#------------------------------------------------------------------------------ #$Date: 2010-11-03 10:57:48 +0200 (Wed, 03 Nov 2010) $ #$Revision: 1704 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2227024.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2227024_Fobs loop_ _publ_author_name 'Owczarzak, Anita M.' 'Przyby\/l, Anna K.' 'Kubicki, Maciej' _publ_section_title ; N-Methyl-2-thiocytisine ; _journal_coeditor_code NK2044 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1942 _journal_volume 66 _journal_year 2010 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.8530 _cell_length_b 10.6964 _cell_length_c 10.8226 _exptl_crystal_F_000 472.00 _reflns_d_resolution_high 0.7329 _[local]_cod_data_source_file nk2044Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' tiocyt in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 90.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3494.03 3467.80 12.41 o 4 0 0 1674.74 1892.19 9.17 o 6 0 0 636.89 637.77 10.24 o 8 0 0 505.38 510.34 6.94 o 10 0 0 276.09 272.46 10.27 o 12 0 0 120.99 125.35 10.93 o 2 1 0 72.89 70.02 0.78 o 3 1 0 2002.10 2025.30 8.01 o 4 1 0 230.56 239.36 1.45 o 5 1 0 722.39 743.82 4.09 o 6 1 0 914.89 920.59 4.61 o 7 1 0 51.28 46.31 2.06 o 8 1 0 63.88 69.55 2.46 o 9 1 0 9.45 11.98 4.82 o 10 1 0 33.90 27.08 5.55 o 11 1 0 161.09 160.23 7.21 o 12 1 0 22.07 22.48 6.03 o 0 2 0 3645.98 3452.61 8.29 o 1 2 0 479.23 507.69 3.19 o 2 2 0 2207.28 2289.64 4.04 o 3 2 0 19.59 17.65 0.84 o 4 2 0 49.66 49.96 0.96 o 5 2 0 1392.01 1458.14 5.22 o 6 2 0 160.80 192.23 2.31 o 7 2 0 847.74 846.57 12.06 o 8 2 0 1.24 0.07 2.05 o 9 2 0 740.04 771.36 8.16 o 10 2 0 449.56 406.74 8.51 o 11 2 0 0.38 -0.48 5.34 o 12 2 0 44.17 46.96 6.74 o 1 3 0 171.93 174.51 1.63 o 2 3 0 154.05 135.93 1.33 o 3 3 0 198.01 192.91 2.17 o 4 3 0 336.06 320.04 2.31 o 5 3 0 1.57 1.13 0.85 o 6 3 0 245.22 226.75 3.41 o 7 3 0 1.99 2.50 1.84 o 8 3 0 99.39 96.73 3.27 o 9 3 0 122.64 114.15 5.63 o 10 3 0 72.38 70.14 4.88 o 11 3 0 4.48 9.88 5.44 o 0 4 0 327.07 330.09 3.91 o 1 4 0 326.43 318.63 2.96 o 2 4 0 1863.80 1997.68 12.44 o 3 4 0 1505.96 1627.81 7.57 o 4 4 0 98.52 102.53 2.08 o 5 4 0 21.20 21.27 1.55 o 6 4 0 257.65 240.06 5.42 o 7 4 0 155.71 158.60 3.62 o 8 4 0 3341.95 3150.68 26.13 o 9 4 0 54.14 55.07 4.58 o 10 4 0 621.22 594.30 8.20 o 11 4 0 11.83 7.95 4.33 o 1 5 0 36.80 39.71 2.55 o 2 5 0 1204.04 1276.18 6.36 o 3 5 0 14.56 8.14 1.64 o 4 5 0 56.42 48.32 1.90 o 5 5 0 510.37 507.23 4.85 o 6 5 0 107.58 92.86 1.60 o 7 5 0 45.62 38.23 2.72 o 8 5 0 1.62 2.56 2.83 o 9 5 0 155.21 150.98 3.99 o 10 5 0 44.63 38.83 3.47 o 11 5 0 233.23 233.20 4.99 o 12 5 0 26.57 24.14 7.95 o 0 6 0 1271.45 1205.32 9.48 o 1 6 0 709.14 668.08 6.62 o 2 6 0 57.41 63.94 2.94 o 3 6 0 121.42 114.37 3.52 o 4 6 0 300.46 314.46 3.48 o 5 6 0 94.36 106.00 1.98 o 6 6 0 7.92 10.28 1.84 o 7 6 0 188.55 196.05 4.36 o 8 6 0 0.51 0.56 3.18 o 9 6 0 43.19 45.65 3.78 o 10 6 0 51.30 49.29 3.93 o 11 6 0 359.09 382.35 7.44 o 1 7 0 7.29 14.07 3.01 o 2 7 0 0.32 1.39 2.79 o 3 7 0 819.91 817.23 6.45 o 4 7 0 532.83 537.40 6.65 o 5 7 0 526.59 511.52 4.99 o 6 7 0 26.47 26.13 2.86 o 7 7 0 93.54 88.29 3.82 o 8 7 0 2.63 3.77 3.20 o 9 7 0 50.54 51.69 3.94 o 10 7 0 131.57 130.36 4.81 o 11 7 0 12.45 12.60 5.39 o 0 8 0 1848.34 1820.52 13.23 o 1 8 0 6.33 7.38 3.20 o 2 8 0 892.77 907.15 7.11 o 3 8 0 3.51 3.24 3.07 o 4 8 0 2.00 4.12 2.27 o 5 8 0 319.73 284.34 4.32 o 6 8 0 0.36 2.51 2.91 o 7 8 0 1.08 -1.23 3.44 o 8 8 0 286.40 308.82 6.99 o 9 8 0 0.57 1.18 3.73 o 10 8 0 341.18 364.11 10.72 o 1 9 0 275.84 272.69 4.85 o 2 9 0 496.64 491.84 7.84 o 3 9 0 1130.75 1074.46 9.36 o 4 9 0 51.68 53.29 2.65 o 5 9 0 880.55 822.23 6.16 o 6 9 0 613.47 571.27 9.13 o 7 9 0 161.44 170.93 4.85 o 8 9 0 51.73 51.82 4.58 o 9 9 0 0.80 1.42 4.00 o 10 9 0 55.81 57.70 6.19 o 0 10 0 8.40 3.10 4.59 o 1 10 0 29.43 30.74 3.61 o 2 10 0 399.65 387.16 5.83 o 3 10 0 243.49 263.04 5.07 o 4 10 0 25.53 20.53 3.26 o 5 10 0 81.26 85.64 3.41 o 6 10 0 1.76 1.72 3.38 o 7 10 0 24.32 33.68 3.51 o 8 10 0 211.10 212.74 5.49 o 9 10 0 214.87 228.23 9.11 o 1 11 0 255.70 266.06 5.49 o 2 11 0 214.41 211.62 5.26 o 3 11 0 27.60 33.84 3.99 o 4 11 0 204.71 213.38 4.75 o 5 11 0 15.03 14.10 3.12 o 6 11 0 6.02 7.30 3.38 o 7 11 0 2.26 0.82 3.85 o 8 11 0 158.75 156.51 7.56 o 0 12 0 90.40 99.46 6.28 o 1 12 0 35.73 37.26 4.09 o 2 12 0 70.51 72.68 4.39 o 3 12 0 10.19 11.76 3.86 o 4 12 0 154.37 157.58 4.67 o 5 12 0 11.04 10.84 3.28 o 6 12 0 141.48 164.05 7.39 o 7 12 0 128.87 134.05 9.93 o 1 13 0 121.64 131.06 5.19 o 2 13 0 27.43 21.02 4.14 o 3 13 0 265.74 263.42 8.71 o 4 13 0 36.39 43.69 8.25 o 5 13 0 182.74 170.99 10.12 o 2 0 1 7514.43 7317.46 14.07 o 3 0 1 597.79 559.92 2.85 o 4 0 1 40.22 37.59 0.91 o 5 0 1 851.51 953.56 4.96 o 6 0 1 697.55 801.81 3.73 o 7 0 1 756.24 790.07 3.44 o 8 0 1 124.84 131.88 2.12 o 9 0 1 839.98 800.98 6.97 o 10 0 1 0.05 0.77 5.14 o 11 0 1 233.06 222.56 10.50 o 12 0 1 15.68 9.87 6.34 o -12 1 1 382.59 405.81 11.80 o -11 1 1 84.10 78.62 6.65 o -10 1 1 2.51 1.89 5.16 o -9 1 1 24.26 21.78 3.10 o -8 1 1 147.62 145.09 4.14 o -7 1 1 428.17 445.99 5.35 o -6 1 1 358.80 382.98 2.44 o -5 1 1 1262.33 1284.23 7.10 o -4 1 1 332.05 398.07 1.64 o -3 1 1 432.43 426.83 2.67 o -2 1 1 2844.34 2914.74 5.50 o -1 1 1 5432.50 5287.97 21.07 o 1 1 1 5464.40 5303.91 14.61 o 2 1 1 2886.50 2940.46 9.14 o 3 1 1 441.15 432.27 2.86 o 4 1 1 340.63 396.15 2.61 o 5 1 1 1290.51 1283.64 5.79 o 6 1 1 377.36 394.28 2.30 o 7 1 1 421.43 435.13 5.39 o 8 1 1 144.10 134.49 2.77 o 9 1 1 23.84 24.45 3.12 o 10 1 1 2.07 -0.27 5.29 o 11 1 1 81.44 81.97 6.37 o 12 1 1 386.95 413.56 9.92 o -12 2 1 151.81 142.76 7.66 o -11 2 1 118.54 125.79 10.70 o -10 2 1 560.31 531.17 9.35 o -9 2 1 162.43 155.91 4.27 o -8 2 1 1406.03 1373.49 6.45 o -7 2 1 76.77 74.92 1.75 o -6 2 1 461.89 443.39 4.80 o -5 2 1 10.19 11.98 1.08 o -4 2 1 139.61 142.71 1.88 o -3 2 1 811.76 792.75 5.75 o -2 2 1 3503.16 3526.39 9.90 o -1 2 1 3452.92 3461.50 14.62 o 0 2 1 6568.60 6697.18 31.81 o 1 2 1 3448.92 3490.05 9.35 o 2 2 1 3518.23 3585.28 15.67 o 3 2 1 815.89 812.11 2.19 o 4 2 1 140.27 145.10 1.41 o 5 2 1 10.20 11.61 1.25 o 6 2 1 457.80 451.51 3.47 o 7 2 1 76.16 74.22 2.39 o 8 2 1 1419.40 1374.55 8.42 o 9 2 1 162.60 160.62 4.90 o 10 2 1 561.91 549.23 11.92 o 11 2 1 118.22 124.40 7.06 o 12 2 1 149.12 150.39 7.95 o -11 3 1 40.65 37.51 6.92 o -10 3 1 224.91 217.64 10.35 o -9 3 1 479.59 461.53 5.42 o -8 3 1 157.02 168.82 6.90 o -7 3 1 289.64 283.45 5.21 o -6 3 1 305.99 310.07 3.44 o -5 3 1 353.31 338.10 2.90 o -4 3 1 1340.14 1368.96 9.72 o -3 3 1 715.79 704.13 5.95 o -2 3 1 374.91 366.48 3.06 o -1 3 1 467.20 454.16 3.88 o 0 3 1 1206.02 1229.69 5.50 o 1 3 1 459.34 456.43 3.45 o 2 3 1 374.48 364.50 3.00 o 3 3 1 708.56 708.08 3.83 o 4 3 1 1310.30 1347.55 5.73 o 5 3 1 358.34 339.18 2.30 o 6 3 1 304.70 313.82 2.41 o 7 3 1 293.91 287.89 2.47 o 8 3 1 152.30 153.83 3.74 o 9 3 1 479.68 462.20 6.80 o 10 3 1 221.43 214.06 6.02 o 11 3 1 42.50 40.91 4.83 o -11 4 1 94.57 94.51 7.09 o -10 4 1 123.85 116.81 4.28 o -9 4 1 377.28 383.13 7.65 o -8 4 1 93.39 91.85 3.67 o -7 4 1 371.08 374.79 5.33 o -6 4 1 191.47 193.03 2.80 o -5 4 1 100.39 107.01 2.02 o -4 4 1 47.51 54.19 1.17 o -3 4 1 804.73 858.80 3.77 o -2 4 1 404.64 432.17 3.15 o -1 4 1 4329.35 4286.12 20.93 o 0 4 1 55.04 57.09 1.39 o 1 4 1 4370.34 4317.41 24.70 o 2 4 1 402.69 435.09 3.38 o 3 4 1 814.65 870.03 5.83 o 4 4 1 46.73 54.17 1.83 o 5 4 1 102.45 108.25 2.21 o 6 4 1 190.74 189.99 2.37 o 7 4 1 371.02 374.77 3.44 o 8 4 1 93.53 93.33 3.50 o 9 4 1 397.36 395.18 10.08 o 10 4 1 124.62 107.38 5.17 o 11 4 1 91.13 85.37 5.42 o -11 5 1 42.87 40.51 4.19 o -10 5 1 222.67 217.25 4.57 o -9 5 1 7.66 9.35 3.09 o -8 5 1 101.81 95.33 3.48 o -7 5 1 81.45 81.61 2.61 o -6 5 1 385.85 369.13 5.18 o -5 5 1 285.20 276.37 3.03 o -4 5 1 758.93 779.48 8.69 o -3 5 1 899.46 866.36 4.73 o -2 5 1 66.33 68.50 2.08 o -1 5 1 512.38 561.21 4.88 o 0 5 1 905.94 1002.54 10.01 o 1 5 1 521.01 561.06 4.52 o 2 5 1 60.75 61.70 2.42 o 3 5 1 881.83 855.42 6.62 o 4 5 1 747.13 760.79 6.55 o 5 5 1 288.23 280.74 3.67 o 6 5 1 383.70 374.22 4.27 o 7 5 1 75.24 71.84 3.02 o 8 5 1 99.58 92.77 3.11 o 9 5 1 7.52 7.13 3.23 o 10 5 1 221.75 219.46 5.67 o 11 5 1 42.56 43.54 3.76 o 12 5 1 25.88 30.64 8.21 o -12 6 1 169.95 158.78 9.97 o -11 6 1 13.19 7.85 4.96 o -10 6 1 442.94 449.84 6.43 o -9 6 1 317.99 312.30 5.26 o -8 6 1 386.47 387.17 5.41 o -7 6 1 167.51 157.51 3.96 o -6 6 1 230.18 209.42 4.36 o -5 6 1 21.14 22.01 1.54 o -4 6 1 38.21 42.28 1.75 o -3 6 1 12.63 15.86 1.82 o -2 6 1 1103.44 1082.90 8.15 o -1 6 1 607.85 638.68 6.78 o 0 6 1 3541.51 3432.70 20.56 o 1 6 1 608.99 640.03 8.31 o 2 6 1 1109.61 1091.44 8.47 o 3 6 1 12.24 14.25 2.41 o 4 6 1 37.20 40.91 1.75 o 5 6 1 21.61 18.40 1.31 o 6 6 1 235.93 220.43 3.84 o 7 6 1 168.37 157.34 3.61 o 8 6 1 388.24 400.10 5.64 o 9 6 1 317.35 306.29 5.53 o 10 6 1 442.84 441.32 7.48 o 11 6 1 12.72 14.11 5.41 o 12 6 1 165.91 183.92 10.92 o -11 7 1 402.98 415.24 12.94 o -10 7 1 68.34 64.55 4.19 o -9 7 1 54.10 53.20 3.83 o -8 7 1 6.11 5.13 3.27 o -7 7 1 147.79 144.12 4.08 o -6 7 1 207.07 200.84 3.82 o -5 7 1 835.66 860.11 10.02 o -4 7 1 112.79 103.53 2.28 o -3 7 1 455.31 455.53 5.08 o -2 7 1 118.04 124.32 3.55 o -1 7 1 189.96 190.24 3.89 o 0 7 1 6.23 4.30 2.96 o 1 7 1 186.78 186.79 3.91 o 2 7 1 117.44 125.33 3.68 o 3 7 1 457.34 451.93 5.42 o 4 7 1 111.28 102.50 2.48 o 5 7 1 824.15 851.79 7.65 o 6 7 1 216.10 201.74 4.80 o 7 7 1 151.47 154.64 4.24 o 8 7 1 6.51 5.34 3.30 o 9 7 1 53.48 54.52 4.10 o 10 7 1 65.96 66.26 4.54 o 11 7 1 392.97 416.94 9.60 o -11 8 1 137.81 136.64 9.77 o -10 8 1 40.09 36.67 5.47 o -9 8 1 594.72 618.99 12.29 o -8 8 1 20.56 20.76 3.56 o -7 8 1 383.04 377.22 6.72 o -6 8 1 0.90 3.07 2.73 o -5 8 1 119.68 115.60 2.82 o -4 8 1 85.49 83.40 3.04 o -3 8 1 68.65 66.02 3.39 o -2 8 1 12.96 8.13 3.04 o -1 8 1 79.84 80.68 3.65 o 0 8 1 238.85 252.26 5.74 o 1 8 1 92.47 96.88 3.61 o 2 8 1 12.99 11.81 3.12 o 3 8 1 64.38 64.90 3.54 o 4 8 1 84.40 83.39 3.31 o 5 8 1 118.84 106.91 3.57 o 6 8 1 0.92 1.10 2.93 o 7 8 1 371.23 375.99 5.88 o 8 8 1 20.95 19.60 3.68 o 9 8 1 600.33 623.46 14.88 o 10 8 1 39.71 40.78 5.75 o 11 8 1 133.06 147.61 10.50 o -10 9 1 13.14 11.48 7.06 o -9 9 1 18.10 22.01 3.97 o -8 9 1 42.53 36.30 3.97 o -7 9 1 85.47 81.97 3.65 o -6 9 1 46.31 43.24 3.25 o -5 9 1 213.47 192.27 3.73 o -4 9 1 243.05 214.88 3.50 o -3 9 1 206.80 201.52 5.86 o -2 9 1 439.77 429.20 5.70 o -1 9 1 229.70 221.48 4.69 o 0 9 1 1288.95 1257.43 8.95 o 1 9 1 223.87 218.83 4.72 o 2 9 1 432.09 421.80 9.13 o 3 9 1 206.44 199.18 4.58 o 4 9 1 253.51 218.21 4.21 o 5 9 1 218.72 203.28 3.95 o 6 9 1 42.77 41.46 3.46 o 7 9 1 86.41 79.86 4.77 o 8 9 1 41.34 36.27 4.13 o 9 9 1 17.78 16.86 4.08 o 10 9 1 12.07 19.24 8.29 o -9 10 1 34.86 29.18 5.50 o -8 10 1 379.36 379.55 6.89 o -7 10 1 50.86 50.97 3.62 o -6 10 1 51.65 55.89 3.67 o -5 10 1 2.13 2.84 2.82 o -4 10 1 402.89 386.78 4.44 o -3 10 1 84.46 82.42 4.18 o -2 10 1 307.45 319.84 5.55 o -1 10 1 690.17 668.82 9.29 o 0 10 1 300.59 305.28 5.39 o 1 10 1 686.99 656.44 7.02 o 2 10 1 299.49 316.63 6.70 o 3 10 1 84.56 81.97 4.19 o 4 10 1 400.60 390.05 5.38 o 5 10 1 2.27 4.11 2.89 o 6 10 1 55.56 63.45 3.91 o 7 10 1 50.20 50.51 4.21 o 8 10 1 387.25 397.17 6.75 o 9 10 1 34.26 32.73 5.97 o -8 11 1 56.29 60.22 6.11 o -7 11 1 97.23 108.73 4.69 o -6 11 1 118.65 114.80 4.18 o -5 11 1 137.65 140.57 3.96 o -4 11 1 302.31 306.31 5.46 o -3 11 1 440.93 433.29 6.39 o -2 11 1 160.61 159.11 4.74 o -1 11 1 61.29 59.34 3.92 o 0 11 1 6.17 6.04 3.80 o 1 11 1 59.15 59.68 3.88 o 2 11 1 156.18 151.13 4.73 o 3 11 1 433.90 437.62 10.04 o 4 11 1 313.12 312.94 5.36 o 5 11 1 135.96 144.00 4.06 o 6 11 1 122.38 127.58 4.66 o 7 11 1 98.50 111.20 6.72 o 8 11 1 58.38 61.49 8.35 o -7 12 1 56.07 64.70 8.41 o -6 12 1 37.99 41.93 4.89 o -5 12 1 11.05 7.72 3.29 o -4 12 1 10.48 13.18 3.48 o -3 12 1 35.39 37.09 4.11 o -2 12 1 61.20 63.01 4.49 o -1 12 1 402.96 418.13 6.58 o 0 12 1 46.92 45.57 4.36 o 1 12 1 410.77 436.02 6.82 o 2 12 1 60.09 64.22 4.31 o 3 12 1 34.62 37.02 4.36 o 4 12 1 10.81 11.75 3.59 o 5 12 1 10.63 8.38 3.37 o 6 12 1 38.61 37.45 8.26 o -5 13 1 239.46 247.91 11.28 o -4 13 1 194.98 194.57 7.79 o -3 13 1 151.32 141.52 7.52 o -2 13 1 78.06 79.83 4.69 o -1 13 1 82.79 84.55 4.75 o 0 13 1 2.80 5.60 4.06 o 1 13 1 80.73 83.17 4.59 o 2 13 1 81.88 82.68 4.88 o 3 13 1 153.15 137.81 11.36 o 4 13 1 196.53 195.60 11.15 o 0 0 2 231.81 262.22 3.68 o 1 0 2 66.23 68.05 0.75 o 2 0 2 8237.90 8342.64 12.48 o 3 0 2 3170.88 3340.86 14.24 o 4 0 2 981.70 1066.74 5.16 o 5 0 2 321.69 330.63 2.61 o 6 0 2 0.79 0.27 1.68 o 7 0 2 45.57 36.73 2.04 o 8 0 2 171.60 180.71 3.73 o 9 0 2 247.20 263.27 4.26 o 10 0 2 529.15 517.50 9.20 o 11 0 2 7.40 7.85 5.34 o 12 0 2 87.22 76.37 6.83 o -12 1 2 208.94 206.73 8.17 o -11 1 2 67.62 65.99 5.95 o -10 1 2 140.06 144.74 5.09 o -9 1 2 101.72 101.30 3.53 o -8 1 2 13.97 16.13 2.85 o -7 1 2 512.93 537.06 3.97 o -6 1 2 318.08 346.89 3.62 o -5 1 2 2268.30 2373.48 11.40 o -4 1 2 1075.56 1111.00 4.57 o -3 1 2 1759.78 1798.90 5.35 o -2 1 2 1502.94 1501.54 6.56 o -1 1 2 4306.27 4322.36 13.93 o 0 1 2 579.21 614.69 3.79 o 1 1 2 4273.26 4291.66 10.98 o 2 1 2 1537.26 1535.59 5.42 o 3 1 2 1775.23 1795.74 6.88 o 4 1 2 1042.35 1092.16 5.31 o 5 1 2 2271.12 2381.15 9.27 o 6 1 2 302.60 329.63 3.05 o 7 1 2 521.56 538.47 3.67 o 8 1 2 14.71 15.90 2.48 o 9 1 2 99.76 95.74 3.29 o 10 1 2 139.75 147.84 6.52 o 11 1 2 62.69 59.12 6.45 o 12 1 2 200.66 203.27 11.41 o -12 2 2 37.14 39.48 6.74 o -11 2 2 495.62 501.02 16.56 o -10 2 2 126.26 130.20 6.78 o -9 2 2 510.81 485.89 8.91 o -8 2 2 272.57 282.07 5.02 o -7 2 2 656.78 625.15 3.45 o -6 2 2 74.02 71.10 1.63 o -5 2 2 16.55 16.33 0.99 o -4 2 2 247.68 283.67 2.69 o -3 2 2 1055.81 1047.56 3.00 o -2 2 2 339.10 347.97 1.44 o -1 2 2 5157.58 5249.75 18.24 o 0 2 2 2528.60 2570.11 10.32 o 1 2 2 5089.89 5209.68 15.96 o 2 2 2 336.43 346.79 2.28 o 3 2 2 1056.38 1048.42 4.06 o 4 2 2 252.68 294.91 1.90 o 5 2 2 16.03 17.44 0.99 o 6 2 2 73.97 70.60 1.49 o 7 2 2 644.10 633.44 3.89 o 8 2 2 274.47 284.63 3.68 o 9 2 2 509.25 481.64 5.59 o 10 2 2 127.08 130.70 5.42 o 11 2 2 493.50 497.28 9.88 o 12 2 2 36.83 36.00 6.00 o -11 3 2 122.37 109.86 6.94 o -10 3 2 187.06 194.77 8.60 o -9 3 2 81.36 79.96 3.65 o -8 3 2 34.48 33.76 3.37 o -7 3 2 375.76 353.78 3.63 o -6 3 2 124.47 118.38 2.51 o -5 3 2 416.04 399.59 4.91 o -4 3 2 475.47 449.46 5.42 o -3 3 2 394.70 392.58 2.38 o -2 3 2 1277.37 1310.86 4.45 o -1 3 2 1090.38 1148.61 7.42 o 0 3 2 1607.28 1544.80 8.23 o 1 3 2 1097.57 1135.57 4.81 o 2 3 2 1274.36 1322.24 8.50 o 3 3 2 403.17 403.43 3.63 o 4 3 2 467.27 442.13 2.24 o 5 3 2 402.64 390.28 3.98 o 6 3 2 121.28 115.70 1.82 o 7 3 2 365.37 336.76 2.81 o 8 3 2 32.50 32.51 2.47 o 9 3 2 79.73 79.45 3.75 o 10 3 2 184.81 198.85 5.97 o 11 3 2 120.70 118.32 5.73 o -11 4 2 59.05 64.84 6.47 o -10 4 2 646.91 631.04 8.24 o -9 4 2 16.10 13.66 3.19 o -8 4 2 613.00 618.07 4.65 o -7 4 2 323.49 321.12 3.56 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120.95 121.98 4.26 o 0 2 12 7.39 6.37 3.49 o 1 2 12 119.02 120.13 4.39 o 2 2 12 299.68 303.52 5.32 o 3 2 12 26.59 23.46 4.41 o 4 2 12 141.78 149.06 4.76 o 5 2 12 27.94 30.34 4.80 o -5 3 12 28.64 26.37 7.88 o -4 3 12 112.04 113.33 6.41 o -3 3 12 140.91 137.68 6.29 o -2 3 12 42.65 39.49 3.93 o -1 3 12 85.54 85.82 4.16 o 0 3 12 162.30 167.75 4.79 o 1 3 12 83.92 83.98 4.17 o 2 3 12 42.13 40.18 3.82 o 3 3 12 141.36 143.70 5.22 o 4 3 12 114.82 119.82 6.15 o 5 3 12 28.88 31.26 6.24 o 6 3 12 7.45 3.68 8.53 o 7 3 12 29.25 33.32 8.39 o -4 4 12 80.25 89.96 6.28 o -3 4 12 565.76 563.49 21.85 o -2 4 12 66.66 67.37 4.88 o -1 4 12 36.55 40.28 3.93 o 0 4 12 143.94 143.32 4.58 o 1 4 12 34.30 31.72 3.88 o 2 4 12 69.38 73.24 4.17 o 3 4 12 561.83 572.02 8.58 o 4 4 12 80.34 82.75 4.85 o 5 4 12 304.82 297.71 9.16 o 6 4 12 9.29 13.68 5.90 o -3 5 12 61.29 66.01 6.15 o -2 5 12 100.21 106.57 5.08 o -1 5 12 58.38 57.94 4.13 o 0 5 12 3.53 5.46 3.79 o 1 5 12 59.84 60.02 4.11 o 2 5 12 98.02 101.68 4.52 o 3 5 12 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