#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:53:41 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181114 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/94/2219417.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219417_Fobs loop_ _publ_author_name 'Fun, Hoong-Kun' 'Kia, Reza' 'Mirkhani, Valiollah' 'Zargoshi, Hasan' _publ_section_title ; {5,5'-Dihydroxy-2,2'-[o-phenylenebis(nitrilomethylidyne)]diphenolato}nickel(II) dihydrate ; _journal_coeditor_code PK2114 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1181 _journal_page_last m1182 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.150 _cell_angle_gamma 90.000 _cell_length_a 10.9049 _cell_length_b 17.6602 _cell_length_c 9.0375 _exptl_crystal_F_000 912.00 _reflns_d_resolution_high 0.6305 _cod_data_source_file pk2114Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ni0h2m in C2/c (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 389.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 17964.24 18117.25 455.53 o 4 0 0 355.32 396.68 27.22 o 6 0 0 7126.63 7533.52 132.14 o 8 0 0 22.50 1.00 15.70 o 10 0 0 877.09 1015.74 66.42 o 12 0 0 19.56 54.34 30.98 o 14 0 0 28.23 -7.49 44.97 o 16 0 0 258.35 167.19 68.95 o 1 1 0 100.46 105.65 8.64 o 3 1 0 31027.22 33563.46 380.44 o 5 1 0 2696.52 2812.61 34.21 o 7 1 0 801.48 835.04 21.58 o 9 1 0 3.46 18.50 13.30 o 11 1 0 310.52 307.74 32.12 o 13 1 0 0.70 0.98 20.73 o 15 1 0 23.57 2.35 35.95 o 0 2 0 18701.53 18084.15 314.88 o 2 2 0 6517.51 6884.29 62.50 o 4 2 0 8527.26 8218.41 78.87 o 6 2 0 1679.14 1562.89 26.20 o 8 2 0 5046.29 5128.92 83.48 o 10 2 0 2386.94 2509.22 68.82 o 12 2 0 42.70 43.64 20.83 o 14 2 0 785.66 777.45 62.14 o 16 2 0 585.63 399.29 90.71 o 1 3 0 4562.17 4910.98 44.67 o 3 3 0 621.24 620.84 12.50 o 5 3 0 194.49 162.62 11.75 o 7 3 0 812.34 886.89 25.69 o 9 3 0 32.62 29.30 13.36 o 11 3 0 1.37 5.50 19.25 o 13 3 0 12.73 18.15 24.56 o 15 3 0 264.64 262.81 45.71 o 0 4 0 4910.43 4584.33 60.90 o 2 4 0 2118.36 2115.06 25.00 o 4 4 0 8158.18 7767.91 67.12 o 6 4 0 4902.92 4859.78 57.69 o 8 4 0 2239.89 2262.58 50.23 o 10 4 0 2741.81 2837.45 72.26 o 12 4 0 838.30 1000.17 79.25 o 14 4 0 1357.28 1353.14 135.84 o 16 4 0 398.35 306.82 68.11 o 1 5 0 1993.05 2060.42 26.10 o 3 5 0 5690.15 5959.76 51.47 o 5 5 0 1143.09 1128.22 23.12 o 7 5 0 1261.03 1395.00 38.63 o 9 5 0 1.10 -7.62 15.44 o 11 5 0 215.71 133.55 35.21 o 13 5 0 151.35 135.78 60.59 o 15 5 0 42.39 84.43 46.44 o 0 6 0 7306.36 7601.32 91.03 o 2 6 0 30.00 11.02 4.67 o 4 6 0 1752.75 1594.96 24.02 o 6 6 0 20424.97 21241.95 201.98 o 8 6 0 3616.14 3733.25 99.17 o 10 6 0 894.50 824.88 57.25 o 12 6 0 1014.77 1060.63 84.88 o 14 6 0 337.66 404.99 108.18 o 16 6 0 242.36 178.01 61.88 o 1 7 0 208.75 218.09 10.56 o 3 7 0 5488.46 5723.58 57.49 o 5 7 0 1.46 7.49 5.72 o 7 7 0 37.70 58.29 12.90 o 9 7 0 291.02 220.20 39.39 o 11 7 0 9.99 10.31 23.78 o 13 7 0 49.25 4.97 34.45 o 15 7 0 8.69 27.60 57.92 o 0 8 0 721.70 991.45 27.23 o 2 8 0 2830.88 2751.06 41.45 o 4 8 0 2891.57 2553.26 35.01 o 6 8 0 5647.28 5796.61 99.30 o 8 8 0 4645.62 4822.69 91.61 o 10 8 0 1565.81 1822.98 83.25 o 12 8 0 1074.24 1158.86 91.45 o 14 8 0 452.06 624.08 183.77 o 16 8 0 452.26 474.95 109.85 o 1 9 0 594.66 634.43 19.55 o 3 9 0 30.61 44.74 9.38 o 5 9 0 3217.05 3301.48 46.51 o 7 9 0 1.32 3.18 14.30 o 9 9 0 5.64 14.60 21.29 o 11 9 0 46.95 31.10 28.18 o 13 9 0 9.28 22.01 37.76 o 15 9 0 8.36 53.19 65.02 o 0 10 0 11350.91 11247.42 157.26 o 2 10 0 2033.17 1850.28 33.98 o 4 10 0 3065.04 2950.02 47.44 o 6 10 0 5444.40 5198.69 105.58 o 8 10 0 453.80 449.63 45.63 o 10 10 0 860.76 923.69 66.07 o 12 10 0 549.48 536.17 69.63 o 14 10 0 814.87 912.01 122.57 o 1 11 0 862.34 871.25 23.15 o 3 11 0 1086.41 1098.74 28.93 o 5 11 0 58.34 35.32 13.42 o 7 11 0 2.48 -7.10 17.73 o 9 11 0 181.40 197.50 36.75 o 11 11 0 23.80 15.94 32.86 o 13 11 0 149.80 106.22 56.11 o 15 11 0 23.91 -11.23 62.32 o 0 12 0 13353.44 13075.86 174.52 o 2 12 0 6708.63 6673.46 81.54 o 4 12 0 2196.39 2151.56 64.78 o 6 12 0 1524.47 1529.34 90.95 o 8 12 0 1345.26 1405.06 81.70 o 10 12 0 249.39 240.77 49.03 o 12 12 0 39.66 89.18 41.19 o 14 12 0 603.21 1229.76 199.37 o 1 13 0 240.27 251.25 17.50 o 3 13 0 13.93 15.85 11.66 o 5 13 0 578.89 551.81 36.70 o 7 13 0 3.02 36.76 22.72 o 9 13 0 334.99 333.69 53.12 o 11 13 0 332.44 227.24 52.12 o 13 13 0 2.56 25.49 52.90 o 15 13 0 7.35 -35.25 69.08 o 0 14 0 34014.54 34750.24 386.83 o 2 14 0 6849.66 6980.04 98.65 o 4 14 0 1122.30 1260.46 51.69 o 6 14 0 307.53 274.86 33.83 o 8 14 0 285.36 279.42 61.55 o 10 14 0 1122.00 1208.43 95.40 o 12 14 0 33.12 56.52 53.33 o 14 14 0 11.01 44.04 64.68 o 1 15 0 2708.47 2782.33 56.00 o 3 15 0 276.80 278.04 27.39 o 5 15 0 75.42 98.93 24.35 o 7 15 0 27.65 46.27 25.75 o 9 15 0 75.74 7.86 29.74 o 11 15 0 0.66 -11.57 35.33 o 13 15 0 94.61 62.68 63.36 o 0 16 0 8739.68 8533.83 181.62 o 2 16 0 14.53 13.34 15.28 o 4 16 0 108.57 125.24 29.43 o 6 16 0 3157.67 3101.90 118.46 o 8 16 0 1582.74 1673.69 104.69 o 10 16 0 1428.78 1647.21 152.17 o 12 16 0 141.61 27.83 60.67 o 1 17 0 946.24 839.65 48.97 o 3 17 0 943.79 964.60 55.14 o 5 17 0 13.49 11.97 22.12 o 7 17 0 568.03 538.14 65.81 o 9 17 0 241.19 188.52 52.23 o 11 17 0 5.89 -14.32 50.38 o 13 17 0 177.95 119.42 72.59 o 0 18 0 673.45 823.27 72.61 o 2 18 0 864.04 917.76 84.08 o 4 18 0 1150.80 1300.37 73.25 o 6 18 0 831.02 946.64 75.10 o 8 18 0 1199.99 1264.59 134.45 o 10 18 0 726.38 744.60 86.47 o 12 18 0 304.36 482.91 251.39 o 1 19 0 273.59 219.53 54.51 o 3 19 0 1.75 34.73 28.11 o 5 19 0 8.57 20.91 28.93 o 7 19 0 287.38 292.72 73.87 o 9 19 0 175.32 197.16 56.05 o 11 19 0 333.22 356.04 120.05 o 0 20 0 125.07 198.41 77.01 o 2 20 0 121.18 97.75 42.43 o 4 20 0 1878.01 2026.75 195.23 o 6 20 0 2477.74 2981.19 131.02 o 8 20 0 517.13 607.86 78.32 o 10 20 0 529.05 494.72 98.98 o 1 21 0 600.31 474.08 77.97 o 3 21 0 213.92 296.15 86.24 o 5 21 0 189.59 120.76 76.05 o 7 21 0 1236.36 1178.16 114.56 o 9 21 0 10.55 -27.54 55.15 o 11 21 0 17.44 -57.83 57.83 o 0 22 0 698.77 739.54 136.83 o 2 22 0 122.36 149.75 105.57 o 4 22 0 17.38 9.77 43.80 o 6 22 0 1329.85 1444.15 223.79 o 8 22 0 617.94 664.11 85.51 o 10 22 0 139.61 120.67 78.14 o 1 23 0 16.13 66.60 47.94 o 3 23 0 473.24 429.92 84.57 o 5 23 0 276.85 242.16 72.54 o 7 23 0 2.21 36.62 52.50 o 9 23 0 161.50 -0.98 62.81 o 0 24 0 1254.69 774.23 147.02 o 2 24 0 778.67 668.14 100.29 o 4 24 0 664.89 403.07 85.22 o 6 24 0 622.49 775.64 270.49 o 8 24 0 33.67 -2.86 76.53 o 1 25 0 196.26 275.94 75.87 o 3 25 0 537.90 426.48 110.18 o 5 25 0 225.26 244.72 79.34 o 7 25 0 4.44 21.53 59.76 o 0 26 0 1486.79 1683.86 228.01 o 2 26 0 877.47 811.39 164.92 o 4 26 0 505.85 445.77 152.35 o 6 26 0 84.90 11.42 107.64 o 1 27 0 545.12 700.27 113.56 o 3 27 0 23.28 74.21 63.92 o -17 1 1 134.22 81.82 54.66 o -15 1 1 5.71 13.85 35.88 o -13 1 1 718.99 843.25 53.85 o -11 1 1 790.46 832.00 47.84 o -9 1 1 1169.84 1191.66 40.99 o -7 1 1 1638.29 1414.79 29.61 o -5 1 1 3724.07 3837.33 45.03 o -3 1 1 151786.34 153995.13 1084.33 o -1 1 1 32118.29 32528.36 300.25 o 1 1 1 2202.44 2559.09 32.96 o 3 1 1 4480.21 4744.56 57.06 o 5 1 1 664.73 601.26 30.77 o 7 1 1 6316.20 6623.30 75.53 o 9 1 1 23.05 20.65 14.03 o 11 1 1 92.04 109.95 22.56 o 13 1 1 1412.99 1393.32 73.29 o -16 2 1 64.29 30.79 39.73 o -14 2 1 79.13 62.38 31.54 o -12 2 1 86.57 48.16 21.24 o -10 2 1 86.03 32.31 18.67 o -8 2 1 56.32 61.14 13.48 o -6 2 1 95.03 130.18 10.02 o -4 2 1 2018.73 2139.45 24.42 o -2 2 1 148.53 120.34 6.22 o 0 2 1 10137.95 10201.26 95.23 o 2 2 1 3699.69 4022.90 41.61 o 4 2 1 2532.51 2550.80 30.24 o 6 2 1 134.76 163.52 14.76 o 8 2 1 604.62 686.25 26.11 o 10 2 1 677.45 670.54 36.57 o 12 2 1 102.25 97.87 24.37 o 14 2 1 1.62 12.32 35.94 o -17 3 1 771.87 740.98 95.38 o -15 3 1 147.04 146.04 39.60 o -13 3 1 296.82 283.64 39.34 o -11 3 1 1500.05 1651.90 69.08 o -9 3 1 2524.68 2576.68 58.07 o -7 3 1 5145.02 4977.17 70.24 o -5 3 1 1230.01 1124.50 17.32 o -3 3 1 14100.44 13912.21 102.15 o -1 3 1 16339.80 16493.11 140.75 o 1 3 1 570.63 364.87 11.23 o 3 3 1 11548.92 11740.08 90.86 o 5 3 1 11287.91 11420.37 96.24 o 7 3 1 1085.64 1088.53 37.02 o 9 3 1 1186.96 1236.05 44.06 o 11 3 1 2605.33 2740.80 75.74 o 13 3 1 597.25 579.69 68.65 o 15 3 1 137.05 113.04 59.19 o -16 4 1 0.94 45.40 42.16 o -14 4 1 5.76 26.38 28.40 o -12 4 1 34.64 -0.18 21.61 o -10 4 1 71.92 62.99 19.07 o -8 4 1 21.48 14.19 10.82 o -6 4 1 138.93 163.30 9.65 o -4 4 1 43.58 29.17 6.10 o -2 4 1 2108.70 2466.79 27.95 o 0 4 1 198.34 298.68 14.80 o 2 4 1 876.05 858.92 17.30 o 4 4 1 144.26 164.58 7.70 o 6 4 1 245.07 273.83 12.98 o 8 4 1 537.06 514.09 22.57 o 10 4 1 415.05 412.06 47.96 o 12 4 1 150.65 148.31 35.15 o 14 4 1 985.83 982.60 91.75 o 16 4 1 0.49 -14.48 87.51 o -15 5 1 442.47 396.41 59.05 o -13 5 1 1770.83 1828.90 149.85 o -11 5 1 1512.09 1759.44 84.23 o -9 5 1 4025.53 4257.18 97.65 o -7 5 1 3548.22 3546.46 59.30 o -5 5 1 429.66 376.97 13.90 o -3 5 1 251.77 199.98 9.61 o -1 5 1 233.02 257.45 9.98 o 1 5 1 8776.35 8563.81 70.79 o 3 5 1 11398.16 10994.49 87.39 o 5 5 1 2498.43 2376.77 29.30 o 7 5 1 11562.92 11236.45 117.03 o 9 5 1 3364.34 3318.77 94.84 o 11 5 1 1960.77 2073.73 77.16 o 13 5 1 2081.84 2643.16 273.11 o 15 5 1 51.12 -5.44 42.33 o -16 6 1 69.66 21.07 41.13 o -14 6 1 128.56 103.72 44.42 o -12 6 1 208.87 253.87 46.93 o -10 6 1 901.23 909.52 78.08 o -8 6 1 339.25 347.51 51.31 o -6 6 1 609.00 697.95 19.87 o -4 6 1 286.88 269.17 12.20 o -2 6 1 318.77 327.73 12.27 o 0 6 1 562.66 667.27 15.79 o 2 6 1 6376.28 7101.14 59.89 o 4 6 1 2501.43 2682.60 36.34 o 6 6 1 66.60 60.72 8.10 o 8 6 1 103.50 73.01 22.99 o 10 6 1 1067.23 977.82 54.90 o 12 6 1 45.23 -4.91 29.28 o 14 6 1 356.94 254.49 69.64 o 16 6 1 4.61 -37.55 90.37 o -15 7 1 124.37 81.65 43.08 o -13 7 1 69.17 71.70 37.73 o -11 7 1 1188.35 1311.85 171.58 o -9 7 1 4721.23 4840.20 121.57 o -7 7 1 3591.74 3743.70 65.74 o -5 7 1 3426.12 3276.48 43.12 o -3 7 1 540.04 509.55 16.72 o -1 7 1 2763.56 2714.32 33.40 o 1 7 1 1955.35 1534.85 24.22 o 3 7 1 29827.77 32197.88 235.64 o 5 7 1 17102.74 18231.41 151.74 o 7 7 1 1056.05 1012.69 27.94 o 9 7 1 1362.74 1381.01 69.15 o 11 7 1 231.51 206.67 38.58 o 13 7 1 622.10 764.57 100.96 o 15 7 1 98.32 87.45 52.76 o -16 8 1 38.00 30.21 53.61 o -14 8 1 83.55 26.20 40.27 o -12 8 1 163.00 150.88 87.30 o -10 8 1 0.72 33.80 23.11 o -8 8 1 1402.86 1488.90 54.07 o -6 8 1 1105.44 1264.07 34.39 o -4 8 1 1688.73 1689.33 30.37 o -2 8 1 881.73 929.95 21.08 o 0 8 1 249.74 304.47 13.32 o 2 8 1 6568.02 6908.69 67.38 o 4 8 1 709.75 767.58 20.89 o 6 8 1 14.56 29.71 9.25 o 8 8 1 64.80 85.68 25.46 o 10 8 1 280.58 220.10 41.93 o 12 8 1 202.45 85.35 47.24 o 14 8 1 230.01 190.66 97.30 o -15 9 1 895.17 1079.56 219.39 o -13 9 1 866.13 964.73 93.76 o -11 9 1 1064.17 1201.82 89.24 o -9 9 1 4471.26 4616.17 123.46 o -7 9 1 583.67 556.80 30.63 o -5 9 1 31.66 9.53 8.87 o -3 9 1 5164.99 4986.76 62.23 o -1 9 1 1281.50 1062.13 31.18 o 1 9 1 26.01 41.45 7.71 o 3 9 1 11387.82 11522.79 106.10 o 5 9 1 3408.14 3420.28 57.53 o 7 9 1 1425.78 1247.28 82.20 o 9 9 1 4199.64 4409.16 121.61 o 11 9 1 2744.88 2803.95 118.26 o 13 9 1 1651.44 1838.38 442.41 o 15 9 1 33.73 114.49 83.06 o -16 10 1 5.29 10.00 69.60 o -14 10 1 128.37 130.87 50.54 o -12 10 1 662.28 615.58 74.38 o -10 10 1 128.45 83.00 29.15 o -8 10 1 61.40 45.17 21.41 o -6 10 1 1988.84 2024.45 50.53 o -4 10 1 4.08 7.60 7.82 o -2 10 1 13.25 19.03 7.58 o 0 10 1 2957.24 3098.81 43.08 o 2 10 1 520.98 470.30 20.02 o 4 10 1 2340.45 2485.69 54.22 o 6 10 1 559.37 549.25 36.90 o 8 10 1 439.76 514.87 63.09 o 10 10 1 176.79 186.95 38.40 o 12 10 1 116.57 37.86 47.66 o 14 10 1 271.28 253.30 78.88 o -15 11 1 9.82 49.61 66.22 o -13 11 1 209.10 227.01 74.28 o -11 11 1 257.32 219.17 50.22 o -9 11 1 677.59 686.17 56.53 o -7 11 1 4487.97 4381.03 116.26 o -5 11 1 4690.90 4610.73 81.71 o -3 11 1 3606.76 3526.28 63.64 o -1 11 1 6357.48 6264.13 67.26 o 1 11 1 9197.40 9402.94 107.78 o 3 11 1 2224.62 2043.96 47.05 o 5 11 1 1119.66 1088.11 41.76 o 7 11 1 2549.13 2485.17 122.48 o 9 11 1 61.33 26.12 25.06 o 11 11 1 460.66 593.38 240.89 o 13 11 1 1265.26 1477.19 316.23 o 15 11 1 81.61 89.04 69.97 o -14 12 1 32.57 39.89 45.30 o -12 12 1 58.66 28.63 39.32 o -10 12 1 71.63 58.32 30.89 o -8 12 1 286.41 227.12 37.04 o -6 12 1 35.71 21.70 17.50 o -4 12 1 613.27 628.46 30.63 o -2 12 1 1012.45 1095.62 33.94 o 0 12 1 803.59 739.28 22.75 o 2 12 1 139.18 153.02 14.86 o 4 12 1 1363.78 1443.22 45.55 o 6 12 1 135.32 92.65 24.89 o 8 12 1 6.21 30.81 24.43 o 10 12 1 181.89 214.85 46.32 o 12 12 1 7.60 45.47 52.00 o 14 12 1 0.69 9.59 62.10 o -15 13 1 3.33 39.33 69.07 o -13 13 1 111.52 210.08 66.29 o -11 13 1 501.57 494.71 68.08 o -9 13 1 212.25 204.00 37.74 o -7 13 1 573.69 645.89 77.37 o -5 13 1 2903.97 2793.54 71.99 o -3 13 1 24138.40 24050.23 243.38 o -1 13 1 17467.29 17068.22 161.36 o 1 13 1 1457.47 1462.67 36.08 o 3 13 1 1271.06 1373.54 45.66 o 5 13 1 1334.75 1331.71 78.14 o 7 13 1 328.33 333.89 42.53 o 9 13 1 23.75 64.10 51.61 o 11 13 1 269.70 311.74 120.53 o 13 13 1 299.68 338.46 162.05 o -14 14 1 95.88 1.99 55.71 o -12 14 1 4.46 35.29 40.81 o -10 14 1 8.02 -4.87 32.19 o -8 14 1 106.80 157.84 36.91 o -6 14 1 78.48 36.55 20.72 o -4 14 1 2261.98 2247.53 60.00 o -2 14 1 2780.50 2967.06 54.44 o 0 14 1 73.03 74.63 12.29 o 2 14 1 1671.70 1520.88 45.99 o 4 14 1 12.34 -8.33 13.61 o 6 14 1 3.69 -6.38 19.96 o 8 14 1 255.41 231.45 44.24 o 10 14 1 5.25 -2.72 41.97 o 12 14 1 29.69 -22.82 49.78 o 14 14 1 59.35 7.18 64.64 o -13 15 1 520.18 452.75 75.29 o -11 15 1 425.52 547.28 83.31 o -9 15 1 1879.49 2187.18 130.03 o -7 15 1 148.99 175.83 51.56 o -5 15 1 85.21 125.32 25.61 o -3 15 1 20620.10 20744.09 245.16 o -1 15 1 817.60 926.43 36.91 o 1 15 1 14.97 7.91 13.36 o 3 15 1 3416.17 3421.39 82.42 o 5 15 1 747.95 868.21 52.28 o 7 15 1 3305.60 3545.31 188.37 o 9 15 1 166.67 201.59 71.22 o 11 15 1 31.11 43.20 51.85 o 13 15 1 772.21 713.88 115.26 o -14 16 1 2.68 -4.54 72.66 o -12 16 1 113.27 45.39 47.21 o -10 16 1 52.83 58.86 45.87 o -8 16 1 3.64 -9.11 27.62 o -6 16 1 1338.19 1397.48 87.70 o -4 16 1 293.98 242.46 38.16 o -2 16 1 340.78 299.28 28.36 o 0 16 1 2862.93 2871.17 72.80 o 2 16 1 30.44 27.30 17.33 o 4 16 1 99.72 65.83 22.83 o 6 16 1 465.98 497.59 50.86 o 8 16 1 25.17 33.82 32.30 o 10 16 1 300.68 259.37 71.72 o 12 16 1 308.48 308.93 84.69 o -13 17 1 517.60 521.85 117.34 o -11 17 1 937.66 998.59 100.67 o -9 17 1 303.37 227.35 54.64 o -7 17 1 1267.13 1447.28 97.18 o -5 17 1 543.31 559.22 52.20 o -3 17 1 1059.36 1256.54 61.50 o -1 17 1 1924.22 2018.40 69.28 o 1 17 1 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