#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2219685.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219685_Fobs loop_ _publ_author_name 'Yang, Minglei' 'Yin, Handong' 'Wang, Daqi' 'Quan, Li' 'Cui, Liansheng' _publ_section_title ; \m-3-Thienylmalonato-\k^2^O^1^:O^3^-bis[triphenyltin(IV)] ; _journal_coeditor_code PV2106 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1316 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.542 _cell_angle_gamma 90.000 _cell_length_a 11.7260 _cell_length_b 21.9051 _cell_length_c 30.1944 _exptl_crystal_F_000 3520.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file pv2106Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 080704d in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 1074.87 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 184.18 136.54 61.51 o 2 0 0 108555.25 118915.09 2813.30 o 3 0 0 1158.39 1128.03 206.66 o 4 0 0 154875.80 161188.39 3865.06 o 5 0 0 648.33 556.02 222.65 o 6 0 0 185437.72 191923.08 4686.78 o 7 0 0 1204.36 1477.38 343.21 o 8 0 0 8110.14 8416.53 601.53 o 9 0 0 1148.34 1241.09 304.34 o 10 0 0 16412.11 18461.74 1089.89 o 11 0 0 606.60 141.46 509.27 o 12 0 0 1485.26 952.12 547.41 o 13 0 0 311.98 -34.44 538.80 o 1 1 0 80095.73 83775.97 1423.47 o 2 1 0 90.69 117.04 60.42 o 3 1 0 114060.50 119239.02 2032.34 o 4 1 0 742.96 782.64 132.08 o 5 1 0 519.84 306.49 141.71 o 6 1 0 37.30 25.74 160.33 o 7 1 0 53426.13 53405.96 1482.30 o 8 1 0 129.75 130.20 174.95 o 9 1 0 1022.20 1078.10 254.07 o 10 1 0 568.70 273.30 225.17 o 11 1 0 7166.76 7976.77 627.37 o 12 1 0 124.46 -66.03 322.74 o 13 1 0 1369.95 1774.72 487.97 o 0 2 0 3713.10 2875.95 101.49 o 1 2 0 413.97 414.07 36.24 o 2 2 0 322.52 245.79 62.80 o 3 2 0 1270.82 1161.35 340.75 o 4 2 0 2281.82 2356.07 172.88 o 5 2 0 1447.56 1389.07 191.97 o 6 2 0 1301.99 1240.45 221.07 o 7 2 0 1566.51 1927.08 243.27 o 8 2 0 5973.36 5852.39 439.72 o 9 2 0 6027.96 6443.12 550.67 o 10 2 0 13.47 -284.54 189.69 o 11 2 0 29.80 -426.50 284.33 o 12 2 0 2319.32 2963.33 515.77 o 13 2 0 1411.32 1588.27 480.13 o 1 3 0 2337.31 1904.06 132.76 o 2 3 0 618.67 778.89 81.35 o 3 3 0 9362.65 7759.27 286.38 o 4 3 0 881.01 763.47 125.44 o 5 3 0 1071.84 1151.87 353.66 o 6 3 0 23174.95 23700.18 546.22 o 7 3 0 1176.97 2152.53 453.43 o 8 3 0 1627.89 1735.23 250.85 o 9 3 0 2045.62 3433.99 343.34 o 10 3 0 527.75 120.21 291.65 o 11 3 0 503.42 159.20 337.47 o 12 3 0 653.22 1341.59 428.56 o 13 3 0 291.03 1497.06 690.10 o 1 4 0 76840.84 78788.17 839.95 o 2 4 0 495.02 639.21 130.23 o 3 4 0 541.88 567.84 94.14 o 4 4 0 4109.24 3630.10 205.96 o 5 4 0 8982.44 8741.15 290.04 o 6 4 0 13412.87 14681.52 678.48 o 7 4 0 768.00 863.84 197.84 o 8 4 0 482.82 1010.99 241.77 o 9 4 0 506.06 850.36 330.74 o 10 4 0 354.86 249.45 358.58 o 11 4 0 38.38 -240.51 235.02 o 12 4 0 210.94 776.21 605.22 o 13 4 0 465.23 333.36 565.86 o 1 5 0 109187.21 103909.70 1132.67 o 2 5 0 2859.96 2431.86 108.75 o 3 5 0 32602.19 28849.90 458.32 o 4 5 0 70.70 88.12 85.83 o 5 5 0 3515.88 3999.22 195.78 o 6 5 0 1284.31 1777.50 182.42 o 7 5 0 5246.78 4974.13 393.91 o 8 5 0 711.37 795.91 221.05 o 9 5 0 1807.04 2926.63 440.12 o 10 5 0 2183.32 2094.17 934.90 o 11 5 0 1132.69 330.97 346.74 o 12 5 0 155.66 457.11 610.14 o 13 5 0 47.63 346.03 363.96 o 0 6 0 150303.92 137635.89 2264.04 o 1 6 0 1732.47 2181.84 117.58 o 2 6 0 15946.16 15508.05 254.25 o 3 6 0 908.83 974.24 117.02 o 4 6 0 76968.59 78416.99 1051.55 o 5 6 0 1807.75 2013.52 172.81 o 6 6 0 22601.86 23302.11 479.23 o 7 6 0 9.47 -46.75 135.52 o 8 6 0 376.11 574.98 187.05 o 9 6 0 93.79 193.97 228.28 o 10 6 0 6330.83 6631.05 399.16 o 11 6 0 270.93 452.93 363.53 o 12 6 0 1902.41 2368.11 1044.38 o 13 6 0 0.50 525.26 564.63 o 1 7 0 3804.06 3505.05 131.05 o 2 7 0 122.73 180.01 70.31 o 3 7 0 111963.36 115713.57 2282.32 o 4 7 0 178.25 129.74 104.86 o 5 7 0 1700.65 2045.78 220.17 o 6 7 0 4297.78 4710.11 231.03 o 7 7 0 56120.38 54856.79 889.45 o 8 7 0 477.24 643.04 224.61 o 9 7 0 7693.03 7183.82 411.50 o 10 7 0 1153.85 1484.95 367.98 o 11 7 0 4752.32 4853.89 915.40 o 12 7 0 2316.41 3169.00 651.35 o 13 7 0 6106.16 3649.79 727.00 o 0 8 0 243346.84 260450.78 4163.81 o 1 8 0 14331.87 12350.91 271.77 o 2 8 0 13037.38 13333.34 254.61 o 3 8 0 1555.40 1728.43 128.82 o 4 8 0 62451.37 63510.56 916.61 o 5 8 0 6697.72 7265.60 259.41 o 6 8 0 34626.39 35274.88 641.92 o 7 8 0 317.80 350.87 166.04 o 8 8 0 11381.37 12695.67 494.12 o 9 8 0 380.57 454.00 242.56 o 10 8 0 18010.50 18206.32 643.57 o 11 8 0 367.98 577.36 263.10 o 12 8 0 562.28 433.00 473.60 o 13 8 0 55.96 255.87 418.24 o 1 9 0 6186.89 5548.87 198.86 o 2 9 0 34.59 104.21 84.78 o 3 9 0 1.03 -64.05 78.01 o 4 9 0 2506.01 3061.86 212.83 o 5 9 0 876.44 724.75 157.01 o 6 9 0 21.33 -26.18 142.34 o 7 9 0 5072.19 5071.94 277.88 o 8 9 0 2498.72 2854.55 417.61 o 9 9 0 2450.17 2384.52 337.35 o 10 9 0 1627.64 1167.83 306.01 o 11 9 0 2585.51 1970.00 843.25 o 12 9 0 759.02 404.44 304.53 o 13 9 0 295.93 324.75 398.56 o 0 10 0 1609.51 2305.17 256.90 o 1 10 0 15252.25 14137.36 320.22 o 2 10 0 146.77 113.75 95.47 o 3 10 0 44.59 41.73 96.08 o 4 10 0 11.00 123.78 124.56 o 5 10 0 15403.69 15768.44 403.96 o 6 10 0 1494.19 1911.81 213.33 o 7 10 0 270.04 280.81 178.98 o 8 10 0 1623.14 1806.83 310.25 o 9 10 0 6800.54 6761.14 408.48 o 10 10 0 12.41 35.48 230.18 o 11 10 0 1099.93 782.30 337.57 o 12 10 0 150.76 -36.29 295.23 o 1 11 0 11899.54 11747.18 379.08 o 2 11 0 28104.56 27553.87 530.28 o 3 11 0 22650.03 24466.58 480.67 o 4 11 0 20628.90 20671.84 386.18 o 5 11 0 168.80 586.32 172.85 o 6 11 0 7584.85 7516.37 311.28 o 7 11 0 5076.23 6065.41 301.19 o 8 11 0 14539.88 13262.69 518.11 o 9 11 0 621.73 943.69 281.08 o 10 11 0 52.63 -82.67 244.03 o 11 11 0 71.79 -123.43 244.41 o 12 11 0 3326.01 1655.14 1328.54 o 0 12 0 4714.27 4539.53 415.78 o 1 12 0 9994.61 10789.36 305.11 o 2 12 0 10.93 -120.98 113.63 o 3 12 0 95.04 73.08 115.30 o 4 12 0 10813.91 10523.11 276.32 o 5 12 0 3615.31 4589.47 298.33 o 6 12 0 13257.41 13290.25 411.46 o 7 12 0 3816.18 4618.36 409.94 o 8 12 0 1429.08 1654.20 311.90 o 9 12 0 154.90 89.77 294.29 o 10 12 0 1239.85 763.93 317.89 o 11 12 0 460.31 108.46 249.39 o 12 12 0 306.23 39.72 243.57 o 1 13 0 44.89 131.79 140.01 o 2 13 0 8.16 -163.08 108.72 o 3 13 0 748.94 767.62 145.69 o 4 13 0 136.54 -209.04 153.94 o 5 13 0 509.12 111.43 178.58 o 6 13 0 523.26 323.73 201.68 o 7 13 0 1.10 -101.81 230.92 o 8 13 0 81.31 83.73 272.30 o 9 13 0 2935.11 1831.98 399.76 o 10 13 0 643.55 448.52 287.70 o 11 13 0 52.66 -132.55 213.52 o 12 13 0 145.79 -226.73 229.66 o 0 14 0 103693.03 105957.88 2012.40 o 1 14 0 312.53 319.43 170.95 o 2 14 0 18541.19 18104.74 469.70 o 3 14 0 1771.16 1812.94 191.99 o 4 14 0 15518.35 16195.33 451.29 o 5 14 0 1408.30 1924.87 252.37 o 6 14 0 21325.74 20369.93 535.54 o 7 14 0 672.41 226.95 306.45 o 8 14 0 520.42 -34.20 285.46 o 9 14 0 1052.23 1660.17 722.70 o 10 14 0 6149.95 4197.68 2933.85 o 11 14 0 28.02 99.21 237.24 o 1 15 0 17791.69 17093.46 437.61 o 2 15 0 20048.67 19711.62 472.53 o 3 15 0 32152.08 32170.49 776.61 o 4 15 0 3689.52 5196.99 350.95 o 5 15 0 134.53 43.49 193.12 o 6 15 0 2356.66 3153.56 313.73 o 7 15 0 6293.39 6840.78 652.58 o 8 15 0 3862.59 3556.43 497.65 o 9 15 0 42.44 140.37 300.61 o 10 15 0 41.43 -377.21 251.47 o 11 15 0 1907.57 902.91 921.36 o 0 16 0 4280.45 4928.18 554.17 o 1 16 0 7157.41 7859.44 316.16 o 2 16 0 71.89 -95.82 188.83 o 3 16 0 279.40 71.03 203.14 o 4 16 0 4693.39 5568.73 409.31 o 5 16 0 2948.75 3665.97 331.24 o 6 16 0 166.97 -233.73 294.07 o 7 16 0 2302.66 2098.21 466.07 o 8 16 0 2785.77 2236.27 464.46 o 9 16 0 0.67 239.26 299.73 o 10 16 0 549.22 199.05 265.17 o 1 17 0 5.74 32.82 201.75 o 2 17 0 8804.45 8141.38 400.53 o 3 17 0 23.02 -217.04 198.30 o 4 17 0 112.94 169.20 238.59 o 5 17 0 115.32 -113.07 226.35 o 6 17 0 5421.45 5697.43 609.62 o 7 17 0 52.60 -419.55 279.70 o 8 17 0 817.39 436.20 487.13 o 9 17 0 56.75 -319.78 275.08 o 10 17 0 526.01 66.80 280.12 o 0 18 0 95.53 -296.46 337.05 o 1 18 0 18705.96 18820.84 601.75 o 2 18 0 186.29 64.71 255.33 o 3 18 0 1041.09 979.81 304.29 o 4 18 0 820.72 894.27 284.60 o 5 18 0 15460.36 16041.65 717.80 o 6 18 0 673.06 763.69 395.78 o 7 18 0 572.55 731.28 398.35 o 8 18 0 174.95 78.52 618.75 o 9 18 0 2457.35 2507.41 516.06 o 10 18 0 245.52 -97.88 309.42 o 1 19 0 684.27 643.95 290.42 o 2 19 0 8346.46 8384.31 439.37 o 3 19 0 896.30 914.18 300.72 o 4 19 0 3235.57 3712.81 405.45 o 5 19 0 148.41 96.04 265.47 o 6 19 0 1948.04 2468.26 521.84 o 7 19 0 1504.96 2524.89 549.12 o 8 19 0 1952.04 3161.63 596.74 o 9 19 0 517.77 212.98 368.43 o 0 20 0 898.19 653.20 476.06 o 1 20 0 121.33 -404.92 269.95 o 2 20 0 416.61 80.75 261.40 o 3 20 0 513.88 109.44 270.16 o 4 20 0 3.03 -335.01 223.34 o 5 20 0 44.80 -297.08 294.22 o 6 20 0 123.37 -430.90 287.26 o 7 20 0 281.09 -289.77 449.00 o 8 20 0 422.49 436.01 416.26 o 1 21 0 173.09 -419.35 279.57 o 2 21 0 210.56 -227.73 275.14 o 3 21 0 1994.18 2362.92 448.51 o 4 21 0 0.98 -69.69 258.91 o 5 21 0 3.88 -443.14 336.25 o 6 21 0 1294.95 1542.58 479.28 o 7 21 0 497.15 231.69 424.87 o 8 21 0 252.50 23.06 399.65 o 0 22 0 5450.00 6674.67 969.34 o 1 22 0 6173.17 7962.56 608.37 o 2 22 0 957.74 1043.40 416.05 o 3 22 0 1475.22 1180.13 411.67 o 4 22 0 2408.71 3218.13 446.85 o 5 22 0 7851.30 8022.92 659.60 o 6 22 0 702.15 1125.18 647.66 o 7 22 0 225.22 290.32 415.32 o 1 23 0 319.76 1.74 355.23 o 2 23 0 5999.29 7589.02 861.09 o 3 23 0 107.20 79.07 345.32 o 4 23 0 2520.98 2906.79 835.26 o 5 23 0 412.74 -174.29 406.65 o 6 23 0 1260.49 456.93 436.62 o 0 24 0 30.67 -575.70 451.46 o 1 24 0 471.77 498.27 400.92 o 2 24 0 5.01 -383.90 334.20 o 3 24 0 45.08 -241.83 358.86 o 4 24 0 80.98 -55.36 496.97 o 5 24 0 0.20 -333.36 445.31 o 1 25 0 9.39 -65.93 828.49 o 2 25 0 5363.48 6865.72 1331.00 o 3 25 0 293.51 578.24 433.98 o 0 26 0 102.45 945.97 635.98 o -13 1 1 0.00 -204.73 369.04 o -12 1 1 727.34 996.32 438.15 o -11 1 1 1122.13 1307.28 404.26 o -10 1 1 190.19 -238.03 181.89 o -9 1 1 2412.33 3883.51 578.16 o -8 1 1 1280.68 1125.85 276.46 o -7 1 1 325.49 480.06 203.10 o -6 1 1 17027.65 16758.51 536.14 o -5 1 1 12935.22 13841.57 582.46 o -4 1 1 1422.92 1583.39 173.73 o -3 1 1 18788.46 18128.84 442.02 o -2 1 1 6354.24 6354.27 342.59 o -1 1 1 751.23 1275.00 354.16 o 1 1 1 35195.61 32266.46 1587.50 o 2 1 1 305.64 409.10 89.45 o 3 1 1 11502.33 10998.47 445.31 o 4 1 1 21687.26 22282.57 547.56 o 5 1 1 695.11 487.45 164.06 o 6 1 1 3047.11 3470.38 249.13 o 7 1 1 12134.64 12394.19 398.73 o 8 1 1 6817.35 6842.01 310.01 o 9 1 1 1523.75 1787.07 276.63 o 10 1 1 506.13 438.86 323.91 o 11 1 1 953.48 643.74 367.45 o 12 1 1 278.06 -66.38 354.02 o 13 1 1 536.99 1118.39 434.47 o -13 2 1 36.60 -475.87 324.07 o -12 2 1 2.15 -441.82 296.52 o -11 2 1 0.93 -415.04 276.69 o -10 2 1 274.63 -171.89 262.15 o -9 2 1 2808.73 3073.87 370.31 o -8 2 1 1406.40 1176.71 277.03 o -7 2 1 14.95 1.27 184.66 o -6 2 1 1452.22 1793.49 256.20 o -5 2 1 1682.75 2045.09 221.68 o -4 2 1 105.86 59.56 91.63 o -3 2 1 871.46 1200.55 148.23 o -2 2 1 611.13 523.57 91.60 o -1 2 1 974.25 934.80 80.08 o 0 2 1 2038.96 1990.96 82.21 o 1 2 1 1974.67 1778.04 148.94 o 2 2 1 21316.20 21701.28 375.91 o 3 2 1 48.07 63.73 65.79 o 4 2 1 898.04 980.56 139.21 o 5 2 1 710.20 664.19 169.64 o 6 2 1 1750.07 2225.14 212.64 o 7 2 1 2167.84 2430.62 292.24 o 8 2 1 3906.12 4240.52 334.08 o 9 2 1 1803.61 2115.71 247.37 o 10 2 1 4.65 -283.16 188.78 o 11 2 1 248.14 185.74 361.07 o 12 2 1 1131.87 1092.85 440.95 o 13 2 1 36.88 601.53 590.46 o -13 3 1 5712.43 7035.09 1076.36 o -12 3 1 345.47 589.42 368.37 o -11 3 1 368.27 89.09 309.21 o -10 3 1 366.12 95.41 279.78 o -9 3 1 59449.33 59683.59 1173.62 o -8 3 1 238.09 333.15 198.41 o -7 3 1 33087.72 31627.26 841.14 o -6 3 1 1645.69 1902.51 252.21 o -5 3 1 83613.68 81915.11 1564.66 o -4 3 1 374.96 247.09 114.35 o -3 3 1 172307.14 179021.75 5785.90 o -2 3 1 198.02 49.41 64.63 o -1 3 1 18973.26 17796.37 233.03 o 1 3 1 257557.75 273792.56 4130.60 o 2 3 1 7.11 -74.99 51.74 o 3 3 1 56945.44 58947.10 772.05 o 4 3 1 180.60 160.51 90.59 o 5 3 1 107644.33 115063.98 1676.56 o 6 3 1 139.33 265.62 141.95 o 7 3 1 93314.26 94948.29 1514.66 o 8 3 1 291.01 222.94 326.54 o 9 3 1 12.01 -245.49 235.29 o 10 3 1 99.87 34.82 214.79 o 11 3 1 14642.03 14294.61 715.29 o 12 3 1 55.67 -106.56 336.90 o 13 3 1 1309.12 1810.75 697.48 o -13 4 1 0.70 645.82 605.22 o -12 4 1 5595.24 7031.42 866.62 o -11 4 1 476.76 178.75 344.35 o -10 4 1 8433.35 9408.00 680.26 o -9 4 1 957.66 1324.45 354.51 o -8 4 1 12679.57 12594.40 450.32 o -7 4 1 3.67 -89.32 157.33 o -6 4 1 134466.64 141304.34 2082.91 o -5 4 1 6530.50 6570.48 361.18 o -4 4 1 11794.92 11811.69 377.14 o -3 4 1 568.08 388.19 88.79 o -2 4 1 18029.52 17303.94 255.00 o -1 4 1 1484.98 1610.22 118.83 o 0 4 1 76081.33 82096.10 967.49 o 1 4 1 3876.11 3080.85 144.97 o 2 4 1 12354.84 12347.94 237.34 o 3 4 1 473.16 454.40 83.69 o 4 4 1 123420.38 125438.66 1582.89 o 5 4 1 205.62 107.28 114.20 o 6 4 1 778.77 1068.59 243.06 o 7 4 1 4035.65 4285.15 306.35 o 8 4 1 49647.10 50400.04 983.38 o 9 4 1 3420.04 3009.34 429.42 o 10 4 1 6127.84 6178.71 479.62 o 11 4 1 55.96 -41.84 313.68 o 12 4 1 5203.98 7524.68 1032.08 o 13 4 1 612.04 755.30 640.90 o -13 5 1 3070.33 3996.68 850.02 o -12 5 1 1977.24 1639.76 658.12 o -11 5 1 53.46 -190.69 311.22 o -10 5 1 878.84 138.88 283.55 o -9 5 1 9642.47 9357.07 1009.93 o -8 5 1 142.97 -65.43 181.64 o -7 5 1 8987.10 9189.02 356.37 o -6 5 1 294.82 244.34 147.80 o -5 5 1 1057.92 679.48 124.80 o -4 5 1 15.71 -111.86 74.57 o -3 5 1 35460.39 33653.39 514.79 o -2 5 1 2251.62 2029.03 95.55 o -1 5 1 16013.32 15202.71 528.67 o 0 5 1 10335.79 8874.47 185.70 o 1 5 1 119775.69 127609.09 1325.45 o 2 5 1 2638.50 2816.33 99.25 o 3 5 1 1997.88 1765.62 168.03 o 4 5 1 1724.25 1862.03 147.79 o 5 5 1 19568.13 19348.54 395.40 o 6 5 1 3838.07 3888.13 197.78 o 7 5 1 8660.59 7312.46 276.18 o 8 5 1 8197.89 7875.73 482.94 o 9 5 1 4541.84 4728.16 505.45 o 10 5 1 3629.37 3155.11 377.74 o 11 5 1 2697.97 4032.64 539.35 o 12 5 1 589.56 1537.17 956.42 o 13 5 1 282.56 618.66 390.08 o -13 6 1 968.65 563.40 505.58 o -12 6 1 383.59 954.51 408.40 o -11 6 1 679.24 720.35 292.63 o -10 6 1 148.11 99.55 243.80 o -9 6 1 11801.41 12074.98 488.51 o -8 6 1 5974.45 6029.60 288.45 o -7 6 1 59.08 -3.73 133.06 o -6 6 1 1187.13 1026.66 164.72 o -5 6 1 3694.86 3730.36 193.20 o -4 6 1 36.02 108.86 96.59 o -3 6 1 2981.39 3212.14 125.06 o -2 6 1 7376.73 6365.26 206.10 o -1 6 1 25401.88 26750.15 367.71 o 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