#------------------------------------------------------------------------------ #$Date: 2009-09-11 11:49:26 +0300 (Fri, 11 Sep 2009) $ #$Revision: 819 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2222430.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2222430_Fobs loop_ _publ_author_name 'Soleimannejad, Janet' 'Aghabozorg, Hossein' 'Manteghi, Faranak' 'Najafi, Shokoh' _publ_section_title ; (2,9-Dimethyl-1,10-phenanthroline)(4-hydroxypyridine-2,6-dicarboxylato)copper(II) trihydrate ; _journal_coeditor_code PV2164 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m761 _journal_page_last m762 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 91.193 _cell_angle_beta 106.836 _cell_angle_gamma 109.263 _cell_length_a 10.0212 _cell_length_b 14.8645 _cell_length_c 15.4418 _exptl_crystal_F_000 1044.00 _reflns_d_resolution_high 0.6965 _[local]_cod_data_source_file pv2164Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sn55blue_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 378.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 11344.19 11695.23 179.30 o 2 0 0 8420.12 9394.50 149.31 o 3 0 0 363.46 496.26 12.07 o 4 0 0 4968.26 5087.07 60.64 o 5 0 0 106.70 108.39 8.24 o 6 0 0 197.88 227.56 14.65 o 7 0 0 117.78 149.65 14.65 o 8 0 0 1396.97 1344.49 78.92 o 9 0 0 1546.42 1387.47 62.86 o 10 0 0 159.04 109.32 27.65 o 11 0 0 270.86 234.97 38.17 o 12 0 0 0.51 13.40 26.14 o -12 1 0 5.95 -5.39 25.32 o -11 1 0 153.77 137.81 30.95 o -10 1 0 1326.38 1351.17 65.19 o -9 1 0 208.40 233.70 27.25 o -8 1 0 1905.16 1805.60 57.98 o -7 1 0 1996.07 1941.97 61.04 o -6 1 0 4720.53 4730.41 73.90 o -5 1 0 1700.86 1673.80 26.54 o -4 1 0 8109.64 7977.08 82.16 o -3 1 0 10.10 1.01 3.18 o -2 1 0 21.40 2.10 3.89 o -1 1 0 555.58 595.43 12.73 o 1 1 0 1961.62 1991.94 38.34 o 2 1 0 2437.24 2567.47 38.33 o 3 1 0 9441.76 9712.35 101.84 o 4 1 0 1712.37 1507.98 24.25 o 5 1 0 6231.87 6691.09 80.66 o 6 1 0 945.37 797.63 23.36 o 7 1 0 1672.61 1678.87 74.43 o 8 1 0 2244.02 2214.78 58.35 o 9 1 0 29.34 7.65 19.49 o 10 1 0 789.79 783.61 77.19 o 11 1 0 385.43 346.11 73.97 o 12 1 0 41.07 56.30 30.46 o -13 2 0 112.51 52.20 31.45 o -12 2 0 1437.87 1337.16 73.27 o -11 2 0 1068.88 1150.81 79.34 o -10 2 0 587.46 636.00 67.45 o -9 2 0 11.15 14.57 14.12 o -8 2 0 274.29 250.44 22.01 o -7 2 0 150.61 139.50 13.02 o -6 2 0 13.89 24.17 6.63 o -5 2 0 319.84 312.10 10.25 o -4 2 0 3522.70 3640.73 60.95 o -3 2 0 3698.69 3543.75 48.15 o -2 2 0 52.74 66.23 8.48 o -1 2 0 13252.99 14222.51 163.69 o 0 2 0 55676.50 58068.72 851.03 o 1 2 0 6154.30 6279.45 100.87 o 2 2 0 52051.73 57528.39 544.67 o 3 2 0 9165.38 9351.25 100.21 o 4 2 0 104.22 187.87 10.34 o 5 2 0 268.30 295.93 14.45 o 6 2 0 0.05 -6.77 6.77 o 7 2 0 64.07 65.99 13.95 o 8 2 0 662.40 672.40 33.86 o 9 2 0 12.77 23.17 19.82 o 10 2 0 757.57 805.15 55.27 o 11 2 0 694.86 694.46 57.25 o 12 2 0 5.77 -14.06 26.47 o -13 3 0 30.73 -6.04 48.80 o -12 3 0 151.36 223.24 43.58 o -11 3 0 266.77 324.56 40.05 o -10 3 0 2145.34 2108.99 67.01 o -9 3 0 108.98 107.54 15.12 o -8 3 0 1848.46 1924.66 46.41 o -7 3 0 9598.71 9911.05 144.41 o -6 3 0 375.42 355.95 12.88 o -5 3 0 6.10 9.12 3.78 o -4 3 0 1613.31 1636.84 23.87 o -3 3 0 1867.31 1759.37 24.83 o -2 3 0 27.37 35.21 4.72 o -1 3 0 330.49 382.57 9.31 o 0 3 0 229.53 195.70 9.99 o 1 3 0 366.11 369.89 12.00 o 2 3 0 21582.68 23223.14 228.21 o 3 3 0 1995.32 2192.67 33.20 o 4 3 0 4002.81 4056.59 70.93 o 5 3 0 752.33 761.72 24.93 o 6 3 0 564.28 522.85 23.47 o 7 3 0 1276.99 1306.63 42.49 o 8 3 0 1558.00 1414.11 154.24 o 9 3 0 210.81 180.75 31.16 o 10 3 0 307.00 229.19 36.65 o 11 3 0 0.74 -14.67 24.22 o 12 3 0 39.81 85.48 54.33 o -13 4 0 160.11 104.11 31.81 o -12 4 0 600.87 630.90 104.36 o -11 4 0 3442.64 3419.51 111.73 o -10 4 0 983.27 1010.33 43.51 o -9 4 0 1.21 10.94 10.23 o -8 4 0 32.19 14.90 9.03 o -7 4 0 420.48 429.17 21.15 o -6 4 0 69.06 75.48 7.48 o -5 4 0 75.35 95.28 6.43 o -4 4 0 5874.06 6047.02 59.87 o -3 4 0 6312.34 6653.42 75.19 o -2 4 0 23413.43 25447.66 216.00 o -1 4 0 185.06 140.12 11.11 o 0 4 0 1686.52 2343.94 33.18 o 1 4 0 23.04 29.65 5.08 o 2 4 0 5334.62 6049.30 70.17 o 3 4 0 9454.81 10112.19 111.01 o 4 4 0 62.86 110.87 9.79 o 5 4 0 146.98 172.28 14.86 o 6 4 0 110.12 120.07 15.67 o 7 4 0 360.75 358.54 26.07 o 8 4 0 76.44 82.22 23.97 o 9 4 0 528.45 545.75 89.47 o 10 4 0 502.82 563.42 51.30 o 11 4 0 592.47 553.45 114.03 o -13 5 0 7.33 -13.72 54.79 o -12 5 0 1535.17 1482.23 74.82 o -11 5 0 425.94 581.92 48.42 o -10 5 0 615.78 569.88 33.12 o -9 5 0 523.63 539.35 26.44 o -8 5 0 5243.76 5333.34 79.99 o -7 5 0 2153.78 2045.57 33.85 o -6 5 0 45.05 35.56 6.94 o -5 5 0 182.88 217.59 8.89 o -4 5 0 1616.19 1690.30 22.40 o -3 5 0 1305.20 1296.03 23.85 o -2 5 0 113.65 93.10 5.79 o -1 5 0 73.62 51.32 6.60 o 0 5 0 1398.05 1524.69 24.36 o 1 5 0 2566.27 2746.57 35.59 o 2 5 0 11146.65 12155.93 114.36 o 3 5 0 4307.55 4205.85 52.78 o 4 5 0 732.13 893.00 27.10 o 5 5 0 751.84 698.99 26.87 o 6 5 0 45.51 34.31 12.71 o 7 5 0 1076.92 1089.98 47.57 o 8 5 0 250.15 282.60 36.34 o 9 5 0 55.54 50.60 24.78 o 10 5 0 4.15 5.02 21.60 o 11 5 0 6.94 11.59 23.55 o -13 6 0 39.84 49.31 29.83 o -12 6 0 3.13 -12.35 21.47 o -11 6 0 5.53 27.09 22.81 o -10 6 0 310.46 267.13 22.40 o -9 6 0 38.99 35.86 10.99 o -8 6 0 255.35 253.16 25.71 o -7 6 0 658.19 635.90 27.91 o -6 6 0 3.49 7.22 5.25 o -5 6 0 185.75 171.14 9.03 o -4 6 0 5324.69 5430.28 56.58 o -3 6 0 16389.04 17744.34 164.90 o -2 6 0 4354.62 4357.88 46.00 o -1 6 0 4453.40 4379.45 46.16 o 0 6 0 6005.92 6102.22 70.27 o 1 6 0 55.30 40.58 6.45 o 2 6 0 188.78 174.65 10.91 o 3 6 0 39.38 20.94 6.64 o 4 6 0 133.63 145.79 13.48 o 5 6 0 656.95 650.88 27.66 o 6 6 0 2.40 -4.84 9.80 o 7 6 0 716.15 708.31 62.56 o 8 6 0 173.73 153.80 28.00 o 9 6 0 22.47 19.23 20.70 o 10 6 0 1058.31 1028.63 59.36 o -13 7 0 35.98 -4.44 26.23 o -12 7 0 285.54 303.56 35.28 o -11 7 0 241.75 243.84 36.64 o -10 7 0 17.97 22.24 12.62 o -9 7 0 19.07 15.25 10.75 o -8 7 0 3429.87 3500.04 66.03 o -7 7 0 1851.65 1814.87 32.29 o -6 7 0 20.71 15.79 5.79 o -5 7 0 404.76 424.75 13.12 o -4 7 0 4547.99 4793.36 55.18 o -3 7 0 2.36 6.95 3.75 o -2 7 0 1213.72 1243.40 24.27 o -1 7 0 188.98 186.56 8.26 o 0 7 0 8472.61 8555.53 95.50 o 1 7 0 22.31 45.18 6.99 o 2 7 0 1742.57 1561.76 31.45 o 3 7 0 2409.78 2264.55 39.69 o 4 7 0 207.15 194.57 15.39 o 5 7 0 363.05 355.04 23.09 o 6 7 0 1039.67 1059.81 42.42 o 7 7 0 740.61 794.81 45.44 o 8 7 0 236.96 203.51 33.72 o 9 7 0 54.68 44.58 22.65 o 10 7 0 26.14 30.49 31.64 o -13 8 0 241.26 315.49 73.28 o -12 8 0 21.55 56.36 22.45 o -11 8 0 281.79 289.62 31.99 o -10 8 0 211.22 207.87 23.22 o -9 8 0 158.67 171.37 18.08 o -8 8 0 118.87 129.07 13.62 o -7 8 0 286.40 276.36 20.60 o -6 8 0 52.91 54.95 7.92 o -5 8 0 1941.44 1667.89 28.67 o -4 8 0 11072.53 10895.89 104.00 o -3 8 0 1047.96 997.10 17.97 o -2 8 0 9251.45 10427.36 99.41 o -1 8 0 2038.03 1893.15 29.99 o 0 8 0 625.75 612.43 18.18 o 1 8 0 248.99 264.76 13.75 o 2 8 0 1274.78 1256.35 30.16 o 3 8 0 724.70 781.81 23.83 o 4 8 0 134.66 110.94 14.54 o 5 8 0 157.50 144.43 19.78 o 6 8 0 982.69 958.06 42.81 o 7 8 0 577.72 542.96 45.65 o 8 8 0 19.50 11.42 26.96 o 9 8 0 99.73 98.82 31.98 o 10 8 0 564.40 507.98 67.42 o -13 9 0 106.04 91.25 31.59 o -12 9 0 65.66 34.87 21.51 o -11 9 0 613.30 614.52 43.07 o -10 9 0 161.52 159.83 25.14 o -9 9 0 1060.63 1143.53 43.70 o -8 9 0 2137.99 2181.93 45.78 o -7 9 0 1212.45 1214.96 28.86 o -6 9 0 417.16 424.53 16.16 o -5 9 0 594.84 542.65 16.98 o -4 9 0 97.72 103.46 8.24 o -3 9 0 85.10 68.53 6.63 o -2 9 0 74.23 93.99 7.44 o -1 9 0 1998.65 2060.28 33.09 o 0 9 0 4359.67 4611.00 57.91 o 1 9 0 8.76 6.48 6.85 o 2 9 0 1990.60 1957.18 40.55 o 3 9 0 991.95 1054.43 28.60 o 4 9 0 1005.61 1048.05 73.23 o 5 9 0 341.59 376.21 33.29 o 6 9 0 1414.70 1569.08 60.81 o 7 9 0 458.16 396.27 38.01 o 8 9 0 90.10 75.08 24.65 o 9 9 0 87.48 90.71 29.50 o -13 10 0 136.85 155.70 31.28 o -12 10 0 44.50 12.01 21.10 o -11 10 0 180.38 200.76 29.20 o -10 10 0 111.46 116.35 23.48 o -9 10 0 85.30 105.01 18.31 o -8 10 0 504.65 498.52 28.78 o -7 10 0 581.46 585.99 23.75 o -6 10 0 37.11 24.64 7.29 o -5 10 0 1188.04 1079.39 23.87 o -4 10 0 3050.74 2789.58 41.04 o -3 10 0 1019.62 1001.38 20.01 o -2 10 0 272.12 305.63 12.14 o -1 10 0 4188.48 4112.36 50.61 o 0 10 0 24.50 5.25 6.64 o 1 10 0 334.05 375.30 19.18 o 2 10 0 111.01 137.84 15.01 o 3 10 0 409.13 393.10 26.62 o 4 10 0 7.20 14.99 13.31 o 5 10 0 286.61 281.72 27.61 o 6 10 0 718.84 707.46 46.05 o 7 10 0 8.51 16.85 24.82 o 8 10 0 0.47 -11.44 26.68 o 9 10 0 61.80 105.89 59.85 o -13 11 0 159.78 166.75 32.07 o -12 11 0 610.85 682.91 54.25 o -11 11 0 1748.85 1755.66 67.30 o -10 11 0 256.74 254.51 30.39 o -9 11 0 281.70 304.88 23.24 o -8 11 0 1291.20 1292.54 51.16 o -7 11 0 5.89 4.05 9.48 o -6 11 0 52.39 38.68 8.20 o -5 11 0 47.41 44.36 8.04 o -4 11 0 0.07 -5.47 5.49 o -3 11 0 38.24 33.97 7.81 o -2 11 0 483.11 542.62 21.80 o -1 11 0 1746.36 1777.87 37.85 o 0 11 0 970.58 961.26 36.41 o 1 11 0 163.85 185.59 26.04 o 2 11 0 466.82 467.93 28.80 o 3 11 0 13.47 25.01 15.19 o 4 11 0 28.96 38.33 18.95 o 5 11 0 70.81 59.10 22.45 o 6 11 0 1519.70 1678.65 277.62 o 7 11 0 140.48 161.08 35.75 o 8 11 0 0.10 20.28 28.18 o -13 12 0 22.11 46.62 26.18 o -12 12 0 32.50 77.74 25.11 o -11 12 0 79.30 70.20 23.23 o -10 12 0 0.23 -5.42 16.41 o -9 12 0 17.12 5.28 12.20 o -8 12 0 646.26 683.26 30.99 o -7 12 0 1323.99 1307.63 39.35 o -6 12 0 15.66 16.20 9.25 o -5 12 0 1324.81 1346.49 31.61 o -4 12 0 288.73 287.10 26.66 o -3 12 0 1125.87 1052.35 27.66 o -2 12 0 1457.89 1422.61 47.13 o -1 12 0 2816.59 2832.24 94.30 o 0 12 0 142.71 127.98 25.76 o 1 12 0 137.80 157.70 17.51 o 2 12 0 229.67 223.27 39.69 o 3 12 0 1.91 13.00 16.40 o 4 12 0 44.99 45.81 20.88 o 5 12 0 96.31 46.84 26.87 o 6 12 0 23.84 34.28 26.83 o 7 12 0 140.43 51.27 30.70 o -13 13 0 91.17 54.17 55.56 o -12 13 0 366.66 307.01 45.12 o -11 13 0 2910.38 3025.37 143.19 o -10 13 0 222.36 190.64 56.25 o -9 13 0 17.24 13.34 17.41 o -8 13 0 1099.67 1067.97 44.31 o -7 13 0 328.49 367.43 28.49 o -6 13 0 54.30 64.72 15.44 o -5 13 0 62.62 70.12 12.06 o -4 13 0 88.54 92.84 11.62 o -3 13 0 102.58 120.41 13.08 o -2 13 0 132.96 121.82 15.57 o -1 13 0 787.66 766.17 32.28 o 0 13 0 381.52 372.88 24.56 o 1 13 0 18.47 48.77 18.37 o 2 13 0 25.46 10.55 16.18 o 3 13 0 952.31 1076.40 55.09 o 4 13 0 116.76 112.96 26.11 o 5 13 0 18.78 1.75 49.49 o 6 13 0 369.96 359.60 89.09 o 7 13 0 43.44 6.10 29.07 o -12 14 0 43.05 35.04 29.25 o -11 14 0 23.20 17.02 24.85 o -10 14 0 18.02 -0.46 22.72 o -9 14 0 265.69 268.30 32.64 o -8 14 0 427.73 387.22 31.09 o -7 14 0 416.37 401.48 30.67 o -6 14 0 145.15 179.87 21.98 o -5 14 0 682.33 740.76 34.51 o -4 14 0 1433.89 1406.95 38.04 o -3 14 0 351.52 312.49 22.60 o -2 14 0 509.60 456.72 26.47 o -1 14 0 550.09 568.84 29.94 o 0 14 0 82.08 67.50 25.10 o 1 14 0 1.88 4.73 16.39 o 2 14 0 16.04 11.12 17.65 o 3 14 0 558.55 566.07 58.11 o 4 14 0 225.19 230.43 39.71 o 5 14 0 22.83 -3.07 25.04 o 6 14 0 16.92 39.23 57.78 o -12 15 0 283.85 351.37 51.72 o -11 15 0 1179.65 1149.37 73.82 o -10 15 0 535.71 564.41 45.18 o -9 15 0 987.34 1006.59 93.90 o -8 15 0 822.71 830.70 50.37 o -7 15 0 0.17 8.03 13.91 o -6 15 0 18.13 10.78 14.15 o -5 15 0 29.52 19.30 12.67 o -4 15 0 37.28 35.01 12.18 o -3 15 0 21.96 6.42 12.88 o -2 15 0 282.74 288.74 23.69 o -1 15 0 1079.80 1054.96 44.07 o 0 15 0 5.15 14.96 19.15 o 1 15 0 43.47 18.11 19.83 o 2 15 0 2009.95 2320.33 81.93 o 3 15 0 1508.96 1572.15 98.50 o 4 15 0 70.86 115.24 33.21 o 5 15 0 126.30 99.36 36.06 o -12 16 0 45.97 80.55 34.21 o -11 16 0 6.04 35.68 31.23 o -10 16 0 89.70 96.38 26.88 o -9 16 0 277.63 313.41 37.49 o -8 16 0 451.27 539.68 48.24 o -7 16 0 137.21 131.76 27.13 o -6 16 0 914.45 895.75 68.05 o -5 16 0 581.97 581.22 59.81 o -4 16 0 1298.64 1240.05 48.54 o -3 16 0 135.96 131.43 21.32 o -2 16 0 953.58 959.50 51.48 o -1 16 0 827.73 841.25 49.73 o 0 16 0 8.06 3.09 19.96 o 1 16 0 76.96 25.65 20.78 o 2 16 0 165.55 146.21 32.00 o 3 16 0 21.70 19.14 26.66 o 4 16 0 78.03 94.92 36.24 o -11 17 0 58.06 80.47 44.74 o -10 17 0 14.63 7.96 23.78 o -9 17 0 457.20 547.13 65.73 o -8 17 0 200.18 237.67 34.14 o -7 17 0 1.41 -14.40 18.65 o -6 17 0 11.29 -1.10 18.59 o -5 17 0 1.31 -10.55 21.62 o -4 17 0 199.48 153.39 31.96 o -3 17 0 282.11 280.33 56.24 o -2 17 0 852.28 891.29 64.29 o -1 17 0 669.35 626.17 144.03 o 0 17 0 13.28 5.46 21.24 o 1 17 0 1095.09 1117.33 97.61 o 2 17 0 1231.23 1402.53 82.63 o 3 17 0 201.72 170.89 41.00 o -10 18 0 21.78 64.14 27.05 o -9 18 0 105.22 112.30 29.28 o -8 18 0 596.97 676.40 52.60 o -7 18 0 0.31 10.81 21.02 o -6 18 0 378.94 402.16 41.80 o -5 18 0 655.85 753.66 62.51 o -4 18 0 76.53 90.71 24.86 o -3 18 0 400.53 422.12 42.01 o -2 18 0 761.18 623.52 168.97 o -1 18 0 199.02 237.17 46.04 o 0 18 0 12.10 19.55 29.70 o 1 18 0 17.29 42.82 31.35 o 2 18 0 230.47 252.63 47.17 o -10 19 0 151.09 118.79 33.51 o -9 19 0 151.10 208.62 38.03 o -8 19 0 58.88 37.34 35.04 o -7 19 0 17.90 6.03 22.30 o -6 19 0 49.54 33.15 29.68 o -5 19 0 207.68 233.76 44.05 o -4 19 0 28.42 62.15 31.69 o -3 19 0 193.90 209.06 33.17 o -2 19 0 496.55 503.06 56.78 o -1 19 0 167.87 214.53 42.86 o 0 19 0 86.99 32.53 34.97 o 1 19 0 676.10 569.37 80.42 o -8 20 0 182.81 196.96 37.32 o -7 20 0 1.76 -9.18 29.70 o -6 20 0 271.88 249.28 66.68 o -5 20 0 404.93 408.53 65.84 o -4 20 0 2.66 -16.53 28.11 o -3 20 0 2.82 2.98 31.79 o -2 20 0 4.80 -1.30 31.92 o -1 20 0 91.40 69.34 36.45 o -6 21 0 11.26 15.24 32.54 o -5 21 0 178.72 204.55 46.24 o -4 21 0 46.73 81.98 38.97 o -3 21 0 43.43 69.04 37.84 o 3 -21 1 81.89 95.44 50.57 o 4 -21 1 33.89 47.46 58.47 o 5 -21 1 1.25 16.54 32.38 o 6 -21 1 1.28 -16.74 29.78 o 0 -20 1 105.28 30.85 42.66 o 1 -20 1 166.93 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