#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2220217.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220217_Fobs loop_ _publ_author_name 'Zhai, Cuiping' 'Yan, Feng-mei' 'Zhao, Pei-zheng' _publ_section_title ; (2,9-Dimethyl-1,10-phenanthroline-\k^2^N,N')bis(2-hydroxybenzoato-\kO)copper(II) ; _journal_coeditor_code HG2438 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1526 _journal_page_last m1527 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.023 _cell_angle_gamma 90.000 _cell_length_a 23.8186 _cell_length_b 12.2576 _cell_length_c 17.9084 _exptl_crystal_F_000 2248.00 _reflns_d_resolution_high 0.8254 _[local]_cod_data_source_file hg2438Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' B in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 394.22 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 798.57 793.84 34.25 o 4 0 0 155411.55 151168.64 2226.71 o 5 0 0 1738.37 1623.46 47.50 o 6 0 0 64219.88 64555.62 813.42 o 7 0 0 796.26 831.80 61.87 o 8 0 0 14914.44 14304.43 227.69 o 9 0 0 2073.71 2086.88 69.87 o 10 0 0 5553.84 5044.02 162.93 o 11 0 0 610.68 812.32 85.76 o 12 0 0 30309.96 28606.24 538.18 o 13 0 0 343.65 514.29 65.83 o 14 0 0 16463.92 16961.58 380.83 o 15 0 0 198.53 245.28 99.86 o 16 0 0 1253.96 1417.57 111.51 o 17 0 0 273.14 291.76 67.68 o 18 0 0 3257.41 3354.29 167.16 o 19 0 0 2996.11 3223.00 179.76 o 20 0 0 1968.99 2088.94 152.57 o 21 0 0 62.63 -1.27 91.78 o 22 0 0 171.84 198.13 74.09 o 23 0 0 214.86 302.88 85.65 o 24 0 0 2652.50 2883.97 195.94 o 25 0 0 69.85 141.13 89.65 o 26 0 0 773.93 570.66 161.94 o 2 1 0 270.30 215.29 22.05 o 3 1 0 100552.44 98097.41 1196.82 o 4 1 0 268.32 251.53 16.78 o 5 1 0 30.60 14.29 14.28 o 6 1 0 39.00 43.77 14.96 o 7 1 0 12895.33 12015.93 154.82 o 8 1 0 33.40 47.18 16.83 o 9 1 0 28888.25 26864.12 305.08 o 10 1 0 383.19 335.72 30.53 o 11 1 0 9567.05 8492.24 158.89 o 12 1 0 1352.21 1419.71 57.31 o 13 1 0 1396.47 1319.30 81.24 o 14 1 0 22.56 40.18 24.55 o 15 1 0 16537.07 15945.82 233.10 o 16 1 0 214.56 280.86 38.10 o 17 1 0 4516.05 4837.02 136.18 o 18 1 0 1231.89 1112.18 77.07 o 19 1 0 362.94 294.27 77.41 o 20 1 0 102.81 108.02 44.21 o 21 1 0 3634.85 3906.00 140.83 o 22 1 0 0.06 41.38 43.07 o 23 1 0 2009.87 2201.04 120.37 o 24 1 0 138.59 221.84 72.66 o 25 1 0 18.74 -9.88 55.31 o 26 1 0 28.02 60.34 61.84 o 0 2 0 38119.99 36807.21 468.20 o 1 2 0 0.56 -9.55 6.37 o 2 2 0 42219.65 42247.12 415.26 o 3 2 0 1336.71 1399.04 34.43 o 4 2 0 517.76 473.60 24.14 o 5 2 0 783.77 781.16 32.34 o 6 2 0 21182.16 20211.98 231.15 o 7 2 0 491.95 518.06 33.07 o 8 2 0 6657.26 5974.32 102.01 o 9 2 0 4.30 1.72 16.57 o 10 2 0 5372.69 5128.40 100.01 o 11 2 0 0.95 -17.97 17.22 o 12 2 0 11696.88 11360.31 174.95 o 13 2 0 80.09 32.26 24.16 o 14 2 0 2415.03 2284.62 77.60 o 15 2 0 13.57 28.04 27.09 o 16 2 0 1211.53 1219.55 71.42 o 17 2 0 7.37 -26.78 26.27 o 18 2 0 2400.66 2624.10 96.61 o 19 2 0 1.76 -19.38 32.40 o 20 2 0 150.70 148.81 46.78 o 21 2 0 979.08 875.19 79.88 o 22 2 0 760.58 777.98 94.64 o 23 2 0 194.89 144.04 62.71 o 24 2 0 660.38 792.93 101.10 o 25 2 0 1.63 40.36 59.50 o 26 2 0 231.45 210.76 109.71 o 1 3 0 38053.82 36893.93 342.12 o 2 3 0 18343.21 18689.54 202.41 o 3 3 0 6648.07 6149.03 82.03 o 4 3 0 616.47 663.40 27.36 o 5 3 0 9934.14 9294.34 113.12 o 6 3 0 26.16 1.90 14.03 o 7 3 0 4639.10 4474.13 85.33 o 8 3 0 1.58 16.78 16.31 o 9 3 0 24634.70 23939.74 321.68 o 10 3 0 415.18 466.59 39.16 o 11 3 0 2470.11 2439.79 79.90 o 12 3 0 86.70 97.10 26.99 o 13 3 0 4951.75 4744.97 121.45 o 14 3 0 302.17 322.85 39.55 o 15 3 0 14557.26 13623.42 214.95 o 16 3 0 17.73 6.24 28.37 o 17 3 0 2868.23 2982.37 98.25 o 18 3 0 0.86 20.40 31.10 o 19 3 0 1609.52 1756.95 85.28 o 20 3 0 345.75 366.22 69.15 o 21 3 0 1742.62 1952.93 215.18 o 22 3 0 0.29 -46.78 60.25 o 23 3 0 110.15 77.98 78.49 o 24 3 0 77.34 192.87 69.98 o 25 3 0 78.91 9.63 58.72 o 26 3 0 8.18 20.61 60.89 o 0 4 0 13289.37 12652.54 206.29 o 1 4 0 9.21 11.24 15.36 o 2 4 0 10893.12 11762.57 138.75 o 3 4 0 10864.01 11416.65 136.56 o 4 4 0 1052.47 1212.53 38.34 o 5 4 0 2903.13 2804.84 57.07 o 6 4 0 10322.50 9516.20 123.64 o 7 4 0 1276.71 1289.82 40.41 o 8 4 0 18766.93 18423.82 206.67 o 9 4 0 68.61 56.55 26.28 o 10 4 0 7811.92 8134.44 140.85 o 11 4 0 0.14 -15.48 19.41 o 12 4 0 11530.53 11457.15 191.87 o 13 4 0 90.85 117.22 31.90 o 14 4 0 2096.32 2071.87 164.32 o 15 4 0 60.97 71.76 31.10 o 16 4 0 380.80 387.82 47.11 o 17 4 0 281.51 278.26 44.39 o 18 4 0 2376.54 2573.43 114.26 o 19 4 0 47.59 -1.13 39.08 o 20 4 0 1129.29 1212.40 91.60 o 21 4 0 273.17 144.91 60.74 o 22 4 0 376.47 393.54 78.90 o 23 4 0 224.19 268.94 73.70 o 24 4 0 1076.41 1041.36 116.71 o 25 4 0 0.08 -3.59 66.69 o 1 5 0 3641.31 3315.60 65.68 o 2 5 0 1166.41 1257.41 49.37 o 3 5 0 47258.44 45952.35 440.36 o 4 5 0 1271.54 1194.40 42.28 o 5 5 0 3519.92 3275.49 67.51 o 6 5 0 35.40 42.14 17.47 o 7 5 0 18152.90 18268.18 247.56 o 8 5 0 5925.60 6195.28 100.78 o 9 5 0 18630.66 18418.08 225.68 o 10 5 0 0.34 54.06 34.38 o 11 5 0 995.84 854.13 52.57 o 12 5 0 24.00 9.34 25.84 o 13 5 0 1500.05 1510.92 70.69 o 14 5 0 289.01 288.04 41.45 o 15 5 0 3248.11 3336.21 101.96 o 16 5 0 1058.56 1099.80 69.09 o 17 5 0 1546.48 1606.33 95.15 o 18 5 0 485.54 477.42 92.72 o 19 5 0 22.20 54.62 45.58 o 20 5 0 49.54 66.84 46.49 o 21 5 0 1938.11 1922.53 154.22 o 22 5 0 0.47 5.13 56.75 o 23 5 0 667.96 628.14 98.27 o 24 5 0 55.27 110.02 66.81 o 25 5 0 22.62 -8.85 62.03 o 0 6 0 6721.27 6281.76 144.65 o 1 6 0 1127.82 1222.55 45.84 o 2 6 0 641.75 571.64 38.67 o 3 6 0 7870.54 8077.82 121.04 o 4 6 0 4780.73 4955.75 97.25 o 5 6 0 812.69 881.99 41.92 o 6 6 0 10363.32 10627.63 148.47 o 7 6 0 1657.80 1837.84 57.54 o 8 6 0 4549.55 4426.98 93.20 o 9 6 0 7.04 11.43 22.49 o 10 6 0 787.65 864.43 53.85 o 11 6 0 89.26 94.43 29.41 o 12 6 0 4908.16 5056.09 120.19 o 13 6 0 2.11 -38.80 25.86 o 14 6 0 566.57 515.03 52.30 o 15 6 0 702.51 644.34 109.38 o 16 6 0 3.07 14.89 37.23 o 17 6 0 2.48 14.36 40.95 o 18 6 0 1548.47 1451.19 135.40 o 19 6 0 278.73 225.67 61.70 o 20 6 0 1120.47 1083.98 94.31 o 21 6 0 31.97 19.38 49.99 o 22 6 0 1.15 0.99 45.99 o 23 6 0 7.97 -3.59 73.66 o 24 6 0 743.33 714.62 103.50 o 1 7 0 7689.29 7483.44 125.65 o 2 7 0 760.50 734.58 46.87 o 3 7 0 1291.98 1175.82 49.42 o 4 7 0 643.46 660.88 40.99 o 5 7 0 20.91 9.21 20.94 o 6 7 0 29.14 -2.19 22.25 o 7 7 0 731.51 693.87 63.33 o 8 7 0 482.86 557.39 46.43 o 9 7 0 5924.21 5811.21 126.35 o 10 7 0 565.79 596.72 55.97 o 11 7 0 229.42 184.58 46.93 o 12 7 0 658.94 560.81 52.00 o 13 7 0 802.85 736.92 69.39 o 14 7 0 816.40 697.31 106.57 o 15 7 0 86.88 158.76 45.45 o 16 7 0 871.01 1058.26 87.33 o 17 7 0 5.23 10.63 39.46 o 18 7 0 30.85 47.71 43.81 o 19 7 0 57.26 42.32 46.90 o 20 7 0 19.54 27.23 48.30 o 21 7 0 327.11 307.06 69.72 o 22 7 0 193.84 155.04 60.07 o 23 7 0 309.94 231.80 97.09 o 0 8 0 2546.57 2638.62 141.73 o 1 8 0 39.62 7.45 21.45 o 2 8 0 213.30 192.90 29.63 o 3 8 0 34.33 12.24 22.26 o 4 8 0 1297.13 1339.93 57.07 o 5 8 0 68.17 31.83 23.45 o 6 8 0 2331.84 2491.68 121.28 o 7 8 0 312.05 414.70 44.24 o 8 8 0 2408.90 2430.14 86.59 o 9 8 0 49.30 44.42 34.25 o 10 8 0 79.19 67.71 32.43 o 11 8 0 68.47 39.48 35.64 o 12 8 0 1031.90 993.16 77.91 o 13 8 0 89.47 77.04 42.18 o 14 8 0 28.16 44.23 58.40 o 15 8 0 7.92 -34.69 37.11 o 16 8 0 418.92 414.90 63.46 o 17 8 0 40.23 25.38 69.83 o 18 8 0 962.54 1152.35 111.70 o 19 8 0 164.50 103.74 53.94 o 20 8 0 249.14 160.35 71.62 o 21 8 0 60.92 87.22 63.24 o 22 8 0 33.85 -84.84 56.56 o 1 9 0 4.09 -5.05 24.98 o 2 9 0 226.76 151.44 31.28 o 3 9 0 1504.67 1559.65 66.90 o 4 9 0 109.25 145.06 31.22 o 5 9 0 2730.04 2637.65 80.60 o 6 9 0 399.11 440.47 56.26 o 7 9 0 201.20 204.56 38.83 o 8 9 0 11.43 -40.87 27.25 o 9 9 0 2609.67 2784.58 112.38 o 10 9 0 0.79 -47.01 31.34 o 11 9 0 465.50 576.79 90.25 o 12 9 0 31.04 7.56 38.47 o 13 9 0 17.77 -49.56 40.55 o 14 9 0 243.84 163.76 51.49 o 15 9 0 323.69 438.53 124.68 o 16 9 0 2.99 106.56 59.06 o 17 9 0 510.65 628.07 94.66 o 18 9 0 0.48 59.24 60.64 o 19 9 0 17.38 -41.28 57.14 o 20 9 0 53.22 -13.74 61.38 o 21 9 0 437.84 390.23 89.88 o 0 10 0 1704.15 1813.21 102.28 o 1 10 0 4.26 5.85 28.04 o 2 10 0 1520.09 1703.65 76.99 o 3 10 0 24.65 -22.03 27.00 o 4 10 0 839.58 1034.31 72.46 o 5 10 0 42.32 56.31 33.09 o 6 10 0 1313.47 1383.31 78.99 o 7 10 0 450.82 454.45 63.08 o 8 10 0 280.85 203.85 65.11 o 9 10 0 106.70 40.40 47.40 o 10 10 0 1.00 18.96 45.06 o 11 10 0 219.96 168.04 59.93 o 12 10 0 167.27 280.69 69.24 o 13 10 0 337.57 266.74 108.94 o 14 10 0 112.34 21.05 54.55 o 15 10 0 91.25 191.08 71.04 o 16 10 0 31.34 -3.01 59.97 o 17 10 0 192.33 307.97 79.37 o 18 10 0 493.02 428.33 90.67 o 19 10 0 83.43 32.57 68.49 o 1 11 0 2153.84 2413.90 85.52 o 2 11 0 65.74 101.99 32.39 o 3 11 0 504.45 531.21 56.61 o 4 11 0 146.32 101.32 44.76 o 5 11 0 2.72 -10.29 41.35 o 6 11 0 8.00 -30.08 54.99 o 7 11 0 116.44 17.64 48.09 o 8 11 0 141.12 85.01 56.29 o 9 11 0 165.40 281.66 66.88 o 10 11 0 296.50 319.68 74.80 o 11 11 0 54.72 44.22 50.85 o 12 11 0 371.52 336.33 77.59 o 13 11 0 0.51 -12.33 51.74 o 14 11 0 9.21 -26.18 56.53 o 15 11 0 143.08 177.75 70.95 o 16 11 0 53.59 -42.55 59.89 o 17 11 0 192.98 272.19 117.03 o 0 12 0 602.80 656.02 117.68 o 1 12 0 8.20 -17.23 40.84 o 2 12 0 105.64 100.87 41.02 o 3 12 0 18.12 1.07 53.93 o 4 12 0 86.50 117.63 53.49 o 5 12 0 97.60 60.86 53.55 o 6 12 0 78.76 60.11 55.19 o 7 12 0 209.51 129.51 60.73 o 8 12 0 12.23 6.49 52.31 o 9 12 0 7.03 -1.55 52.74 o 10 12 0 9.28 -25.37 51.54 o 11 12 0 52.69 59.97 58.29 o 12 12 0 210.24 169.18 73.10 o 13 12 0 394.07 243.82 78.80 o 14 12 0 12.02 49.74 66.73 o 15 12 0 17.84 -56.30 58.82 o 1 13 0 71.47 220.90 66.42 o 2 13 0 233.40 203.39 79.53 o 3 13 0 482.63 380.93 173.67 o 4 13 0 251.83 273.39 87.46 o 5 13 0 31.76 70.67 72.13 o 6 13 0 166.21 160.73 91.12 o 7 13 0 59.20 16.12 71.19 o 8 13 0 137.49 77.49 81.44 o 9 13 0 19.43 -19.67 55.74 o 10 13 0 492.21 521.03 142.12 o 11 13 0 48.04 -15.97 85.56 o 12 13 0 120.43 -54.68 71.46 o 0 14 0 58.03 -131.47 98.72 o 1 14 0 11.94 -92.01 94.14 o 2 14 0 30.82 -60.13 109.53 o 3 14 0 43.65 -41.66 72.17 o 4 14 0 0.35 39.55 78.43 o 5 14 0 207.19 163.15 89.32 o 6 14 0 196.76 254.88 101.94 o 7 14 0 264.49 238.06 238.10 o 8 14 0 11.79 -40.94 80.42 o -27 1 1 0.01 -52.61 66.91 o -26 1 1 91.22 19.43 72.81 o -25 1 1 4.55 78.94 61.30 o -24 1 1 14.36 18.68 57.85 o -23 1 1 11.98 28.52 50.64 o -22 1 1 262.49 187.73 53.03 o -21 1 1 0.03 35.01 40.71 o -20 1 1 110.19 144.73 47.47 o -19 1 1 162.99 175.44 44.69 o -18 1 1 30.75 12.35 31.45 o -17 1 1 10.25 28.16 31.57 o -16 1 1 14.50 29.15 30.65 o -15 1 1 22.14 37.54 28.74 o -14 1 1 1200.28 1277.67 67.07 o -13 1 1 326.61 298.69 33.29 o -12 1 1 1207.70 1282.42 72.70 o -11 1 1 74.06 35.19 20.63 o -10 1 1 1635.21 1521.50 51.46 o -9 1 1 519.55 613.00 33.36 o -8 1 1 7.80 31.44 15.05 o -7 1 1 598.15 493.46 27.10 o -6 1 1 13.25 32.25 18.15 o -5 1 1 9436.99 9730.29 119.80 o -4 1 1 620.66 691.83 26.66 o -3 1 1 25498.22 24446.00 276.52 o -2 1 1 1212.17 1167.55 32.39 o 1 1 1 7669.01 7122.78 134.64 o 2 1 1 64.38 102.16 11.68 o 3 1 1 39446.04 40545.79 400.21 o 4 1 1 921.95 1016.89 31.16 o 5 1 1 430.22 411.99 24.50 o 6 1 1 837.13 900.96 35.51 o 7 1 1 2473.75 2742.22 64.30 o 8 1 1 122.89 113.74 16.84 o 9 1 1 109.84 138.61 19.11 o 10 1 1 270.80 282.39 30.15 o 11 1 1 992.37 995.96 53.24 o 12 1 1 8.42 7.93 23.57 o 13 1 1 1969.14 1962.86 70.03 o 14 1 1 214.15 175.91 32.59 o 15 1 1 200.14 218.02 44.53 o 16 1 1 594.65 567.65 49.62 o 17 1 1 45.89 16.99 32.59 o 18 1 1 1609.87 1674.32 92.95 o 19 1 1 623.43 697.35 69.95 o 20 1 1 159.42 123.07 45.00 o 21 1 1 20.87 21.60 41.67 o 22 1 1 301.17 386.45 69.99 o 23 1 1 8.85 40.45 42.89 o 24 1 1 83.35 69.33 50.75 o 25 1 1 9.80 55.56 60.05 o 26 1 1 171.11 115.46 68.66 o -26 2 1 99.92 134.54 70.64 o -25 2 1 184.16 229.87 71.80 o -24 2 1 38.31 19.90 54.79 o -23 2 1 7.07 -5.72 54.81 o -22 2 1 35.10 37.78 66.07 o -21 2 1 427.28 444.97 74.55 o -20 2 1 744.07 912.05 78.34 o -19 2 1 553.86 600.64 74.14 o -18 2 1 205.04 154.87 40.37 o -17 2 1 642.64 629.80 60.29 o -16 2 1 426.32 490.21 61.09 o -15 2 1 10.87 -9.78 23.33 o -14 2 1 123.48 90.50 43.03 o -13 2 1 1773.40 1663.41 64.00 o -12 2 1 0.36 -6.00 18.41 o -11 2 1 416.02 495.64 49.63 o -10 2 1 1.79 12.10 17.67 o -9 2 1 102.33 91.61 21.29 o -8 2 1 4586.66 4962.00 88.60 o -7 2 1 1539.12 1513.11 55.56 o -6 2 1 8672.47 8453.96 129.84 o -5 2 1 7021.53 6792.66 92.23 o -4 2 1 725.38 868.90 28.47 o -3 2 1 8201.65 8393.52 104.49 o -2 2 1 2794.92 2680.56 53.59 o -1 2 1 11270.12 10909.72 141.85 o 0 2 1 1505.56 1530.71 33.98 o 1 2 1 105.47 146.73 15.72 o 2 2 1 1506.74 1402.64 33.31 o 3 2 1 1433.32 1382.66 50.51 o 4 2 1 5652.22 5559.92 84.85 o 5 2 1 12627.44 12153.89 153.85 o 6 2 1 56.63 107.88 29.51 o 7 2 1 578.77 515.49 32.09 o 8 2 1 930.72 751.21 50.01 o 9 2 1 144.14 168.75 24.92 o 10 2 1 1299.84 1398.48 65.70 o 11 2 1 1333.96 1394.38 57.71 o 12 2 1 512.67 526.44 43.05 o 13 2 1 749.17 708.32 49.80 o 14 2 1 1734.62 1856.50 73.38 o 15 2 1 99.86 85.10 31.19 o 16 2 1 354.81 346.55 44.10 o 17 2 1 1039.09 971.17 64.75 o 18 2 1 209.65 195.36 46.61 o 19 2 1 80.75 48.77 37.71 o 20 2 1 32.01 6.43 38.07 o 21 2 1 8.31 -11.52 36.92 o 22 2 1 236.16 184.29 52.96 o 23 2 1 12.25 -19.65 54.04 o 24 2 1 0.64 -7.47 54.07 o 25 2 1 35.37 -3.71 58.77 o -26 3 1 6.39 -20.33 59.71 o -25 3 1 38.89 78.50 64.68 o -24 3 1 211.32 199.41 68.15 o -23 3 1 119.32 92.98 59.97 o -22 3 1 2.38 -21.73 50.47 o -21 3 1 79.88 60.09 54.43 o -20 3 1 42.22 53.43 51.79 o -19 3 1 101.15 61.50 39.56 o -18 3 1 208.43 237.52 44.84 o -17 3 1 19.56 44.33 29.87 o -16 3 1 337.67 342.18 43.14 o -15 3 1 872.55 855.16 56.39 o -14 3 1 797.89 836.40 52.31 o -13 3 1 5444.88 5670.97 118.30 o -12 3 1 942.30 786.05 49.80 o -11 3 1 586.46 546.52 39.82 o -10 3 1 6077.86 5828.97 111.01 o -9 3 1 52.51 23.92 16.10 o -8 3 1 957.26 990.31 34.48 o -7 3 1 680.33 828.85 62.46 o -6 3 1 15.25 67.23 20.29 o -5 3 1 11133.80 11456.43 131.83 o -4 3 1 16751.36 17250.25 179.59 o -3 3 1 12967.58 13923.00 149.12 o -2 3 1 17977.51 18736.25 189.17 o -1 3 1 97487.08 98920.66 860.74 o 0 3 1 5712.97 5542.21 74.28 o 1 3 1 76403.83 79614.93 700.69 o 2 3 1 31192.43 31587.17 299.32 o 3 3 1 2574.31 2748.20 49.88 o 4 3 1 2086.26 2223.54 52.81 o 5 3 1 52.76 36.93 16.10 o 6 3 1 1362.30 1501.00 48.40 o 7 3 1 3188.36 3053.08 70.82 o 8 3 1 191.97 144.32 30.89 o 9 3 1 1190.26 1133.03 50.37 o 10 3 1 5045.03 4828.90 101.46 o 11 3 1 1559.50 1792.17 89.23 o 12 3 1 0.83 -7.95 21.80 o 13 3 1 12.05 -21.80 22.93 o 14 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