 12 8 1 18.09 12.88 6.35 o 14 8 1 127.80 102.74 13.87 o 16 8 1 328.62 327.84 22.68 o -17 9 1 6.24 5.86 5.84 o -15 9 1 0.42 -1.44 4.92 o -13 9 1 7.07 25.64 5.96 o -11 9 1 31.54 36.33 7.05 o -9 9 1 193.23 197.66 9.19 o -7 9 1 6.01 1.52 5.47 o -5 9 1 296.95 214.56 12.32 o -3 9 1 117.65 82.19 6.68 o -1 9 1 234.61 227.76 8.92 o 1 9 1 197.96 246.52 15.08 o 3 9 1 20.63 8.52 3.96 o 5 9 1 41.05 43.65 4.41 o 7 9 1 59.02 61.73 7.81 o 9 9 1 20.81 14.69 5.45 o 11 9 1 33.05 21.37 6.40 o 13 9 1 2.75 1.35 4.15 o 15 9 1 134.33 136.41 47.37 o -16 10 1 531.67 525.84 19.62 o -14 10 1 128.29 115.99 11.30 o -12 10 1 1027.90 965.93 20.51 o -10 10 1 34.23 14.34 6.71 o -8 10 1 39.68 64.38 7.32 o -6 10 1 30.79 32.57 7.34 o -4 10 1 20.42 3.57 4.63 o -2 10 1 830.00 775.05 17.89 o 0 10 1 2010.31 2143.20 60.53 o 2 10 1 330.81 404.46 12.19 o 4 10 1 1239.74 1249.03 17.77 o 6 10 1 25.54 21.45 5.98 o 8 10 1 851.40 820.75 18.36 o 10 10 1 13.58 17.02 5.36 o 12 10 1 9.68 5.58 7.88 o 14 10 1 13.85 3.31 11.64 o -13 11 1 370.06 368.21 13.49 o -11 11 1 125.02 148.27 9.04 o -9 11 1 6.28 0.34 7.17 o -7 11 1 141.16 153.50 8.22 o -5 11 1 296.22 286.89 8.26 o -3 11 1 283.10 316.03 11.96 o -1 11 1 244.72 260.88 14.22 o 1 11 1 571.59 551.72 22.45 o 3 11 1 644.38 650.01 17.49 o 5 11 1 501.78 503.43 11.00 o 7 11 1 233.75 216.76 10.60 o 9 11 1 64.73 53.61 10.39 o 11 11 1 142.32 142.82 17.07 o -10 12 1 132.39 127.62 9.58 o -8 12 1 43.12 50.77 10.01 o -6 12 1 0.45 -6.46 6.70 o -4 12 1 55.95 47.11 6.58 o -2 12 1 79.93 99.10 11.22 o 0 12 1 53.67 71.87 8.02 o 2 12 1 9.28 6.28 5.22 o 4 12 1 27.33 17.36 8.54 o 6 12 1 134.87 152.64 21.07 o 8 12 1 0.12 0.83 6.41 o -5 13 1 186.45 145.31 11.96 o -3 13 1 18.98 17.77 8.21 o -1 13 1 88.31 100.88 7.06 o 1 13 1 118.77 151.70 24.14 o 3 13 1 298.34 274.02 16.33 o -24 0 2 408.40 434.79 13.37 o -22 0 2 371.23 378.18 13.14 o -20 0 2 5326.50 5147.20 65.41 o -18 0 2 2613.57 2743.88 33.99 o -16 0 2 2275.24 2491.87 36.50 o -14 0 2 3853.31 3929.75 46.48 o -12 0 2 22553.42 22292.23 327.82 o -10 0 2 11466.52 9590.55 111.60 o -8 0 2 76386.74 76825.84 2154.61 o -6 0 2 19975.72 22486.64 388.03 o -4 0 2 9984.46 9924.91 126.85 o 0 0 2 22756.99 21834.79 501.25 o 2 0 2 105326.98 84567.29 4377.81 o 4 0 2 90958.73 84139.44 1967.95 o 6 0 2 45975.70 48348.24 923.49 o 8 0 2 2961.42 2895.13 61.84 o 10 0 2 79.00 31.97 4.47 o 12 0 2 3040.92 2836.20 48.43 o 14 0 2 20.88 22.68 7.23 o 16 0 2 4348.16 4518.83 72.32 o 18 0 2 577.43 602.44 23.30 o 20 0 2 655.03 606.43 24.63 o -23 1 2 82.73 84.09 5.99 o -21 1 2 493.22 532.81 11.85 o -19 1 2 401.84 409.70 9.45 o -17 1 2 300.45 280.75 7.41 o -15 1 2 2843.32 2810.46 24.13 o -13 1 2 2240.29 2264.62 20.59 o -11 1 2 817.13 888.68 9.40 o -9 1 2 291.02 236.89 4.24 o -7 1 2 4428.58 4318.63 39.03 o -5 1 2 1112.81 808.19 9.48 o -3 1 2 14088.68 13974.57 140.36 o -1 1 2 9.50 13.34 2.50 o 1 1 2 1083.27 1395.92 34.95 o 3 1 2 15427.48 15596.40 221.31 o 5 1 2 12348.58 13053.78 109.90 o 7 1 2 3662.02 3884.00 47.65 o 9 1 2 49.94 52.01 3.38 o 11 1 2 980.62 1202.05 12.40 o 13 1 2 55.03 37.98 4.02 o 15 1 2 1197.51 1149.65 13.03 o 17 1 2 541.97 462.26 25.66 o 19 1 2 162.47 172.49 14.77 o 21 1 2 27.57 48.12 15.64 o -24 2 2 74.39 48.82 8.31 o -22 2 2 47.33 57.44 6.19 o -20 2 2 835.78 826.08 13.10 o -18 2 2 1605.26 1531.27 16.19 o -16 2 2 63.06 76.00 4.80 o -14 2 2 157.16 159.53 4.55 o -12 2 2 3130.11 3380.29 26.56 o -10 2 2 8.87 3.49 2.18 o -8 2 2 712.57 653.62 8.66 o -6 2 2 2621.80 2898.24 27.03 o -4 2 2 12474.91 11134.38 110.51 o -2 2 2 5801.26 5614.33 42.17 o 0 2 2 139.65 219.10 4.15 o 2 2 2 6090.89 6681.27 77.99 o 4 2 2 6033.54 6872.53 46.66 o 6 2 2 2786.73 3024.83 20.39 o 8 2 2 630.63 383.54 5.67 o 10 2 2 47.59 64.10 3.31 o 12 2 2 1542.60 1639.95 16.51 o 14 2 2 4.00 14.92 3.73 o 16 2 2 151.44 156.31 7.26 o 18 2 2 117.37 92.14 11.04 o 20 2 2 175.16 217.75 9.93 o -23 3 2 820.92 812.13 19.78 o -21 3 2 1171.46 1160.99 21.28 o -19 3 2 3275.13 3280.79 30.26 o -17 3 2 2838.14 2946.63 25.81 o -15 3 2 2252.94 2080.82 18.37 o -13 3 2 1886.65 1848.55 15.34 o -11 3 2 2673.59 2806.80 20.23 o -9 3 2 713.85 671.47 5.70 o -7 3 2 3055.90 3007.80 25.60 o -5 3 2 9033.77 9210.53 109.82 o -3 3 2 28233.58 28968.35 388.97 o -1 3 2 11743.83 10759.68 149.07 o 1 3 2 3323.13 2869.69 23.89 o 3 3 2 4350.45 3968.64 28.10 o 5 3 2 8906.99 8830.67 71.45 o 7 3 2 14382.38 15562.85 140.65 o 9 3 2 2824.85 3199.86 24.58 o 11 3 2 1362.22 1470.00 18.41 o 13 3 2 700.48 640.83 10.68 o 15 3 2 1785.35 1866.37 38.86 o 17 3 2 1213.17 1224.74 24.34 o 19 3 2 320.20 314.89 15.33 o -22 4 2 671.90 681.01 16.24 o -20 4 2 737.48 731.71 14.88 o -18 4 2 163.99 147.25 16.37 o -16 4 2 594.21 616.00 19.02 o -14 4 2 1979.19 2028.39 30.90 o -12 4 2 2216.05 2163.04 25.12 o -10 4 2 528.86 298.48 8.27 o -8 4 2 3101.99 2873.51 26.12 o -6 4 2 1283.36 1432.33 11.38 o -4 4 2 7095.89 7879.44 73.36 o -2 4 2 11317.44 12365.63 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