#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:34:24 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181176 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/55/2225562.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2225562_Fobs loop_ _publ_author_name 'Boechat, Nubia' 'Kover, Warner B.' 'Ferreira, Sabrina B.' 'Wardell, Solange M. S. V.' 'Wardell, James L.' 'Tiekink, Edward R. T.' _publ_section_title ; N-(4-Chlorophenyl)ethanimidamide ; _journal_coeditor_code HG2664 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o958 _journal_volume 66 _journal_year 2010 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.6460 _cell_length_b 9.0192 _cell_length_c 19.3281 _exptl_crystal_F_000 704.00 _reflns_d_resolution_high 0.7702 _cod_data_source_file hg2664Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 0511 R = New: Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 222.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2092.49 1998.67 50.69 o 4 0 0 2684.42 2706.58 74.18 o 6 0 0 937.54 1094.03 50.91 o 8 0 0 0.33 1.85 18.00 o 10 0 0 932.18 949.15 70.90 o 12 0 0 82.18 37.67 62.79 o 2 1 0 29915.87 27730.64 419.29 o 4 1 0 11833.01 11762.94 197.82 o 6 1 0 3173.10 3280.99 73.47 o 8 1 0 75.54 89.52 16.61 o 10 1 0 117.28 123.47 22.10 o 12 1 0 78.11 51.24 33.09 o 0 2 0 263.01 255.87 14.50 o 2 2 0 49342.14 46547.46 769.08 o 4 2 0 1770.90 1865.02 43.26 o 6 2 0 1804.22 1874.09 52.80 o 8 2 0 3227.10 3522.59 124.61 o 10 2 0 0.39 -4.77 23.56 o 12 2 0 5.26 23.71 47.09 o 2 3 0 1161.31 942.68 24.74 o 4 3 0 13122.07 13565.08 204.16 o 6 3 0 1687.96 1919.40 51.28 o 8 3 0 1.53 12.72 11.55 o 10 3 0 53.51 23.53 31.72 o 12 3 0 1.61 -15.70 40.81 o 0 4 0 10099.33 10401.67 201.47 o 2 4 0 607.46 657.47 17.79 o 4 4 0 1132.94 1234.41 38.68 o 6 4 0 333.88 371.46 13.44 o 8 4 0 316.72 300.64 18.08 o 10 4 0 227.50 222.28 23.48 o 2 5 0 1799.89 2289.32 47.63 o 4 5 0 8.55 -2.05 10.36 o 6 5 0 336.77 312.17 23.76 o 8 5 0 140.19 132.78 28.55 o 10 5 0 0.05 51.54 38.32 o 0 6 0 1146.64 1307.95 53.18 o 2 6 0 161.54 202.82 12.12 o 4 6 0 332.83 356.92 26.00 o 6 6 0 46.74 27.29 24.47 o 8 6 0 95.97 84.36 24.90 o 10 6 0 0.70 -20.70 34.48 o 2 7 0 286.89 293.75 18.35 o 4 7 0 0.14 -8.63 15.70 o 6 7 0 16.21 18.36 24.82 o 8 7 0 1.20 -17.58 24.32 o 10 7 0 38.11 67.02 40.63 o 0 8 0 962.31 1118.60 66.83 o 2 8 0 92.14 87.27 13.32 o 4 8 0 56.75 66.20 32.49 o 6 8 0 119.58 88.28 29.57 o 8 8 0 20.02 39.02 36.55 o 2 9 0 135.05 141.23 23.56 o 4 9 0 474.93 418.71 51.70 o 6 9 0 129.91 104.23 37.51 o 8 9 0 18.49 41.44 42.93 o 0 10 0 726.39 801.20 92.61 o 2 10 0 368.02 346.15 27.93 o 4 10 0 51.96 44.13 42.96 o 6 10 0 57.96 73.68 50.67 o 2 11 0 489.12 583.37 81.33 o 4 11 0 264.11 343.42 58.91 o 1 1 1 608.67 583.71 10.01 o 2 1 1 1111.52 1305.58 20.71 o 3 1 1 7698.63 7552.10 91.06 o 4 1 1 34.07 39.27 4.77 o 5 1 1 320.29 313.13 9.70 o 6 1 1 418.81 390.27 12.92 o 7 1 1 271.79 304.37 13.59 o 8 1 1 495.65 508.44 20.07 o 9 1 1 6.13 5.63 10.68 o 10 1 1 153.75 166.52 16.01 o 11 1 1 0.20 -19.93 14.71 o 12 1 1 5.64 14.32 24.14 o 0 2 1 10789.29 9718.95 132.73 o 1 2 1 3408.26 3192.73 37.98 o 2 2 1 681.47 608.61 13.67 o 3 2 1 109.14 89.89 4.35 o 4 2 1 3954.83 4128.32 55.26 o 5 2 1 2560.22 2605.92 42.99 o 6 2 1 69.26 38.07 7.14 o 7 2 1 67.29 73.77 8.37 o 8 2 1 224.52 203.24 14.01 o 9 2 1 71.30 72.90 11.98 o 10 2 1 51.30 41.87 13.75 o 11 2 1 15.66 41.38 18.01 o 12 2 1 76.54 70.10 27.92 o 1 3 1 4638.79 4384.31 52.03 o 2 3 1 10.88 6.07 2.84 o 3 3 1 13.59 12.64 4.15 o 4 3 1 915.06 820.38 15.39 o 5 3 1 76.44 60.45 5.65 o 6 3 1 627.95 640.16 18.88 o 7 3 1 146.42 144.33 10.50 o 8 3 1 329.78 340.22 17.12 o 9 3 1 227.84 237.13 15.12 o 10 3 1 2.00 -2.92 13.99 o 11 3 1 4.57 -4.77 15.00 o 12 3 1 40.36 71.45 32.13 o 0 4 1 886.17 941.09 23.39 o 1 4 1 4176.74 4343.13 53.40 o 2 4 1 213.91 258.36 9.29 o 3 4 1 1871.77 1974.54 37.97 o 4 4 1 1624.66 1643.75 35.22 o 5 4 1 88.49 73.63 9.71 o 6 4 1 483.49 513.30 13.12 o 7 4 1 248.92 232.81 9.53 o 8 4 1 1166.58 1220.61 33.68 o 9 4 1 40.90 43.09 9.31 o 10 4 1 0.85 15.46 12.25 o 11 4 1 16.06 19.87 17.38 o 1 5 1 2291.03 2380.30 33.45 o 2 5 1 1070.92 1120.79 21.04 o 3 5 1 294.75 230.65 11.98 o 4 5 1 410.05 409.01 16.47 o 5 5 1 35.20 27.51 9.18 o 6 5 1 13.57 3.16 9.36 o 7 5 1 65.10 82.94 13.90 o 8 5 1 18.25 29.92 15.21 o 9 5 1 67.52 77.95 19.05 o 10 5 1 70.27 82.39 28.00 o 11 5 1 61.55 52.29 26.31 o 0 6 1 1849.93 1954.25 45.16 o 1 6 1 1.91 0.76 5.04 o 2 6 1 95.48 91.13 8.21 o 3 6 1 938.61 960.89 26.24 o 4 6 1 130.49 112.30 11.95 o 5 6 1 686.59 713.32 26.41 o 6 6 1 73.62 41.44 11.88 o 7 6 1 81.05 66.35 14.79 o 8 6 1 35.36 52.10 16.00 o 9 6 1 16.01 1.10 19.33 o 10 6 1 155.06 143.35 29.15 o 1 7 1 469.83 455.31 15.50 o 2 7 1 25.30 22.37 6.81 o 3 7 1 358.75 408.41 20.05 o 4 7 1 256.97 248.49 18.22 o 5 7 1 2.46 -4.84 12.74 o 6 7 1 119.80 97.71 16.24 o 7 7 1 38.72 42.76 18.80 o 8 7 1 0.11 -2.88 20.76 o 9 7 1 50.24 64.82 29.95 o 10 7 1 55.01 68.68 39.92 o 0 8 1 56.25 53.58 13.70 o 1 8 1 9.29 3.13 8.93 o 2 8 1 265.12 267.76 18.85 o 3 8 1 4.68 20.17 13.69 o 4 8 1 76.20 93.03 19.42 o 5 8 1 250.46 215.13 23.12 o 6 8 1 62.53 47.63 19.64 o 7 8 1 159.42 115.64 25.95 o 8 8 1 36.84 27.16 28.48 o 9 8 1 0.14 -10.82 30.06 o 1 9 1 23.42 46.06 14.40 o 2 9 1 121.08 122.26 11.76 o 3 9 1 86.79 69.91 18.69 o 4 9 1 53.07 79.79 22.27 o 5 9 1 74.16 65.36 22.49 o 6 9 1 11.89 16.79 28.31 o 7 9 1 2.49 6.69 27.34 o 0 10 1 143.29 116.01 30.02 o 1 10 1 4.84 28.18 14.41 o 2 10 1 26.15 36.99 15.03 o 3 10 1 0.16 14.92 21.51 o 4 10 1 39.87 20.43 25.51 o 5 10 1 0.08 6.68 31.39 o 6 10 1 16.25 48.57 31.21 o 1 11 1 0.19 31.13 36.27 o 2 11 1 3.64 -24.72 33.34 o 3 11 1 1.18 22.42 38.77 o 4 11 1 4.56 -3.08 31.14 o 1 0 2 4148.88 -2.09 2.81 o 2 0 2 16255.41 15237.40 262.58 o 3 0 2 792.52 971.27 35.34 o 4 0 2 17.86 9.90 6.37 o 5 0 2 3816.30 4284.06 86.71 o 6 0 2 0.38 8.06 9.21 o 7 0 2 1.19 0.52 9.62 o 8 0 2 4067.77 4695.71 118.56 o 9 0 2 1089.57 1141.43 68.88 o 10 0 2 3.80 12.60 19.42 o 11 0 2 345.38 366.38 34.98 o 12 0 2 361.37 442.34 62.16 o 1 1 2 171.92 159.82 4.46 o 2 1 2 11028.69 10029.91 121.58 o 3 1 2 128.52 115.05 5.32 o 4 1 2 4617.83 4348.59 59.80 o 5 1 2 744.13 745.50 16.06 o 6 1 2 333.23 348.44 12.50 o 7 1 2 1069.67 1067.56 25.72 o 8 1 2 0.12 11.28 8.86 o 9 1 2 64.48 55.58 12.30 o 10 1 2 161.75 149.35 16.31 o 11 1 2 13.07 12.43 15.72 o 12 1 2 6.46 -5.23 24.66 o 0 2 2 36972.97 33213.61 459.90 o 1 2 2 3202.06 2986.67 37.63 o 2 2 2 995.93 957.59 15.31 o 3 2 2 2049.09 1961.82 32.06 o 4 2 2 3.58 6.47 3.31 o 5 2 2 544.99 679.83 15.46 o 6 2 2 2587.93 2787.10 46.28 o 7 2 2 75.85 62.17 8.51 o 8 2 2 126.17 124.01 11.96 o 9 2 2 73.54 69.81 13.66 o 10 2 2 109.96 82.88 16.70 o 11 2 2 133.52 135.80 22.62 o 12 2 2 8.41 21.69 25.93 o 1 3 2 194.15 176.84 5.99 o 2 3 2 148.88 199.84 6.62 o 3 3 2 1003.59 1009.05 16.78 o 4 3 2 2493.14 2601.11 35.11 o 5 3 2 623.53 620.16 16.17 o 6 3 2 719.26 672.68 16.70 o 7 3 2 0.26 13.11 7.26 o 8 3 2 149.88 133.93 12.61 o 9 3 2 90.07 67.50 12.03 o 10 3 2 3.85 -7.27 12.15 o 11 3 2 19.74 4.28 14.02 o 12 3 2 17.38 60.41 32.13 o 0 4 2 178.81 159.48 9.11 o 1 4 2 0.34 -3.77 3.37 o 2 4 2 1825.06 1965.18 26.74 o 3 4 2 144.72 120.11 6.40 o 4 4 2 144.12 174.25 7.64 o 5 4 2 8.45 9.18 3.93 o 6 4 2 37.05 30.88 6.30 o 7 4 2 378.63 390.68 14.55 o 8 4 2 305.57 290.99 14.07 o 9 4 2 21.27 20.76 12.50 o 10 4 2 89.92 73.46 13.26 o 11 4 2 1.77 -2.27 13.47 o 1 5 2 347.88 388.62 10.28 o 2 5 2 312.30 308.03 8.67 o 3 5 2 9.24 9.40 2.89 o 4 5 2 93.60 126.35 10.45 o 5 5 2 26.45 42.26 9.40 o 6 5 2 17.59 13.53 11.58 o 7 5 2 101.13 99.38 13.42 o 8 5 2 6.23 7.49 14.38 o 9 5 2 102.72 72.56 9.54 o 10 5 2 30.89 31.22 21.65 o 11 5 2 3.71 28.75 32.45 o 0 6 2 1.12 11.68 7.40 o 1 6 2 118.77 132.22 7.47 o 2 6 2 86.48 107.06 7.29 o 3 6 2 645.69 680.51 18.10 o 4 6 2 85.61 107.59 11.80 o 5 6 2 1.52 7.40 10.61 o 6 6 2 11.99 18.52 12.09 o 7 6 2 24.61 28.25 13.85 o 8 6 2 0.01 7.28 18.73 o 9 6 2 38.06 24.75 22.50 o 10 6 2 49.86 59.27 24.53 o 1 7 2 271.30 281.42 11.30 o 2 7 2 9.03 10.57 5.81 o 3 7 2 98.86 97.78 7.82 o 4 7 2 129.71 104.04 13.41 o 5 7 2 83.30 54.20 14.26 o 6 7 2 137.73 132.80 17.65 o 7 7 2 86.85 83.93 20.14 o 8 7 2 34.05 29.32 22.85 o 9 7 2 17.03 13.62 21.09 o 0 8 2 106.45 91.10 15.56 o 1 8 2 86.08 77.93 10.08 o 2 8 2 88.24 83.42 9.09 o 3 8 2 94.08 97.36 11.51 o 4 8 2 5.92 7.08 14.59 o 5 8 2 157.69 172.78 21.89 o 6 8 2 50.37 34.07 20.96 o 7 8 2 4.28 12.31 21.85 o 8 8 2 54.89 41.94 25.89 o 9 8 2 16.79 12.39 25.02 o 1 9 2 218.54 228.48 18.01 o 2 9 2 522.91 545.39 21.56 o 3 9 2 0.82 3.59 19.60 o 4 9 2 178.10 177.32 27.08 o 5 9 2 11.66 21.54 23.02 o 6 9 2 17.75 20.93 23.00 o 7 9 2 57.70 51.54 28.38 o 0 10 2 516.51 571.76 42.89 o 1 10 2 0.02 -6.60 15.59 o 2 10 2 74.25 70.81 16.55 o 3 10 2 67.74 82.55 25.06 o 4 10 2 2.31 7.26 27.52 o 5 10 2 67.20 85.15 29.50 o 6 10 2 28.62 47.11 30.74 o 1 11 2 2.02 14.16 44.87 o 2 11 2 38.75 33.82 35.70 o 3 11 2 38.02 47.27 36.83 o 4 11 2 75.77 161.70 46.94 o 1 1 3 155.63 178.90 4.28 o 2 1 3 6681.65 6004.65 74.12 o 3 1 3 0.45 0.67 3.09 o 4 1 3 66.38 91.75 6.07 o 5 1 3 4.18 13.68 4.61 o 6 1 3 324.98 316.03 14.93 o 7 1 3 27.37 28.20 7.95 o 8 1 3 96.10 93.57 10.22 o 9 1 3 87.42 97.80 12.54 o 10 1 3 1.67 -3.22 12.71 o 11 1 3 121.46 106.34 18.00 o 12 1 3 8.69 21.67 23.70 o 0 2 3 1505.25 1538.33 30.07 o 1 2 3 2704.20 2469.64 30.83 o 2 2 3 181.62 166.66 5.06 o 3 2 3 738.34 756.85 13.69 o 4 2 3 22.16 10.76 4.07 o 5 2 3 8.34 5.02 4.42 o 6 2 3 256.34 272.36 11.67 o 7 2 3 277.03 306.73 12.55 o 8 2 3 854.32 840.44 26.05 o 9 2 3 170.78 174.87 14.91 o 10 2 3 4.19 -9.73 18.99 o 11 2 3 172.76 179.79 23.54 o 12 2 3 20.37 4.67 23.56 o 1 3 3 71.67 70.97 4.33 o 2 3 3 1879.40 1772.22 26.87 o 3 3 3 640.26 667.44 14.58 o 4 3 3 3496.83 3572.67 52.87 o 5 3 3 7.27 1.50 4.32 o 6 3 3 4.40 11.59 5.55 o 7 3 3 33.40 30.72 7.37 o 8 3 3 5.82 11.86 8.01 o 9 3 3 40.31 34.63 10.31 o 10 3 3 108.35 134.24 17.99 o 11 3 3 3.04 8.05 14.57 o 12 3 3 91.40 80.37 37.67 o 0 4 3 5846.30 5579.87 95.14 o 1 4 3 1100.34 1118.91 17.10 o 2 4 3 1457.90 1476.78 23.79 o 3 4 3 0.19 5.75 3.32 o 4 4 3 442.08 401.57 12.90 o 5 4 3 228.80 275.31 10.35 o 6 4 3 1782.45 1921.91 36.27 o 7 4 3 1047.55 1110.82 30.70 o 8 4 3 72.34 93.19 10.88 o 9 4 3 13.56 9.67 8.92 o 10 4 3 185.77 195.95 17.45 o 11 4 3 104.20 105.96 26.61 o 1 5 3 530.04 489.27 11.89 o 2 5 3 444.23 418.96 10.87 o 3 5 3 6.26 -0.71 3.43 o 4 5 3 1343.85 1402.58 29.26 o 5 5 3 64.75 61.85 11.22 o 6 5 3 1124.97 1145.56 36.64 o 7 5 3 41.97 21.99 11.69 o 8 5 3 104.10 100.50 16.96 o 9 5 3 246.45 209.39 16.08 o 10 5 3 594.72 602.78 43.29 o 11 5 3 56.42 91.53 34.96 o 0 6 3 918.40 972.48 31.36 o 1 6 3 283.56 317.66 10.97 o 2 6 3 678.02 718.21 20.16 o 3 6 3 0.04 1.55 4.57 o 4 6 3 9.13 21.02 9.70 o 5 6 3 166.05 135.59 14.00 o 6 6 3 339.15 328.87 21.53 o 7 6 3 90.79 74.44 14.50 o 8 6 3 1413.35 1568.97 55.61 o 9 6 3 143.44 107.39 25.37 o 10 6 3 3.22 7.26 24.24 o 1 7 3 2.19 15.39 6.55 o 2 7 3 1139.67 1274.80 26.49 o 3 7 3 264.07 237.84 12.61 o 4 7 3 797.65 780.38 30.16 o 5 7 3 107.86 84.10 14.88 o 6 7 3 20.22 31.22 13.85 o 7 7 3 73.46 71.10 16.86 o 8 7 3 42.22 49.36 22.28 o 9 7 3 2.25 -28.22 23.42 o 0 8 3 765.93 772.70 32.62 o 1 8 3 34.90 29.17 8.09 o 2 8 3 76.57 62.03 8.08 o 3 8 3 89.02 99.29 10.62 o 4 8 3 13.88 23.06 15.14 o 5 8 3 44.39 35.04 16.61 o 6 8 3 471.51 468.74 29.90 o 7 8 3 21.18 28.40 23.61 o 8 8 3 7.48 4.78 28.15 o 9 8 3 23.79 -2.02 29.72 o 1 9 3 39.75 23.68 10.29 o 2 9 3 131.70 118.36 11.90 o 3 9 3 34.05 23.80 8.22 o 4 9 3 127.33 139.65 21.52 o 5 9 3 1.10 -15.87 20.38 o 6 9 3 4.07 20.65 28.78 o 7 9 3 31.37 34.41 27.31 o 0 10 3 4.32 29.27 28.09 o 1 10 3 2.77 13.58 13.90 o 2 10 3 44.54 35.17 16.26 o 3 10 3 2.00 3.17 23.86 o 4 10 3 50.99 66.22 26.91 o 5 10 3 2.94 3.74 25.57 o 6 10 3 0.24 -33.80 26.01 o 1 11 3 4.10 14.63 35.98 o 2 11 3 17.11 10.12 34.12 o 3 11 3 0.13 -22.32 37.23 o 4 11 3 1.53 -54.86 65.46 o 0 0 4 2180.77 1990.78 66.15 o 1 0 4 653.96 650.24 18.84 o 2 0 4 4436.34 4086.51 86.42 o 3 0 4 20076.69 19707.79 358.12 o 4 0 4 249.13 284.37 12.80 o 5 0 4 360.40 256.32 13.16 o 6 0 4 131.34 161.70 12.34 o 7 0 4 715.41 696.76 28.17 o 8 0 4 422.26 412.34 23.57 o 9 0 4 41.22 45.68 13.75 o 10 0 4 18.93 22.90 20.17 o 11 0 4 51.42 73.20 26.38 o 12 0 4 173.07 170.71 58.08 o 1 1 4 2337.69 2191.67 27.34 o 2 1 4 143.71 162.72 5.06 o 3 1 4 664.29 618.09 12.23 o 4 1 4 663.33 640.61 14.94 o 5 1 4 1213.49 1140.32 22.15 o 6 1 4 124.46 141.89 9.23 o 7 1 4 1188.54 1276.01 29.43 o 8 1 4 91.78 104.24 10.89 o 9 1 4 495.17 492.49 20.65 o 10 1 4 156.62 120.80 16.75 o 11 1 4 13.72 33.42 20.39 o 12 1 4 0.45 -27.54 27.19 o 0 2 4 5841.34 5552.85 96.89 o 1 2 4 1097.88 1018.22 16.47 o 2 2 4 0.08 1.20 2.68 o 3 2 4 72.92 50.31 4.30 o 4 2 4 506.05 514.11 13.43 o 5 2 4 2091.92 2104.54 36.73 o 6 2 4 26.55 27.29 6.37 o 7 2 4 577.84 583.00 18.03 o 8 2 4 150.53 134.81 12.44 o 9 2 4 763.63 773.76 28.53 o 10 2 4 408.38 459.81 24.23 o 11 2 4 355.24 347.45 38.06 o 12 2 4 51.07 15.67 23.36 o 1 3 4 2825.30 2813.42 37.92 o 2 3 4 32.91 43.66 3.68 o 3 3 4 137.43 178.27 7.49 o 4 3 4 18.50 33.45 4.75 o 5 3 4 34.49 39.63 6.16 o 6 3 4 598.01 657.85 16.71 o 7 3 4 735.55 748.38 20.14 o 8 3 4 432.78 468.21 17.64 o 9 3 4 95.56 93.76 12.46 o 10 3 4 26.91 21.80 14.07 o 11 3 4 26.77 9.79 19.21 o 0 4 4 28.64 23.17 6.66 o 1 4 4 2.45 8.48 4.05 o 2 4 4 411.13 438.57 10.75 o 3 4 4 145.39 132.65 7.06 o 4 4 4 26.98 22.95 4.94 o 5 4 4 205.12 199.70 8.99 o 6 4 4 470.71 466.82 14.95 o 7 4 4 0.06 -3.56 5.68 o 8 4 4 390.58 434.73 18.16 o 9 4 4 0.67 -1.49 8.50 o 10 4 4 19.99 12.60 12.60 o 11 4 4 96.74 68.76 18.30 o 1 5 4 1.98 7.50 4.76 o 2 5 4 0.17 8.51 4.50 o 3 5 4 99.87 137.11 6.28 o 4 5 4 49.91 61.63 9.79 o 5 5 4 121.83 133.31 10.57 o 6 5 4 139.58 127.72 7.87 o 7 5 4 34.71 32.60 5.88 o 8 5 4 12.84 6.30 6.05 o 9 5 4 78.86 61.44 13.52 o 10 5 4 10.17 -13.30 13.34 o 11 5 4 7.91 40.81 65.93 o 0 6 4 2.60 22.78 8.88 o 1 6 4 2.70 7.78 5.66 o 2 6 4 5.24 4.57 5.51 o 3 6 4 56.48 50.03 4.67 o 4 6 4 195.61 185.18 12.14 o 5 6 4 179.45 169.27 15.01 o 6 6 4 105.00 90.27 13.64 o 7 6 4 6.74 17.87 13.47 o 8 6 4 44.63 42.93 21.05 o 9 6 4 13.01 35.51 18.96 o 10 6 4 5.81 15.51 23.04 o 1 7 4 236.85 216.77 10.52 o 2 7 4 46.37 45.72 6.76 o 3 7 4 14.16 12.86 4.33 o 4 7 4 56.51 45.24 12.74 o 5 7 4 219.35 223.72 18.10 o 6 7 4 94.50 69.81 16.30 o 7 7 4 2.91 9.35 17.86 o 8 7 4 3.29 -0.49 19.90 o 9 7 4 28.47 39.09 25.15 o 0 8 4 57.28 74.87 14.69 o 1 8 4 19.42 19.18 7.59 o 2 8 4 7.99 5.36 6.88 o 3 8 4 581.89 651.52 19.64 o 4 8 4 65.09 32.00 16.16 o 5 8 4 8.12 0.22 16.42 o 6 8 4 18.91 39.41 19.67 o 7 8 4 0.01 15.43 22.26 o 8 8 4 3.97 30.95 23.29 o 1 9 4 108.65 101.28 11.45 o 2 9 4 6.83 12.03 9.53 o 3 9 4 34.17 29.13 11.56 o 4 9 4 39.42 29.77 19.56 o 5 9 4 3.06 11.36 21.86 o 6 9 4 72.48 66.27 28.55 o 7 9 4 266.25 252.67 32.08 o 0 10 4 12.45 4.32 18.98 o 1 10 4 79.97 62.34 14.08 o 2 10 4 5.47 -1.63 16.15 o 3 10 4 77.44 85.43 26.24 o 4 10 4 10.59 19.16 23.91 o 5 10 4 137.61 123.85 32.17 o 6 10 4 0.79 -22.04 26.52 o 1 11 4 120.98 105.27 39.40 o 2 11 4 1.56 17.11 42.26 o 3 11 4 0.69 33.56 38.42 o 1 1 5 410.58 475.60 9.35 o 2 1 5 262.58 286.93 7.12 o 3 1 5 22.62 29.12 3.09 o 4 1 5 18.76 18.61 2.89 o 5 1 5 21.09 19.51 4.70 o 6 1 5 88.86 88.54 7.64 o 7 1 5 33.49 32.20 7.82 o 8 1 5 75.89 79.51 10.28 o 9 1 5 5.10 7.27 8.98 o 10 1 5 359.47 354.19 20.84 o 11 1 5 87.64 103.64 27.75 o 12 1 5 8.08 19.01 37.16 o 0 2 5 1778.86 1638.53 46.48 o 1 2 5 7524.84 7249.54 79.53 o 2 2 5 19.98 20.32 3.94 o 3 2 5 1420.05 1370.23 23.15 o 4 2 5 3.47 4.08 4.07 o 5 2 5 0.07 2.36 4.55 o 6 2 5 178.23 155.02 7.99 o 7 2 5 83.16 97.50 8.67 o 8 2 5 302.17 336.17 14.95 o 9 2 5 47.82 43.99 11.38 o 10 2 5 63.40 62.56 16.83 o 11 2 5 9.53 51.55 22.72 o 12 2 5 103.93 123.95 33.68 o 1 3 5 1683.66 1539.80 25.06 o 2 3 5 209.89 190.77 6.86 o 3 3 5 194.43 205.66 7.63 o 4 3 5 1189.18 1127.69 20.44 o 5 3 5 22.62 29.80 7.63 o 6 3 5 229.35 216.36 9.94 o 7 3 5 432.38 465.72 14.61 o 8 3 5 246.91 250.16 11.70 o 9 3 5 186.46 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8.66 o 3 4 8 186.12 178.47 8.49 o 4 4 8 118.96 122.20 8.40 o 5 4 8 613.92 622.06 18.19 o 6 4 8 145.90 175.63 11.00 o 7 4 8 0.13 -3.09 6.78 o 8 4 8 9.91 1.57 9.73 o 9 4 8 137.16 119.91 11.97 o 10 4 8 0.41 13.97 29.45 o 11 4 8 0.13 7.76 18.77 o 1 5 8 96.34 119.58 8.17 o 2 5 8 0.07 5.15 5.93 o 3 5 8 44.27 50.28 7.38 o 4 5 8 97.12 102.30 8.81 o 5 5 8 43.78 30.78 6.19 o 6 5 8 128.61 119.79 10.18 o 7 5 8 76.17 77.34 8.87 o 8 5 8 5.91 8.52 8.40 o 9 5 8 13.30 23.00 16.46 o 10 5 8 37.79 87.22 30.47 o 0 6 8 158.04 155.08 14.38 o 1 6 8 297.44 330.26 13.72 o 2 6 8 155.30 158.18 9.96 o 3 6 8 1.96 6.42 6.55 o 4 6 8 245.15 223.10 11.92 o 5 6 8 17.35 13.95 8.27 o 6 6 8 7.41 -6.69 7.59 o 7 6 8 24.46 31.49 10.45 o 8 6 8 69.33 71.56 15.60 o 9 6 8 16.65 24.24 27.59 o 1 7 8 194.63 203.31 10.87 o 2 7 8 794.67 839.88 22.10 o 3 7 8 355.41 360.68 13.60 o 4 7 8 40.15 33.34 7.19 o 5 7 8 4.00 2.02 10.77 o 6 7 8 34.99 38.93 11.04 o 7 7 8 182.97 164.50 14.14 o 8 7 8 2.21 -18.24 20.99 o 9 7 8 7.42 50.00 30.87 o 0 8 8 834.42 949.23 35.67 o 1 8 8 12.30 30.34 9.44 o 2 8 8 48.44 68.69 9.76 o 3 8 8 5.31 3.01 7.66 o 4 8 8 14.55 10.32 7.26 o 5 8 8 14.16 4.96 19.51 o 6 8 8 182.71 215.03 27.95 o 7 8 8 4.52 30.17 24.33 o 8 8 8 18.18 18.12 25.00 o 1 9 8 322.03 303.41 18.39 o 2 9 8 1.77 -13.20 11.78 o 3 9 8 278.35 301.66 25.54 o 4 9 8 421.40 465.66 34.53 o 5 9 8 53.72 87.78 26.22 o 6 9 8 174.23 128.18 26.91 o 0 10 8 51.46 22.50 33.14 o 1 10 8 56.78 45.63 21.78 o 2 10 8 270.08 282.17 26.10 o 3 10 8 94.01 87.01 28.19 o 4 10 8 15.04 29.79 27.14 o 5 10 8 2.57 32.34 27.42 o 1 11 8 0.18 -9.57 37.44 o 1 1 9 622.94 747.18 16.40 o 2 1 9 128.09 163.13 8.33 o 3 1 9 8.07 6.53 6.92 o 4 1 9 0.45 9.87 5.59 o 5 1 9 0.67 11.68 8.50 o 6 1 9 216.37 232.87 14.97 o 7 1 9 1.25 -2.14 12.46 o 8 1 9 24.53 13.98 11.28 o 9 1 9 183.26 172.74 17.35 o 10 1 9 280.09 267.44 29.98 o 11 1 9 0.50 -17.84 23.15 o 0 2 9 378.55 569.14 18.62 o 1 2 9 1448.46 1515.43 25.37 o 2 2 9 368.77 365.68 10.17 o 3 2 9 1384.16 1340.06 21.60 o 4 2 9 134.12 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