#------------------------------------------------------------------------------ #$Date: 2009-12-10 09:06:56 +0200 (Thu, 10 Dec 2009) $ #$Revision: 927 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2223885.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2223885_Fobs loop_ _publ_author_name 'Xu, Jie' 'Chai, Wenxiang' 'Lin, Jian' 'Shi, Hongsheng' 'Shu, Kangying' _publ_section_title ; Poly[(\m~5~-5-carboxylatotetrahydrofuran-2,3,4-tricarboxylic acid)sodium] ; _journal_coeditor_code KP2234 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1419 _journal_page_last m1420 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.904 _cell_angle_gamma 90.000 _cell_length_a 8.0663 _cell_length_b 13.4167 _cell_length_c 9.7358 _exptl_crystal_F_000 552.00 _reflns_d_resolution_high 0.7717 _[local]_cod_data_source_file kp2234Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 148.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 743.13 724.74 7.35 o 3 0 0 514.94 698.34 10.56 o 4 0 0 3934.73 4226.87 90.39 o 5 0 0 3538.56 3847.11 81.58 o 6 0 0 1609.67 1571.76 20.84 o 7 0 0 50.37 45.99 1.47 o 8 0 0 132.59 142.07 2.80 o 9 0 0 969.62 971.86 45.31 o 1 1 0 2905.08 2615.01 87.94 o 2 1 0 347.82 310.07 3.28 o 3 1 0 4.88 3.68 0.37 o 4 1 0 230.82 254.49 3.45 o 5 1 0 0.38 2.84 0.75 o 6 1 0 361.88 361.56 3.21 o 7 1 0 109.37 99.94 1.43 o 8 1 0 78.70 73.70 1.90 o 9 1 0 0.00 0.67 0.51 o 0 2 0 0.84 0.59 0.13 o 1 2 0 197.31 162.64 1.31 o 2 2 0 339.78 366.16 3.01 o 3 2 0 130.50 146.46 1.45 o 4 2 0 208.83 176.76 2.38 o 5 2 0 82.25 57.80 1.05 o 6 2 0 135.19 118.88 1.49 o 7 2 0 861.46 894.85 8.41 o 8 2 0 87.80 79.74 1.56 o 9 2 0 12.87 15.53 0.99 o 1 3 0 1083.90 979.17 11.71 o 2 3 0 215.13 225.75 2.74 o 3 3 0 153.88 156.66 1.36 o 4 3 0 1990.00 2072.41 21.73 o 5 3 0 161.27 153.35 1.69 o 6 3 0 513.14 538.67 4.67 o 7 3 0 34.54 33.16 1.02 o 8 3 0 154.84 160.00 1.80 o 9 3 0 1.14 1.94 0.47 o 0 4 0 976.72 850.06 9.07 o 1 4 0 6759.67 6541.19 98.44 o 2 4 0 3455.65 3294.00 45.29 o 3 4 0 338.52 288.46 2.23 o 4 4 0 52.05 58.89 0.98 o 5 4 0 31.58 26.09 0.78 o 6 4 0 631.94 653.21 5.97 o 7 4 0 5.48 3.80 0.54 o 8 4 0 527.85 550.90 4.48 o 9 4 0 35.46 39.65 1.93 o 1 5 0 4706.38 4816.64 60.06 o 2 5 0 5150.46 5363.71 75.55 o 3 5 0 2750.96 2879.69 45.25 o 4 5 0 782.69 856.73 6.93 o 5 5 0 352.33 321.23 2.94 o 6 5 0 1746.52 1780.86 16.70 o 7 5 0 183.13 178.49 1.75 o 8 5 0 282.97 292.67 2.64 o 9 5 0 0.13 0.07 0.81 o 0 6 0 48.47 62.48 1.05 o 1 6 0 227.14 195.26 3.86 o 2 6 0 116.02 131.95 1.07 o 3 6 0 373.05 374.55 3.05 o 4 6 0 132.06 133.68 1.29 o 5 6 0 296.70 295.38 2.62 o 6 6 0 488.35 442.23 3.41 o 7 6 0 48.92 48.00 1.05 o 8 6 0 0.45 1.27 0.96 o 9 6 0 64.90 68.58 2.67 o 1 7 0 3697.91 3778.34 38.87 o 2 7 0 281.46 280.38 3.11 o 3 7 0 5.70 3.88 0.34 o 4 7 0 129.85 134.65 1.30 o 5 7 0 579.90 540.39 4.65 o 6 7 0 69.39 74.28 1.39 o 7 7 0 257.81 244.28 1.74 o 8 7 0 288.61 286.50 4.82 o 0 8 0 2039.49 2052.97 45.72 o 1 8 0 152.54 152.73 1.38 o 2 8 0 458.80 476.93 3.96 o 3 8 0 172.45 177.77 1.43 o 4 8 0 1.41 1.43 0.26 o 5 8 0 34.02 30.56 0.99 o 6 8 0 193.30 222.60 3.73 o 7 8 0 12.26 11.84 1.24 o 8 8 0 18.43 15.99 1.86 o 1 9 0 255.95 256.18 3.10 o 2 9 0 1201.55 1172.33 10.54 o 3 9 0 131.89 118.60 1.42 o 4 9 0 446.23 478.71 4.60 o 5 9 0 584.23 547.35 8.51 o 6 9 0 318.74 305.45 4.44 o 7 9 0 403.16 410.23 6.30 o 8 9 0 0.20 0.05 0.91 o 0 10 0 177.90 190.00 2.46 o 1 10 0 942.86 933.26 8.32 o 2 10 0 7.64 12.01 0.67 o 3 10 0 1.87 1.52 0.41 o 4 10 0 546.34 541.10 4.91 o 5 10 0 0.28 1.09 0.75 o 6 10 0 1.92 2.26 0.92 o 7 10 0 1.60 1.34 1.27 o 8 10 0 281.94 302.78 5.24 o 1 11 0 69.03 68.24 0.90 o 2 11 0 234.79 215.78 2.49 o 3 11 0 1167.69 1139.09 13.39 o 4 11 0 152.00 156.44 1.95 o 5 11 0 93.44 91.95 2.20 o 6 11 0 121.80 129.29 5.08 o 7 11 0 420.02 432.27 7.32 o 0 12 0 184.46 185.20 2.32 o 1 12 0 273.66 267.04 2.50 o 2 12 0 51.45 58.65 1.17 o 3 12 0 295.24 273.21 2.47 o 4 12 0 66.39 63.99 0.94 o 5 12 0 27.34 32.38 1.63 o 6 12 0 4.37 5.38 1.19 o 7 12 0 45.77 45.13 2.20 o 1 13 0 11.63 12.90 0.78 o 2 13 0 0.04 0.72 0.41 o 3 13 0 26.72 32.48 0.67 o 4 13 0 260.61 253.03 3.91 o 5 13 0 9.92 10.76 2.07 o 6 13 0 115.82 119.95 5.32 o 0 14 0 318.22 313.14 3.78 o 1 14 0 392.68 386.13 3.66 o 2 14 0 11.41 12.12 0.55 o 3 14 0 137.57 137.84 1.79 o 4 14 0 253.43 245.72 5.23 o 5 14 0 41.89 35.03 1.82 o 1 15 0 167.06 164.27 1.69 o 2 15 0 279.26 280.62 2.95 o 3 15 0 16.08 13.15 1.17 o 4 15 0 99.57 94.39 3.02 o 0 16 0 552.43 554.32 7.38 o 1 16 0 51.67 53.25 0.88 o 2 16 0 2.25 1.80 0.41 o 3 16 0 18.85 20.38 1.53 o 1 17 0 28.55 26.53 0.98 o 2 17 0 16.79 16.70 2.21 o -10 1 1 9.34 -0.04 0.50 o -9 1 1 96.35 89.23 1.85 o -8 1 1 77.62 72.05 1.67 o -7 1 1 240.61 233.81 5.73 o -6 1 1 40.26 35.61 1.06 o -5 1 1 1613.76 1790.08 16.53 o -4 1 1 596.08 587.79 4.66 o -3 1 1 142.35 85.33 0.85 o -2 1 1 322.50 316.37 2.37 o -1 1 1 146.38 134.05 1.02 o 1 1 1 10.86 9.45 0.41 o 2 1 1 674.57 718.04 4.70 o 3 1 1 545.67 563.23 3.84 o 4 1 1 1424.51 1474.98 20.41 o 5 1 1 210.75 214.03 1.75 o 6 1 1 75.99 73.02 0.82 o 7 1 1 101.72 101.11 1.21 o 8 1 1 2.09 2.89 0.42 o 9 1 1 184.04 190.04 2.79 o -10 2 1 8.92 5.97 2.07 o -9 2 1 98.41 95.89 1.53 o -8 2 1 175.11 173.42 2.72 o -7 2 1 185.64 175.14 4.78 o -6 2 1 143.01 141.93 1.72 o -5 2 1 225.38 258.01 2.52 o -4 2 1 2889.88 3042.76 30.03 o -3 2 1 993.57 1052.73 8.64 o -2 2 1 760.17 816.81 6.24 o -1 2 1 4226.46 3995.18 38.55 o 0 2 1 1092.08 1005.32 7.44 o 1 2 1 38.69 37.15 0.99 o 2 2 1 1069.46 1033.30 7.60 o 3 2 1 33.08 37.63 0.61 o 4 2 1 1268.68 1356.87 10.61 o 5 2 1 87.95 84.18 0.86 o 6 2 1 115.34 108.71 1.43 o 7 2 1 303.59 291.92 3.34 o 8 2 1 1.75 1.99 0.41 o 9 2 1 57.01 61.17 1.23 o -9 3 1 3.50 4.02 0.56 o -8 3 1 67.20 65.31 1.16 o -7 3 1 1401.21 1376.60 30.51 o -6 3 1 11.19 16.66 3.04 o -5 3 1 99.39 95.16 1.37 o -4 3 1 5.79 9.40 0.46 o -3 3 1 4104.75 4153.12 43.12 o -2 3 1 889.37 852.64 6.56 o -1 3 1 242.70 245.99 2.38 o 0 3 1 1460.92 1418.69 11.40 o 1 3 1 59.82 69.61 0.87 o 2 3 1 293.42 305.09 5.65 o 3 3 1 975.30 1039.07 7.15 o 4 3 1 2161.60 2294.13 19.52 o 5 3 1 75.86 73.85 0.69 o 6 3 1 4.90 4.92 0.35 o 7 3 1 98.85 91.79 1.12 o 8 3 1 100.17 108.79 1.16 o 9 3 1 13.81 17.84 1.44 o -9 4 1 8.71 8.01 0.95 o -8 4 1 165.48 153.37 1.86 o -7 4 1 96.11 96.48 2.00 o -6 4 1 121.91 110.25 1.37 o -5 4 1 2.37 1.71 0.33 o -4 4 1 1.40 4.87 0.35 o -3 4 1 310.45 338.12 2.83 o -2 4 1 23.16 12.37 0.37 o -1 4 1 422.48 395.79 3.18 o 0 4 1 782.59 899.57 7.01 o 1 4 1 354.89 350.84 1.85 o 2 4 1 921.95 949.85 12.41 o 3 4 1 955.21 949.19 10.43 o 4 4 1 223.43 272.99 1.64 o 5 4 1 8.91 6.60 0.28 o 6 4 1 87.80 93.06 1.51 o 7 4 1 122.50 128.61 1.36 o 8 4 1 0.03 0.17 0.29 o 9 4 1 6.72 4.56 3.88 o -9 5 1 0.54 -0.46 1.11 o -8 5 1 63.66 63.02 1.44 o -7 5 1 8.83 4.25 0.58 o -6 5 1 2.50 2.51 0.68 o -5 5 1 1379.42 1507.41 15.56 o -4 5 1 128.26 134.28 1.47 o -3 5 1 2543.34 2571.25 26.11 o -2 5 1 1431.22 1385.92 11.45 o -1 5 1 485.81 557.58 3.71 o 0 5 1 5.43 17.70 0.58 o 1 5 1 2270.39 2242.65 34.20 o 2 5 1 436.71 436.61 5.95 o 3 5 1 4363.57 4659.55 73.60 o 4 5 1 999.74 1033.06 6.58 o 5 5 1 94.72 87.80 0.68 o 6 5 1 53.79 60.54 0.58 o 7 5 1 8.70 7.00 0.67 o 8 5 1 0.15 0.15 0.71 o 9 5 1 147.11 162.18 3.80 o -9 6 1 70.82 71.71 3.53 o -8 6 1 0.56 0.54 0.30 o -7 6 1 230.50 217.18 2.65 o -6 6 1 605.17 588.87 5.10 o -5 6 1 167.66 158.31 2.02 o -4 6 1 1204.97 1327.60 11.08 o -3 6 1 87.82 75.60 1.02 o -2 6 1 214.52 242.51 1.91 o -1 6 1 85.28 94.97 1.04 o 0 6 1 18.47 29.03 0.39 o 1 6 1 293.73 298.46 3.32 o 2 6 1 1592.39 1622.42 63.40 o 3 6 1 368.78 336.39 4.45 o 4 6 1 373.28 396.75 4.42 o 5 6 1 190.82 204.00 2.86 o 6 6 1 126.03 109.66 1.17 o 7 6 1 0.08 0.36 0.19 o 8 6 1 10.15 10.70 3.65 o -9 7 1 47.39 47.21 3.63 o -8 7 1 26.82 36.31 1.70 o -7 7 1 5.15 6.86 0.39 o -6 7 1 843.78 836.34 7.39 o -5 7 1 3.98 4.35 0.22 o -4 7 1 27.93 28.76 0.66 o -3 7 1 265.83 268.33 3.06 o -2 7 1 665.45 644.58 5.10 o -1 7 1 7.22 6.01 0.28 o 0 7 1 0.00 0.72 0.17 o 1 7 1 0.28 0.42 0.17 o 2 7 1 77.62 86.56 0.67 o 3 7 1 189.40 177.82 4.39 o 4 7 1 2.10 3.43 0.77 o 5 7 1 514.43 492.34 6.21 o 6 7 1 146.19 158.88 2.97 o 7 7 1 74.32 62.31 1.90 o 8 7 1 26.01 24.35 1.78 o -8 8 1 37.11 40.70 1.82 o -7 8 1 169.04 173.51 2.24 o -6 8 1 110.07 122.07 0.98 o -5 8 1 597.72 601.25 4.30 o -4 8 1 85.27 94.49 0.96 o -3 8 1 79.15 76.27 0.78 o -2 8 1 398.94 409.81 6.02 o -1 8 1 449.53 469.19 2.97 o 0 8 1 105.64 116.96 0.97 o 1 8 1 159.15 168.86 1.49 o 2 8 1 491.87 526.57 4.40 o 3 8 1 256.64 252.05 3.74 o 4 8 1 255.94 272.55 3.51 o 5 8 1 267.55 236.37 3.43 o 6 8 1 0.33 2.26 0.86 o 7 8 1 38.43 43.65 1.78 o 8 8 1 2.42 1.49 1.20 o -8 9 1 16.84 25.60 3.68 o -7 9 1 84.16 89.27 2.39 o -6 9 1 714.02 713.31 5.86 o -5 9 1 181.64 187.92 1.65 o -4 9 1 2.24 2.57 0.27 o -3 9 1 1.36 2.46 0.21 o -2 9 1 696.03 698.26 5.86 o -1 9 1 200.97 227.05 1.70 o 0 9 1 883.18 937.10 7.14 o 1 9 1 1102.45 1153.02 9.89 o 2 9 1 13.52 19.18 0.72 o 3 9 1 503.09 494.51 9.15 o 4 9 1 314.39 289.41 3.80 o 5 9 1 5.87 3.84 0.90 o 6 9 1 28.72 24.33 1.51 o 7 9 1 210.50 212.62 4.14 o 8 9 1 12.51 12.64 2.21 o -8 10 1 4.12 6.38 1.34 o -7 10 1 23.95 23.14 2.07 o -6 10 1 41.77 46.40 1.27 o -5 10 1 126.90 118.37 1.18 o -4 10 1 1062.67 1052.14 9.90 o -3 10 1 739.81 768.98 6.27 o -2 10 1 88.42 92.40 1.14 o -1 10 1 86.01 78.31 0.94 o 0 10 1 110.20 108.90 1.20 o 1 10 1 274.97 251.87 2.81 o 2 10 1 536.35 539.84 4.52 o 3 10 1 72.35 62.02 1.86 o 4 10 1 46.24 45.23 2.74 o 5 10 1 393.04 370.22 5.42 o 6 10 1 50.35 51.43 2.13 o 7 10 1 3.14 4.47 1.36 o -7 11 1 20.66 20.57 1.63 o -6 11 1 3.55 4.98 1.09 o -5 11 1 65.69 66.88 1.31 o -4 11 1 0.32 1.37 0.32 o -3 11 1 78.76 70.82 1.11 o -2 11 1 136.09 136.18 1.81 o -1 11 1 257.69 229.93 2.09 o 0 11 1 274.74 248.01 2.10 o 1 11 1 858.24 806.57 6.63 o 2 11 1 36.54 37.84 1.15 o 3 11 1 230.51 213.34 3.12 o 4 11 1 8.98 11.28 1.11 o 5 11 1 0.13 1.29 0.86 o 6 11 1 1.06 0.36 0.84 o 7 11 1 172.36 165.88 3.66 o -7 12 1 24.45 26.42 2.04 o -6 12 1 0.33 -0.37 0.84 o -5 12 1 504.00 478.48 9.40 o -4 12 1 479.35 481.12 5.41 o -3 12 1 407.65 398.68 3.92 o -2 12 1 196.74 191.81 2.23 o -1 12 1 87.42 91.72 1.13 o 0 12 1 142.82 126.86 1.31 o 1 12 1 9.54 9.88 0.44 o 2 12 1 969.93 965.25 9.34 o 3 12 1 8.36 10.69 0.42 o 4 12 1 160.47 176.04 3.09 o 5 12 1 158.97 152.68 3.43 o 6 12 1 272.66 248.61 4.43 o -6 13 1 9.92 13.38 1.63 o -5 13 1 10.74 13.22 1.70 o -4 13 1 113.72 109.71 4.46 o -3 13 1 114.09 108.61 1.63 o -2 13 1 92.13 89.45 2.00 o -1 13 1 874.01 830.14 7.09 o 0 13 1 9.12 12.55 0.54 o 1 13 1 1095.77 1058.32 9.43 o 2 13 1 35.18 32.51 0.93 o 3 13 1 67.51 63.90 1.91 o 4 13 1 52.02 52.43 2.87 o 5 13 1 13.30 18.21 2.00 o 6 13 1 34.86 43.53 3.31 o -6 14 1 51.51 47.41 2.12 o -5 14 1 236.87 240.92 4.43 o -4 14 1 0.11 0.88 0.78 o -3 14 1 32.72 33.26 2.28 o -2 14 1 183.23 185.54 2.86 o -1 14 1 377.31 384.30 3.75 o 0 14 1 290.03 277.63 2.57 o 1 14 1 13.79 12.62 0.51 o 2 14 1 35.79 37.63 0.88 o 3 14 1 217.95 211.53 5.65 o 4 14 1 12.51 15.44 1.38 o 5 14 1 11.05 14.32 1.53 o -5 15 1 0.19 0.72 1.03 o -4 15 1 0.78 0.56 0.78 o -3 15 1 24.90 22.78 0.84 o -2 15 1 2.18 3.76 0.61 o -1 15 1 16.57 18.26 0.83 o 0 15 1 107.78 103.86 1.35 o 1 15 1 92.18 85.03 1.29 o 2 15 1 2.38 1.99 0.51 o 3 15 1 37.15 42.77 1.74 o 4 15 1 13.12 13.58 1.85 o -4 16 1 100.12 107.30 2.82 o -3 16 1 18.64 25.00 2.63 o -2 16 1 2.72 2.59 0.56 o -1 16 1 58.11 65.04 1.16 o 0 16 1 23.38 24.55 0.74 o 1 16 1 16.92 17.80 0.95 o 2 16 1 265.54 270.51 4.06 o 3 16 1 44.36 42.20 2.02 o -2 17 1 0.51 0.39 0.48 o -1 17 1 5.99 4.64 0.59 o 0 17 1 6.35 6.21 1.28 o 1 17 1 15.69 19.48 1.20 o -10 0 2 145.21 141.23 5.98 o -9 0 2 152.22 155.70 4.28 o -8 0 2 825.43 822.12 17.84 o -7 0 2 741.90 726.71 9.60 o -6 0 2 41.66 50.21 1.54 o -5 0 2 737.83 722.71 8.71 o -4 0 2 0.72 0.97 0.95 o -3 0 2 295.03 328.76 3.72 o -2 0 2 7306.75 6941.64 111.51 o -1 0 2 188.96 190.23 2.13 o 0 0 2 14932.94 14799.68 220.37 o 1 0 2 22179.62 21518.80 582.16 o 2 0 2 291.73 339.24 3.10 o 3 0 2 168.31 181.90 2.08 o 4 0 2 565.04 575.07 5.44 o 5 0 2 1432.39 1484.99 15.61 o 6 0 2 2682.67 2783.85 33.57 o 7 0 2 12.15 14.01 1.19 o 8 0 2 24.57 30.19 0.96 o 9 0 2 74.99 72.12 1.83 o -10 1 2 2.32 1.66 1.44 o -9 1 2 5.42 5.46 0.98 o -8 1 2 472.11 457.37 7.06 o -7 1 2 318.66 311.36 4.47 o -6 1 2 126.96 114.33 1.72 o -5 1 2 124.63 124.11 1.84 o -4 1 2 532.08 607.44 5.17 o -3 1 2 793.22 875.88 7.05 o -2 1 2 1730.75 1677.21 14.31 o -1 1 2 10345.55 9965.91 161.92 o 0 1 2 127.00 147.53 0.94 o 1 1 2 6633.75 6549.42 51.00 o 2 1 2 269.16 283.15 2.22 o 3 1 2 650.12 742.46 6.05 o 4 1 2 401.81 460.21 3.10 o 5 1 2 586.51 584.42 4.20 o 6 1 2 30.11 34.78 0.73 o 7 1 2 24.28 28.29 0.63 o 8 1 2 108.54 110.16 1.22 o 9 1 2 59.13 69.93 1.91 o -10 2 2 3.38 4.27 1.04 o -9 2 2 23.94 26.28 5.17 o -8 2 2 183.89 169.53 2.77 o -7 2 2 238.07 232.23 3.25 o -6 2 2 689.90 677.73 6.18 o -5 2 2 0.06 1.25 0.44 o -4 2 2 0.37 0.80 0.29 o -3 2 2 65.20 69.57 1.00 o -2 2 2 1560.50 1616.46 14.08 o -1 2 2 2044.80 1904.41 17.29 o 0 2 2 5753.95 5470.57 67.62 o 1 2 2 878.17 743.72 4.76 o 2 2 2 7.31 3.36 0.24 o 3 2 2 54.79 71.49 1.06 o 4 2 2 199.72 256.49 1.84 o 5 2 2 1217.72 1262.95 9.27 o 6 2 2 194.62 181.49 1.47 o 7 2 2 968.33 1002.66 7.69 o 8 2 2 115.49 108.78 1.73 o 9 2 2 105.52 104.45 2.50 o -10 3 2 50.00 46.81 3.93 o -9 3 2 0.08 0.37 1.29 o -8 3 2 7.87 7.53 1.14 o -7 3 2 730.77 714.66 10.66 o -6 3 2 38.87 37.46 0.86 o -5 3 2 2353.32 2581.56 25.82 o -4 3 2 93.30 113.47 1.17 o -3 3 2 1220.96 1269.62 10.74 o -2 3 2 104.10 103.95 1.03 o -1 3 2 2258.86 2270.72 18.23 o 0 3 2 1644.51 1762.77 16.87 o 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