#------------------------------------------------------------------------------
#$Date: 2016-04-03 04:26:01 +0300 (Sun, 03 Apr 2016) $
#$Revision: 181167 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/46/2224680.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2224680_Fobs
loop_
_publ_author_name
'\"Ozdemir Tar\?i, Gonca'
'Tanak, Hasan'
'Macit, Mustafa'
'Er\,sahin, Ferda'
'Is\?ik, \,Samil'
_publ_section_title
;
 (<i>E</i>)-4-Methyl-2-{[tris(hydroxymethyl)methyl]iminiomethyl}phenolate
;
_journal_coeditor_code           IM2160
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              o85
_journal_volume                  66
_journal_year                    2010
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                87.584
_cell_angle_beta                 77.192
_cell_angle_gamma                79.215
_cell_length_a                   6.7501
_cell_length_b                   8.5036
_cell_length_c                   11.1290
_exptl_crystal_F_000             256.00
_reflns_d_resolution_high        0.8110
_cod_data_source_file            im2160Isup2.hkl
_cod_data_source_block           I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' samf36 in P -1'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            57.59
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 567.56 535.73 9.29 o
2 0 0 110.15 96.79 0.82 o
3 0 0 1.42 0.55 0.42 o
4 0 0 81.39 93.17 1.71 o
5 0 0 117.06 128.76 0.97 o
6 0 0 67.52 72.52 1.00 o
7 0 0 2.23 2.52 0.53 o
-7 1 0 32.08 31.18 0.65 o
-6 1 0 0.30 0.64 0.48 o
-5 1 0 166.47 169.14 1.45 o
-4 1 0 95.74 92.75 2.02 o
-3 1 0 244.69 238.94 2.19 o
-2 1 0 258.41 283.97 1.62 o
-1 1 0 2404.18 2556.08 27.06 o
0 1 0 50.40 63.90 0.95 o
1 1 0 1160.75 1119.35 8.29 o
2 1 0 18.16 12.80 0.54 o
3 1 0 558.03 578.77 2.96 o
4 1 0 4.12 3.97 0.47 o
5 1 0 36.84 33.86 0.99 o
6 1 0 0.00 0.04 0.51 o
7 1 0 2.33 2.31 0.56 o
8 1 0 4.57 4.19 0.69 o
-7 2 0 0.08 0.01 0.47 o
-6 2 0 205.09 221.80 1.39 o
-5 2 0 137.81 136.80 1.85 o
-4 2 0 87.03 78.31 1.20 o
-3 2 0 152.81 157.41 2.76 o
-2 2 0 283.35 283.48 1.43 o
1 2 0 571.93 547.76 4.15 o
2 2 0 389.94 396.51 2.56 o
3 2 0 19.13 19.52 0.48 o
4 2 0 1.96 3.65 0.40 o
5 2 0 129.97 125.69 1.18 o
6 2 0 55.66 63.13 0.75 o
7 2 0 44.19 44.19 0.77 o
8 2 0 0.64 0.94 0.73 o
-7 3 0 53.64 52.54 0.62 o
-6 3 0 3.00 3.00 0.43 o
-5 3 0 42.83 43.15 0.83 o
-4 3 0 0.04 0.03 0.39 o
-3 3 0 10.96 13.58 0.39 o
-2 3 0 615.62 622.73 7.95 o
-1 3 0 2117.34 2210.34 19.97 o
0 3 0 657.00 668.03 3.07 o
1 3 0 0.41 0.05 0.36 o
2 3 0 33.51 36.08 0.56 o
3 3 0 122.64 117.44 1.04 o
4 3 0 5.42 5.07 0.44 o
5 3 0 19.02 19.77 0.50 o
6 3 0 2.12 3.39 0.44 o
7 3 0 10.99 11.00 0.61 o
8 3 0 5.19 5.96 0.75 o
-6 4 0 10.71 10.89 0.48 o
-5 4 0 48.23 50.03 1.80 o
-4 4 0 0.66 0.68 0.39 o
-3 4 0 58.67 48.54 0.60 o
-2 4 0 114.45 125.34 2.09 o
-1 4 0 948.15 937.56 10.87 o
0 4 0 142.65 160.97 1.67 o
1 4 0 297.91 337.17 2.14 o
2 4 0 3.79 2.39 0.39 o
3 4 0 1.21 1.44 0.36 o
4 4 0 68.59 67.05 0.66 o
5 4 0 4.42 3.80 0.46 o
6 4 0 132.74 131.22 1.51 o
7 4 0 1.83 2.17 0.58 o
-6 5 0 17.60 17.13 0.48 o
-5 5 0 27.31 26.68 1.14 o
-4 5 0 2.71 3.23 0.34 o
-3 5 0 0.97 0.91 0.47 o
-2 5 0 412.45 420.16 5.94 o
-1 5 0 314.67 324.58 1.41 o
0 5 0 63.48 57.40 0.54 o
1 5 0 35.01 39.56 0.49 o
2 5 0 68.25 72.04 0.57 o
3 5 0 31.56 36.00 0.51 o
4 5 0 177.94 172.85 1.23 o
5 5 0 24.11 23.33 0.63 o
6 5 0 3.77 4.33 0.52 o
7 5 0 0.62 0.61 0.55 o
-5 6 0 0.01 0.62 0.46 o
-4 6 0 10.45 10.09 0.39 o
-3 6 0 0.05 0.68 0.41 o
-2 6 0 0.38 0.33 0.41 o
-1 6 0 107.22 106.14 1.60 o
0 6 0 142.92 144.62 3.33 o
1 6 0 39.12 40.65 0.84 o
2 6 0 0.30 0.46 0.38 o
3 6 0 0.36 0.89 0.40 o
4 6 0 1.23 0.95 0.41 o
5 6 0 2.94 2.96 0.48 o
6 6 0 8.16 9.50 0.51 o
7 6 0 34.26 35.39 0.69 o
-4 7 0 1.14 1.50 0.38 o
-3 7 0 4.10 5.77 0.40 o
-2 7 0 7.58 8.29 0.45 o
-1 7 0 179.51 181.55 2.24 o
0 7 0 198.06 204.34 3.36 o
1 7 0 1.44 1.68 0.47 o
2 7 0 0.20 0.22 0.36 o
3 7 0 72.72 62.25 0.52 o
4 7 0 38.04 37.89 0.53 o
5 7 0 3.41 4.73 0.47 o
6 7 0 0.60 1.08 0.52 o
-4 8 0 0.44 0.54 0.41 o
-3 8 0 21.81 22.06 0.59 o
-2 8 0 0.75 1.56 0.47 o
-1 8 0 10.05 8.08 0.45 o
0 8 0 1.58 1.50 0.44 o
1 8 0 40.85 39.17 0.60 o
2 8 0 7.55 6.69 0.39 o
3 8 0 23.56 24.53 0.49 o
4 8 0 6.77 6.63 0.47 o
5 8 0 4.75 3.52 0.50 o
6 8 0 19.07 20.50 0.66 o
-2 9 0 34.25 30.39 0.99 o
-1 9 0 20.01 19.72 0.58 o
0 9 0 0.60 0.52 0.41 o
1 9 0 58.52 60.22 1.29 o
2 9 0 0.11 1.12 0.51 o
3 9 0 11.87 12.62 0.57 o
4 9 0 6.56 7.51 0.50 o
5 9 0 10.65 11.61 0.54 o
0 10 0 0.03 0.74 0.65 o
1 10 0 9.24 10.38 0.59 o
2 10 0 1.85 2.23 0.41 o
3 10 0 2.63 2.42 0.58 o
-3 -10 1 23.53 21.85 0.48 o
-2 -10 1 2.36 1.89 0.58 o
-1 -10 1 6.98 8.74 0.63 o
0 -10 1 1.58 1.84 0.50 o
-5 -9 1 1.56 2.10 0.52 o
-4 -9 1 2.43 1.90 0.44 o
-3 -9 1 34.27 34.65 0.69 o
-2 -9 1 0.02 0.14 0.40 o
-1 -9 1 16.58 17.98 0.56 o
0 -9 1 9.38 9.88 0.54 o
1 -9 1 1.20 0.52 0.54 o
2 -9 1 17.97 18.60 0.96 o
-6 -8 1 17.47 18.25 0.60 o
-5 -8 1 8.09 8.68 0.49 o
-4 -8 1 119.14 113.58 2.14 o
-3 -8 1 15.84 16.44 0.46 o
-2 -8 1 15.42 13.59 0.39 o
-1 -8 1 16.80 15.29 0.41 o
0 -8 1 21.35 24.10 0.73 o
1 -8 1 0.31 0.81 0.44 o
2 -8 1 96.67 88.44 2.73 o
3 -8 1 15.64 15.38 0.75 o
4 -8 1 0.40 0.55 0.41 o
-6 -7 1 6.34 6.24 0.55 o
-5 -7 1 30.98 31.49 1.10 o
-4 -7 1 116.28 118.00 1.07 o
-3 -7 1 66.33 60.59 0.72 o
-2 -7 1 13.34 13.40 0.43 o
-1 -7 1 9.23 8.22 0.44 o
0 -7 1 7.61 8.41 0.48 o
1 -7 1 469.77 466.64 16.03 o
2 -7 1 26.10 26.79 0.46 o
3 -7 1 45.38 42.06 0.67 o
4 -7 1 4.20 4.85 0.48 o
5 -7 1 4.74 4.44 0.46 o
-7 -6 1 2.74 2.14 0.56 o
-6 -6 1 10.92 12.95 0.55 o
-5 -6 1 49.08 49.81 0.58 o
-4 -6 1 400.32 399.90 3.04 o
-3 -6 1 0.00 0.00 0.40 o
-2 -6 1 22.73 23.52 0.42 o
-1 -6 1 230.25 228.87 1.84 o
0 -6 1 314.42 294.25 4.14 o
1 -6 1 14.40 15.62 1.51 o
2 -6 1 303.85 289.05 0.90 o
3 -6 1 4.86 5.93 0.66 o
4 -6 1 19.68 18.16 0.67 o
5 -6 1 0.00 0.11 0.33 o
-7 -5 1 0.45 1.05 0.54 o
-6 -5 1 0.65 0.98 0.48 o
-5 -5 1 660.20 683.53 2.88 o
-4 -5 1 29.36 26.96 0.49 o
-3 -5 1 4.22 4.37 0.50 o
-2 -5 1 103.43 111.66 1.20 o
-1 -5 1 38.46 41.69 0.51 o
0 -5 1 169.41 169.98 0.78 o
1 -5 1 666.91 652.63 3.58 o
2 -5 1 26.77 30.11 0.62 o
3 -5 1 13.57 9.86 0.39 o
4 -5 1 8.80 9.30 0.49 o
5 -5 1 8.51 10.28 0.53 o
6 -5 1 1.82 1.58 0.44 o
-7 -4 1 3.14 3.48 0.57 o
-6 -4 1 60.25 58.08 0.68 o
-5 -4 1 162.82 157.46 1.52 o
-4 -4 1 1004.32 977.97 7.78 o
-3 -4 1 2.66 1.26 0.39 o
-2 -4 1 162.92 172.21 0.85 o
-1 -4 1 132.48 143.11 0.85 o
0 -4 1 97.19 86.98 0.56 o
1 -4 1 1066.79 1050.57 5.80 o
2 -4 1 382.87 398.11 5.26 o
3 -4 1 18.20 15.48 0.44 o
4 -4 1 22.22 22.37 0.84 o
5 -4 1 7.53 7.17 0.43 o
6 -4 1 10.49 9.93 0.44 o
-7 -3 1 5.98 5.65 0.63 o
-6 -3 1 90.55 83.00 0.76 o
-5 -3 1 245.95 249.78 2.82 o
-4 -3 1 0.17 0.95 0.42 o
-3 -3 1 19.95 26.73 0.63 o
-2 -3 1 0.01 0.29 0.39 o
-1 -3 1 938.46 940.31 4.92 o
0 -3 1 544.90 535.33 2.13 o
1 -3 1 1136.05 1182.45 4.33 o
2 -3 1 512.64 534.29 1.35 o
3 -3 1 0.36 0.95 0.37 o
4 -3 1 19.85 18.67 0.51 o
5 -3 1 2.37 2.58 0.36 o
6 -3 1 3.63 3.61 0.39 o
7 -3 1 19.39 20.66 0.85 o
-7 -2 1 47.20 46.29 0.81 o
-6 -2 1 62.94 67.28 0.67 o
-5 -2 1 459.34 455.96 4.82 o
-4 -2 1 18.74 18.77 0.49 o
-3 -2 1 25.34 24.79 0.53 o
-2 -2 1 69.96 65.56 0.69 o
-1 -2 1 1558.99 1444.27 10.02 o
0 -2 1 317.72 322.73 1.25 o
1 -2 1 1940.77 2052.28 17.18 o
2 -2 1 185.46 188.37 2.74 o
3 -2 1 72.63 68.58 2.46 o
4 -2 1 0.03 0.14 0.36 o
5 -2 1 401.03 389.38 1.78 o
6 -2 1 0.16 0.34 0.42 o
7 -2 1 33.52 33.36 1.04 o
-7 -1 1 1.98 2.79 0.61 o
-6 -1 1 345.13 351.05 2.74 o
-5 -1 1 184.86 174.75 1.89 o
-4 -1 1 29.08 36.22 0.53 o
-3 -1 1 178.33 175.55 1.07 o
-2 -1 1 8.51 7.49 0.45 o
-1 -1 1 779.65 779.71 5.50 o
0 -1 1 305.32 311.89 2.04 o
1 -1 1 2344.95 2450.47 28.43 o
2 -1 1 158.23 150.67 1.20 o
3 -1 1 389.47 375.29 2.48 o
4 -1 1 89.90 90.84 0.70 o
5 -1 1 16.97 15.83 0.39 o
6 -1 1 5.74 5.11 0.43 o
7 -1 1 3.61 4.06 0.46 o
-7 0 1 19.96 20.47 0.68 o
-6 0 1 0.13 0.46 0.53 o
-5 0 1 19.59 19.09 0.54 o
-4 0 1 14.55 12.62 0.43 o
-3 0 1 0.17 0.24 0.32 o
-2 0 1 135.59 144.98 1.42 o
-1 0 1 156.39 160.04 1.44 o
0 0 1 2118.19 2202.64 32.95 o
1 0 1 509.17 537.08 2.30 o
2 0 1 275.02 252.00 2.20 o
3 0 1 144.39 165.78 3.41 o
4 0 1 96.93 97.29 1.10 o
5 0 1 0.00 0.30 0.43 o
6 0 1 109.43 108.50 0.97 o
7 0 1 44.10 43.13 0.74 o
8 0 1 1.09 1.26 0.51 o
-7 1 1 0.47 0.19 0.57 o
-6 1 1 186.51 190.40 2.89 o
-5 1 1 248.89 253.82 4.99 o
-4 1 1 5.72 4.34 0.39 o
-3 1 1 35.23 37.77 0.59 o
-2 1 1 2.07 5.20 0.40 o
-1 1 1 12.51 8.83 0.48 o
0 1 1 262.61 267.19 2.52 o
1 1 1 402.32 341.01 2.20 o
2 1 1 304.72 312.52 1.98 o
3 1 1 535.68 542.86 1.81 o
4 1 1 126.48 140.38 1.35 o
5 1 1 49.05 47.61 1.55 o
6 1 1 21.05 21.38 0.58 o
7 1 1 4.67 4.02 0.48 o
8 1 1 54.81 61.22 0.74 o
-7 2 1 1.82 1.64 0.60 o
-6 2 1 12.07 12.42 0.48 o
-5 2 1 1.43 1.89 0.46 o
-4 2 1 21.14 15.75 2.04 o
-3 2 1 208.65 199.26 2.41 o
-2 2 1 550.40 557.89 3.99 o
-1 2 1 400.77 443.14 4.69 o
0 2 1 0.73 3.06 0.67 o
1 2 1 4.81 3.53 0.49 o
2 2 1 1355.30 1301.61 16.59 o
3 2 1 215.63 229.03 1.51 o
4 2 1 20.64 23.10 0.49 o
5 2 1 26.34 26.34 0.61 o
6 2 1 187.02 174.94 1.81 o
7 2 1 10.20 12.49 0.57 o
8 2 1 0.04 -0.14 0.52 o
-7 3 1 0.21 -0.07 0.51 o
-6 3 1 15.66 15.88 0.49 o
-5 3 1 90.70 94.22 4.87 o
-4 3 1 137.42 135.31 1.35 o
-3 3 1 0.05 0.12 0.38 o
-2 3 1 16.19 17.61 0.45 o
-1 3 1 649.82 606.62 1.90 o
0 3 1 2277.94 2234.79 43.04 o
1 3 1 0.90 0.77 0.42 o
2 3 1 276.94 297.88 2.77 o
3 3 1 443.64 431.03 2.73 o
4 3 1 0.77 1.37 0.42 o
5 3 1 164.03 169.29 0.93 o
6 3 1 0.55 0.73 0.54 o
7 3 1 0.63 0.53 0.70 o
8 3 1 18.96 19.70 0.67 o
-6 4 1 2.91 2.79 0.48 o
-5 4 1 9.38 8.81 0.45 o
-4 4 1 45.45 44.17 0.58 o
-3 4 1 15.30 14.10 0.42 o
-2 4 1 271.21 266.47 2.30 o
-1 4 1 1.64 1.43 0.39 o
0 4 1 282.36 267.03 3.78 o
1 4 1 947.78 937.73 1.88 o
2 4 1 119.98 128.95 0.79 o
3 4 1 3.88 4.94 0.40 o
4 4 1 0.03 0.03 0.42 o
5 4 1 125.43 122.40 0.82 o
6 4 1 0.11 0.44 0.45 o
7 4 1 49.66 53.39 0.79 o
8 4 1 0.32 0.41 0.65 o
-6 5 1 32.84 29.24 1.57 o
-5 5 1 0.02 0.15 0.37 o
-4 5 1 2.48 1.40 0.38 o
-3 5 1 3.16 3.72 0.37 o
-2 5 1 294.74 291.48 4.41 o
-1 5 1 1.75 1.28 0.46 o
0 5 1 0.20 0.06 0.36 o
1 5 1 5.02 6.59 0.47 o
2 5 1 200.24 202.69 1.93 o
3 5 1 55.01 54.96 0.60 o
4 5 1 108.04 110.74 0.73 o
5 5 1 180.26 183.20 2.78 o
6 5 1 45.18 42.90 0.72 o
7 5 1 30.95 34.66 1.35 o
-5 6 1 12.95 12.06 0.45 o
-4 6 1 0.02 -0.07 0.44 o
-3 6 1 0.44 0.73 0.31 o
-2 6 1 1.16 1.74 0.81 o
-1 6 1 4.10 2.76 0.41 o
0 6 1 0.44 0.91 0.46 o
1 6 1 165.85 181.01 0.99 o
2 6 1 64.19 54.41 0.51 o
3 6 1 27.40 27.55 0.47 o
4 6 1 2.42 2.43 0.42 o
5 6 1 70.16 68.28 0.77 o
6 6 1 0.73 0.79 0.51 o
7 6 1 65.75 67.24 1.75 o
-4 7 1 2.11 2.20 0.42 o
-3 7 1 0.40 0.10 0.36 o
-2 7 1 10.41 11.92 0.38 o
-1 7 1 4.37 4.79 0.39 o
0 7 1 373.32 374.38 5.38 o
1 7 1 73.34 76.92 2.12 o
2 7 1 77.35 73.12 0.66 o
3 7 1 11.41 11.38 0.44 o
4 7 1 15.54 16.62 0.46 o
5 7 1 4.44 4.50 0.48 o
6 7 1 4.85 5.79 0.53 o
7 7 1 10.96 14.22 0.74 o
-3 8 1 17.56 18.72 0.46 o
-2 8 1 12.63 12.84 0.57 o
-1 8 1 1.67 1.55 0.51 o
0 8 1 8.75 10.37 0.42 o
1 8 1 65.89 64.36 0.64 o
2 8 1 1.12 1.65 0.48 o
3 8 1 78.53 77.09 1.02 o
4 8 1 10.79 10.18 0.54 o
5 8 1 5.63 5.73 0.54 o
6 8 1 3.56 3.22 0.59 o
-2 9 1 0.00 0.28 0.40 o
-1 9 1 22.51 21.90 1.07 o
0 9 1 1.54 0.75 0.46 o
1 9 1 0.03 0.28 0.46 o
2 9 1 0.06 -0.42 0.52 o
3 9 1 0.33 0.38 0.41 o
4 9 1 0.73 0.70 0.47 o
5 9 1 1.11 1.48 0.53 o
0 10 1 40.54 39.75 0.64 o
1 10 1 4.57 3.17 0.50 o
2 10 1 4.21 4.21 0.56 o
3 10 1 0.47 0.23 0.58 o
-3 -10 2 2.38 2.62 0.43 o
-2 -10 2 14.19 15.88 0.69 o
-1 -10 2 2.04 2.16 0.58 o
0 -10 2 3.50 4.62 0.52 o
-4 -9 2 81.93 78.51 2.74 o
-3 -9 2 64.73 65.81 1.04 o
-2 -9 2 0.42 1.09 0.38 o
-1 -9 2 0.44 1.07 0.40 o
0 -9 2 0.01 0.38 0.53 o
1 -9 2 9.36 8.30 0.55 o
2 -9 2 7.32 3.87 0.50 o
-5 -8 2 54.42 54.91 1.27 o
-4 -8 2 17.75 17.37 0.43 o
-3 -8 2 6.09 8.41 0.36 o
-2 -8 2 21.31 21.88 0.81 o
-1 -8 2 18.07 18.83 0.79 o
0 -8 2 29.34 30.17 0.54 o
1 -8 2 0.10 0.24 0.43 o
2 -8 2 3.74 4.86 0.42 o
3 -8 2 20.59 17.77 1.11 o
4 -8 2 2.88 4.24 0.51 o
-6 -7 2 30.03 31.64 0.70 o
-5 -7 2 0.02 0.15 0.45 o
-4 -7 2 32.39 33.60 0.52 o
-3 -7 2 78.19 79.23 0.59 o
-2 -7 2 36.83 33.75 0.47 o
-1 -7 2 2.30 3.19 0.34 o
0 -7 2 97.61 96.87 1.34 o
1 -7 2 68.98 74.87 1.13 o
2 -7 2 179.30 174.40 7.29 o
3 -7 2 70.37 65.45 0.59 o
4 -7 2 21.28 21.42 1.26 o
5 -7 2 1.51 1.58 0.46 o
-6 -6 2 5.22 4.73 0.52 o
-5 -6 2 83.68 86.01 0.69 o
-4 -6 2 47.86 44.21 0.58 o
-3 -6 2 73.34 76.50 0.59 o
-2 -6 2 59.26 57.43 0.58 o
-1 -6 2 105.58 104.67 2.28 o
0 -6 2 72.40 67.92 0.80 o
1 -6 2 42.05 38.77 0.40 o
2 -6 2 3.90 3.85 0.42 o
3 -6 2 0.03 0.29 0.43 o
4 -6 2 8.83 7.65 0.46 o
5 -6 2 3.87 4.21 0.54 o
-7 -5 2 0.03 -0.23 0.70 o
-6 -5 2 0.00 0.24 0.55 o
-5 -5 2 93.38 100.62 0.75 o
-4 -5 2 146.29 139.18 1.47 o
-3 -5 2 81.04 79.48 0.93 o
-2 -5 2 23.97 23.84 0.50 o
-1 -5 2 37.30 36.19 0.83 o
0 -5 2 45.62 51.75 0.62 o
1 -5 2 6.93 6.09 0.37 o
2 -5 2 241.11 239.68 2.87 o
3 -5 2 39.95 38.13 0.99 o
4 -5 2 128.38 124.85 1.40 o
5 -5 2 2.97 2.94 0.40 o
6 -5 2 1.17 0.98 0.43 o
-7 -4 2 0.04 0.07 0.68 o
-6 -4 2 1.39 1.78 0.52 o
-5 -4 2 22.68 21.53 0.54 o
-4 -4 2 213.77 208.69 2.39 o
-3 -4 2 88.20 83.86 0.62 o
-2 -4 2 110.20 117.27 1.35 o
-1 -4 2 57.14 61.35 0.55 o
0 -4 2 315.25 324.78 1.73 o
1 -4 2 219.93 220.21 1.17 o
2 -4 2 191.75 197.51 1.97 o
3 -4 2 7.22 6.77 0.40 o
4 -4 2 40.74 38.11 0.51 o
5 -4 2 1.05 0.66 0.34 o
6 -4 2 6.85 8.12 0.47 o
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