#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2220219.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220219_Fobs loop_ _publ_author_name 'Thiruvalluvar, A.' 'Balamurugan, S.' 'Butcher, R. J.' 'Pandiarajan, K.' 'Devanathan, D.' _publ_section_title ; 2-r-(4-Chlorophenyl)-6-c-phenyl-3,4,5,6-tetrahydro-2H-thiopyran-4-one 1-oxide ; _journal_coeditor_code HG2443 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2367 _journal_volume 64 _journal_year 2008 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.5195 _cell_length_b 25.7589 _cell_length_c 5.2248 _exptl_crystal_F_000 664.00 _reflns_d_resolution_high 0.7504 _[local]_cod_data_source_file hg2443Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AT_KP108A in Pnma C17H15CLO2S Z=4' _shelx_refln_list_code 4 _shelx_F_calc_maximum 156.54 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z-1/2' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 24505.26 26289.21 395.28 o 4 0 0 1282.73 1563.76 17.44 o 6 0 0 1548.26 1678.40 21.00 o 8 0 0 6.97 7.97 1.44 o 10 0 0 499.89 475.98 10.60 o 12 0 0 294.74 279.25 11.36 o 14 0 0 78.74 89.25 7.93 o 2 1 0 972.97 967.16 8.09 o 4 1 0 1291.46 1437.38 13.73 o 6 1 0 2655.88 3199.89 29.63 o 8 1 0 55.14 65.41 1.75 o 10 1 0 7.22 23.47 2.33 o 12 1 0 117.83 122.43 5.79 o 14 1 0 19.28 17.42 4.40 o 0 2 0 7199.16 -0.07 0.10 o 2 2 0 870.15 891.06 7.21 o 4 2 0 11536.51 12446.43 112.28 o 6 2 0 450.06 506.65 6.37 o 8 2 0 46.64 44.49 1.45 o 10 2 0 450.56 479.68 8.63 o 12 2 0 137.01 143.94 5.81 o 14 2 0 38.61 41.38 4.70 o 2 3 0 10349.26 10976.52 81.89 o 4 3 0 559.18 719.04 6.60 o 6 3 0 119.48 112.97 1.93 o 8 3 0 354.43 343.84 5.17 o 10 3 0 50.04 43.07 2.52 o 12 3 0 154.21 144.49 4.71 o 14 3 0 2.26 1.81 3.47 o 0 4 0 4661.08 4847.49 46.69 o 2 4 0 4058.82 4257.43 28.01 o 4 4 0 766.41 724.68 6.17 o 6 4 0 1678.92 1574.31 17.11 o 8 4 0 1.61 2.06 1.57 o 10 4 0 118.24 111.84 3.36 o 12 4 0 69.16 77.41 3.81 o 14 4 0 36.32 30.92 3.85 o 2 5 0 2147.93 2136.43 14.21 o 4 5 0 252.33 305.13 2.99 o 6 5 0 63.19 69.15 1.75 o 8 5 0 246.11 215.50 3.47 o 10 5 0 15.43 10.49 1.96 o 12 5 0 136.14 126.23 4.12 o 14 5 0 1.19 2.67 3.44 o 0 6 0 8644.37 8701.71 80.70 o 2 6 0 3431.68 3366.99 23.44 o 4 6 0 1980.05 1797.92 15.47 o 6 6 0 2.42 -0.18 0.67 o 8 6 0 257.87 248.33 3.79 o 10 6 0 310.40 274.17 5.44 o 12 6 0 114.69 122.25 4.00 o 14 6 0 87.52 86.33 5.67 o 2 7 0 310.85 302.09 2.27 o 4 7 0 1209.32 1125.84 9.88 o 6 7 0 73.64 57.95 1.32 o 8 7 0 113.17 115.66 2.61 o 10 7 0 3.05 2.16 2.26 o 12 7 0 169.44 159.42 4.50 o 14 7 0 4.24 7.01 3.66 o 0 8 0 7373.99 7434.67 73.28 o 2 8 0 628.41 657.86 5.57 o 4 8 0 323.04 396.95 3.68 o 6 8 0 348.22 308.36 3.55 o 8 8 0 454.09 410.21 5.64 o 10 8 0 398.58 373.10 6.64 o 12 8 0 325.08 361.85 6.93 o 14 8 0 127.40 135.03 5.50 o 2 9 0 350.53 395.30 3.81 o 4 9 0 274.02 234.19 2.47 o 6 9 0 685.23 671.91 7.19 o 8 9 0 28.81 24.29 1.73 o 10 9 0 94.92 95.60 3.38 o 12 9 0 144.16 153.41 4.77 o 14 9 0 18.80 23.91 3.37 o 0 10 0 1078.24 1068.22 12.73 o 2 10 0 3583.15 3585.84 32.27 o 4 10 0 2918.08 2912.68 24.18 o 6 10 0 23.50 35.32 1.61 o 8 10 0 935.27 904.23 10.30 o 10 10 0 603.45 584.58 9.26 o 12 10 0 243.65 243.40 6.45 o 14 10 0 117.20 112.70 4.44 o 2 11 0 1191.68 1180.65 10.96 o 4 11 0 153.15 158.95 1.84 o 6 11 0 152.05 122.34 1.95 o 8 11 0 97.80 101.01 2.48 o 10 11 0 14.88 21.46 2.47 o 12 11 0 44.48 38.27 3.06 o 14 11 0 51.13 50.86 4.22 o 0 12 0 2783.21 2495.96 30.55 o 2 12 0 0.44 2.78 0.80 o 4 12 0 516.01 471.29 4.25 o 6 12 0 1915.65 1784.29 17.34 o 8 12 0 1020.60 952.19 10.60 o 10 12 0 86.88 65.62 2.99 o 12 12 0 75.43 84.55 5.80 o 14 12 0 64.74 71.20 4.53 o 2 13 0 5.80 4.92 0.59 o 4 13 0 511.07 536.73 4.77 o 6 13 0 161.08 169.54 2.43 o 8 13 0 232.46 209.15 3.96 o 10 13 0 0.18 -0.35 2.19 o 12 13 0 56.41 45.62 3.39 o 14 13 0 10.26 2.73 3.58 o 0 14 0 341.83 379.77 5.23 o 2 14 0 54.66 43.89 1.18 o 4 14 0 853.18 740.75 6.40 o 6 14 0 34.62 45.38 1.44 o 8 14 0 3.30 2.85 1.43 o 10 14 0 55.94 61.88 2.98 o 12 14 0 59.30 66.50 4.00 o 14 14 0 19.94 21.61 5.86 o 2 15 0 9.29 18.30 1.03 o 4 15 0 11.60 9.92 0.96 o 6 15 0 15.17 16.62 1.25 o 8 15 0 1.74 -1.16 1.30 o 10 15 0 0.36 -0.62 2.14 o 12 15 0 96.01 98.73 5.54 o 0 16 0 7873.04 7574.62 91.62 o 2 16 0 514.06 524.38 5.37 o 4 16 0 5.32 3.14 0.68 o 6 16 0 9.20 9.74 1.22 o 8 16 0 0.64 -0.54 1.28 o 10 16 0 37.89 33.14 2.52 o 12 16 0 62.90 70.45 3.37 o 2 17 0 4.87 4.70 1.24 o 4 17 0 201.70 162.71 2.17 o 6 17 0 140.26 119.61 2.11 o 8 17 0 0.00 -1.15 1.39 o 10 17 0 16.69 13.48 2.30 o 12 17 0 37.13 40.17 3.03 o 0 18 0 1347.26 1208.49 15.37 o 2 18 0 708.20 642.83 6.81 o 4 18 0 954.32 903.41 9.80 o 6 18 0 305.91 274.94 3.37 o 8 18 0 65.97 67.29 2.18 o 10 18 0 57.06 56.61 2.84 o 12 18 0 29.24 25.93 2.82 o 2 19 0 238.04 255.70 3.39 o 4 19 0 38.33 44.55 1.59 o 6 19 0 41.73 38.39 1.53 o 8 19 0 3.97 8.78 1.78 o 10 19 0 11.88 9.62 2.25 o 12 19 0 4.38 -0.49 2.61 o 0 20 0 1432.40 1283.13 16.35 o 2 20 0 91.87 85.00 2.02 o 4 20 0 260.28 216.08 3.46 o 6 20 0 319.43 306.52 3.93 o 8 20 0 7.67 9.32 1.98 o 10 20 0 36.56 35.16 2.52 o 12 20 0 30.11 28.38 3.63 o 2 21 0 31.28 29.17 1.58 o 4 21 0 0.91 4.88 1.46 o 6 21 0 2.67 1.41 1.15 o 8 21 0 0.21 -0.43 1.84 o 10 21 0 0.70 -2.12 2.12 o 12 21 0 3.60 4.04 3.24 o 0 22 0 263.73 255.74 4.26 o 2 22 0 188.86 172.60 2.87 o 4 22 0 261.74 241.75 3.76 o 6 22 0 13.14 8.67 1.18 o 8 22 0 2.23 3.12 1.84 o 10 22 0 33.20 36.63 2.72 o 2 23 0 19.06 27.52 1.77 o 4 23 0 6.48 6.20 1.50 o 6 23 0 33.47 30.72 1.91 o 8 23 0 3.42 3.59 1.91 o 10 23 0 8.34 6.83 2.36 o 0 24 0 523.62 500.08 7.35 o 2 24 0 15.71 20.84 1.76 o 4 24 0 1.30 0.87 1.49 o 6 24 0 22.63 30.53 2.86 o 8 24 0 4.31 2.89 1.93 o 10 24 0 8.95 1.46 2.39 o 2 25 0 9.76 15.84 1.70 o 4 25 0 1.37 -1.07 1.49 o 6 25 0 3.65 2.33 1.95 o 8 25 0 9.64 6.52 2.20 o 10 25 0 0.21 -2.13 2.30 o 0 26 0 1.07 0.27 1.99 o 2 26 0 15.07 18.12 1.79 o 4 26 0 50.61 58.14 2.32 o 6 26 0 0.01 -2.02 2.02 o 8 26 0 10.69 14.41 2.70 o 10 26 0 24.59 30.47 2.73 o 2 27 0 0.08 -1.56 1.56 o 4 27 0 9.14 7.78 1.76 o 6 27 0 13.01 9.15 2.36 o 8 27 0 8.00 14.60 3.68 o 0 28 0 26.68 27.17 3.70 o 2 28 0 6.87 5.89 1.69 o 4 28 0 32.44 37.00 2.99 o 6 28 0 68.95 71.55 5.16 o 8 28 0 58.10 73.43 4.19 o 2 29 0 4.14 4.19 1.72 o 4 29 0 2.50 1.57 1.97 o 6 29 0 1.98 4.07 2.54 o 8 29 0 4.25 10.04 3.32 o 0 30 0 13.29 15.35 2.62 o 2 30 0 39.08 41.52 2.59 o 4 30 0 33.06 37.81 2.76 o 6 30 0 7.16 7.34 2.66 o 2 31 0 1.61 0.40 1.88 o 4 31 0 0.97 1.78 2.39 o 6 31 0 0.61 -1.99 2.85 o 0 32 0 14.88 18.60 3.39 o 2 32 0 4.74 5.70 2.10 o 4 32 0 1.18 -2.59 2.59 o 2 33 0 0.00 -2.14 2.18 o 4 33 0 0.77 1.68 2.65 o 0 34 0 0.00 -2.96 2.96 o 2 34 0 1.98 1.23 3.22 o 1 0 1 2481.32 2557.34 22.11 o 2 0 1 274.96 275.53 7.44 o 3 0 1 3417.64 3493.01 28.93 o 4 0 1 1.49 10.71 1.22 o 5 0 1 245.19 202.72 3.49 o 6 0 1 711.02 836.78 9.79 o 7 0 1 698.56 720.86 9.99 o 8 0 1 8.01 34.33 4.00 o 9 0 1 10.18 14.95 2.21 o 10 0 1 71.17 81.07 3.05 o 11 0 1 0.54 -1.99 2.15 o 12 0 1 6.36 9.94 3.71 o 13 0 1 0.05 -3.58 3.58 o 14 0 1 50.07 54.69 5.20 o 15 0 1 42.84 45.67 6.37 o 0 1 1 12051.30 12001.73 103.92 o 1 1 1 2487.61 2783.87 16.58 o 2 1 1 14634.53 15778.91 90.20 o 3 1 1 762.15 781.67 4.73 o 4 1 1 1376.21 1551.42 10.04 o 5 1 1 1066.49 1192.43 7.83 o 6 1 1 544.72 596.53 4.95 o 7 1 1 0.45 8.27 1.23 o 8 1 1 865.48 838.49 8.20 o 9 1 1 37.43 52.19 1.87 o 10 1 1 241.17 236.98 3.38 o 11 1 1 18.31 12.91 1.66 o 12 1 1 211.53 212.27 4.46 o 13 1 1 0.32 0.29 2.68 o 14 1 1 133.49 146.95 4.34 o 15 1 1 0.13 1.47 2.89 o 1 2 1 190.66 198.77 1.39 o 2 2 1 4110.79 4390.46 25.76 o 3 2 1 1113.82 1154.30 6.75 o 4 2 1 231.96 247.47 2.61 o 5 2 1 380.39 370.44 3.16 o 6 2 1 18.44 31.65 1.11 o 7 2 1 98.47 103.77 1.84 o 8 2 1 13.89 33.30 1.82 o 9 2 1 0.41 -1.15 1.46 o 10 2 1 133.64 111.76 2.44 o 11 2 1 6.34 9.94 1.64 o 12 2 1 2.66 12.58 2.11 o 13 2 1 0.00 -2.35 2.35 o 14 2 1 47.86 48.87 3.25 o 15 2 1 25.28 28.11 3.20 o 0 3 1 5159.33 5461.42 45.16 o 1 3 1 1075.42 908.06 5.11 o 2 3 1 1212.67 1637.56 8.71 o 3 3 1 781.29 831.30 4.67 o 4 3 1 1711.85 1625.43 10.14 o 5 3 1 1907.14 2030.60 14.29 o 6 3 1 712.86 693.67 5.54 o 7 3 1 13.83 22.68 0.98 o 8 3 1 583.39 559.01 5.82 o 9 3 1 0.61 -1.44 1.44 o 10 3 1 140.18 150.99 2.70 o 11 3 1 4.43 1.07 1.76 o 12 3 1 138.57 133.88 3.14 o 13 3 1 3.96 -2.36 2.36 o 14 3 1 83.63 81.10 3.58 o 15 3 1 0.22 0.58 2.70 o 1 4 1 8049.01 7686.44 40.09 o 2 4 1 49.44 71.06 0.83 o 3 4 1 853.41 793.41 4.60 o 4 4 1 788.65 843.79 5.81 o 5 4 1 214.49 200.48 1.93 o 6 4 1 62.81 63.72 1.13 o 7 4 1 9.21 9.94 0.90 o 8 4 1 79.59 75.91 1.71 o 9 4 1 0.71 0.48 1.37 o 10 4 1 96.38 84.45 2.07 o 11 4 1 8.79 8.41 1.86 o 12 4 1 0.59 4.46 1.92 o 13 4 1 0.66 -2.28 2.28 o 14 4 1 50.27 58.15 3.17 o 15 4 1 2.23 -2.65 2.65 o 0 5 1 534.85 527.49 3.90 o 1 5 1 4729.66 4963.99 25.86 o 2 5 1 2481.05 2813.89 15.35 o 3 5 1 1331.93 1369.44 8.37 o 4 5 1 17.27 124.03 1.52 o 5 5 1 68.71 70.05 1.07 o 6 5 1 149.39 127.00 1.59 o 7 5 1 45.89 53.94 1.24 o 8 5 1 620.08 582.15 5.03 o 9 5 1 33.87 31.54 1.63 o 10 5 1 122.02 122.15 2.39 o 11 5 1 53.22 47.27 2.20 o 12 5 1 113.29 107.25 2.77 o 13 5 1 0.54 -1.85 1.85 o 14 5 1 79.79 78.72 3.37 o 15 5 1 1.11 -2.28 2.63 o 1 6 1 3822.62 3838.69 19.69 o 2 6 1 61.56 54.66 0.62 o 3 6 1 2135.35 2110.57 12.72 o 4 6 1 593.59 622.77 3.97 o 5 6 1 62.63 57.31 1.03 o 6 6 1 84.79 91.54 1.35 o 7 6 1 419.94 406.47 3.47 o 8 6 1 10.48 20.79 1.18 o 9 6 1 8.40 19.05 1.52 o 10 6 1 166.95 167.31 3.03 o 11 6 1 0.32 2.17 1.71 o 12 6 1 0.43 0.98 1.86 o 13 6 1 1.08 -1.88 1.88 o 14 6 1 36.21 33.95 2.83 o 0 7 1 671.58 646.47 5.11 o 1 7 1 849.36 831.85 4.40 o 2 7 1 4231.22 4255.61 22.70 o 3 7 1 221.79 218.64 1.63 o 4 7 1 576.48 622.74 4.05 o 5 7 1 88.51 107.61 1.22 o 6 7 1 499.40 520.87 4.33 o 7 7 1 73.37 66.87 1.33 o 8 7 1 617.98 579.50 4.75 o 9 7 1 295.28 288.24 3.41 o 10 7 1 103.86 107.84 2.54 o 11 7 1 3.95 3.71 1.71 o 12 7 1 138.48 144.66 3.13 o 13 7 1 37.41 31.70 2.24 o 14 7 1 86.74 93.87 3.49 o 1 8 1 97.80 95.53 0.87 o 2 8 1 1265.34 1280.76 7.36 o 3 8 1 2833.59 2826.31 17.43 o 4 8 1 184.93 189.17 1.48 o 5 8 1 1979.89 1990.19 13.06 o 6 8 1 0.09 2.69 0.71 o 7 8 1 155.86 139.38 1.88 o 8 8 1 16.66 24.04 1.18 o 9 8 1 346.28 332.61 3.77 o 10 8 1 48.57 57.34 1.91 o 11 8 1 13.15 9.14 1.79 o 12 8 1 0.14 4.58 1.87 o 13 8 1 0.39 1.34 1.95 o 14 8 1 23.67 19.18 2.72 o 0 9 1 451.61 458.30 3.82 o 1 9 1 251.00 291.90 1.79 o 2 9 1 5694.63 5758.84 33.33 o 3 9 1 1260.29 1283.74 7.61 o 4 9 1 1624.93 1730.31 10.51 o 5 9 1 97.85 112.89 1.20 o 6 9 1 391.39 454.05 3.40 o 7 9 1 306.37 308.43 2.65 o 8 9 1 521.77 496.41 4.15 o 9 9 1 661.85 601.60 6.06 o 10 9 1 247.21 249.67 3.69 o 11 9 1 27.20 27.01 1.99 o 12 9 1 206.94 206.73 3.74 o 13 9 1 65.57 55.31 2.49 o 14 9 1 80.81 78.78 3.86 o 1 10 1 2007.58 2043.85 12.08 o 2 10 1 6.92 21.14 0.65 o 3 10 1 616.33 700.73 4.43 o 4 10 1 476.36 472.12 3.05 o 5 10 1 43.23 46.43 0.91 o 6 10 1 0.03 8.97 0.65 o 7 10 1 421.92 401.61 3.18 o 8 10 1 35.86 47.87 1.23 o 9 10 1 40.87 47.44 1.67 o 10 10 1 16.05 16.80 1.73 o 11 10 1 6.20 4.42 1.76 o 12 10 1 4.70 9.64 1.94 o 13 10 1 7.23 8.57 2.03 o 14 10 1 8.45 12.87 2.23 o 0 11 1 1133.68 1047.16 8.72 o 1 11 1 1239.04 1240.28 7.80 o 2 11 1 2998.04 3113.72 19.44 o 3 11 1 44.90 50.75 0.86 o 4 11 1 428.53 409.26 2.79 o 5 11 1 90.16 98.33 1.09 o 6 11 1 716.16 678.27 4.78 o 7 11 1 434.13 410.28 3.23 o 8 11 1 856.08 801.21 6.48 o 9 11 1 255.66 230.99 2.75 o 10 11 1 177.54 170.30 2.90 o 11 11 1 9.90 6.86 1.67 o 12 11 1 125.78 119.32 2.92 o 13 11 1 24.85 25.53 2.18 o 14 11 1 64.28 64.60 3.20 o 1 12 1 74.21 60.25 0.85 o 2 12 1 83.25 119.05 1.22 o 3 12 1 18.97 20.70 0.62 o 4 12 1 0.05 2.31 0.59 o 5 12 1 127.99 108.54 1.22 o 6 12 1 0.23 3.53 0.68 o 7 12 1 203.00 183.67 1.94 o 8 12 1 31.62 32.51 1.33 o 9 12 1 9.05 8.23 1.12 o 10 12 1 37.02 34.37 1.67 o 11 12 1 0.83 0.04 1.73 o 12 12 1 5.43 6.49 1.92 o 13 12 1 9.98 8.92 2.38 o 14 12 1 5.99 7.54 2.56 o 0 13 1 183.71 161.70 1.92 o 1 13 1 298.78 382.17 2.65 o 2 13 1 466.68 519.23 3.40 o 3 13 1 13.81 12.81 0.59 o 4 13 1 353.79 306.00 2.33 o 5 13 1 0.00 0.13 0.68 o 6 13 1 418.45 373.42 3.13 o 7 13 1 23.76 42.86 1.27 o 8 13 1 305.29 286.95 3.06 o 9 13 1 31.84 27.48 1.29 o 10 13 1 51.29 58.11 1.88 o 11 13 1 19.41 18.59 1.87 o 12 13 1 53.71 58.15 2.74 o 13 13 1 7.69 6.05 2.37 o 14 13 1 34.03 33.45 2.81 o 1 14 1 157.52 143.88 1.28 o 2 14 1 206.45 218.61 1.72 o 3 14 1 155.63 147.34 1.40 o 4 14 1 73.70 61.32 1.01 o 5 14 1 6.21 8.32 0.75 o 6 14 1 14.46 16.34 0.94 o 7 14 1 72.14 76.88 1.41 o 8 14 1 5.38 7.46 1.10 o 9 14 1 19.41 17.60 1.22 o 10 14 1 44.73 44.31 1.81 o 11 14 1 0.24 -1.49 1.91 o 12 14 1 1.32 -0.21 2.15 o 13 14 1 0.01 -2.22 2.22 o 0 15 1 280.53 242.88 2.77 o 1 15 1 14.33 14.44 0.73 o 2 15 1 820.06 910.43 6.00 o 3 15 1 2.66 3.45 0.60 o 4 15 1 75.08 77.53 1.08 o 5 15 1 31.29 21.66 0.85 o 6 15 1 6.26 20.11 0.99 o 7 15 1 0.23 1.96 0.95 o 8 15 1 46.07 50.89 1.44 o 9 15 1 4.49 3.58 1.20 o 10 15 1 44.77 47.59 2.31 o 11 15 1 0.00 -1.96 1.96 o 12 15 1 52.81 51.31 3.08 o 13 15 1 0.85 1.19 2.33 o 1 16 1 129.95 120.99 1.23 o 2 16 1 4.93 7.27 0.75 o 3 16 1 91.94 87.59 1.10 o 4 16 1 2.10 2.06 0.63 o 5 16 1 136.50 148.01 1.54 o 6 16 1 3.01 4.15 0.90 o 7 16 1 19.50 16.72 1.10 o 8 16 1 0.62 -0.69 1.02 o 9 16 1 23.59 23.65 1.55 o 10 16 1 22.78 16.45 1.77 o 11 16 1 6.46 6.96 2.08 o 12 16 1 3.91 2.70 2.18 o 13 16 1 1.12 -0.52 2.33 o 0 17 1 526.10 464.27 4.91 o 1 17 1 15.05 13.58 0.73 o 2 17 1 695.17 714.05 4.76 o 3 17 1 28.17 33.20 0.82 o 4 17 1 218.74 215.89 1.93 o 5 17 1 0.42 2.33 0.80 o 6 17 1 150.15 157.80 1.78 o 7 17 1 0.23 -0.75 1.01 o 8 17 1 148.96 141.41 2.23 o 9 17 1 1.56 0.52 1.38 o 10 17 1 58.87 57.89 2.11 o 11 17 1 0.06 -1.89 1.89 o 12 17 1 35.95 29.42 2.42 o 13 17 1 0.00 -2.16 2.16 o 1 18 1 53.71 50.18 0.96 o 2 18 1 53.09 55.72 1.01 o 3 18 1 84.80 83.86 1.21 o 4 18 1 2.35 2.72 0.75 o 5 18 1 80.41 81.06 1.32 o 6 18 1 10.49 8.31 0.97 o 7 18 1 12.68 12.01 1.20 o 8 18 1 4.66 7.20 1.22 o 9 18 1 4.02 2.47 1.42 o 10 18 1 23.28 22.93 1.90 o 11 18 1 0.37 -1.92 1.92 o 12 18 1 0.10 -2.04 2.04 o 0 19 1 156.73 129.68 2.09 o 1 19 1 186.87 171.12 1.67 o 2 19 1 299.76 349.61 2.79 o 3 19 1 11.67 7.66 0.76 o 4 19 1 232.47 217.84 2.18 o 5 19 1 211.52 189.43 2.04 o 6 19 1 261.52 268.34 2.65 o 7 19 1 5.71 3.14 1.11 o 8 19 1 152.59 152.55 2.30 o 9 19 1 3.20 1.59 1.41 o 10 19 1 53.81 50.23 2.17 o 11 19 1 0.07 -1.73 1.86 o 12 19 1 36.06 41.00 2.41 o 1 20 1 414.69 381.09 3.00 o 2 20 1 2.08 8.44 0.80 o 3 20 1 128.18 119.92 1.43 o 4 20 1 13.90 24.70 0.96 o 5 20 1 0.37 1.43 0.89 o 6 20 1 5.47 6.43 1.03 o 7 20 1 26.39 22.80 1.31 o 8 20 1 0.32 1.30 1.22 o 9 20 1 0.00 -1.37 1.37 o 10 20 1 0.09 -1.17 1.73 o 11 20 1 0.62 1.27 1.93 o 12 20 1 0.29 -2.02 2.02 o 0 21 1 105.37 116.13 2.04 o 1 21 1 30.52 28.91 1.10 o 2 21 1 256.66 259.36 2.26 o 3 21 1 55.81 53.12 1.17 o 4 21 1 172.03 162.12 1.88 o 5 21 1 102.73 103.22 1.51 o 6 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308.80 5.80 o 1 1 5 174.61 157.46 2.94 o 2 1 5 337.38 313.63 4.20 o 3 1 5 66.58 59.00 2.00 o 4 1 5 88.36 81.36 2.23 o 5 1 5 134.36 118.17 2.74 o 6 1 5 10.68 13.60 1.90 o 7 1 5 40.66 46.39 2.24 o 8 1 5 6.50 7.48 2.79 o 9 1 5 1.57 -1.05 2.93 o 10 1 5 12.94 19.45 3.39 o 1 2 5 0.99 6.89 1.72 o 2 2 5 94.27 109.16 2.58 o 3 2 5 0.80 2.04 1.43 o 4 2 5 2.11 3.21 1.59 o 5 2 5 21.18 23.12 1.79 o 6 2 5 45.93 49.03 2.26 o 7 2 5 24.03 29.19 2.37 o 8 2 5 0.91 -0.91 1.96 o 9 2 5 14.90 10.89 2.91 o 10 2 5 23.70 16.97 3.67 o 0 3 5 508.92 451.64 7.53 o 1 3 5 167.43 153.08 2.91 o 2 3 5 513.92 450.59 5.32 o 3 3 5 83.51 104.05 2.28 o 4 3 5 149.42 129.70 2.59 o 5 3 5 136.13 145.69 2.78 o 6 3 5 32.99 31.31 1.98 o 7 3 5 95.94 105.31 2.69 o 8 3 5 25.83 26.93 2.06 o 9 3 5 24.11 29.19 3.01 o 10 3 5 17.21 17.90 3.10 o 1 4 5 8.07 7.68 1.76 o 2 4 5 96.67 115.73 2.62 o 3 4 5 3.13 4.90 1.51 o 4 4 5 43.64 56.12 2.12 o 5 4 5 34.72 55.39 2.22 o 6 4 5 47.46 51.20 2.37 o 7 4 5 0.11 7.04 1.75 o 8 4 5 3.46 5.71 1.82 o 9 4 5 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6 47.19 53.14 3.38 o 4 0 6 74.37 72.52 4.33 o 5 0 6 72.78 53.49 5.15 o 6 0 6 42.19 39.98 5.89 o 7 0 6 9.95 6.81 6.57 o 1 1 6 4.81 14.50 2.02 o 2 1 6 39.03 30.79 2.18 o 3 1 6 12.46 16.30 2.14 o 4 1 6 2.61 11.06 2.36 o 5 1 6 0.15 14.12 2.89 o 6 1 6 30.01 32.53 3.93 o 7 1 6 0.47 3.17 2.56 o 0 2 6 37.09 42.27 3.26 o 1 2 6 99.87 109.27 2.88 o 2 2 6 12.27 12.57 2.09 o 3 2 6 59.66 68.33 2.80 o 4 2 6 69.08 64.30 2.96 o 5 2 6 109.39 119.50 3.95 o 6 2 6 29.18 36.15 4.05 o 7 2 6 41.82 43.05 3.05 o 1 3 6 1.27 5.46 1.94 o 2 3 6 13.47 10.29 2.27 o 3 3 6 16.29 21.67 2.40 o 4 3 6 0.03 11.00 2.39 o 5 3 6 0.38 14.70 2.51 o 6 3 6 5.99 8.57 2.55 o 7 3 6 0.64 5.54 2.60 o 0 4 6 129.43 123.49 5.05 o 1 4 6 70.57 71.29 3.19 o 2 4 6 34.05 39.57 2.62 o 3 4 6 100.25 115.69 3.52 o 4 4 6 92.78 110.41 3.51 o 5 4 6 166.50 165.71 4.08 o 6 4 6 40.38 50.41 2.89 o 7 4 6 104.62 106.19 5.12 o 1 5 6 0.22 -1.65 2.37 o 2 5 6 0.13 0.78 2.48 o 3 5 6 32.73 52.62 3.07 o 4 5 6 1.30 8.97 2.70 o 5 5 6 12.59 26.91 2.95 o 6 5 6 0.00 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