#------------------------------------------------------------------------------ #$Date: 2016-04-03 04:48:17 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181195 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/74/2227483.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2227483_Fobs loop_ _publ_author_name 'Ng, Seik Weng' _publ_section_title ; Redetermination of 4-(dimethylamino)pyridinium tribromide ; _journal_coeditor_code HB5583 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2223 _journal_volume 66 _journal_year 2010 _space_group_IT_number 18 _symmetry_space_group_name_Hall 'P 2 2ab' _symmetry_space_group_name_H-M 'P 21 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.7253 _cell_length_b 17.6696 _cell_length_c 4.1689 _exptl_crystal_F_000 688.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file hb5583Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21212 999 Friedel pairs' _shelx_refln_list_code 4 _shelx_f_calc_maximum 395.87 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7461.77 7579.51 171.93 o 4 0 0 9331.09 9739.70 232.33 o 6 0 0 90023.13 93944.65 1148.15 o 8 0 0 12860.56 14092.72 195.02 o 10 0 0 440.17 438.45 32.56 o 12 0 0 9336.65 9050.82 190.93 o 14 0 0 1369.15 1397.56 82.14 o 16 0 0 210.71 219.96 99.79 o 18 0 0 7.24 16.73 55.52 o 1 1 0 365.55 384.63 4.88 o 2 1 0 49.23 57.24 3.45 o 3 1 0 320.55 366.92 7.49 o 4 1 0 772.79 867.86 19.71 o 5 1 0 2467.83 2606.36 40.23 o 6 1 0 10018.20 10745.75 116.64 o 7 1 0 10849.42 11527.69 126.49 o 8 1 0 696.65 758.76 24.24 o 9 1 0 1280.11 1310.11 32.53 o 10 1 0 1910.83 1943.38 34.55 o 11 1 0 1210.74 1285.39 54.45 o 12 1 0 9227.51 9489.50 140.32 o 13 1 0 14871.34 14749.53 198.51 o 14 1 0 2825.01 2792.40 88.70 o 15 1 0 362.02 358.92 40.58 o 16 1 0 1474.53 1527.49 65.24 o 17 1 0 19.51 20.87 48.90 o 18 1 0 3126.29 2981.20 87.28 o 19 1 0 7239.43 6813.59 188.64 o 0 2 0 233.92 263.32 11.89 o 1 2 0 20367.68 21552.52 189.51 o 2 2 0 27.33 32.76 4.72 o 3 2 0 6760.85 7517.67 71.46 o 4 2 0 0.54 0.88 6.86 o 5 2 0 26697.88 27977.74 247.12 o 6 2 0 275.88 323.07 14.74 o 7 2 0 29648.77 30519.53 302.10 o 8 2 0 45.74 69.64 12.31 o 9 2 0 2823.59 3153.28 63.84 o 10 2 0 0.33 -25.17 20.50 o 11 2 0 2170.37 2293.34 60.80 o 12 2 0 22.65 61.29 27.04 o 13 2 0 7621.66 7827.53 126.21 o 14 2 0 88.65 58.29 31.18 o 15 2 0 465.79 474.35 43.67 o 16 2 0 26.20 64.56 35.86 o 17 2 0 868.30 846.64 56.22 o 18 2 0 32.77 44.10 41.84 o 19 2 0 12.74 84.56 39.83 o 1 3 0 65.41 82.20 6.91 o 2 3 0 306.87 312.47 11.76 o 3 3 0 918.33 941.67 17.56 o 4 3 0 341.60 383.08 11.84 o 5 3 0 2288.93 2358.21 29.58 o 6 3 0 10586.87 10972.62 106.07 o 7 3 0 5143.30 5234.66 58.74 o 8 3 0 992.28 1024.78 26.94 o 9 3 0 1449.78 1540.47 46.42 o 10 3 0 2139.52 2194.62 56.62 o 11 3 0 830.57 901.43 42.84 o 12 3 0 13190.09 13575.75 185.00 o 13 3 0 8479.02 8335.39 130.72 o 14 3 0 4427.37 4484.35 113.69 o 15 3 0 149.38 198.59 36.83 o 16 3 0 1389.07 1430.95 63.87 o 17 3 0 113.04 149.40 37.72 o 18 3 0 4567.91 4531.10 96.18 o 0 4 0 156716.44 152882.33 2360.23 o 1 4 0 930.74 952.16 15.49 o 2 4 0 1252.14 1206.95 31.53 o 3 4 0 209.04 215.16 9.84 o 4 4 0 1858.26 1960.03 25.89 o 5 4 0 1477.25 1554.31 29.57 o 6 4 0 58200.36 59085.00 480.24 o 7 4 0 137.48 155.02 10.72 o 8 4 0 5507.98 5532.84 59.49 o 9 4 0 225.56 254.39 23.22 o 10 4 0 511.92 496.66 29.40 o 11 4 0 1255.15 1335.16 49.93 o 12 4 0 7509.44 7667.18 111.32 o 13 4 0 120.12 112.92 27.65 o 14 4 0 1566.51 1598.48 55.72 o 15 4 0 222.81 226.22 34.90 o 16 4 0 6.65 -0.38 30.93 o 17 4 0 224.76 221.89 38.57 o 18 4 0 30.28 -2.86 36.54 o 1 5 0 2629.35 2688.49 33.81 o 2 5 0 1532.34 1498.63 24.66 o 3 5 0 1644.93 1695.49 25.28 o 4 5 0 3126.03 3283.20 36.93 o 5 5 0 46.26 75.91 8.87 o 6 5 0 10014.70 10281.18 95.28 o 7 5 0 14523.59 14766.85 132.33 o 8 5 0 205.65 210.08 12.71 o 9 5 0 691.30 695.82 20.66 o 10 5 0 107.70 95.61 21.55 o 11 5 0 10.78 37.07 22.08 o 12 5 0 13384.83 13312.04 163.56 o 13 5 0 11607.26 11637.33 150.57 o 14 5 0 1923.79 1965.47 110.36 o 15 5 0 208.24 258.23 44.50 o 16 5 0 1354.49 1541.74 59.90 o 17 5 0 9.19 13.40 33.50 o 18 5 0 2410.52 2542.92 75.72 o 0 6 0 4218.39 4250.29 81.35 o 1 6 0 61847.04 62667.01 604.15 o 2 6 0 10.86 14.23 7.90 o 3 6 0 7894.51 8034.38 75.10 o 4 6 0 37.36 26.68 9.94 o 5 6 0 16539.97 17119.94 148.12 o 6 6 0 2369.39 2485.92 33.87 o 7 6 0 36941.64 36840.72 307.41 o 8 6 0 274.08 295.71 14.84 o 9 6 0 549.08 564.08 28.58 o 10 6 0 81.99 114.07 22.22 o 11 6 0 1331.02 1374.67 44.82 o 12 6 0 818.68 847.15 40.47 o 13 6 0 6867.16 6944.99 110.51 o 14 6 0 554.90 527.01 38.26 o 15 6 0 106.23 84.79 31.92 o 16 6 0 39.58 92.92 33.68 o 17 6 0 39.30 38.49 35.00 o 18 6 0 339.65 326.01 60.27 o 1 7 0 881.18 893.10 19.78 o 2 7 0 1079.94 1152.69 28.24 o 3 7 0 3012.92 3239.24 39.53 o 4 7 0 11.52 23.11 10.07 o 5 7 0 845.34 757.68 24.92 o 6 7 0 10394.25 10605.02 99.03 o 7 7 0 2223.62 2274.87 37.30 o 8 7 0 1455.20 1501.41 43.32 o 9 7 0 823.42 823.78 26.72 o 10 7 0 1189.59 1155.83 40.17 o 11 7 0 47.45 36.98 22.66 o 12 7 0 16499.39 16206.67 190.67 o 13 7 0 1760.53 1786.43 54.69 o 14 7 0 5206.40 5212.12 91.61 o 15 7 0 57.65 45.87 32.76 o 16 7 0 1653.82 1606.50 60.33 o 17 7 0 79.27 176.13 53.50 o 18 7 0 4620.29 4746.58 135.20 o 0 8 0 63078.10 61285.90 949.51 o 1 8 0 1574.41 1551.85 31.90 o 2 8 0 633.87 663.45 18.21 o 3 8 0 517.82 516.76 17.75 o 4 8 0 436.65 469.24 17.25 o 5 8 0 2661.66 2756.76 66.73 o 6 8 0 35811.24 36390.89 361.33 o 7 8 0 414.36 453.11 22.32 o 8 8 0 4062.91 4159.21 55.90 o 9 8 0 530.44 551.17 22.99 o 10 8 0 410.14 458.23 29.26 o 11 8 0 1766.00 1757.97 48.90 o 12 8 0 4987.55 5047.91 84.60 o 13 8 0 12.13 14.97 26.02 o 14 8 0 2175.62 2231.19 62.00 o 15 8 0 365.58 391.27 58.69 o 16 8 0 149.87 123.14 49.63 o 17 8 0 844.24 897.75 72.38 o 1 9 0 1622.04 1612.98 34.27 o 2 9 0 2350.04 2317.80 33.51 o 3 9 0 850.89 905.06 19.13 o 4 9 0 5340.43 5718.21 64.87 o 5 9 0 8.78 16.71 12.67 o 6 9 0 5359.21 5375.38 82.64 o 7 9 0 10753.99 10796.76 124.70 o 8 9 0 1397.30 1407.48 37.11 o 9 9 0 452.69 436.66 25.03 o 10 9 0 84.76 109.44 30.87 o 11 9 0 12.71 15.64 22.04 o 12 9 0 10071.87 10035.03 132.55 o 13 9 0 9759.04 9848.28 184.13 o 14 9 0 934.64 1044.01 81.69 o 15 9 0 14.04 -2.25 42.73 o 16 9 0 463.31 411.89 59.07 o 17 9 0 150.84 192.79 56.46 o 0 10 0 4528.76 4426.76 93.18 o 1 10 0 22819.70 22532.44 260.42 o 2 10 0 15.91 13.42 10.12 o 3 10 0 1896.59 1833.50 27.79 o 4 10 0 370.99 369.49 15.47 o 5 10 0 8809.58 8747.16 94.15 o 6 10 0 4150.83 4178.19 67.54 o 7 10 0 19646.71 19561.79 207.58 o 8 10 0 673.00 712.69 39.00 o 9 10 0 82.80 110.25 20.04 o 10 10 0 345.47 350.08 40.15 o 11 10 0 463.08 447.60 45.11 o 12 10 0 2958.90 2846.18 106.62 o 13 10 0 4196.01 3997.45 109.00 o 14 10 0 660.36 644.93 58.64 o 15 10 0 360.90 358.65 81.73 o 16 10 0 29.88 80.70 50.52 o 17 10 0 26.49 28.85 51.97 o 1 11 0 3176.24 3097.83 47.11 o 2 11 0 1192.88 1130.46 28.87 o 3 11 0 970.89 978.73 21.84 o 4 11 0 486.45 477.60 18.90 o 5 11 0 4349.48 4146.91 50.49 o 6 11 0 5324.19 5288.57 84.76 o 7 11 0 185.94 217.88 23.68 o 8 11 0 2176.51 2100.49 52.21 o 9 11 0 738.12 779.69 79.03 o 10 11 0 851.47 899.45 54.57 o 11 11 0 846.78 970.98 59.24 o 12 11 0 8542.62 8293.99 162.26 o 13 11 0 951.54 969.78 64.78 o 14 11 0 3497.61 3568.60 109.41 o 15 11 0 88.90 81.29 47.00 o 16 11 0 1044.06 1023.14 102.59 o 0 12 0 53212.48 53054.36 836.21 o 1 12 0 3280.58 3208.26 49.71 o 2 12 0 1862.76 1840.36 37.84 o 3 12 0 476.39 496.73 17.19 o 4 12 0 541.04 585.85 29.57 o 5 12 0 3135.61 3117.20 48.65 o 6 12 0 21376.51 21243.95 225.42 o 7 12 0 819.60 891.16 33.92 o 8 12 0 5686.84 5531.07 91.40 o 9 12 0 413.23 437.23 41.68 o 10 12 0 198.03 227.30 37.87 o 11 12 0 2109.29 1942.89 74.18 o 12 12 0 2651.87 2648.84 88.88 o 13 12 0 1.51 27.89 41.34 o 14 12 0 2047.42 2048.35 111.21 o 15 12 0 603.25 606.62 64.01 o 16 12 0 43.41 -12.42 47.63 o 1 13 0 758.31 771.31 28.81 o 2 13 0 3787.91 3820.03 58.66 o 3 13 0 87.77 69.71 16.90 o 4 13 0 1762.31 1767.42 35.86 o 5 13 0 243.98 264.07 22.75 o 6 13 0 1717.69 1726.28 39.34 o 7 13 0 6438.24 6342.10 80.84 o 8 13 0 1196.74 1166.92 45.35 o 9 13 0 211.75 176.48 35.79 o 10 13 0 32.98 48.49 34.30 o 11 13 0 402.13 371.60 85.11 o 12 13 0 1898.69 1992.67 82.29 o 13 13 0 8784.67 8436.87 356.89 o 14 13 0 65.76 87.50 44.74 o 15 13 0 0.31 16.39 45.30 o 0 14 0 2383.13 2381.18 105.12 o 1 14 0 5697.90 5645.98 76.77 o 2 14 0 22.23 53.49 17.46 o 3 14 0 226.88 224.25 21.74 o 4 14 0 554.29 523.03 27.61 o 5 14 0 4136.84 4232.00 61.30 o 6 14 0 3443.55 3433.36 55.63 o 7 14 0 8572.81 8645.14 101.95 o 8 14 0 672.41 623.19 44.36 o 9 14 0 9.57 -10.29 31.99 o 10 14 0 325.23 248.59 40.59 o 11 14 0 65.94 39.78 38.43 o 12 14 0 2314.86 2124.87 83.64 o 13 14 0 2703.19 2608.46 137.24 o 14 14 0 586.33 534.44 60.29 o 15 14 0 1123.12 1173.31 79.66 o 1 15 0 3223.46 3277.67 63.94 o 2 15 0 469.15 474.52 29.32 o 3 15 0 73.48 58.70 19.62 o 4 15 0 307.06 288.06 24.94 o 5 15 0 5458.79 5371.76 81.30 o 6 15 0 2714.02 2658.26 56.25 o 7 15 0 163.15 161.96 25.32 o 8 15 0 1450.60 1571.83 55.31 o 9 15 0 509.73 465.53 53.45 o 10 15 0 311.74 300.16 56.08 o 11 15 0 2081.19 2204.58 82.73 o 12 15 0 4010.17 4006.08 165.43 o 13 15 0 600.48 624.45 61.12 o 14 15 0 2200.95 2188.64 181.44 o 0 16 0 26954.46 27457.61 461.36 o 1 16 0 3381.55 3404.15 67.65 o 2 16 0 2089.06 2085.64 53.19 o 3 16 0 106.25 121.81 27.94 o 4 16 0 149.52 123.52 26.15 o 5 16 0 3009.97 3128.27 61.20 o 6 16 0 9202.05 9019.17 120.37 o 7 16 0 817.38 771.05 54.47 o 8 16 0 5150.67 4949.35 117.12 o 9 16 0 139.81 118.53 37.21 o 10 16 0 24.12 63.20 32.72 o 11 16 0 2784.47 2725.70 107.35 o 12 16 0 707.23 728.37 66.74 o 13 16 0 77.67 76.56 47.39 o 1 17 0 339.35 356.16 42.30 o 2 17 0 4074.34 4027.49 92.60 o 3 17 0 13.69 16.66 24.44 o 4 17 0 1964.28 1843.95 54.37 o 5 17 0 167.01 181.21 29.55 o 6 17 0 1174.92 1156.81 49.01 o 7 17 0 3361.11 3391.70 101.29 o 8 17 0 1435.57 1598.43 57.90 o 9 17 0 2.96 4.76 30.53 o 10 17 0 100.55 146.90 36.71 o 11 17 0 331.30 264.90 41.49 o 12 17 0 966.10 928.30 56.58 o 0 18 0 2182.25 2100.19 81.20 o 1 18 0 3910.19 3967.59 88.61 o 2 18 0 10.50 28.85 26.01 o 3 18 0 2.07 -2.17 26.08 o 4 18 0 510.88 543.03 37.86 o 5 18 0 1550.16 1565.14 53.79 o 6 18 0 2609.63 2580.33 66.98 o 7 18 0 5284.93 5526.75 99.97 o 8 18 0 241.00 248.54 81.96 o 9 18 0 64.43 42.25 49.68 o 10 18 0 210.10 122.18 51.53 o 11 18 0 2.40 8.49 46.09 o 1 19 0 2376.74 2365.51 62.90 o 2 19 0 111.37 154.22 30.99 o 3 19 0 231.11 296.16 33.90 o 4 19 0 0.42 -5.34 28.38 o 5 19 0 1937.60 1800.97 59.39 o 6 19 0 1526.83 1537.47 58.63 o 7 19 0 354.14 415.15 39.86 o 8 19 0 501.57 535.15 51.37 o 9 19 0 227.37 293.39 58.04 o 10 19 0 12.45 -46.86 49.97 o 0 20 0 5422.02 5612.27 225.92 o 1 20 0 1202.33 1166.91 51.86 o 2 20 0 836.18 854.10 46.66 o 3 20 0 1.28 12.97 30.17 o 4 20 0 3.87 -10.57 30.78 o 5 20 0 1967.33 2037.36 64.44 o 6 20 0 2491.23 2479.91 63.35 o 7 20 0 307.08 302.25 47.21 o 8 20 0 2265.83 2311.10 101.29 o 9 20 0 32.62 64.99 55.30 o 1 21 0 73.43 132.73 34.53 o 2 21 0 2186.93 2281.94 77.67 o 3 21 0 3.29 10.72 32.24 o 4 21 0 2730.44 2862.68 76.20 o 5 21 0 109.79 137.43 35.60 o 6 21 0 745.68 795.84 45.43 o 7 21 0 1280.97 1313.93 70.51 o 0 22 0 2159.67 2133.99 98.60 o 1 22 0 2952.84 3206.87 80.75 o 2 22 0 175.96 135.70 37.22 o 3 22 0 34.43 31.96 35.43 o 4 22 0 457.99 423.76 43.95 o 5 22 0 396.70 431.25 45.88 o 0 0 1 3516.78 3390.08 50.35 o 1 0 1 10846.29 11132.87 112.14 o 2 0 1 2297.07 2265.56 28.10 o 3 0 1 1513.90 1606.53 23.71 o 4 0 1 5993.63 5797.05 55.55 o 5 0 1 19700.50 19678.62 178.47 o 6 0 1 6011.32 6057.76 63.64 o 7 0 1 10517.65 10971.26 137.33 o 8 0 1 1752.45 1697.26 38.65 o 9 0 1 718.41 679.26 28.91 o 10 0 1 2581.21 2521.80 51.97 o 11 0 1 8655.98 8840.48 114.41 o 12 0 1 2730.89 2763.80 58.51 o 13 0 1 1.32 34.24 29.62 o 14 0 1 856.88 897.51 77.64 o 15 0 1 10.41 44.23 33.66 o 16 0 1 928.06 917.94 62.08 o 17 0 1 16.99 21.11 34.86 o 18 0 1 561.20 626.89 55.76 o -18 1 1 2913.12 2914.45 88.27 o -17 1 1 3550.97 3673.33 93.99 o -16 1 1 961.67 933.41 63.44 o -15 1 1 4099.33 3970.69 91.43 o -14 1 1 7552.13 7447.80 126.31 o -13 1 1 2629.10 2468.62 105.55 o -12 1 1 3455.48 3386.59 64.41 o -11 1 1 6106.96 6065.01 87.99 o -10 1 1 1701.18 1724.18 43.68 o -9 1 1 2477.95 2551.30 49.66 o -8 1 1 10935.43 11054.80 126.36 o -7 1 1 5162.27 5041.22 76.12 o -6 1 1 1102.93 1111.53 25.91 o -5 1 1 1527.42 1563.61 26.21 o -4 1 1 663.08 680.17 15.58 o -3 1 1 151.79 149.74 13.41 o -2 1 1 3555.42 3546.51 35.84 o -1 1 1 940.10 959.66 12.56 o 0 1 1 71.74 72.14 5.10 o 1 1 1 939.97 910.29 13.26 o 2 1 1 3554.07 3633.77 56.11 o 3 1 1 151.12 155.12 9.21 o 4 1 1 662.25 662.66 15.16 o 5 1 1 1526.13 1547.43 34.93 o 6 1 1 1103.30 1097.53 25.76 o 7 1 1 5163.38 5173.31 56.41 o 8 1 1 10934.78 10946.78 120.30 o 9 1 1 2476.95 2527.00 78.87 o 10 1 1 1699.00 1782.04 44.32 o 11 1 1 6102.49 6215.91 89.61 o 12 1 1 3454.95 3397.56 64.49 o 13 1 1 2630.96 2774.02 78.33 o 14 1 1 7554.43 7604.88 166.22 o 15 1 1 4099.02 4154.31 94.80 o 16 1 1 960.74 1083.62 60.87 o 17 1 1 3550.81 3624.95 84.91 o 18 1 1 2911.68 2929.58 80.40 o -18 2 1 209.81 222.29 46.74 o -17 2 1 516.66 588.98 67.15 o -16 2 1 44.65 87.45 38.14 o -15 2 1 23.72 35.80 34.34 o -14 2 1 1182.11 1066.97 53.47 o -13 2 1 910.83 1007.49 78.06 o -12 2 1 1963.96 1970.25 51.14 o -11 2 1 4820.21 4762.50 76.19 o -10 2 1 1480.33 1547.52 42.30 o -9 2 1 4337.80 4431.36 67.59 o -7 2 1 6972.81 7155.27 79.01 o -6 2 1 8691.90 9000.53 91.44 o -5 2 1 13122.97 13502.57 138.80 o -4 2 1 22095.53 22711.90 248.24 o -3 2 1 18602.82 18749.04 205.27 o -2 2 1 83346.71 81719.47 779.64 o -1 2 1 26811.04 26582.01 258.13 o 0 2 1 144.63 151.77 5.99 o 1 2 1 26811.14 26810.77 297.98 o 2 2 1 83350.52 84521.61 919.20 o 3 2 1 18598.04 19381.12 194.65 o 4 2 1 22098.68 22759.61 190.96 o 5 2 1 13120.26 13646.33 129.48 o 6 2 1 8692.22 8731.44 220.28 o 7 2 1 6973.10 7147.45 72.80 o 8 2 1 14984.92 15075.39 137.63 o 9 2 1 4338.08 4495.97 55.20 o 10 2 1 1481.19 1481.48 31.51 o 11 2 1 4820.30 4866.63 70.39 o 12 2 1 1966.14 1970.90 54.39 o 13 2 1 907.83 965.05 44.45 o 14 2 1 1181.07 1263.83 53.47 o 15 2 1 23.68 81.43 31.97 o 16 2 1 44.78 77.18 34.21 o 17 2 1 517.65 506.11 45.43 o 18 2 1 209.59 161.52 40.48 o -18 3 1 2888.46 2718.76 86.49 o -17 3 1 3916.10 3851.36 105.36 o -16 3 1 800.44 818.54 54.39 o -15 3 1 4627.64 4654.15 98.40 o -14 3 1 7285.17 7132.99 122.31 o -13 3 1 1901.34 1842.80 61.71 o -12 3 1 2179.70 2170.54 53.34 o -11 3 1 6059.08 6074.05 88.59 o -10 3 1 2378.87 2476.26 53.54 o -9 3 1 5914.72 5713.44 171.31 o -8 3 1 8896.05 9074.98 106.58 o -7 3 1 3200.45 3079.75 53.85 o -6 3 1 835.35 847.63 25.90 o -5 3 1 3255.69 3299.55 49.88 o -4 3 1 1322.70 1340.81 29.55 o -3 3 1 3584.50 3613.45 51.07 o -2 3 1 2330.46 2355.78 35.66 o -1 3 1 1725.58 1674.16 25.21 o 0 3 1 2096.83 2116.24 28.60 o 1 3 1 1726.05 1716.05 35.65 o 2 3 1 2329.96 2333.51 37.28 o 3 3 1 3586.97 3705.04 70.07 o 4 3 1 1322.15 1337.43 21.92 o 5 3 1 3255.96 3322.05 38.46 o 6 3 1 836.97 898.49 25.52 o 7 3 1 3202.48 3220.99 44.18 o 8 3 1 8896.68 8939.81 89.76 o 9 3 1 5914.97 6042.70 68.49 o 10 3 1 2377.46 2420.30 40.41 o 11 3 1 6053.46 6227.69 96.54 o 12 3 1 2178.53 2178.41 56.72 o 13 3 1 1902.89 1962.61 77.10 o 14 3 1 7291.04 7163.74 112.41 o 15 3 1 4629.01 4631.96 90.20 o 16 3 1 800.84 795.03 48.48 o 17 3 1 3917.60 3930.36 88.09 o 18 3 1 2884.21 2978.48 81.95 o -18 4 1 542.64 573.91 49.46 o -17 4 1 82.12 41.86 47.40 o -16 4 1 927.18 944.71 56.38 o -15 4 1 93.46 179.03 38.03 o -14 4 1 481.49 502.08 42.35 o -13 4 1 10.81 15.42 25.08 o -12 4 1 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