#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:53:41 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181114 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/94/2219419.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219419_Fobs loop_ _publ_author_name 'Luo, Jie-Wei' 'Zhou, Li' 'He, Rui' 'Wang, Gui-Yu' 'Qin, Da-Bin' _publ_section_title ; Bis(3-bromomethyl-2-methoxy-1-naphthyl)methane ; _journal_coeditor_code PV2087 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1861 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 99.327 _cell_angle_beta 98.326 _cell_angle_gamma 96.296 _cell_length_a 10.6812 _cell_length_b 11.1429 _cell_length_c 18.4311 _exptl_crystal_F_000 1032.00 _reflns_d_resolution_high 0.7701 _cod_data_source_file pv2087Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Y2461 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 273.95 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1584.21 1455.50 23.54 o 3 0 0 1730.16 1637.11 29.76 o 4 0 0 17.28 22.08 9.78 o 5 0 0 310.30 318.42 26.10 o 6 0 0 24.05 52.95 18.25 o 7 0 0 8649.06 8733.52 286.64 o 8 0 0 224.18 255.11 42.06 o 9 0 0 544.48 551.04 64.76 o 10 0 0 190.41 223.77 54.76 o 11 0 0 625.70 777.91 98.52 o 12 0 0 84.17 95.19 33.57 o 13 0 0 44.24 71.52 58.65 o -13 1 0 952.40 1387.51 219.57 o -12 1 0 4.89 6.76 13.18 o -11 1 0 270.05 278.80 31.32 o -10 1 0 1.70 -1.94 8.90 o -9 1 0 782.17 743.66 56.80 o -8 1 0 427.52 392.75 30.17 o -7 1 0 2319.76 2149.77 88.92 o -6 1 0 59.85 92.39 19.55 o -5 1 0 304.97 318.09 24.79 o -4 1 0 1093.98 975.52 34.24 o -3 1 0 1338.78 1210.01 27.62 o -2 1 0 22831.44 22510.66 374.69 o 2 1 0 1041.96 850.17 18.74 o 3 1 0 6790.53 6070.46 103.85 o 4 1 0 1651.41 1740.18 44.63 o 5 1 0 18343.36 17124.42 369.71 o 6 1 0 6.26 -2.77 9.03 o 7 1 0 1244.79 1146.15 49.11 o 8 1 0 2199.20 2311.45 119.78 o 9 1 0 514.14 481.67 68.51 o 10 1 0 969.22 1000.09 105.14 o 11 1 0 63.72 62.73 80.33 o 12 1 0 17.68 -18.90 40.73 o 13 1 0 17.49 39.59 53.44 o -13 2 0 33.88 37.08 36.09 o -12 2 0 70.55 61.22 24.77 o -11 2 0 843.51 833.10 43.72 o -10 2 0 2332.45 2384.82 99.03 o -9 2 0 1730.32 1586.60 78.99 o -8 2 0 1884.73 1742.83 58.85 o -7 2 0 246.28 211.45 15.29 o -6 2 0 290.10 270.65 14.14 o -5 2 0 3705.94 3424.68 130.26 o -4 2 0 747.79 599.42 20.47 o -3 2 0 7928.09 7441.45 243.78 o -2 2 0 20.77 35.09 3.27 o -1 2 0 2703.59 2423.79 33.01 o 0 2 0 0.69 10.65 2.71 o 1 2 0 8813.43 8451.30 151.86 o 2 2 0 12796.35 12671.96 229.96 o 3 2 0 8364.12 7899.02 145.76 o 4 2 0 1548.19 1270.89 35.41 o 5 2 0 15979.32 15383.05 338.13 o 6 2 0 631.58 623.45 34.25 o 7 2 0 3732.90 3681.37 104.85 o 8 2 0 2930.06 2918.66 102.48 o 9 2 0 308.62 305.94 43.01 o 10 2 0 2112.44 2191.78 166.26 o 11 2 0 100.39 218.83 75.12 o 12 2 0 313.06 367.74 161.86 o 13 2 0 152.33 164.58 84.57 o -13 3 0 31.97 55.66 55.56 o -12 3 0 1723.63 1713.49 62.83 o -11 3 0 116.64 117.56 24.59 o -10 3 0 217.69 193.88 20.62 o -9 3 0 2461.38 2274.30 68.08 o -8 3 0 233.44 234.38 17.32 o -7 3 0 239.55 263.78 22.56 o -6 3 0 11310.43 10186.00 398.06 o -5 3 0 11797.89 10542.19 469.67 o -4 3 0 4737.94 4636.96 219.34 o -3 3 0 4958.50 4436.50 54.32 o -2 3 0 27154.57 27215.65 425.56 o -1 3 0 27.68 21.76 4.15 o 0 3 0 1062.71 923.78 22.99 o 1 3 0 484.96 401.72 16.67 o 2 3 0 8816.16 7974.45 147.17 o 3 3 0 9336.43 9135.99 192.42 o 4 3 0 24.44 19.59 9.66 o 5 3 0 349.39 371.03 31.55 o 6 3 0 691.38 595.22 38.23 o 7 3 0 166.32 167.43 27.95 o 8 3 0 1276.41 1315.82 74.44 o 9 3 0 1887.37 1858.08 135.95 o 10 3 0 1822.05 1946.46 111.52 o 11 3 0 11.05 12.06 38.12 o 12 3 0 638.87 687.30 131.62 o -13 4 0 49.09 44.39 20.87 o -12 4 0 360.38 370.63 37.83 o -11 4 0 372.44 402.34 28.78 o -10 4 0 40.08 37.57 13.89 o -9 4 0 633.60 533.50 32.53 o -8 4 0 1.72 -0.99 7.87 o -7 4 0 1284.16 1252.78 39.97 o -6 4 0 2556.96 2416.42 57.03 o -5 4 0 31.19 22.84 6.82 o -4 4 0 13909.83 13064.16 196.44 o -3 4 0 10803.23 10267.57 140.74 o -2 4 0 2219.44 2105.37 45.02 o -1 4 0 203.23 170.26 9.42 o 0 4 0 3741.61 3400.92 194.60 o 1 4 0 3517.41 2842.56 57.03 o 2 4 0 73.58 77.96 11.33 o 3 4 0 9929.63 9483.32 199.33 o 4 4 0 3066.00 2814.91 74.63 o 5 4 0 519.28 533.58 35.36 o 6 4 0 2977.34 2911.22 94.76 o 7 4 0 1112.79 1083.00 78.42 o 8 4 0 764.82 791.16 62.30 o 9 4 0 390.33 407.57 68.15 o 10 4 0 35.96 71.25 42.41 o 11 4 0 82.77 97.93 68.27 o 12 4 0 309.59 368.71 114.26 o -13 5 0 4.77 -14.43 14.43 o -12 5 0 500.58 474.16 45.17 o -11 5 0 625.91 645.53 67.57 o -10 5 0 1680.72 1720.84 60.31 o -9 5 0 1090.83 989.05 48.06 o -8 5 0 715.70 682.36 34.22 o -7 5 0 185.22 180.91 24.53 o -6 5 0 2681.67 2699.06 129.69 o -5 5 0 1153.75 1214.86 27.82 o -4 5 0 1163.15 1177.59 26.10 o -3 5 0 109.13 137.65 10.08 o -2 5 0 102.29 114.06 12.03 o -1 5 0 12125.92 11046.24 181.90 o 0 5 0 7034.97 6219.46 122.99 o 1 5 0 12528.79 11883.70 260.98 o 2 5 0 6916.82 6835.44 159.67 o 3 5 0 18.95 26.03 11.85 o 4 5 0 79.59 148.57 43.67 o 5 5 0 107.96 142.04 25.64 o 6 5 0 1100.83 981.83 59.36 o 7 5 0 805.97 768.25 60.40 o 8 5 0 612.32 584.34 61.72 o 9 5 0 1.13 -9.42 39.42 o 10 5 0 107.48 71.19 39.79 o 11 5 0 794.27 925.60 102.05 o 12 5 0 7.86 -25.74 55.72 o -13 6 0 12.01 0.20 8.08 o -12 6 0 446.98 457.00 33.78 o -11 6 0 266.41 279.08 38.89 o -10 6 0 310.16 347.83 26.46 o -9 6 0 96.21 72.56 22.00 o -8 6 0 538.48 492.73 59.05 o -7 6 0 4803.61 5296.32 383.44 o -6 6 0 3.29 6.95 6.89 o -5 6 0 3441.70 3690.81 65.14 o -4 6 0 132.11 151.29 32.70 o -3 6 0 10071.34 9828.58 174.65 o -2 6 0 2848.72 2515.87 52.20 o -1 6 0 18.44 36.37 10.66 o 0 6 0 476.02 441.74 51.47 o 1 6 0 4273.13 4041.86 96.03 o 2 6 0 1797.51 1648.99 54.66 o 3 6 0 75.39 68.91 18.14 o 4 6 0 6246.23 5671.72 152.26 o 5 6 0 4526.39 4339.48 135.80 o 6 6 0 2002.30 1951.02 91.84 o 7 6 0 207.93 230.29 43.44 o 8 6 0 1158.79 1197.82 112.76 o 9 6 0 88.74 82.59 40.20 o 10 6 0 93.12 93.65 46.91 o 11 6 0 105.93 157.73 59.91 o -12 7 0 381.99 405.13 33.40 o -11 7 0 470.47 593.81 40.53 o -10 7 0 20.80 23.00 12.98 o -9 7 0 3343.86 3447.11 170.87 o -8 7 0 407.82 441.31 31.06 o -7 7 0 595.83 687.14 35.12 o -6 7 0 1100.24 1103.78 36.04 o -5 7 0 165.17 189.96 22.91 o -4 7 0 2634.41 2859.19 80.20 o -3 7 0 4.38 -1.41 8.05 o -2 7 0 8416.22 7841.00 148.15 o -1 7 0 1076.14 950.92 33.49 o 0 7 0 1.69 -1.00 6.80 o 1 7 0 3970.76 4082.35 106.81 o 2 7 0 1585.82 1540.94 73.68 o 3 7 0 795.98 733.72 54.45 o 4 7 0 2527.40 2301.17 91.08 o 5 7 0 50.49 41.41 28.46 o 6 7 0 2874.55 2864.20 148.68 o 7 7 0 881.96 850.26 76.76 o 8 7 0 3.62 -34.15 42.19 o 9 7 0 377.09 413.23 72.38 o 10 7 0 161.01 223.82 65.28 o -12 8 0 83.55 54.44 21.86 o -11 8 0 34.12 4.09 12.88 o -10 8 0 356.12 414.60 40.40 o -9 8 0 156.85 124.76 27.60 o -8 8 0 597.13 651.33 77.62 o -7 8 0 2037.33 2258.45 69.00 o -6 8 0 2811.85 2952.33 86.00 o -5 8 0 433.50 451.45 36.51 o -4 8 0 316.31 300.47 46.28 o -3 8 0 133.66 152.35 21.42 o -2 8 0 4098.99 3902.31 98.32 o -1 8 0 3579.29 3224.77 77.64 o 0 8 0 1820.86 1784.57 55.62 o 1 8 0 1035.88 1035.52 65.55 o 2 8 0 1259.01 1170.34 74.17 o 3 8 0 95.40 95.30 30.80 o 4 8 0 24.97 8.15 35.76 o 5 8 0 625.46 498.50 68.97 o 6 8 0 419.14 527.55 62.92 o 7 8 0 152.79 180.36 49.01 o 8 8 0 416.17 295.72 116.74 o 9 8 0 1706.29 1738.96 171.01 o 10 8 0 171.62 147.31 99.90 o -11 9 0 37.22 38.47 25.06 o -10 9 0 47.99 77.39 37.64 o -9 9 0 0.80 -1.11 13.19 o -8 9 0 335.16 341.83 41.75 o -7 9 0 554.95 667.64 41.54 o -6 9 0 511.82 685.19 39.66 o -5 9 0 1690.79 1707.23 64.61 o -4 9 0 3882.72 4007.22 101.08 o -3 9 0 47.24 45.34 17.36 o -2 9 0 2902.28 2983.50 89.81 o -1 9 0 6451.41 6243.76 200.02 o 0 9 0 733.50 702.76 41.24 o 1 9 0 1067.42 1121.03 52.21 o 2 9 0 1176.92 1103.28 67.32 o 3 9 0 4488.16 4351.38 152.20 o 4 9 0 164.36 185.48 47.96 o 5 9 0 9.32 21.34 31.16 o 6 9 0 23.42 19.34 26.66 o 7 9 0 934.00 966.78 113.51 o 8 9 0 28.62 7.61 26.47 o 9 9 0 145.17 138.76 55.70 o -11 10 0 718.92 857.65 91.18 o -10 10 0 416.06 430.57 67.01 o -9 10 0 5.37 -2.75 21.83 o -8 10 0 99.66 126.71 30.08 o -7 10 0 864.56 1146.09 62.48 o -6 10 0 456.06 484.04 38.14 o -5 10 0 3.38 -2.14 10.12 o -4 10 0 13.79 21.44 15.55 o -3 10 0 1650.60 1700.41 65.42 o -2 10 0 57.24 50.98 18.51 o -1 10 0 1228.77 1369.86 59.74 o 0 10 0 1307.23 1375.98 61.55 o 1 10 0 2925.44 2800.87 115.27 o 2 10 0 124.66 96.45 26.50 o 3 10 0 256.02 188.63 42.09 o 4 10 0 58.27 52.10 31.25 o 5 10 0 184.67 190.11 64.05 o 6 10 0 99.71 88.96 41.32 o 7 10 0 57.04 34.11 34.00 o 8 10 0 654.61 600.99 115.64 o -10 11 0 225.83 263.86 54.92 o -9 11 0 94.10 125.47 34.92 o -8 11 0 892.59 1029.81 58.85 o -7 11 0 249.57 329.12 44.64 o -6 11 0 2352.24 2968.33 100.12 o -5 11 0 493.71 542.07 43.78 o -4 11 0 18.73 17.15 16.64 o -3 11 0 1750.37 1930.04 77.50 o -2 11 0 86.78 117.35 30.76 o -1 11 0 112.79 102.81 26.61 o 0 11 0 45.88 49.45 24.23 o 1 11 0 164.71 148.53 38.47 o 2 11 0 260.97 285.02 42.06 o 3 11 0 926.92 999.76 76.81 o 4 11 0 2691.03 2685.78 116.48 o 5 11 0 232.03 281.62 74.08 o 6 11 0 585.05 558.54 94.04 o 7 11 0 189.85 199.17 60.39 o -8 12 0 424.03 594.67 56.23 o -7 12 0 94.54 122.47 35.53 o -6 12 0 354.02 565.11 53.64 o -5 12 0 0.58 5.87 13.80 o -4 12 0 56.41 62.63 25.49 o -3 12 0 686.09 792.11 55.86 o -2 12 0 1714.03 2013.25 102.96 o -1 12 0 480.59 484.24 143.69 o 0 12 0 15.04 7.23 23.71 o 1 12 0 9.21 -1.79 14.77 o 2 12 0 1128.72 1243.84 80.86 o 3 12 0 410.10 168.24 121.16 o 4 12 0 3.82 2.73 23.45 o 5 12 0 479.14 348.36 134.37 o -7 13 0 122.62 127.58 31.62 o -6 13 0 3.15 14.44 30.66 o -5 13 0 421.75 403.04 131.11 o -4 13 0 290.09 288.13 94.96 o -3 13 0 389.61 383.76 128.85 o -2 13 0 13.95 -11.57 20.54 o -1 13 0 1877.52 2043.86 97.09 o 0 13 0 1.71 -5.03 21.65 o 1 13 0 23.96 37.90 29.86 o 2 13 0 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1 2047.73 2086.47 79.04 o 2 -10 1 98.02 105.35 25.54 o 3 -10 1 895.82 845.56 51.72 o 4 -10 1 3319.11 3604.40 119.75 o 5 -10 1 2912.49 3196.07 113.64 o 6 -10 1 86.42 104.75 25.93 o 7 -10 1 14.45 1.44 14.04 o 8 -10 1 127.25 143.92 39.27 o 9 -10 1 43.62 58.74 26.50 o 10 -10 1 4.74 -56.37 56.37 o -9 -9 1 910.94 933.83 106.53 o -8 -9 1 514.94 530.11 79.71 o -7 -9 1 653.26 654.86 94.69 o -6 -9 1 859.61 748.65 75.38 o -5 -9 1 345.44 290.45 48.69 o -4 -9 1 169.20 147.18 47.59 o -3 -9 1 140.74 138.23 32.48 o -2 -9 1 234.07 286.40 31.36 o -1 -9 1 327.15 313.23 29.80 o 0 -9 1 2876.60 2658.37 76.37 o 1 -9 1 6196.14 6093.93 136.78 o 2 -9 1 4007.25 4093.34 107.92 o 3 -9 1 3624.19 3690.07 89.98 o 4 -9 1 5066.43 5205.24 129.31 o 5 -9 1 3.45 -9.29 10.47 o 6 -9 1 996.65 1121.60 46.85 o 7 -9 1 1524.28 1787.98 61.44 o 8 -9 1 1001.62 1290.37 68.36 o 9 -9 1 28.46 12.16 19.82 o 10 -9 1 865.06 1082.16 65.28 o 11 -9 1 81.07 80.95 22.41 o -10 -8 1 0.64 -7.59 42.03 o -9 -8 1 198.71 240.40 63.72 o -8 -8 1 144.69 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